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Journal articles on the topic 'Chemistry, Organic. Electrolysis'

Author: Grafiati

Published: 4 June 2021

Last updated: 1 February 2022

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1

Schulz, Lara, and Siegfried Waldvogel. "Solvent Control in Electro-Organic Synthesis." Synlett 30, no. 03 (2018): 275–86. http://dx.doi.org/10.1055/s-0037-1610303.

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Exploiting the solvent control within electro-organic conversions is a far underestimated parameter in prep-scale electrolysis. The beneficial application in several transformations is outlined and in particular discussed for the dehydrogenative coupling of arenes and heteroarenes. This simple electrolytic strategy in fluorinated solvents allows the modulation of the substrate’s nucleophilicity and the stabilization of the intermediates as well as of the final product from over-oxidation.1 Introduction2 Solvent Effects in Kolbe Electrolysis and Anodic Fluorination3 Unique Solvent Effects of 1,

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2

Sbei, Najoua, Tomas Hardwick, and Nisar Ahmed. "Green Chemistry: Electrochemical Organic Transformations via Paired Electrolysis." ACS Sustainable Chemistry & Engineering 9, no. 18 (2021): 6148–69. http://dx.doi.org/10.1021/acssuschemeng.1c00665.

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3

Gu, Z. H., T. Z. Fahidy, R. Hornsey, and A. Nathan. "A study of the electrochemical synthesis of ZnO thin films." Canadian Journal of Chemistry 75, no. 11 (1997): 1439–44. http://dx.doi.org/10.1139/v97-173.

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The principal characteristics of the cathode deposition of zinc oxide from slightly acidified aqueous zinc nitrate solution at 65 °C were studied via potentiodynamic electrolysis, potentiostatic electrolysis, and X-ray diffraction patterns. The results indicate the reliability of a low-temperature electrolytic path of synthesis, and avenues of further exploration. Keywords: zinc oxide, cathode deposition, XRD patterns, FBM theory.

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4

Pletcher, Derek, Robert A. Green, and Richard C. D. Brown. "Flow Electrolysis Cells for the Synthetic Organic Chemistry Laboratory." Chemical Reviews 118, no. 9 (2017): 4573–91. http://dx.doi.org/10.1021/acs.chemrev.7b00360.

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5

Ren, Jie, Mengqi Yao, Wu Yang, Yan Li, and Jinzhang Gao. "Recent progress in the application of glow-discharge electrolysis plasma." Open Chemistry 12, no. 12 (2014): 1213–21. http://dx.doi.org/10.2478/s11532-014-0575-6.

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AbstractNon-equilibrium plasma makes it is possible to modify surface chemistry, synthetize polymer materials, and oxidize some organic compounds completely by generation of energetic and chemically active species in gas or liquid phases. Glow-discharge electrolysis plasma (GDEP) has been intensely studied for applications in chemistry and in material, environmental, and biomedical engineering during the last few years because of the very highly active chemical species produced during the glow-discharge electrolysis (GDE) process. A brief review is already available regarding applications of g

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6

Hlavatý, Jaromír, and Jiří Volke. "Use of Nafion membranes in laboratory organic electrosynthesis." Collection of Czechoslovak Chemical Communications 53, no. 12 (1988): 3164–70. http://dx.doi.org/10.1135/cccc19883164.

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Electrolysis of quaternary ammonium bromides and iodides in a divided cell with a Nafion membrane yields quaternary polyhalogenides at a carbon anode in water-ethanolic anolytes. The electrodialysis of tetrabutylammonium iodide in a cell with a Nafion membrane enables generation of tetrabutylammonium hydroxide. In electrolytic reduction of nitrobenzene in presence of 1,3-dibromopropane, N-phenylisooxazolidine results in an approx. 60% yield. This electrosynthesis takes place in dimethylformamide with tetrabutylammonium bromide at a glassy-carbon cathode in a divided cell. In the electroreducti

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7

Bouchard, Luc, Ian Marcotte, Jean Marc Chapuzet, and Jean Lessard. "Electroreduction of 1-methyl 5-nitroindole, 5-nitrobenzofurane, and 5-nitrobenzothiophene in acidic and basic hydroorganic media: Generation and trapping of iminoquinone-type intermediates and electrosynthesis of ring-substituted amino derivatives." Canadian Journal of Chemistry 81, no. 10 (2003): 1108–18. http://dx.doi.org/10.1139/v03-149.

