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Dissertations / Theses on the topic 'Crystal X-ray studies'

Author: Grafiati

Published: 5 June 2025

Last updated: 1 August 2025

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1

Erskine, Peter Thomas. "X-ray crystallographic studies of 5-aminolaevulinic acid dehydratase." Thesis, Birkbeck (University of London), 1996. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.299090.

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2

Sinha, Debashis. "X-Ray, Dielectric, and electro-optic studies on fluorinated achiral and chiral liquid crystals." Thesis, University of North Bengal, 2015. http://hdl.handle.net/123456789/2742.

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3

Ince-Cushman, Alexander Charles. "Rotation studies in fusion plasmas via imaging X-ray crystal spectroscopy." Thesis, Massachusetts Institute of Technology, 2008. http://hdl.handle.net/1721.1/53259.

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Thesis (Ph. D.)--Massachusetts Institute of Technology, Dept. of Nuclear Science and Engineering, 2008.<br>Cataloged from PDF version of thesis.<br>Includes bibliographical references (p. 173-178).<br>The increase in plasma performance associated with turbulence suppression via flow shear in magnetically confined fusion plasmas has been well documented. Currently, the standard methods for both generating and measuring plasma rotation involves neutral beam injection (NBI). In the large, high density plasmas envisaged for next generation reactors, such as ITER, NBI will be considerably more diff

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4

Lubhelwana, Siyanda. "Crystal isostructurality and X-ray diffraction studies of cyclodextrin inclusion compounds." Master's thesis, University of Cape Town, 2005. http://hdl.handle.net/11427/6324.

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Includes bibliographical references.<br>The first part of this dissertation is an update on the isostructurality method of PXRD analysis (lsoPXRD), the last update having been published in 2001 The scope of the isostructurality part of this dissertation includes organic inclusion complexes of all three natural cyclodextrins (a-,

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5

Treacy, Jon. "Synchrotron studies of TiO2 single crystal surfaces." Thesis, University of Manchester, 2014. https://www.research.manchester.ac.uk/portal/en/theses/synchrotron-studies-of-tio2-single-crystal-surfaces(4c8a0ee8-b2b8-460c-a174-b4478256d4e7).html.

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Titanium dioxide (TiO2) is an abundant, inexpensive and non-toxic material that is most commonly used as a white pigment in paints. Since the discovery by Fujishima and Honda in 1972 that water splits into hydrogen and oxygen gas at the surface of TiO2 on exposure to sunlight, there has been a massive research effort into understanding and improving the photoactivity of TiO2. One aspect of this is the characterisation of so-called ‘model’ surfaces, i.e. very large single crystal faces with low levels of contamination at ultra high vacuum (UHV) pressures, allowing the study of a single structur

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6

James, Sian Catherine. "Synthetic end structural studies of bismuth and antimony alkoxides, amides and halides." Thesis, University of Bristol, 1999. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.299600.

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7

Chan, Fung Choy. "Powder X-ray diffraction studies of structural and kinetic aspects of polymorphism." Thesis, King's College London (University of London), 1999. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.327050.

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8

Hodgson, Susan Marie. "Structural studies of lithium compounds." Thesis, University of Newcastle Upon Tyne, 1989. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.244863.

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9

Butterworth, Susanna. "Single crystal X-ray diffraction studies on small, medium and large molecules." Thesis, Durham University, 1996. http://etheses.dur.ac.uk/5352/.

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Chapter 1. Production of crystals for diffraction analysis would be assisted by the devising of a set of rules which, given molecular formula, could predict crystal formation conditions. By studying trends in structural properties of a group of closely related simple molecules, deductions could be drawn which could then be applied more generally. Chalcone derivatives with minor substituent differences were recrystallised. X-ray diffraction data collected and the structures solved and refined. Additionally, NMR and UV studies were performed, investigating an observed dimerisation reaction. Chap

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10

Todd, Alan Kenneth. "Single crystal X ray diffraction studies of DNA and DNA drug complexes." Thesis, University of Reading, 1999. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.270250.

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11

Crabtree, Simon Peter. "Synthesis, structure and reaction studies of diphosphine rhodium complexes." Thesis, Durham University, 1996. http://etheses.dur.ac.uk/5299/.

