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Relevant bibliographies by topics / Amine chirale

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Academic literature on the topic 'Amine chirale'

Author: Grafiati

Published: 4 June 2021

Last updated: 12 February 2022

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Journal articles on the topic "Amine chirale"

1

Nodzewska, Aneta, Agnieszka Wadolowska, Katarzyna Podgorska, Damian Pawelski, and Ryszard Lazny. "Synthesis of Solid-phase Supported Chiral Amines and Investigation of Stereoselectivity of Aldol Reactions of Amine-free Tropinone Enolate." Current Organic Chemistry 23, no. 17 (2019): 1867–79. http://dx.doi.org/10.2174/1385272823666190916145332.

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Seven selected chiral mono-, di-, and tridentate amines supported on insoluble polymer were effectively prepared from corresponding primary amines or secondary amino alcohols and Merrifield resin. The reaction of the polymer-supported amines with excess n-butyllithium gave the corresponding lithium amide bases, which were tested in the aldol reactions of tropinone with benzaldehyde. The deprotonation reactions were carried out with or without separation of the lithium enolate from polymer-supported reagents. Using the procedure with separation of lithium enolate from supported chiral reagent d

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2

Liu, Lei, Dong-Hao Wang, Fei-Fei Chen, et al. "Development of an engineered thermostable amine dehydrogenase for the synthesis of structurally diverse chiral amines." Catalysis Science & Technology 10, no. 8 (2020): 2353–58. http://dx.doi.org/10.1039/d0cy00071j.

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Malcolmson, Steven J., Kangnan Li, and Xinxin Shao. "2-Azadienes as Enamine Umpolung Synthons for the Preparation of Chiral Amines." Synlett 30, no. 11 (2019): 1253–68. http://dx.doi.org/10.1055/s-0037-1611770.

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The development of new strategies for the preparation of chiral amines is an important objective in organic synthesis. In this Synpacts, we summarize our approach for catalytically accessing nucleophilic aminoalkyl metal species from 2-azadienes, and its application in generating a number of important but elusive chiral amine scaffolds. Reductive couplings with ketones and imines afford 1,2-amino tertiary alcohols and 1,2-diamines, respectively, whereas fluoroarylations of gem-difluoro-2-azadienes deliver α-trifluoromethylated benzylic amines.1 Introduction2 Background: Umpolung Strategies for

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Wünsch, Matthias, David Schröder, Tanja Fröhr, et al. "Asymmetric synthesis of propargylamines as amino acid surrogates in peptidomimetics." Beilstein Journal of Organic Chemistry 13 (November 15, 2017): 2428–41. http://dx.doi.org/10.3762/bjoc.13.240.

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The amide moiety of peptides can be replaced for example by a triazole moiety, which is considered to be bioisosteric. Therefore, the carbonyl moiety of an amino acid has to be replaced by an alkyne in order to provide a precursor of such peptidomimetics. As most amino acids have a chiral center at Cα, such amide bond surrogates need a chiral moiety. Here the asymmetric synthesis of a set of 24N-sulfinyl propargylamines is presented. The condensation of various aldehydes with Ellman’s chiral sulfinamide provides chiralN-sulfinylimines, which were reacted with (trimethylsilyl)ethynyllithium to

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5

Fraschetti, Caterina, Marco Pierini, Claudio Villani, Francesco Gasparrini, Antonello Filippi, and Maurizio Speranza. "Gas-phase structure and relative stability of proton-bound homo- and heterochiral clusters of tetra-amide macrocycles with amines." Collection of Czechoslovak Chemical Communications 74, no. 2 (2009): 275–97. http://dx.doi.org/10.1135/cccc2008155.

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The structure, stability, and CID pattern of proton-bound homochiral and heterochiral complexes, formed in the gas phase by the combination of two molecules of a chiral macrocyclic tetra-amide and an amine B, i.e. CH3NH2, (CH3)2NH, or (S)-(–)-1-phenylethylamine, have been examined by ESI-ITMS-CID mass spectrometry. With B = CH3NH2, the CID pattern is characterized by the predominant loss of B, accompanied by a much less extensive release of one tetra-amide molecule. With (S)-(–)-1-phenylethylamine, loss of a tetra-amide molecule efficiently competes with loss of B. Finally, with (CH3)2NH, loss

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6

Rychlewska, Urszula, Wioletta Bendzinska-Berus, Agnieszka Janiak, and Beata Warzajtis. "Mono- & ditrityl ethers, amines & amides – a family of multifaceted materials." Acta Crystallographica Section A Foundations and Advances 70, a1 (2014): C670. http://dx.doi.org/10.1107/s2053273314093292.