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Preparative electrolysis of 1-methyl-5-nitroindole (1b, X = NCH3), 5-nitrobenzofurane (1c, X = O), and 5-nitrobenzothiophene (1d, X = S) at Hg, in acidic hydromethanolic media, leads to the formation of the corresponding 4-substituted amino derivatives 5, which result from the 100% regioselective addition to iminoquinone-type intermediate 4 of methanol or of any other good nucleophile present in the electrolytic solution. In acidic medium, the iminoquinonium intermediates 4b and 4c were trapped in a cycloaddition reaction with cyclopentadiene added to the electrolysis medium. The regiochemistr

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8

Rodrigo, Sachini, Disni Gunasekera, Jyoti P. Mahajan, and Long Luo. "Alternating current electrolysis for organic synthesis." Current Opinion in Electrochemistry 28 (August 2021): 100712. http://dx.doi.org/10.1016/j.coelec.2021.100712.

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9

TAKEHARA, Zen-ichiro, and Zempachi OGUMI. "New electrolysis methods." Journal of Synthetic Organic Chemistry, Japan 43, no. 6 (1985): 575–82. http://dx.doi.org/10.5059/yukigoseikyokaishi.43.575.

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10

Scheide, Marcos R., Celso R. Nicoleti, Guilherme M. Martins, and Antonio L. Braga. "Electrohalogenation of organic compounds." Organic & Biomolecular Chemistry 19, no. 12 (2021): 2578–602. http://dx.doi.org/10.1039/d0ob02459g.

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In this review we target sp, sp<sup>2</sup> and sp<sup>3</sup> carbon fluorination, chlorination, bromination and iodination reactions using electrolysis as a redox medium. Mechanistic insights and substrate reactivity are also discussed.

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11

Jones, Alan M., and Craig E. Banks. "The Shono-type electroorganic oxidation of unfunctionalised amides. Carbon–carbon bond formation via electrogenerated N-acyliminium ions." Beilstein Journal of Organic Chemistry 10 (December 18, 2014): 3056–72. http://dx.doi.org/10.3762/bjoc.10.323.

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N-acyliminium ions are useful reactive synthetic intermediates in a variety of important carbon–carbon bond forming and cyclisation strategies in organic chemistry. The advent of an electrochemical anodic oxidation of unfunctionalised amides, more commonly known as the Shono oxidation, has provided a complementary route to the C–H activation of low reactivity intermediates. In this article, containing over 100 references, we highlight the development of the Shono-type oxidations from the original direct electrolysis methods, to the use of electroauxiliaries before arriving at indirect electrol

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12

Selt, Maximilian, Stamo Mentizi, Dieter Schollmeyer, Robert Franke, and Siegfried R. Waldvogel. "Selective and Scalable Dehydrogenative Electrochemical Synthesis of 3,3′,5,5′-Tetramethyl-2,2′-biphenol." Synlett 30, no. 18 (2019): 2062–67. http://dx.doi.org/10.1055/s-0039-1690706.

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3,3′,5,5′-Tetramethyl-2,2′-biphenol is a compound of high technical significance, as it exhibits superior properties as building block for ligands in the transition-metal catalysis. However, side reactions and overoxidation are challenging issues in the conventional synthesis of this particular biphenol. Here, an electrochemical method is presented as powerful and sustainable alternative to conventional chemical strategies, which gives good yields up to 51%. Despite using inexpensive and well-available bromide-containing supporting electrolytes, the issue of bromination and general byproduct f

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13

Cheong, Amoy Kam, Yvon Bolduc та Jean Lessard. "Electrocatalytic hydrogenation of ketones and of α- and β-diketones on Raney metal electrodes". Canadian Journal of Chemistry 71, № 11 (1993): 1850–56. http://dx.doi.org/10.1139/v93-232.

