Relevant bibliographies by topics / Chiralpak AD

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  1. Journal articles
  2. Dissertations / Theses

Academic literature on the topic 'Chiralpak AD'

Author: Grafiati
Published: 4 June 2021
Last updated: 11 February 2022

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Journal articles on the topic "Chiralpak AD"

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Zhang, Ping, Yuhan He, Sheng Wang, et al. "Chiral Separation and Determination of Etoxazole Enantiomers in Vegetables by Normal-Phase and Reverse-Phase High Performance Liquid Chromatography." Molecules 25, no. 14 (2020): 3134. http://dx.doi.org/10.3390/molecules25143134.

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The chiral separation of etoxazole enantiomers on Lux Cellulose-1, Lux Cellulose-3, Chiralpak IC, and Chiralpak AD chiral columns was carefully investigated by normal-phase high performance liquid chromatography and reverse-phase high performance liquid chromatography (HPLC). Hexane/isopropanol, hexane/n-butanol, methanol/water, and acetonitrile/water were used as mobile phase at a flow rate of 0.8 mL/min. The effects of chiral stationary phase, mobile phase component, mobile phase ratio, and temperature on etoxazole separation were also studied. Etoxazole enantiomers were baseline separated o
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R., Čižmáriková, Némethy A., Valentová J., Hroboňová K., and Adamcová K. "Synthesis of new compounds of the aryloxyaminopropanol type and their HPLC enantioseparation." Acta Facultatis Pharmaceuticae Universitatis Comenianae 60, no. 2 (2013): 37–42. http://dx.doi.org/10.2478/afpuc-2013-0023.

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Abstract This article describes a preparation of some new compounds of the aryloxyaminopropanol type derived from 4-hydroxyphenylpropan- 1-one with phenylamino, cyclohexylamino and isobutylamino group in the hydrophilic part and methoxymethyl or ethoxymethyl substituent in the lipophilic part of the molecule. The purity of the prepared compounds was checked by thinlayer chromatography and the structure was confirmed on the basis of interpretation of the IR, UV, 1H NMR and 13C NMR spectra. An enantioseparation of the prepared compounds was performed by using high-performance liquid chromatograp
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Zhang, Tao, Mengya Liao, Ye Tian, et al. "HPLC Determination of Enantiomeric Purity of Letermovir Based on CHIRALPAK AD." Journal of Chromatographic Science 54, no. 9 (2016): 1495–500. http://dx.doi.org/10.1093/chromsci/bmw042.

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QIU, GeBin, LeYi ZHENG, QuanZhen LV, JinBo ZHANG, Jun WEN, and ZhanYing HONG. "Enantiomeric separation of arotinolol by Chiralpak AD-H chiral column HPLC method." Pharmaceutical Care and Research 15, no. 5 (2015): 351–53. http://dx.doi.org/10.5428/pcar20150509.

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Ning, Jian G. "Direct chiral separation with Chiralpak AD converted to the reversed-phase mode." Journal of Chromatography A 805, no. 1-2 (1998): 309–14. http://dx.doi.org/10.1016/s0021-9673(98)00035-1.

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Kalíková, Květa, Radim Geryk, Jiří Vozka, and Eva Tesařová. "Evaluation of differences between Chiralpak IA and Chiralpak AD-RH amylose-based chiral stationary phases in reversed-phase high-performance liquid chromatography." Journal of Separation Science 38, no. 5 (2015): 711–19. http://dx.doi.org/10.1002/jssc.201401002.

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Čižmáriková, R., S. Chudáčiková, J. Valentová, and A. Némethy. "Synthesis and enantioseparation of derivatives of propranolol." Acta Facultatis Pharmaceuticae Universitatis Comenianae 59, no. 1 (2012): 5–13. http://dx.doi.org/10.2478/v10219-012-0012-x.

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Synthesis and enantioseparation of derivatives of propranololPropranolol is one of the first prepared and in therapeutic praxis used beta- adrenolytics. In this paper novel derivatives of propranolol with cyclohexylamino and pyrrolidin-1-yl groups in hydrophilic part were prepared. HPLC-enantioseparation propranolol (as reference compound) and of the prepared derivatives has been achieved using a Chiralpak AD CSP based on the amylose tris (3,5-dimethylphenylcarbamate).(R)-enantiomer of the propranolol was prepared by stereoselective synthesis using Jacobsen catalyst.
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Fang, Ying Ying, Xiao Ling Zha, Hui Li, and Wei Fang Yu. "Determination of Henry Constants of Azelnidipine Enantiomers on Chiralpak AD Column at Different Temperatures." Advanced Materials Research 1078 (December 2014): 78–81. http://dx.doi.org/10.4028/www.scientific.net/amr.1078.78.

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Simulated moving bed (SMB) chromatographic separation has become a highly promising method for chiral separation due to the less solvent consumption and efficient utilization of stationary phase. As reported, Azelnidipine exists two isomeric forms, it is necessary to product azelnidipine single enantiomer for medical safety and drug developmen. However, the separation of azelnidipine enantiomers on SMB is complex, requiring many operating parameters. And the SMB processes with temperature gradient (non-isotherm) mode may have significant advantages over the traditional isothermal mode. In this
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Wang, Fang, Thomas Dowling, Dean Ellison, and Jean Wyvratt. "Comparison study of Chiralpak AD-H with AD columns in chromatographic enantioseparation of dihydropyrimidinone acid and its methyl ester." Journal of Chromatography A 1034, no. 1-2 (2004): 117–23. http://dx.doi.org/10.1016/j.chroma.2004.02.035.

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Ye, Yun K., Barbara Lord, and Rodger W. Stringham. "Memory effect of mobile phase additives in chiral separations on a Chiralpak AD column." Journal of Chromatography A 945, no. 1-2 (2002): 139–46. http://dx.doi.org/10.1016/s0021-9673(01)01491-1.

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Dissertations / Theses on the topic "Chiralpak AD"

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Svobodová, Dagmar. "Chirální analýza residuí léčiv v odpadních vodách." Master's thesis, Vysoké učení technické v Brně. Fakulta chemická, 2011. http://www.nusl.cz/ntk/nusl-216766.

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The theoretical part shortly describes chirality with focus on chiral pharmaceuticals. The processes of their absorption, distribution, metabolism and elimination in human body are discussed. These points are very important to understand possible fate of chiral drugs in the environment as there is only little data concerning their environmental behaviour. The occurrence and enantioselective toxicity of chiral drugs is also discussed here. One of the chapters describes non-steroidal anti-inflammatory drugs, as they are analyzed in the wastewater in the experimental part, and their occurrence in
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