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In the course of our recent study on the possible transfer of chirality from the stereogenic center(s) to the inherently helical triphenylmethyl (Tr) substituent we have structurally characterized mono- and ditrityl derivatives of chiral alcohols, amines and amides. During the course of our investigations we have experienced various kinds of packing peculiarities caused by the presence of sterically demanding chiral molecules, e.g. quasi-isomorphism between a pair of enantiomerically pure and racemic crystals, microporosity, lattice inclusion, multiplication of asymmetric units and pseudosymme

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Yu, Qiuhan, Weiwen Lu, Zhiqiang Ding, Min Wei, and Zhenya Dai. "Synthesis of novel chiral fluorescent sensors and their application in enantioselective discrimination of chiral carboxylic acids." Journal of Chemical Research 43, no. 9-10 (2019): 340–46. http://dx.doi.org/10.1177/1747519819867619.

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Novel chiral fluorescent sensors are synthesized from a dibromide containing a tetraphenylethylene moiety and enantiomerically pure amino alcohols and an amine. The sensors are applied for the chiral recognition of a wide range of chiral carboxylic acids and related derivatives.

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8

Burns, Christopher J., Leslie D. Field, Kikuko Hashimoto, Damon D. Ridley, Brian J. Petteys, and Michael Rose. "Synthesis of Stereoisomerically Pure Monoether Lipids." Australian Journal of Chemistry 52, no. 5 (1999): 387. http://dx.doi.org/10.1071/ch99001.

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Four stereoisomerically pure lipids have been synthesized which contain chirally pure phytanol (obtained through resolution of a chiral amide) and chiral glycerol moieties. The lipids were obtained in 7–13% overall yield in eight steps from commercially available materials.

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9

Li, Mao-Lin, Jin-Han Yu, Yi-Hao Li, Shou-Fei Zhu, and Qi-Lin Zhou. "Highly enantioselective carbene insertion into N–H bonds of aliphatic amines." Science 366, no. 6468 (2019): 990–94. http://dx.doi.org/10.1126/science.aaw9939.

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Aliphatic amines strongly coordinate, and therefore easily inhibit, the activity of transition-metal catalysts, posing a marked challenge to nitrogen-hydrogen (N–H) insertion reactions. Here, we report highly enantioselective carbene insertion into N–H bonds of aliphatic amines using two catalysts in tandem: an achiral copper complex and chiral amino-thiourea. Coordination by a homoscorpionate ligand protects the copper center that activates the carbene precursor. The chiral amino-thiourea catalyst then promotes enantioselective proton transfer to generate the stereocenter of the insertion pro

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10

Wang, Hongyue, Ge Qu, Jun-Kuan Li, et al. "Data mining of amine dehydrogenases for the synthesis of enantiopure amino alcohols." Catalysis Science & Technology 10, no. 17 (2020): 5945–52. http://dx.doi.org/10.1039/d0cy01373k.

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Five amine dehydrogenases (AmDHs) derived from amino acid dehydrogenases have been identified and evaluated for the stereoselective amination of α-/β-functionalized carbonyl compounds to synthesize chiral amino alcohols.

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Dissertations / Theses on the topic "Amine chirale"

1

Wilden, Andreas. "Synthese chiraler metallorganischer Amino-Cyclopentadienyl-Komplexe /." Aachen : Mainz, 2009. http://d-nb.info/994128207/04.

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2

Heuson, Egon. "Recherche de nouvelles transaminases pour la synthèse d'amines chirales." Thesis, Clermont-Ferrand 2, 2015. http://www.theses.fr/2015CLF22659/document.

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3

Queval, Pierre. "Phosphures borane de lithium." Caen, 2011. http://www.theses.fr/2011CAEN2053.

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Les phosphures borane de lithium sont des espèces obtenues par déprotonation de phosphines borane secondaires par une base de type alkyllithien. L’analyse de ces composés, dont la structure est peu connue, par spectroscopie de résonance magnétique nucléaire multinoyaux a mis en évidence des interactions entre les atomes de lithium et d’hydrogènes du groupement borane et l’absence d’interaction PLi. En accord avec la structure de ces composés, une réactivité duale de P-nucléophile et de réducteur a été mise en évidence par réaction avec des dérivés carbonylés. L’issue de la réaction dépend des

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4

Garnier, Jean-Marc. "Réactions de cyclisations électrophiles 5-endo énantiosélectives et diastéréospécifiquesApplications à la synthèse de produits naturels." Paris 11, 2007. http://www.theses.fr/2007PA112323.