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The electrocatalytic hydrogenation (ECH) of various ketones was investigated at codeposited Raney metal electrodes in aqueous methanol. The influence of different parameters (pH, supporting electrolyte, and water percentage) on the ECH of cyclohexanone and acetophenone was studied. The relative ease of electrohydrogenation of a variety of monoketones was determined in competitive electrolyses. The ECH of α- and β-diketones was carried out and different products were obtained selectively by the right choice of catalytic material and electrolysis conditions. The diastereoselectivity of the forma

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14

Rusling, James F. "Green synthesis via electrolysis in microemulsions." Pure and Applied Chemistry 73, no. 12 (2001): 1895–905. http://dx.doi.org/10.1351/pac200173121895.

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Electrolysis in microemulsions is a promising approach for environmentally friendly chemical synthetic methods of the future. Employing microemulsions instead of organic solvents for electrosynthesis has the advantages of lower toxicity and cost, high dissolving power for reactants and mediators of unlike solubility, enhancement of reaction rates by controlling the reduction potentials of mediators, possible reaction pathway control, and recycling of microemulsion components. This paper reviews recent progress in using microemulsions for direct and mediated electrosynthesis, including formatio

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15

Polat, Kamran, Mustafa Uçar, M. Levent Aksu, and Hüseyin Ünver. "Electrochemical behaviour of 1-{[(3-halophenyl)imino]methyl}-2-naphthol Schiff bases on graphite electrodes." Canadian Journal of Chemistry 82, no. 7 (2004): 1150–56. http://dx.doi.org/10.1139/v04-021.

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An electrochemical study of the reduction of 1-{[(3-halophenyl)imino]methyl}-2-naphthol compounds on graphite electrodes was carried out. All the compounds were dissolved in a 1:4 (volume fraction) mixture of tetrahydrofuran (THF) and methanol. NaClO4 (0.1 mol L1) was used as the supporting electrolyte. Cyclic voltammetry, chronoamperometry, constant-potential coulometry (bulk electrolysis), and constant-potential preparative electrolysis were employed. The cyclic voltammetric data revealed that the reduction on graphite was irreversible and followed an EC mechanism. The diffusion coefficient

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16

Sbei, Najoua, Samina Aslam, and Nisar Ahmed. "Organic synthesis via Kolbe and related non-Kolbe electrolysis: an enabling electro-strategy." Reaction Chemistry & Engineering 6, no. 8 (2021): 1342–66. http://dx.doi.org/10.1039/d1re00047k.

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17

Xu, Huizhu, Ke Ye, Kai Zhu, et al. "Efficient bifunctional catalysts synthesized from three-dimensional Ni/Fe bimetallic organic frameworks for overall urea electrolysis." Dalton Transactions 49, no. 17 (2020): 5646–52. http://dx.doi.org/10.1039/d0dt00605j.

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18

Rodrigo, Sachini, Chanchamnan Um, Jason C. Mixdorf, Disni Gunasekera, Hien M. Nguyen, and Long Luo. "Alternating Current Electrolysis for Organic Electrosynthesis: Trifluoromethylation of (Hetero)arenes." Organic Letters 22, no. 17 (2020): 6719–23. http://dx.doi.org/10.1021/acs.orglett.0c01906.

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19

Mahmoud, Mohamed, Prathap Parameswaran, César I. Torres, and Bruce E. Rittmann. "Relieving the fermentation inhibition enables high electron recovery from landfill leachate in a microbial electrolysis cell." RSC Advances 6, no. 8 (2016): 6658–64. http://dx.doi.org/10.1039/c5ra25918e.

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The energy value of the organic matter in landfill leachate can be captured with a microbial electrolysis cell (MEC), which oxidizes organic compounds at an anode and generates H<sub>2</sub>gas at a cathode.

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20

Ali, Noralisya, Chee Yeoh, Seng Lau, and Meng Tay. "An enhanced treatment efficiency for diluted palm oil mill effluent using a photo-electro-fenton hybrid system." Journal of the Serbian Chemical Society 84, no. 5 (2019): 517–26. http://dx.doi.org/10.2298/jsc181016103a.

