Relevant bibliographies by topics / Bicyclo[3.1.0]hexan

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  1. Journal articles
  2. Dissertations / Theses
  3. Book chapters

Academic literature on the topic 'Bicyclo[3.1.0]hexan'

Author: Grafiati
Published: 4 June 2021
Last updated: 14 February 2022

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Journal articles on the topic "Bicyclo[3.1.0]hexan"

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Sims, CG, BW Skelton, D. Wege, and AH White. "Some Transformations of 1,6,7,7-Tetrachlorobicyclo[4.1.0]heptan-3-one. Crystal and Molecular Structure of 4-(Dichloromethylene)-1-methyl-5,6-dihydro-1h-indazol-7(4H)-one." Australian Journal of Chemistry 44, no. 11 (1991): 1575. http://dx.doi.org/10.1071/ch9911575.

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Treatment of the title tetrachloro ketone with triethylamine generates 6,7,7-trichlorobicyclo-[4.1.0]hept-1(2)-en-3-one (4), which can be trapped by furan to give two cycloadducts. In the absence of trapping agent, compound (4) undergoes a methylenecyclopropane rearrangement to yield 5-chloro-6-( dichloromethylene ) bicyclo [3.1.0]hexan-2-one. The strained enone (4) can also be intercepted by diazomethane, which affords the title indazolone, whose characterization was supported by a single-crystal X-ray study.
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Mennen, Steven, Athimoolam Arunachalampillai, Deborah Choquette, Harikrishna Muppalla, and Krishna Sheena. "Scalable Synthesis of 6,6-Dimethylbicyclo[3.1.0]hexan-3-one." Synlett 28, no. 17 (2017): 2330–34. http://dx.doi.org/10.1055/s-0036-1588484.

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A simple five-step process for the conversion of technical grade (+)-3-carene into 6,6-dimethylbicyclo[3.1.0]hexan-3-one was developed. A robust process was required that delivered the 6,6-dimethylbicyclo[3.1.0]hexan-3-one, minimized chromatography, reduced the excess of silver salts, and avoided toxic chromium oxidants. A simple and scalable process that relies on crystallization and distillation was developed and demonstrated to produce hundreds of grams of 6,6-dimethylbicyclo[3.1.0]hexan-3-one.
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3

Sorensen, T. S., and F. Sun. "In situ preparation of cyclopropanones with the bicyclo[3.1.0]hexan-6-one skeleton (substituted examples of the Loftfield intermediate). Confirmation of a very facile intramolecular alkyl cyclopropanone – dienol rearrangement." Canadian Journal of Chemistry 74, no. 1 (1996): 79–87. http://dx.doi.org/10.1139/v96-010.

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Four substituted bicyclo[3.1.0]hexan-6-ones (cyclopropanones) were prepared in situ, starting from the corresponding 2,6-dibromocyclohexanone and reductively removing the bromine atoms with the organometallic salt PPN+Cr(CO)4NO− The reaction is essentially instantaneous at −78 or−100 °C, and can be conveniently carried out in an NMR tube for easy characterization of the products by low-temperature 1H and 13C NMR spectroscopy. The1,5-di-tert-butyl and 1-tert-butyl analogs were thermally stable to ca. 0 °C, but the 1-tert-butyl-5-methyl and 1-tert-butyl-5-ethyl derivatives were extremely labile,
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Kirmse, Wolfgang, and Georg Hellwig. "Desaminierungsreaktionen, 51. Zerfall von Bicyclo[3.1.0]hexan-exo-6-diazonium-Ionen." Chemische Berichte 122, no. 2 (1989): 389–92. http://dx.doi.org/10.1002/cber.19891220231.

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Nishino, Hiroshi, and Kentaro Asahi. "Synthesis of Bicyclo[3.1.0]hexan-2-ones by Manganese(III) Oxidation in Ethanol." Synthesis 2009, no. 03 (2009): 409–23. http://dx.doi.org/10.1055/s-0028-1083324.

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Wang, Xiaoxia, Jianyong Li, Ting Yuan, Bingxin You, Guanqun Xie, and Xin Lv. "Additive Tuned Selective Synthesis of Bicyclo[3.3.0]octan-1-ols and Bicyclo[3.1.0]hexan-1-ols Mediated by AllylSmBr." Journal of Organic Chemistry 83, no. 16 (2018): 8984–94. http://dx.doi.org/10.1021/acs.joc.8b01170.

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Choo, Jaebum, Whe-Yi Chiang, Soo-No Lee, and Jaan Laane. "Far-Infrared Spectra and Ring-Puckering Potential Energy Function of Bicyclo[3.1.0]hexan-3-one." Journal of Physical Chemistry 99, no. 30 (1995): 11636–39. http://dx.doi.org/10.1021/j100030a002.

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8

Hamon, DPG, and NJ Shirley. "A Convenient Synthesis of 5-Alkylbicyclo[3.1.0]hexan-2-ones Including the Natural Product Sabina Ketone." Australian Journal of Chemistry 40, no. 7 (1987): 1321. http://dx.doi.org/10.1071/ch9871321.

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Simple 5-alkylbicyclo[3.1.0]hexan-2-ones, including the natural product sabina ketone, can be prepared in four steps from aromatic ethers via Birch reduction, hydrogen chloride addition, hydrolysis and then base treatment of the resultant 4-chlorocyclohexanones.
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9

Maslivetc, Vladimir, Colby Barrett, Nicolai A. Aksenov, Marina Rubina, and Michael Rubin. "Intramolecular nucleophilic addition of carbanions generated from N-benzylamides to cyclopropenes." Organic & Biomolecular Chemistry 16, no. 2 (2018): 285–94. http://dx.doi.org/10.1039/c7ob02068f.