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A series of complexes of the type [Rh(diphos)(C(_7)H(_8))](BF(_4)) (1) have been synthesised and two of these species [diphos = Bu(^1)(_2)P(CH(_2))(_2)PBu(^1)(_2), Cy(_2)P(l,2-trans-cyclopentane)PCy(_2)] have been characterised by X-ray crystallography. The influence of the chelating diphosphine on the structural characteristics and NMR parameters of these compounds has been investigated. Complexes of the type (1) are active catalysts for the hydroformylation of l-hexene(120ºC, 450psi 2:1 H(_2):C0). However, they are inactive for the related hydroesterification process and this is attributed t

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12

Aziz, Fauziah Haji. "Indexing and structural studies of materials by high-resolution X-ray powder diffraction." Thesis, University of Surrey, 1989. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.232903.

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13

Fraser, Kelly A. "Crystallographic studies of complexes of transition and post-transition metals." Thesis, University of Newcastle Upon Tyne, 1994. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.238817.

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14

Terry, Ann Elizabeth. "Shear flow studies of liquid crystalline polymers." Thesis, University of Bristol, 1997. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.390373.

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15

Nicklow, Rhea A. "Synthesis and Single Crystal X-Ray Diffraction Studies of Ca2NF and Other Compounds." Youngstown State University / OhioLINK, 2000. http://rave.ohiolink.edu/etdc/view?acc_num=ysu1004535239.

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16

Andersson, Charlotta. "Structural studies of Erwinia carotovora L-Asparaginase by X-ray crystallography." Thesis, Linköping University, The Department of Physics, Chemistry and Biology, 2006. http://urn.kb.se/resolve?urn=urn:nbn:se:liu:diva-6188.

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<p>Bacterial L-asparaginases (E.C.3.5.1.1) are enzymes that catalyze the hydrolysis of L-asparagine to aspartic acid. For the past 30 years these enzymes have been used as therapeutic agents in the treatment of acute childhood lymphoblastic leukemia. The presence of a low rate glutaminase activity however causes serious side-effects to patients in treatment, as glutamine depletion give rise to neurotoxicity, anaphylaxis, and other hypersensitivity reactions. The interest in the enzyme from Erwinia carotovora originates from the fact that it shows a decreased glutaminase activity, and therefore

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17

Rawas, A. "The crystal structure of some biphenyl derivatives and X-ray diffraction studies of some liquid crystal materials." Thesis, University of Hull, 1985. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.377046.

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18

Badger, J. "X-ray crystallographic studies of cubic insulin and of the ribosomal proteins L30 and S5." Thesis, University of York, 1986. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.483027.

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19

Miyake, Osamu. "Studies on molecular diversity, evolutional process, and X-ray crystal structure of bacterial alginate lyases." Kyoto University, 2004. http://hdl.handle.net/2433/145440.

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Kyoto University (京都大学)<br>0048<br>新制・課程博士<br>博士(農学)<br>甲第11202号<br>農博第1450号<br>新制||農||900(附属図書館)<br>学位論文||H16||N3974(農学部図書室)<br>22786<br>UT51-2004-T171<br>京都大学大学院農学研究科応用生命科学専攻<br>(主査)教授村田幸作, 教授加藤暢夫, 教授井上國世<br>学位規則第4条第1項該当

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20

Zhang, Wen. "Structure and Function Studies of Selenium Substituted Nucleic Acids." Digital Archive @ GSU, 2012. http://digitalarchive.gsu.edu/chemistry_diss/63.

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Nucleic acids are responsible for the storage of genetic information and directly participate in gene replication, transcription and expression, and thereby the control of nucleic acids leads to the regulation of genetic information flow and gene expression. Meanwhile, many non-coding RNAs are in-volved in signal transduction directly. Moreover, nucleic acid-based therapeutic strategies have been lead to drug candidates and are effective tools in drug discovery and disease study at the molecular level as well as the genetic level. Consequently, the 3D crystal structure study and related functi

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21

Potnis, Prashant. "Single crystal ferroelectrics : macroscopic and microscopic studies." Thesis, University of Oxford, 2011. http://ora.ox.ac.uk/objects/uuid:96973376-8596-4fc9-9c53-c58379a766a5.

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The aim of this thesis was to improve the understanding of microstructure in single crystal ferroelectrics. This was achieved through macroscopic testing of Lead Magnesium Niobate – Lead Titanate (PMN-PT) and microscopic observations of Barium Titanate (BT) single crystals. Multi-axial polarization rotation tests on PMN-PT showed a gradual increase in the change in dielectric displacement due to ferroelectric switching as the electric field is applied at increasing angles to the initial polarization direction. A relatively high remnant polarization for loading angle near to 90° suggested that

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22

Cameron, Christopher Alistair. "High-pressure studies on molecular systems at ambient and low temperatures." Thesis, University of Edinburgh, 2015. http://hdl.handle.net/1842/9952.