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Ce mémoire est consacré aux réactions de cyclisations électrophiles énantiosélectives et diastéréospécifiques 5 endo d’acides carboxyliques bétagamma éthyléniques et d’hydroxamates pour fournir des halolactones et des halolactames. Dans une première partie, la synthèse et le screening de nouveaux complexes iodés d’amines chirales ont été examinés comme source d’halogène pour les réactions de cyclisations électrophiles 5-endo. Dans les meilleures conditions, des excès énantiomériques modérés (jusqu’à 45% de ee) ont été obtenus pour la iodolactonisation. La meilleure amine chirale testée est la

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5

Seidel, Christian. "Experimentelle und theoretische Untersuchungen zur Modifizierung der Substratspezifität einer Amin-Pyruvat-Aminotransferase." Doctoral thesis, Universitätsbibliothek Leipzig, 2013. http://nbn-resolving.de/urn:nbn:de:bsz:15-qucosa-125429.

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Mit Aminotransferasen können chirale Amine auf biotechnologischem Weg hergestellt werden. Diese besitzen große Bedeutung als Bausteine für weitere Synthesen in der pharmazeutischen und agrochemischen Industrie. Da natürlich vorkommende Enzyme oft nicht die gewünschte Substratspezifität für bestimmte industrielle Anwendungen besitzen, ist eine Optimierung durch Mutagenese notwendig. Solche Entwicklungen sind jedoch oft mit hohem Zeit- und Kostenaufwand verbunden. Die Optimierung kann entweder ungezielt durch empirische Methoden oder gezielt unter Einbeziehung von Informationen über das Enzym er

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6

Fu, Peng. "Amino Acid-Based Catalysts for Synthesis of Chiral Amines." Thesis, Boston College, 2009. http://hdl.handle.net/2345/1528.

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Ghislieri, Diego. "Application of engineered amine oxidases for the synthesis of chiral amines." Thesis, University of Manchester, 2013. https://www.research.manchester.ac.uk/portal/en/theses/application-of-engineered-amine-oxidases-for-the-synthesis-of-chiral-amines(de93d851-97f8-4422-8dc4-0f7402488021).html.

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The development of cost-effective and sustainable catalytic methods for the production of enantiomerically pure chiral amines is a key challenge facing the pharmaceutical and fine chemical industries. There is an increasing demand for broadly applicable synthetic methods which deliver the desired amine product in high yield and enantiomeric excess (e.e.). Previously we have described the development of variants of monoamine oxidase from Aspergillus niger (MAO-N) which are able to mediate the complete conversion of racemic amines to the corresponding enantiomerically pure products in a single s

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8

Costodes, Taty Cyprien Alain. "Synthèse de diaminocalix[4]arènes chiraux : propriétés conformationnelles et catalyse chirale." Lyon 1, 1993. http://www.theses.fr/1993LYO10130.

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Les diaminocalix|4|arenes chiraux sont des macrocycles constitues de quatre unites phenoliques lies par des ponts methyleniques. La fonction amine chirale qui induit la chiralite dans le calix|4|arene est greffee en position para sur deux unites phenoliques dans un ordre alternatif. De par leur analogie de structure avec les recepteurs moleculaires ditopiques et de forme avec les cyclodextrines, les diaminocalix|4|arenes peuvent avoir des proprietes de mime enzymatique. Il s'avere qu'en greffant deux fonctions amines chirales, ces composes sont a la fois hydrosolubles et liposolubles. En persp

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9

Abrahamson, Michael J. "Development of an amine dehydrogenase." Diss., Georgia Institute of Technology, 2012. http://hdl.handle.net/1853/50138.

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Biocatalysts are increasingly prevalent in the large-scale synthesis of enantiomerically pure compounds. However, many sought-after reactions lack a suitable enzymatic production route. This work describes the development of a novel amine dehydrogenase through the application of directed evolution altering the substrate specificity of an existing leucine dehydrogenase scaffold. Eleven rounds of directed evolution completely altered the enzyme’s specificity and successfully created amination activity. The resulting amine dehydrogenase asymmetrically catalyzes methyl isobutyl ketone and free amm

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10

Hours, Raphaelle. "Directed evolution of amino acid dehydrogenases for biocatalysis of chiral amines." Thesis, University of Cambridge, 2018. https://www.repository.cam.ac.uk/handle/1810/275471.