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Photocatalysis, electrolysis and Fenton process are three important advanced oxidation processes (AOPs) which produce hydroxyl radical in order to degrade organic matter in wastewater within 4-6 hours under ambient conditions. A photocatalysis, electrolysis and Fenton (photo-electro-Fenton) process hybrid system has been carried out to treat the diluted palm oil mill effluent (POME) in this study. An electrolytic cell was set up with a stainless steel anode and a platinum wire cathode with the applied cell voltage of 1.5 V. The diluted POME was then treated in the cell with the mixture of tita

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21

Wang, C. R., J. Wang, X. G. Ma, H. Li, and S. Z. Zhang. "Mineralization of Quinoline by BDD Anodes: Variable Effects and Its Effluent Characteristics." Journal of Chemistry 2015 (2015): 1–8. http://dx.doi.org/10.1155/2015/617850.

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BDD anodes were selected for quinoline mineralization and influence of operating parameters, such as current density, initial quinoline concentration, supporting electrolyte, and initial pH was investigated. Based on the consideration of quinoline removal efficiency and average current efficiency, at initial quinoline concentration of 50 mg L−1and pH of 7, the optimal condition was confirmed as current density of 75 mA cm−2, electrolysis time of 1.5 h, and Na2SO4concentration of 0.05 mol L−1by orthogonal test. At different electrolysis time, its effluent characteristics were focused on. The bi

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22

Kiakojouri, Ali, Ebrahim Nadimi, and Irmgard Frank. "Ab-Initio Molecular Dynamics Simulation of Condensed-Phase Reactivity: The Electrolysis of Amino Acids and Peptides." Molecules 25, no. 22 (2020): 5415. http://dx.doi.org/10.3390/molecules25225415.

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Electrolysis is a potential candidate for a quick method of wastewater cleansing. However, it is necessary to know what compounds might be formed from bioorganic matter. We want to know if there are toxic intermediates and if it is possible to influence the product formation by the variation in initial conditions. In the present study, we use Car–Parrinello molecular dynamics to simulate the fastest reaction steps under such circumstances. We investigate the behavior of amino acids and peptides under anodic conditions. Such highly reactive situations lead to chemical reactions within picosecon

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23

Martínez, Natalia P., Mauricio Isaacs, and Kamala Kanta Nanda. "Paired electrolysis for simultaneous generation of synthetic fuels and chemicals." New Journal of Chemistry 44, no. 15 (2020): 5617–37. http://dx.doi.org/10.1039/c9nj06133a.

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24

Lu, Lingxiang, Niankai Fu, and Song Lin. "Three-Component Chlorophosphinoylation of Alkenes via Anodically Coupled Electrolysis." Synlett 30, no. 10 (2019): 1199–203. http://dx.doi.org/10.1055/s-0039-1689934.

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We report the development of an electrocatalytic protocol for the chlorophosphinoylation of simple alkenes. Driven by electricity and mediated by a Mn catalyst, the heterodifunctionalization reaction takes place with high efficiency and regioselectivity. Cyclic voltammetry data are consistent with a mechanistic scenario based on anodically coupled electrolysis in which the generation of two distinct radical intermediates occur simultaneously on the anode and are both mediated by the Mn catalyst.

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25

Myren, Tessa H. T., Taylor A. Stinson, Zachary J. Mast, Chloe G. Huntzinger, and Oana R. Luca. "Chemical and Electrochemical Recycling of End-Use Poly(ethylene terephthalate) (PET) Plastics in Batch, Microwave and Electrochemical Reactors." Molecules 25, no. 12 (2020): 2742. http://dx.doi.org/10.3390/molecules25122742.

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This work describes new methods for the chemical recycling of end-use poly(ethylene terephthalate) (PET) in batch, microwave and electrochemical reactors. The reactions are based on basic hydrolysis of the ester moieties in the polymer framework and occur under mild reaction conditions with low-cost reagents. We report end-use PET depolymerization in refluxing methanol with added NaOH with 75% yield of terephthalic acid in batch after 12 h, while yields up to 65% can be observed after only 40 min under microwave irradiation at 85 °C. Using basic conditions produced in the electrochemical reduc

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26

Holzhäuser, F. Joschka, Joel B. Mensah, and Regina Palkovits. "(Non-)Kolbe electrolysis in biomass valorization – a discussion of potential applications." Green Chemistry 22, no. 2 (2020): 286–301. http://dx.doi.org/10.1039/c9gc03264a.

