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Dissertations / Theses on the topic 'Aldolic reaction'

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Published: 4 June 2021

Last updated: 7 February 2022

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1

Lima, Dimas José da Paz. "Síntese do fragmento C11-C26 do potente agente antitumoral (-)-dictiostatina." [s.n.], 2010. http://repositorio.unicamp.br/jspui/handle/REPOSIP/248476.

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Orientador: Luiz Carlos Dias<br>Tese (doutorado) - Universidade Estadual de Campinas, Instituto de Química<br>Made available in DSpace on 2018-08-16T13:59:46Z (GMT). No. of bitstreams: 1 Lima_DimasJosedaPaz_D.pdf: 6787500 bytes, checksum: 4cdb1c2dbc5967cdef9ab7564d8c0118 (MD5) Previous issue date: 2010<br>Resumo: A (-)-dictiostatina (1) é uma macrolactona de origem marinha, que foi isolada por Pettit e col. em 1994 da esponja Spongia sp. e posteriormente, por Wright e col. a partir da esponja Lithistida. A (-)-dictiostatina (1) exibe uma potente atividade antitumoral, inibindo a proliferação

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2

Hansch, Markus. "Die Zirconiumalkoxid-katalysierte Aldol-Tishchenko-Reaktion von Keton-Aldolen." Doctoral thesis, [S.l.] : [s.n.], 2005. http://deposit.ddb.de/cgi-bin/dokserv?idn=975299727.

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3

Mahal, Amrik Singh. "Asymmetric aldol reactions." Thesis, University of Kent, 1992. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.302987.

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4

Tang, Gongkun [Verfasser]. "Novel Organocatalysts with Pyrrolidine and Brönsted Acids for Aldol Reaction and other Reactions / Gongkun Tang." Wuppertal : Universitätsbibliothek Wuppertal, 2013. http://d-nb.info/1038029023/34.

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5

Maggiotti, Virginie. "Direct biocatalytic asymmetric aldol reactions." Thesis, University of Oxford, 2003. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.275468.

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6

Tan, Duygu. "Silicon Tetrachloride Mediated Asymmetric Aldol Addition Reaction." Master's thesis, METU, 2013. http://etd.lib.metu.edu.tr/upload/12615396/index.pdf.

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Aldol addition reaction is one of the most important and most studied carbon-carbon bond forming reactions in organic chemistry. Recent studies focused on the catalytic version of this chemistry. Different from the classical Mukaiyama-type aldol reactions, chiral lewis bases have been used as promoters. In the presence of SiCl4, these reactions proceed through a cyclic transition state leading to anti aldol product as a major product with moderate-to-good diastereo and enantioselectivities. Phosphoramide derivatives, BINAPO, BINAPO derivatives, N,N-dioxides and N-oxides have been extensively u

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7

Goodman, J. M. "Studies on the boron-mediated aldol reaction." Thesis, University of Cambridge, 1989. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.316774.

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8

Tokuda, Osamu. "Studies on organocatalytic direct asymmetric aldol reaction." 京都大学 (Kyoto University), 2007. http://hdl.handle.net/2433/136966.

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9

Vickery, Benjamin David. "New strategies for asymmetric Aldol reactions." Thesis, Imperial College London, 1998. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.301299.

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10

Nixon, Tracy Dawn. "Catalyst design for the asymmetric phospho-aldol reaction." Thesis, University of Leeds, 2005. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.424504.

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11

Lou, Samuel. "Stereochemical Control of Polyketides through Asymmetric Aldol Reaction." Master's thesis, Virginia Tech, 2000. http://hdl.handle.net/10919/37095.

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Polyketides are a group of complex natural products that can inhibit the growth of bacteria, viruses, fungi, and tumor cells. Most polyketides are very difficult to extract from bacteria. Therefore, numerous syntheses of polyketide-related synthons have been attempted. <p> However, controlling the stereochemistry of the polyketide poses the most challenging task for researchers. The aim of this report is to discuss control of the stereochemistry of the polyketide-related synthons in asymmetric aldol reactions. Several important methodologies for stereochemical control in the aldol reac

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12

Sakamoto, Ryu. "Development of Amine-catalyzed Asymmetric Reactions Using Hetero-functionalized Acetaldehydes as Nucleophiles." 京都大学 (Kyoto University), 2014. http://hdl.handle.net/2433/188503.