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Pressure and temperature are two environmental variables that are increasingly being exploited by solid-state researchers probing structure-property relationships in the crystalline state. Modern high-pressure apparatus is capable of generating many billions of Pascals in the laboratory, and therefore can produce significantly greater alterations to crystalline materials than changes in temperature, which can typically be varied by only a few thousand Kelvin. Many systems such as single-molecule magnets exhibit interesting properties under low-temperature regimes that can be substantially alte

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23

Salazar, Lupe E. Pulcha. "Lower rim calix[4]arene derivatives and their complexes with univalent cations : solution, complexation and X-ray diffraction studies." Thesis, University of Surrey, 2001. http://epubs.surrey.ac.uk/843331/.

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Following an introoduction on calixarene chemistry and their metal-ion complexes including some of their applications, the aims of the work are described. Thus, the first part of this thesis concerns the detemination of the standard enthalpies of solution, sH°, of new lithium and sodiimi 1:1 electrolytes based on eth p=tert-butycalix[4]arene tetraethanoate containing various anions in acetonitrile at 298.15 K. Using these data in conjunction with previously reported sH° values for the free metal-ion salts and the ligand and standard enthalpies of complexation, cH°H° of allcali-

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24

Normile, Peter Stephen. "Neutron and resonant X-ray magnetic scattering studies of single-crystal Uâ†1â†-â†#chi#Puâ†#chi#Sb." Thesis, University of Liverpool, 2001. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.250591.

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25

Lamble, G. M. "Surface extended X-ray absorption fine structure studies of chlorine and caesium adsorbed on silver single crystal surfaces." Thesis, University of Liverpool, 1986. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.380102.

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26

Roshi, Aleksander. "Quenched Random Disorder Studies In Liquid Crystal + Aerosil Dispersions." Link to electronic thesis, 2005. http://www.wpi.edu/Pubs/ETD/Available/etd-042705-123130/.

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Dissertation (Ph.D.) -- Worcester Polytechnic Institute.<br>Keywords: smectic-A to smectic-C; nematic to smectic-A; isotropic-nematic; phase transition; quenched random disorder; liquid crystal; gel structure; turbidity; gel dynamics; x-ray intensity fluctuation spectroscopy ( XIFS ); ac-calorimetry; x-ray diffraction Includes bibliographical references (p. 210-218).

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27

Dhuvad, Pratikkumar. "FIRST-PRINCIPLES STUDIES OF FERROELECTRIC PROPERTIES IN ORGANIC CRYSTAL AND PEROVSKITE SUPERLATTICES." Diss., Temple University Libraries, 2018. http://cdm16002.contentdm.oclc.org/cdm/ref/collection/p245801coll10/id/524696.

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Physics<br>Ph.D.<br>This thesis discusses structural and ferroelectric properties of two well-known classes of materials, perovskite oxides and Hydrogen bonded ferroelectrics, using first-principles calculations. Certain aspects of first principles calculations are central to the problems presented in this thesis. Such as the ability to calculate polarization based on the modern theory of polarization and calculation of ferroelectric property under finite electric displacement field. Therefore, these fundamental theoretical approaches are discussed following an opening section on the basic met

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28

Krug, Klaus Gerold [Verfasser]. "In-situ surface X-ray diffraction studies of homoepitaxial growth and dissolution at gold single crystal electrodes / Klaus Gerold Krug." Kiel : Universitätsbibliothek Kiel, 2010. http://d-nb.info/1019951265/34.

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29

Kuryachiy, Viacheslav G. "Irradiated single crystal 3C-SiC as a maximum temperature sensor." [Tampa, Fla] : University of South Florida, 2008. http://purl.fcla.edu/usf/dc/et/SFE0002774.

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30

Muroyama, Norihiro. "Studies of inorganic crystal structures and gas adsorption process in mesoporous crystals : new approach through analysis of electron charge distribution by synchrotron powder X-ray diffraction /." Stockholm : Department of Physical, Inorganic and Structural Chemistry, Stockholm university, 2008. http://urn.kb.se/resolve?urn=urn:nbn:se:su:diva-7367.