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By applying the principles of Darwinian natural selection in the laboratory, directed evolution has become a powerful practical approach to study enzymes and optimize them to catalyze industrially relevant transformations. In this thesis, I applied this strategy to the engineering of amino acid dehydrogenases for biocatalysis of chiral amines, focusing on two crucial features for successful directed evolution experiments. A first key aspect is the development of technologies allowing the screening of large libraries of enzyme variants to explore sequence space efficiently. Massive scale-down o

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Books on the topic "Amine chirale"

1

Nugent, Thomas C., ed. Chiral Amine Synthesis. Wiley-VCH Verlag GmbH & Co. KGaA, 2010. http://dx.doi.org/10.1002/9783527629541.

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2

Steensma, Maria. Chiral separation of amino-alcohols and amines by fractional reactive extraction. s.n.], 2005.

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3

1949-, Schuster Herbert F., ed. Asymmetric synthesis: Construction of chiral molecules using amino acids. Wiley, 1987.

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4

Chapman, Daniel Taylor. The enzymatic resolution of chiral amines via substrate engineering. typescript, 1998.

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5

Rahman, Shirley Katherine. Preparation and use of chiral lithium amide bases in organic synthesis. University of Salford, 1988.

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6

Hewitt, Jacqueline Diane. Enantioselective preparation of CIS-Bicyclo [3.3.0] octane derivatives using chiral lithium amide bases. University of Salford, 1990.

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7

Valéry, Paul. Lettres a une amie: 1938-1944 / textes presente et annote par Marcelle Chirac. Fondation de Lourmarin Laurent Vibert\Association des amis de Lourmarin, 1988.

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8

Nugent, Thomas C. Chiral Amine Synthesis: Methods, Developments and Applications. Wiley & Sons, Incorporated, John, 2010.

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9

Chiral Amine Synthesis: Methods, Developments and Applications. Wiley-VCH Verlag GmbH, 2010.

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10

Nugent, Thomas C. Chiral Amine Synthesis: Methods, Developments and Applications. Wiley & Sons, Limited, John, 2010.

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Book chapters on the topic "Amine chirale"

1

Nugent, Thomas C. "Asymmetric Reductive Amination." In Chiral Amine Synthesis. Wiley-VCH Verlag GmbH & Co. KGaA, 2010. http://dx.doi.org/10.1002/9783527629541.ch7.

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2

Charette, André B. "Stereoselective Synthesis of α-Branched Amines by Nucleophilic Addition of Unstabilized Carbanions to Imines." In Chiral Amine Synthesis. Wiley-VCH Verlag GmbH & Co. KGaA, 2010. http://dx.doi.org/10.1002/9783527629541.ch1.

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3

Wang, Da-Wei, Yong-Gui Zhou, Qing-An Chen, and Duo-Sheng Wang. "Enantioselective Reduction of Nitrogen-Based Heteroaromatic Compounds." In Chiral Amine Synthesis. Wiley-VCH Verlag GmbH & Co. KGaA, 2010. http://dx.doi.org/10.1002/9783527629541.ch10.

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4

Reznichenko, Alexander L., and Kai C. Hultzsch. "Asymmetric Hydroamination." In Chiral Amine Synthesis. Wiley-VCH Verlag GmbH & Co. KGaA, 2010. http://dx.doi.org/10.1002/9783527629541.ch11.

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5

Boudet, Nadège, and Simon B. Blakey. "Enantioselective CH Amination." In Chiral Amine Synthesis. Wiley-VCH Verlag GmbH & Co. KGaA, 2010. http://dx.doi.org/10.1002/9783527629541.ch12.

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6

Dai, Lun-Zhi, and Min Shi. "Chiral Amines Derived from Asymmetric Aza-Morita-Baylis-Hillman Reaction." In Chiral Amine Synthesis. Wiley-VCH Verlag GmbH & Co. KGaA, 2010. http://dx.doi.org/10.1002/9783527629541.ch13.

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Turner, Nicholas J., and Matthew D. Truppo. "Biocatalytic Routes to Nonracemic Chiral Amines." In Chiral Amine Synthesis. Wiley-VCH Verlag GmbH & Co. KGaA, 2010. http://dx.doi.org/10.1002/9783527629541.ch14.

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8

Friestad, Gregory K. "Asymmetric Methods for Radical Addition to Imino Compounds." In Chiral Amine Synthesis. Wiley-VCH Verlag GmbH & Co. KGaA, 2010. http://dx.doi.org/10.1002/9783527629541.ch2.