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The bio-availability of organic acids as platform chemicals and the potential of electrochemistry to directly integrate renewable energy into new value chains drive (Non-)Kolbe electrolysis to become an attractive tool in future electro-bio-refinery.

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27

Sengmany, Stéphane, Thierry Martens, Anthony Ollivier, Marine Rey, and Eric Léonel. "Direct Phosphonylation of N-Carbamate-tetrahydroisoquinoline by Convergent Paired Electrolysis." Synlett 31, no. 12 (2020): 1191–96. http://dx.doi.org/10.1055/s-0039-1690899.

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Mild experimental conditions for a direct phosphonylation of an easily cleavable N-carbamate-tetrahydroisoquinoline have been described under constant current electrolysis. The developed electrochemical process allowed to prepare α-aminophosphonates in moderate to good yields. On the basis of the experimental results, a mechanism proceeding through a convergent paired electrochemical process was enabled to be postulated.

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28

Logan, Bruce E., Douglas Call, Shaoan Cheng, et al. "Microbial Electrolysis Cells for High Yield Hydrogen Gas Production from Organic Matter." Environmental Science & Technology 42, no. 23 (2008): 8630–40. http://dx.doi.org/10.1021/es801553z.

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29

Shang, Xiao, Xuan Liu, and Yujie Sun. "Flexible on-site halogenation paired with hydrogenation using halide electrolysis." Green Chemistry 23, no. 5 (2021): 2037–43. http://dx.doi.org/10.1039/d0gc04362a.

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30

Merica, Simona G., Wojceich Jedral, Susan Lait, Peter Keech, and Nigel J. Bunce. "Electrochemical reduction and oxidation of DDT." Canadian Journal of Chemistry 77, no. 7 (1999): 1281–87. http://dx.doi.org/10.1139/v99-113.

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Electrolysis has been studied as a possible method to treat DDT wastes. In methanol, the major process was dehydrochlorination to DDE followed by further reduction. In an aqueous emulsion containing 1% heptane and 0.1% Triton SP-175®, DDT was reduced at a deposited lead electrode with sodium sulphate as the supporting electrolyte by sequential hydrodechlorination of the aliphatic chlorine atoms. An excellent material balance was achieved, but the current efficiency was poor, even at low current densities. Electrooxidation of DDT was also investigated; in aqueous solutions or emulsion, little o

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31

Kulangiappar, K., M. Ramaprakash, D. Vasudevan, and T. Raju. "Electrochemical bromination of cyclic and acyclic enes using biphasic electrolysis." Synthetic Communications 46, no. 2 (2016): 145–53. http://dx.doi.org/10.1080/00397911.2015.1125498.

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32

Jud, Wolfgang, C. Oliver Kappe, and David Cantillo. "Catalyst-Free Oxytrifluoromethylation of Alkenes through Paired Electrolysis in Organic-Aqueous Media." Chemistry - A European Journal 24, no. 65 (2018): 17234–38. http://dx.doi.org/10.1002/chem.201804708.

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33

Matsuda, Yoshiharu, Masayuki Morita, Hiroshi Yamamoto, Hiroyuki Watanabe, Tooru Seita, and Akira Akimoto. "Chlorination of Poly(vinyltoluene) by Electrolysis in an Organic/Water Suspension System." Bulletin of the Chemical Society of Japan 58, no. 11 (1985): 3413–14. http://dx.doi.org/10.1246/bcsj.58.3413.

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34

Kunugi, Yoshihito, Po‐Chang Chen, Tsutomu Nonaka, Yong‐Bo Chong, and Nobuatsu Watanabe. "Electrolysis of Emulsions of Organic Compounds on Hydrophobic Electrodes." Journal of The Electrochemical Society 140, no. 10 (1993): 2833–36. http://dx.doi.org/10.1149/1.2220918.

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35

Chmielarz, Paweł, Tomasz Pacześniak, Katarzyna Rydel-Ciszek, Izabela Zaborniak, Paulina Biedka, and Andrzej Sobkowiak. "Synthesis of naturally-derived macromolecules through simplified electrochemically mediated ATRP." Beilstein Journal of Organic Chemistry 13 (November 20, 2017): 2466–72. http://dx.doi.org/10.3762/bjoc.13.243.