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13

Joensuu, Pekka Matias. "Development of catalytic stereoselective reductive aldol reactions." Thesis, University of Edinburgh, 2008. http://hdl.handle.net/1842/2576.

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The chemistry of enolates can be considered one of the cornerstone areas in organic chemistry. Regioselective generation of an enolate in the presence of several enolisable sites can often prove to be a difficult task. Discoveries in recent years have led to new areas of enolate formation in the presence of other carbonyl groups. These include reductive aldol chemistry where direct reductive aldol coupling of an alpha,beta - unsaturated carbonyl group in presence of a carbonyl electrophile enables often perfectly regioselective reactions to occur. This tandem conjugate reductionelectrophilic t

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14

Kilburn, J. D. "Diastereoselective aldol reactions of #beta#-silyl enolates." Thesis, University of Cambridge, 1986. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.377832.

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15

Freiria, Marta. "Novel rhodium (I) catalysed tandem hydrosilylation - intramolecular aldol reaction." Thesis, University College London (University of London), 2003. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.409927.

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16

Curati, Federico. "Synthesis of a chiral, water soluble porphyrin containing a pyrrolidine unit and initial study of its catalytic activity." Master's thesis, Alma Mater Studiorum - Università di Bologna, 2018. http://amslaurea.unibo.it/16731/.

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Asymmetric organocatalysis have taken hold in the last decades due to affordability and lack of toxicity of their catalysts. Unfortunately, organocatalytic enantioselective reactions in an environmentally friendly and safe solvent as water are still scarce. During the training internship our aim has been to find an effective water soluble organocatalyst able to drive in an enantioselective fashion a reaction, to maximize the diasteromeric and the enantiomeric excess. Pursuing this objective we synthesized a meso 3-sulfonatophenyl porphyrin with a chiral aminoaldehyde substituent, with the sulf

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17

Taylor, Anthony Philip. "Regio- and diastereo-selectivity in directed aldol reactions of cyclopent-2-enone and but-2-en-4-olide." Thesis, University of Bath, 1988. https://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.380865.

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18

Brown, Paul. "Tandem Michael/aldol and Michael/Michael cyclisation reactions." Thesis, Bangor University, 2006. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.429866.

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19

Chibale, Kelly. "Asymmetric aldol reactions and phenylthio migrations in synthesis." Thesis, University of Cambridge, 1992. https://www.repository.cam.ac.uk/handle/1810/272239.

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20

panda, santanu. "N-PROLINYLANTHRANILAMIDE BASED ORGANOCATALYSTS FOR ASYMMETRIC ALDOL REACTIONS." Case Western Reserve University School of Graduate Studies / OhioLINK, 2013. http://rave.ohiolink.edu/etdc/view?acc_num=case1371815461.

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21

Han, Zhenfu. "Studies on Aldol Reactions with Titanium-Based Reagents." 京都大学 (Kyoto University), 2002. http://hdl.handle.net/2433/149447.

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22

Kephart, Susan E. "Synthetic and mechanistic studies on a silicon-mediated aldol reaction." Diss., Pasadena, Calif. : California Institute of Technology, 1995. http://resolver.caltech.edu/CaltechETD:etd-10312007-082516.

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23

Tempkin, Orin 1967. "New chiral catalyts for the asymmetric Mukaiyama-type aldol reaction." Thesis, Massachusetts Institute of Technology, 1994. http://hdl.handle.net/1721.1/17349.

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24

Bondock, Samir. "Mechanism and synthetic use of Paternò-Büchi reactions spin mapping and photo aldol reactions /." [S.l. : s.n.], 2003. http://deposit.ddb.de/cgi-bin/dokserv?idn=968091725.

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25

Banks, James. "Synthesis of naturally occurring compounds via key aldol reactions." Thesis, University of Nottingham, 2009. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.522994.