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9

Terada, Masahiro, and Norie Momiyama. "Enantioselective Synthesis of Amines by Chiral Brønsted Acid Catalysts." In Chiral Amine Synthesis. Wiley-VCH Verlag GmbH & Co. KGaA, 2010. http://dx.doi.org/10.1002/9783527629541.ch3.

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Kočcovský, Pavel, and Sigitas Stončcius. "Reduction of Imines with Trichlorosilane Catalyzed by Chiral Lewis Bases." In Chiral Amine Synthesis. Wiley-VCH Verlag GmbH & Co. KGaA, 2010. http://dx.doi.org/10.1002/9783527629541.ch4.

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Conference papers on the topic "Amine chirale"

1

Lüdtke, Diogo Seibert, and Maria Eduarda Contreira. "Enantioselective Arylation of Aliphatic Aldehydes Catalyzed by Chiral Amino Alcohols derived from Amino Acids." In 15th Brazilian Meeting on Organic Synthesis. Editora Edgard Blücher, 2013. http://dx.doi.org/10.5151/chempro-15bmos-bmos2013_2013914213953.

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Kroutil, Wolfgang, Robert C. Simon, Eduardo Busto, et al. "Preparation of chiral prim-, and sec-amines employing biocatalysts." In 15th Brazilian Meeting on Organic Synthesis. Editora Edgard Blücher, 2013. http://dx.doi.org/10.5151/chempro-15bmos-speech5.

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Krzemiński, Marek, and Marta Ćwiklińska. "Synthesis of chiral amines using terpenyl spiroborate esters as catalysts." In The 20th International Electronic Conference on Synthetic Organic Chemistry. MDPI, 2016. http://dx.doi.org/10.3390/ecsoc-20-a046.

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Ghosh, Sudipa, Hui Fang Tan, M. S. Uddin, and K. Hidajat. "Enantioselective Separation of Chiral Aromatic Amino Acids with Surface Functionalized Magnetic Nanoparticles." In 14th Asia Pacific Confederation of Chemical Engineering Congress. Research Publishing Services, 2012. http://dx.doi.org/10.3850/978-981-07-1445-1_431.

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Maniram, K. A., and K. Sreekumar. "Liquid crystalline poly(ester-amide)s containing chiral groups for second harmonic generation." In Smart Materials, Structures and MEMS, edited by Vasu K. Aatre, Vijay K. Varadan, and Vasundara V. Varadan. SPIE, 1998. http://dx.doi.org/10.1117/12.305573.

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Muñoz*, Gaspar Diaz, and Gregory B. Dudley. "Synthesis of (–)-(R)-angustureine by formal alkynylation of a chiral ß-amino ester." In 15th Brazilian Meeting on Organic Synthesis. Editora Edgard Blücher, 2013. http://dx.doi.org/10.5151/chempro-15bmos-bmos2013_201372919131.

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Vallribera, Adelina, Marcial Morena-Manas, Elisenda Trepat, and Rosa Sebastian. "Asymmetric Synthesis of Quaternary a-Amino Acids Using D-Ribonolactone Acetonide as a Chiral Auxiliary." In The 3rd International Electronic Conference on Synthetic Organic Chemistry. MDPI, 1999. http://dx.doi.org/10.3390/ecsoc-3-01717.

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Sepulveda-Argues, Jose, F. Casado-Bellver, Eugenia Gonzalez-Rosende, Amparo Asensio, Patricia Cava-Montesinos, and J. Jorda-Gregori. "Asymmetric synthesis of cis-4,5-disubstituted oxazolidin-2-ones via chiral a-amino epoxides derived from L-Serine." In The 4th International Electronic Conference on Synthetic Organic Chemistry. MDPI, 2000. http://dx.doi.org/10.3390/ecsoc-4-01787.

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Cahard, Dominique, Baptiste Thierry, and Jean-Christophe Plaquevent. "New Chiral Phase Transfer Supported Catalysts in The Asymmetric Synthesis of a -Amino Acids : The Importance of a Spacer." In The 4th International Electronic Conference on Synthetic Organic Chemistry. MDPI, 2000. http://dx.doi.org/10.3390/ecsoc-4-01812.

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Malik, Poonam, and Ravi Bhushan. "Synthesis of (S)-naproxen based amide bond forming chiral reagent and application for liquid chromatographic resolution of (RS)-salbutamol." In ADVANCES IN BASIC SCIENCE (ICABS 2019). AIP Publishing, 2019. http://dx.doi.org/10.1063/1.5122389.

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