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The flavonoid-based macroinitiator was received for the first time by the transesterification reaction of quercetin with 2-bromoisobutyryl bromide. In accordance with the “grafting from” strategy, a naturally-occurring star-like polymer with a polar 3,3',4',5,6-pentahydroxyflavone core and hydrophobic poly(tert-butyl acrylate) (PtBA) side arms was synthesized via a simplified electrochemically mediated ATRP (seATRP), utilizing only 78 ppm by weight (wt) of a catalytic CuII complex. To demonstrate the possibility of temporal control, seATRP was carried out utilizing a multiple-step potential el

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36

Monteil, Hélène, Nihal Oturan, Yoan Péchaud, and Mehmet A. Oturan. "Efficient removal of diuretic hydrochlorothiazide from water by electro-Fenton process using BDD anode: a kinetic and degradation pathway study." Environmental Chemistry 16, no. 8 (2019): 613. http://dx.doi.org/10.1071/en19121.

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Environmental contextHydrochlorothiazide, a common diuretic pharmaceutical, occurs in environmental waters because current treatment technologies are unable to eliminate it from wastewater. To remove this environmentally hazardous chemical from water, we developed an advanced electrochemical oxidation process to efficiently degrade and mineralise the compound. Wider application of the process holds the promise of general, efficient destruction of pharmaceuticals in aqueous media. AbstractThe degradation and the mineralisation of the diuretic hydrochlorothiazide were studied by an advanced elec

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37

Yuan, Deng, Qin Jingjing, Hu Xiaohong, et al. "Electrolysis for Colored Organic Wastewater Treatment——Introduction of a Comprehensive Experiment of the Physical Chemistry Laboratory." University Chemistry 30, no. 6 (2015): 67–74. http://dx.doi.org/10.3866/pku.dxhx20150667.

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38

Wang, Lei. "Aqueous organic dye discoloration induced by contact glow discharge electrolysis." Journal of Hazardous Materials 171, no. 1-3 (2009): 577–81. http://dx.doi.org/10.1016/j.jhazmat.2009.06.037.

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39

Harada, Yasuhiro, Shojiro Maki, Haruki Niwa, Takashi Hirano, and Shosuke Yamamura. "Synthesis of (±)-Isoitalicene by Electrolysis under Irradiation as a Key Step." Synlett 1998, no. 12 (1998): 1313–14. http://dx.doi.org/10.1055/s-1998-1982.

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40

Mahdavi, Behzad, Philippe Chambrion, Julie Binette, Eric Martel, and Jean Lessard. "Electrocatalytic hydrogenation of conjugated enones on nickel boride, nickel, and Raney nickel electrodes." Canadian Journal of Chemistry 73, no. 6 (1995): 846–52. http://dx.doi.org/10.1139/v95-105.

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The selectivity of the electrocatalytic hydrogenation (ECH) of conjugated enones to the corresponding carbonyl compounds has been investigated in aqueous methanol under constant current at nickel boride, fractal nickel, and Raney nickel electrodes made of pressed powders. The influence of various parameters (water percentage, pH, concentration of substrate, and current density) on the selectivity of the carbon–carbon double bond hydrogenation was studied with cyclohex-2-en-1-one at nickel boride electrodes. Under given electrolysis conditions, fractal nickel electrodes were found to give the h

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41

Saji, Tetsuo, Katsuyoshi Hoshino, Yoshiyuki Ishii, and Masayuki Goto. "Formation of organic thin films by electrolysis of surfactants with the ferrocenyl moiety." Journal of the American Chemical Society 113, no. 2 (1991): 450–56. http://dx.doi.org/10.1021/ja00002a011.

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42

Pandolfi, Fabiana, Isabella Chiarotto, and Marta Feroci. "Electrochemically modified Corey–Fuchs reaction for the synthesis of arylalkynes. The case of 2-(2,2-dibromovinyl)naphthalene." Beilstein Journal of Organic Chemistry 14 (April 23, 2018): 891–99. http://dx.doi.org/10.3762/bjoc.14.76.