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26

Georgiou, Irene. "Organocatalysis using bifunctional aminoboronic acids : application to the asymmetric aldol reaction." Thesis, Durham University, 2012. http://etheses.dur.ac.uk/3540/.

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The organocatalytic iminium activation strategy acting cooperatively with a Lewis acidic group has been applied to the development of a novel generation of proline-based aminoboronic acid catalysts. Key steps for their synthesis included (-)-sparteine mediated asymmetric deprotonation of N-Boc-pyrrolidine, copper(I) catalysed borylation of alkylhalides and catalysed hydroboration of alkenes. The evaluation of the first proline-based aminoboronic acids is described in the context of organocatalysed aldol reactions between p-nitrobenzaldehyde and acetone. Enhanced reactivity and enantioselectivi

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27

Gledhill, Alexandra Cathleen. "Designing new metallo-organic catalysts for the asymmetric phospho-aldol reaction." Thesis, University of Leeds, 2009. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.507721.

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28

Yeste, Sonia Lozano. "Boron-BINOL catalysed asymmetric Mannich and aldol type reaction : novel boronate esters." Thesis, University of Bath, 2007. https://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.516904.

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29

Le, Sann Christine. "Enantioselective synthesis of N-Acetylcysteamine thioester putative intermediates to polyketides." Thesis, University of Bristol, 2001. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.340274.

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30

Balnaves, Andrew Stuart. "Scope and limitations of the aldol reaction for the synthesis of difluorinated polyols." Thesis, University of Birmingham, 1999. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.396231.

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31

Cosgrove, Nichola Elizabeth. "Studies on the phospho-aldol reaction catalysed by aluminium salcyan and related complexes." Thesis, University of Leeds, 2011. http://etheses.whiterose.ac.uk/1737/.

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The phospho-aldol (PA) reaction is one of the most versatile reactions for the formation of phosphorus-carbon [P-C] bonds. The reaction is a base-catalysed addition reaction between a hydrogen-phosphonate ester and a carbonyl substrate, affording alpha-functionalised phosphonate esters. These PA products have found a wide-spread application in biomedical science. Since the PA reaction is capable of affording products with new stereocentres, considerable effort has been devoted over the last few decades to developing asymmetric catalytic variants of the PA reaction. Through the manipulation of

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32

Fanjul, Sandra. "New highly selective and easily displaced chiral auxiliary for aldol reactions." Thesis, University of Edinburgh, 2008. http://hdl.handle.net/1842/10886.

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An efficient route for the synthesis of a new highly selective and easily displaced chiral auxiliary I for the asymmetric boron-mediated aldol reaction has been developed in 5 steps from norephedrine. The novel chiral auxiliary has been shown to mediate <i>anti </i>and <i>syn</i> propionate and glycolate aldol reactions with a range of aldehydes in excellent yield (60-98%) and with good to excellent diastereoselectivity. Details of the methods which have been used to assign the absolute and relative stereochemistry of the aldol adducts are also summarised. The facile displacement of auxiliary

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33

Shaw, Christopher J. "Towards aziridine-2-carboxylates via studies of aldol reactions of azidoacetates." Thesis, University of Reading, 1999. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.287660.

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34

Bañón, Caballero Abraham. "Recoverable binam derivatives as organocatalysts in asymmetric synthesis." Doctoral thesis, Universidad de Alicante, 2014. http://hdl.handle.net/10045/42322.

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35

Lumby, Ralph James Richard. "Novel transition-metal-catalysed reactions using diethylzinc as the stoichiometric reductant." Thesis, University of Edinburgh, 2009. http://hdl.handle.net/1842/3890.

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Modern organic chemistry strives to achieve rapid molecular complexity from simple achiral substrates. One method by which this may be achieved is with enolate formation followed by attack on an electrophile which can generate one, two or even more new stereocentres in one step. However regioselective generation of an enolate in the presence of several enolisable sites has always proved problematical. A partial answer to this problem has been provided by the development of the reductive aldol reaction. The first part of this thesis is concerned with describing a highly diastereoselective Co(II

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36

Belletti, Giada. "Organocatalytic Enantioselective Vinylogous Aldol-Lactonization Cascade Reaction of 3-Alkylidene Oxindoles to Trifluoromethyl Ketones." Master's thesis, Alma Mater Studiorum - Università di Bologna, 2017. http://amslaurea.unibo.it/14463/.