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An unusual reaction is described, involving a formal intramolecular nucleophilic substitution of bromocyclopropanes with nitrogen ylides generated in situ from N-benzyl carboxamides. This reaction involves cyclopropene intermediates and allows for the facile preparation of 3-azabicyclo[3.1.0]hexan-2-ones.
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Watanabe, Mizuki, Takaaki Kobayashi, Yoshihiko Ito, Shizuo Yamada, and Satoshi Shuto. "Conformational Restriction of Histamine with a Rigid Bicyclo[3.1.0]hexane Scaffold Provided Selective H3 Receptor Ligands." Molecules 25, no. 16 (2020): 3562. http://dx.doi.org/10.3390/molecules25163562.

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We designed and synthesized conformationally rigid histamine analogues with a bicyclo[3.1.0]hexane scaffold. All the compounds were selectively bound to the H3 receptor subtype over the H4 receptor subtype. Notably, compound 7 showed potent binding affinity and over 100-fold selectivity for the H3 receptors (Ki = 5.6 nM for H3 and 602 nM for H4). These results suggest that the conformationally rigid bicyclo[3.1.0]hexane structure can be a useful scaffold for developing potent ligands selective for the target biomolecules.
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Dissertations / Theses on the topic "Bicyclo[3.1.0]hexan"

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Langer, Rainer. "Design und Synthese neuer flüssigkristalliner Substanzen mit zentraler Bicyclo[3.1.0]hexaneinheit." [S.l.] : [s.n.], 2003. http://deposit.ddb.de/cgi-bin/dokserv?idn=968492738.

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Jung, Grace Lorena. "Thermal rearrangement of functionalized 6-exo-(1-alkenyl)bicyclo\3.1.0]hex-2-enes application to the total synthesis of (+)-sinularene." Thesis, University of British Columbia, 1985. http://hdl.handle.net/2429/25806.

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This thesis describes firstly, a study involving the thermal rearrangement of substituted 6-e̲x̲o̲-(1-alkenyl) bicyclo-[3.1.0]hexenes, and secondly, the application of this type of transformation to a total synthesis of (±)-sinularene (1̲2̲5̲). The 6-e̲x̲o̲-(1-alkenyl)bicyclo[3.1.0]hexenes (1̲8̲7̲, 1̲8̲9̲, 1̲9̲2̲, 1̲9̲4̲, 2̲4̲0̲, 2̲7̲4̲ and 340) were prepared and thermolyzed in sealed tubes to afford the corresponding bicyclo[3.2.1]octa-2,6-dienes (1̲8̲8̲, 1̲9̲0̲, 1̲9̲3̲, 1̲9̲5̲, 2̲4̲1̲, 2̲7̲6̲ and 3̲4̲1̲) in generally excellent yields. With the exception of 1̲9̲0̲, the thermolysis products w
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Langer, Rainer. "Design und Synthese neuer flüssigkristalliner Substanzen mit zentraler Bicyclo[3.1.0]hexaneinheit." Doctoral thesis, 2003. http://hdl.handle.net/11858/00-1735-0000-0006-B0BA-6.

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Li, Jing. "Synthesis of Donor-based Analogues as Inhibitors of Mycobacterial Glycosyltransferases." Phd thesis, 2009. http://hdl.handle.net/10048/869.

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Tuberculosis (TB) is the disease arising from infection by Mycobacterial tuberculosis and kills millions of people every year. Difficulties in the treatment of TB and the emergence of multiple-drug resistant and extreme-drug resistant M. tuberculosis strains have increased interest in finding new antimycobacterial agents. The cell wall of mycobacteria is essential for the survival of these bacteria and enzymes involved in its assembly are key targets for anti-mycobacterial chemotherapy. One of the largest components of the cell wall is the arabinogalactan, which is composed of arabinofurano
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Langer, Rainer [Verfasser]. "Design und Synthese neuer flüssigkristalliner Substanzen mit zentraler Bicyclo[3.1.0]hexaneinheit / vorgelegt von Rainer Langer." 2003. http://d-nb.info/968492738/34.

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Book chapters on the topic "Bicyclo[3.1.0]hexan"

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Whitesell, James K., and Mark A. Minton. "Bicyclo[3.1.0]hexanes." In Stereochemical Analysis of Alicyclic Compounds by C-13 NMR Spectroscopy. Springer Netherlands, 1987. http://dx.doi.org/10.1007/978-94-009-3161-9_8.

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2

Li, Jie Jack, and Minmin Yang. "Bicyclo[3.1.0]hexanes." In Drug Discovery with Privileged Building Blocks. CRC Press, 2021. http://dx.doi.org/10.1201/9781003190806-7.

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3

Piers, Edward. "The Preparation and Thermal Rearrangement of Functionalized 6-(1-Alkenyl)Bicyclo[3.1.0]Hex-2-Enes. Applications to synthesis." In Strain and Its Implications in Organic Chemistry. Springer Netherlands, 1989. http://dx.doi.org/10.1007/978-94-009-0929-8_3.

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4

"3. durch Photoisomerisierung von 2,3-Diaza-bicyclo[3.1.0]hex-2-enen unter Ringöffnung." In En,X- und In,X-Verbindungen, edited by Heinz Kropf and Ernst Schaumann. Georg Thieme Verlag, 1993. http://dx.doi.org/10.1055/b-0035-112204.

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You might also be interested in the extended bibliographies on the topic 'Bicyclo[3.1.0]hexan' for particular source types:
Journal articles
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