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31

Mohamed, Tahir Mohamed Ibrahim. "Combination of single crystal X-ray diffraction & Â¹Â³C CP/MAS solid state NMR spectroscopy : studies of structures & dynamics of molecular organic crystals." Thesis, University of Oxford, 2002. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.249427.

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32

Sanchez-Ballester, Noelia M. "Supramolecular studies with functionalised group 15 ligands." Thesis, Loughborough University, 2010. https://dspace.lboro.ac.uk/2134/6062.

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This thesis has been divided into five sections. The first chapter introduces the main themes of this thesis, including the description of the concepts of supramolecular chemistry, crystal engineering, hydrogen bonding and graph set analysis. The final section of chapter one describes a typical X-ray experiment used to determine the structures of the compounds presented in this thesis. Chapter two describes the synthesis and single crystal structures of copper(I) complexes with pyridine- and pyrazine-carboxylic acids. A series of novel solvent inclusion compounds of copper(I) complexes with py

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33

Atalay, Ramazan. "Optical and Structural Properties of Indium Nitride Epilayers Grown by High-Pressure Chemical Vapor Deposition and Vibrational Studies of ZGP Single Crystal." Digital Archive @ GSU, 2012. http://digitalarchive.gsu.edu/phy_astr_diss/60.

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The objective of this dissertation is to shed light on the physical properties of InN epilayers grown by High-Pressure Chemical Vapor Deposition (HPCVD) for optical device applications. Physical properties of HPCVD grown InN layers were investigated by X-ray diffraction, Raman scattering, infrared reflection spectroscopies, and atomic force microscopy. The dependencies of physical properties as well as surface morphologies of InN layers grown either directly on sapphire substrates or on GaN/sapphire templates on varied growth conditions were studied. The effect of crucial growth parameters suc

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34

Nickels, Elizabeth Anne. "Structural and thermogravimetric studies of group I and II borohydrides." Thesis, University of Oxford, 2010. http://ora.ox.ac.uk/objects/uuid:f18f8f7c-1837-4b96-b4bb-5f964e93899c.

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This thesis investigates the structure and thermal behaviour of LiBH4, NaBH4, KBH4, LiK(BH4)2, Ca(BH4)2 and Sr(BH4)2. LiK(BH4)2 is the first mixed alkali metal borohydride and was synthesised and characterised during this work. The crystal structures of these borohydrides were studied using variable temperature neutron and synchrotron X-ray diffraction. The synthesis of isotopically enriched samples of 7Li11BD4, Li11BD4, Na11BD4 and K11BD4 allowed high quality neutron diffraction data to be collected. Particular attention was paid to the exact geometry of the borohydride ions which were genera

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35

Larsson, Anna. "Structural Studies of Three Glycosidases." Doctoral thesis, Uppsala : Acta Universitatis Upsaliensis : Universitetsbiblioteket [distributör], 2006. http://urn.kb.se/resolve?urn=urn:nbn:se:uu:diva-6339.

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36

Rossiter, Angelina Jane. "Solubility and crystal growth of sodium nitrate from mixed alcohol – water solvents." Thesis, Curtin University, 2009. http://hdl.handle.net/20.500.11937/505.

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Due to the ductile nature of the sodium nitrate crystal which deforms plastically under high levels of strain, most of the crystal growth studies in aqueous solution have focussed on the influence of tensile strain, supersaturation and dislocation, using x-ray surface topography to characterise the dislocation structure of the crystal. Most of the crystal growth studies have also focussed on growth from the melt since single crystals of sodium nitrate find application in optical pumping experiments, are a potential substitute for calcite in the preparation of polarising prisms and are interest

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37

Diorio, Nicholas John Jr. "From Synthesis to Piezoelectric Studies of Central-Ring-Substituted Bent-Core Liquid Crystals and Their Composites." Kent State University / OhioLINK, 2013. http://rave.ohiolink.edu/etdc/view?acc_num=kent1375098839.

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38

Eckhardt, Kai, Volodymyr Bon, Jürgen Getzschmann, Julia Grothe, Florian M. Wisser, and Stefan Kaskel. "Crystallographic insights into (CH3NH3)3(Bi2I9): a new lead-free hybrid organic–inorganic material as a potential absorber for photovoltaics." Saechsische Landesbibliothek- Staats- und Universitaetsbibliothek Dresden, 2017. http://nbn-resolving.de/urn:nbn:de:bsz:14-qucosa-219347.