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The electrochemical reduction of 2-(2,2-dibromovinyl)naphthalene in a DMF solution (Pt cathode) yields selectively 2-ethynylnaphthalene or 2-(bromoethynyl)naphthalene in high yields, depending on the electrolysis conditions. In particular, by simply changing the working potential and the supporting electrolyte, the reaction can be directed towards the synthesis of the terminal alkyne (Et4NBF4) or the bromoalkyne (NaClO4). This study allowed to establish that 2-(bromoethynyl)naphthalene can be converted into 2-ethynylnaphthalene by cathodic reduction.

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43

Zhao, Dongni, Yuezhen Lu, and Dongge Ma. "Effects of Structure and Constituent of Prussian Blue Analogs on Their Application in Oxygen Evolution Reaction." Molecules 25, no. 10 (2020): 2304. http://dx.doi.org/10.3390/molecules25102304.

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The importance of advanced energy-conversion devices such as water electrolysis has manifested dramatically over the past few decades because it is the current mainstay for the generation of green energy. Anodic oxygen evolution reaction (OER) in water splitting is one of the biggest obstacles because of its extremely high kinetic barrier. Conventional OER catalysts are mainly noble-metal oxides represented by IrO2 and RuO2, but these compounds tend to have poor sustainability. The attention on Prussian blue (PB) and its analogs (PBA) in the field of energy conversion systems was concentrated

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44

Hyo Kim, Byeong, Young Moo Jun, Yong Rack Choi, Doo Byung Lee, and Woonphil Baik. "Electrochemical Synthesis of 2,1-Benzisoxazoles by Controlled Potential Cathodic Electrolysis." HETEROCYCLES 48, no. 4 (1998): 749. http://dx.doi.org/10.3987/com-97-8077.

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45

Petrosyan, V. A., M. E. Niyazymbetov, S. P. Kolesnikov, and V. Ya Li. "Formation of organotrichlorogermanes upon the electrolysis of GeCl4 in the presence of organic halides." Bulletin of the Academy of Sciences of the USSR Division of Chemical Science 36, no. 2 (1987): 422. http://dx.doi.org/10.1007/bf00959406.

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46

Salem, R. R. "Theory of the electrolysis of water." Protection of Metals 44, no. 2 (2008): 120–25. http://dx.doi.org/10.1134/s0033173208020021.

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47

Shimakoshi, Hisashi, and Yoshio Hisaeda. "Bioinspired Molecular Transformations by Biorelated Metal Complexes Combined with Electrolysis and Photoredox Systems." Journal of Synthetic Organic Chemistry, Japan 76, no. 9 (2018): 894–903. http://dx.doi.org/10.5059/yukigoseikyokaishi.76.894.

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48

Fry, Albert J., and Andrew H. Singh. "Cobalt(salen)-Electrocatalyzed Reduction of Benzal Chloride. Dependence of Products upon Electrolysis Potential." Journal of Organic Chemistry 59, no. 26 (1994): 8172–77. http://dx.doi.org/10.1021/jo00105a038.

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Shmychkova, O., I. Borovik, D. Girenko, P. Davydenko, and A. Velichenko. "The effect of impurities on the stability of low concentrated eco-friendly solutions of NaOCl." Voprosy Khimii i Khimicheskoi Tekhnologii, no. 4 (July 2021): 142–50. http://dx.doi.org/10.32434/0321-4095-2021-137-4-142-150.

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Abstract:

The synthesis of hypochlorous acid from low concentrated chloride-containing electrolytes has been studied on various oxide materials at the anode current density of 50 mA cm–2. Boron doped diamond, platinized titanium, metallic titanium doped with platinum and palladium and materials based on lead (IV) oxide modified with fluorine and surfactants turned out to be promising for the synthesis of hypochlorous acid by electrolysis. Whereas, given the stability of oxidant synthesis during cumulative electrolysis, titanium modified with platinum and palladium as well as pre-treated lead (IV) oxide

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50

Kong, Fanjun, Fangtian Yu, Wenqian Lu, Zhengqiu Yuan, and Bin Qian. "An Organic/Inorganic Synergistic Electrolysis for Overcharge Protection of Electric Vehicle Batteries." Industrial & Engineering Chemistry Research 58, no. 5 (2019): 1787–93. http://dx.doi.org/10.1021/acs.iecr.8b05278.

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