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In this work, an highly enantioselective vinylogous aldol-lactonization cascade reaction of 3-alkylidene oxindole to α,β-unsaturated trifluoromethyl ketone, promoted by bifunctional organocatalysts, is presented. The reaction proceed through 1,2-addition followed by cascade lactonization to afford an unsaturated lactone bearing a chiral trifluoromethylated tetrasubstituted carbon stereocenter with high enantioselectivity and moderate yield. Nevertheless, also the two E/Z isomers of the correspondent 1,2-addition product are obtained.

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37

Leung, Sze-kar, and 梁詩嘉. "Novel reactions of oxabicyclic compounds and reductive aldol cyclizations of activated alkynes." Thesis, The University of Hong Kong (Pokfulam, Hong Kong), 2004. http://hub.hku.hk/bib/B44570156.

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38

Donghi, Monica. "Synthesis of polyketide-type libraries via aldol reactions performed on solid phase." Thesis, University of Cambridge, 2000. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.621510.

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39

Kinnaird, James Welsh Auld. "Synthetic studies towards polyketide libraries via aldol reactions performed on solid support." Thesis, University of Cambridge, 2001. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.621046.

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40

Seifert, Andrea. "Säurekatalysierte Tandem-Aldol- Meerwein-Ponndorf-Verley-Reaktionen." Doctoral thesis, Humboldt-Universität zu Berlin, Mathematisch-Naturwissenschaftliche Fakultät I, 2010. http://dx.doi.org/10.18452/16242.

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Im Rahmen dieser Dissertation wurde die säurekatalysierte Tandem-Aldol-MPV-Reaktion zur Darstellung von 1,3-Diolethern als Eintopfverfahren entwickelt. Dabei konnte ein Syntheseprotokoll entwickelt werden, das durch geschickte Wahl der Reaktionspartner, eines Katalysatorsystems aus LiClO4/ Trifluoressigsäure und geeigneter Reaktionsbedingungen ermöglichte, die klassische dreistufige Synthese von 1,3-Diolethern auf ein effizientes Eintopfverfahren zu reduzieren. Die Kombination mit umfangreichen mechanistischen Untersuchungen ermöglichte erstmals die Entwicklung einer asymmetrischen Variante d

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41

Zhang, Wanying. "A Mechanistic Approach Towards the Discovery of Catalytic Acylation Reactions." Thesis, Université d'Ottawa / University of Ottawa, 2017. http://hdl.handle.net/10393/35646.

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The development of new, efficient methods for the formation of carbon-carbon bonds using transition metal catalysis has broad applications in the field of organic chemistry and is the key to efficient chemical synthesis. Many efforts had been made to develop efficient ways to make these linkages particularly with the aid of metals such as Rh, Pd, Ni, Ru and Cu. Our group is primarily focused on exploring how these transition metals can activate typically inert functional groups, paving way to new synthetic routes to construct more complex molecules. Chapter 1 describes attempts that were cond

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42

Liu, Jing. "Synthesis of resveratrol and its analogs, phase-transfer catalyzed asymmetric glycolate aldol reactions, and total synthesis of 8,9-methylamido-geldanamycin /." Diss., CLICK HERE for online access, 2007. http://contentdm.lib.byu.edu/ETD/image/etd1998.pdf.

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43

Issa, Issa. "Synthesis of monoterpenoid derivatives and evaluation for biocatalytic transformations." Thesis, University of Manchester, 2016. https://www.research.manchester.ac.uk/portal/en/theses/synthesis-of-monoterpenoid-derivatives-and-evaluation-for-biocatalytic-transformations(c06f8f06-e42c-48f0-bf29-d5bb92fd1353).html.