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The crystal structure of a new bismuth-based light-absorbing material for the application in solar cells was determined by single crystal X-ray diffraction for the first time. (CH3NH3)3(Bi2I9) (MBI) is a promising alternative to recently rapidly progressing hybrid organic–inorganic perovskites due to the higher tolerance against water and low toxicity. Single crystal X-ray diffraction provides detailed structural information as an essential prerequisite to gain a fundamental understanding of structure property relationships, while powder diffraction studies demonstrate a high degree of crystal

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39

Eckhardt, Kai, Volodymyr Bon, Jürgen Getzschmann, Julia Grothe, Florian M. Wisser, and Stefan Kaskel. "Crystallographic insights into (CH3NH3)3(Bi2I9): a new lead-free hybrid organic–inorganic material as a potential absorber for photovoltaics." Royal Society of Chemistry, 2016. https://tud.qucosa.de/id/qucosa%3A30174.

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The crystal structure of a new bismuth-based light-absorbing material for the application in solar cells was determined by single crystal X-ray diffraction for the first time. (CH3NH3)3(Bi2I9) (MBI) is a promising alternative to recently rapidly progressing hybrid organic–inorganic perovskites due to the higher tolerance against water and low toxicity. Single crystal X-ray diffraction provides detailed structural information as an essential prerequisite to gain a fundamental understanding of structure property relationships, while powder diffraction studies demonstrate a high degree of crystal

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40

Majumder, Bimal. "X-ray diffraction studies on liquid crystals." Thesis, University of North Bengal, 1988. http://hdl.handle.net/123456789/667.

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41

Alexopoulos, Eftichia. "Crystallographic and modeling studies of intermolecular interactions of biological interest." Doctoral thesis, [S.l.] : [s.n.], 2004. http://deposit.ddb.de/cgi-bin/dokserv?idn=972659137.

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42

Whatling, Shaun Gary. "Computer simulation studies of liquid crystals." Thesis, University of Southampton, 1997. https://eprints.soton.ac.uk/421720/.

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43

Rodriguez, Asiloe Jasmina Mora. "High resolution powder diffraction studies of molecular solids." Thesis, Keele University, 1996. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.321299.

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44

Kammoe, Astride Lorette. "Synthesis and Characterization of Multifunctional Organic/ inorganic Hybrid Materials obtained by the "wet chemistry" approach." Doctoral thesis, Universitätsbibliothek Chemnitz, 2015. http://nbn-resolving.de/urn:nbn:de:bsz:ch1-qucosa-175649.

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Die vorliegende Arbeit fokussiert auf die Synthese von organisch/anorganischen Hybridmaterialien mit multifunktionalen Eigenschaften unter ausschliesslicher Darstellung dieser Materialen mit Hilfe des „wet chemistry“ Zugangs. Ausgehend von der Darstellung und Charakterisierung von isomorphen bzw. isostrukturellen Hybridmaterialien der allgemeinen Zusammensetzung catena-{[Me3NH][MCl3·2H2O]}n (Mtac) (MII = Mn, Co, Ni, Cu, tac = [Me3NH]Cl3·2H2O]) speziell mittels IR und UV/vis Spektroskopie ist beschrieben, wie sich aus diesen entsprechende bi-, tri-, und auch tetra-heterometallische Koordination

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45

Xu, Xuelian. "X-ray and neutron diffraction studies of organic molecular crystals." Thesis, University of Strathclyde, 2005. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.416190.

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46

Hammond, Deborah Bernice. "Structural studies of dye molecules adsorbed on silver halide crystals." Thesis, University of Cambridge, 1995. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.389886.

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47

Mandal, Pradip Kumar. "X-ray diffraction studies on liquid crystals in solid and mesomorphic phase." Thesis, University of North Bengal, 1985. http://hdl.handle.net/123456789/626.

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48

Hodder, Benjamin. "Guided mode studies of smectic liquid crystals." Thesis, University of Essex, 2000. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.302633.

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49

Mitra, Mukul Kumar. "Determination of order parameters of liquid crystals from birefringence, x-ray and magnetic anisotrophy studies." Thesis, University of North Bengal, 1987. http://hdl.handle.net/123456789/822.

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50

Mannix, Daniel. "X-ray and neutron scattering studies of f-electron multilayers and single crystals." Thesis, University of Liverpool, 1998. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.263708.

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