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Monoterpenoid derivatives are some of the most effective asymmetric controllers used in organic synthesis. They are also precursors in target syntheses, especially in synthesis of natural products with useful biological properties. However, there are still significant opportunities to develop new structural synthetic modifications. This project target focuses on employing commercially available chiral pool cyclic ketones, such as R-(-)-carvone, (+)-isomenthone, and (-)-isopinocamphone to create new potential substrates for biocatalytic modifications, via terpenone enolate alkylations, aldol ad

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44

Perez, Carla Cristina 1979. "Síntese formal dos policetídeos bicíclicos salinecetais A e B." [s.n.], 2012. http://repositorio.unicamp.br/jspui/handle/REPOSIP/248357.

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Orientador: Luiz Carlos Dias<br>Tese (doutorado) - Universidade Estadual de Campinas, Instituto de Química<br>Made available in DSpace on 2018-08-20T16:20:14Z (GMT). No. of bitstreams: 1 Perez_CarlaCristina_D.pdf: 5128114 bytes, checksum: d3cf5087b543e1096ea7da56cdaadc47 (MD5) Previous issue date: 2012<br>Resumo: Os salinecetais A e B foram isolados em 2007 por Fenical e colaboradores a partir da actinobactéria marinha Salinispora arenicola, e mostraram ser importantes alvos na quimioprevenção do câncer como inibidores da ornitina descarboxilase. Concluímos a síntese do fragmento avançado C-

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45

D'Elia, Valerio. "Synthesis, characterization and application of alpha-beta-oligopeptides as bifunctional organocatalysts for the aldol reaction." kostenfrei, 2009. http://www.opus-bayern.de/uni-regensburg/volltexte/2010/1166/.

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46

Bibi, Ahtaram [Verfasser]. "Primary Amine Containing Bifunctional Catalysts for Asymmetric Aldol and Mannich Reactions / Ahtaram Bibi." Bremen : IRC-Library, Information Resource Center der Jacobs University Bremen, 2012. http://d-nb.info/1035220229/34.

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47

Hyatt, Sarah. "Contributions of correlated motions in dendritic catalysis stereoselectivity of asymmetric direct aldol reactions /." Connect to resource, 2006. http://hdl.handle.net/1811/6622.

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Thesis (Honors)--Ohio State University, 2006.<br>Title from first page of PDF file. Document formatted into pages: contains 59 p.; also includes graphics. Includes bibliographical references (p. 45-46). Available online via Ohio State University's Knowledge Bank.

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48

Barman, Sanmitra. "Helical transition metal complexes as catalysts for asymmetric sulfoxidations and aldol addition reactions." Diss., Kansas State University, 2010. http://hdl.handle.net/2097/7015.

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Doctor of Philosophy<br>Department of Chemistry<br>Christopher J. Levy<br>Stepped helical salen complexes with vanadium as the central metal were synthesized and characterized. The helicity in these complexes arise from the fused phenyl rings (phenanthryl and benz[a]anthryl) as sidearms, whereas the chirality arises from the chiral cyclohexyl diamine or binaphthyl diamine backbones. These complexes showed good yields and moderate enantioselectivity in asymmetric sulfoxidation reactions with methylphenyl sulfide as the substrate and H2O2 or cumene hydroperoxide as the oxidants. To further impro

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49

Crossman, Julia Stephanie, and julia crossman@flinders edu au. "Biomimetic Approaches to the Synthesis of Polyketide Derived Marine Natural Products; (-)-Maurenone and the Spiculoic Acids." Flinders University. SoCPES, 2007. http://catalogue.flinders.edu.au./local/adt/public/adt-SFU20080212.134949.

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This thesis describes the total synthesis of the polyketide derived marine natural product (-)-maurenone (14) and synthetic studies of a model system for the marine polyketides, the spiculoic acids (20, 22-24). A biomimetic approach involving cyclisation of linear polyketide precursors to install the complex chemical frameworks was employed. Maurenone is a polypropionate derived metabolite isolated from pulmonate molluscs collected off the coast of Costa Rica. While structural assignment following isolation revealed a relatively uncommon tetra-substituted dihydropyrone moiety the only ster

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50

Wade, Charles. "Studies towards the total synthesis of isoavenaciolide and the development of the amino tartrate aldol reaction." Thesis, University of Sheffield, 2001. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.341816.

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