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Relevant bibliographies by topics / Enantiomer separation

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Academic literature on the topic 'Enantiomer separation'

Author: Grafiati

Published: 4 June 2021

Last updated: 9 February 2022

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Journal articles on the topic "Enantiomer separation"

1

Hocking, Martin B., and Aga Z.-Q. Khan. "Chromatographic enantiomer separation and circular dichroism (CD) spectra of three 4-endosubstituted-3,6-diphenyl-3,6-phenylphosphorylcyclohexenes." Canadian Journal of Chemistry 85, no. 9 (2007): 600–602. http://dx.doi.org/10.1139/v07-088.

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Three enantiomeric pairs of Diels–Alder adducts of 2,5-diphenylphosphole-1-oxide have been resolved by elution of each of the enantiomers with 95% ethanol from a swollen microcrystalline triacetylcellulose stationary phase. The degree of separation achieved in each case was confirmed by comparing the absorbance maximum of the UV spectrum of each separated enantiomer with that of a similar concentration of the relevant racemic mixture. The circular dichroism (CD) spectrum of each of the separated enantiomers was recorded, and spectral parameters are listed.Key words: enantiomer separations, thr

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Wu, Xiuli, Yange Zhang, Wenzhen Li, et al. "A Validated LC Method for the Enantiomeric Separation of EAI045 on Chiral Stationary Phase." Journal of Chromatographic Science 58, no. 6 (2020): 562–68. http://dx.doi.org/10.1093/chromsci/bmz125.

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Abstract A simple and accurate chiral liquid chromatographic method was developed for enantiomeric resolution and determination of 2-(5-fluoro-2-hydroxyphenyl)-2-(1-oxo-2,3-dihydro-1H-isoindol-2-yl)-N-(1,3-thiazol-2-yl)acetamide (EAI045). The enantiomers of EAI045 were baseline resolved on a Chiralpak AD-H (250 mm × 4.6 mm, 5 μm) column using a mobile phase system containing n-hexane: 2-propanol (75: 25 v/v) at a flow rate of 1 mL min−1 at 30°C. The eluted analytes were subsequently detected with an ultraviolet detector at 254 nm. The effects of organic modifiers and temperature on the enantio

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Suraj Koorpet R, Akshay N, Nishanth G, Chandan R S, and Anand Kumar Tengli. "A Review on Chiral Columns/Stationary Phases for HPLC." International Journal of Research in Pharmaceutical Sciences 11, no. 2 (2020): 2466–80. http://dx.doi.org/10.26452/ijrps.v11i2.2240.

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The chiral separation of pharmaceutical molecules and their precursors is one of the important areas of application of HPLC in pharmaceutical analysis for obtaining enantiomerically pure drug. The latter procedures include the use of so-called chiral selectors to enantio-selectively recognise and isolate the enantiomer. The direct approaches, i.e. those which do not derivate the compound of interest before separation, are addressed in detail, since they are now the most common approaches. The role of stereochemistry in medicinal products is being given greater emphasis to medical practice. For

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Li, Zhi Wei, Xing Jia, Chun Mei Xu, Lei Liu, and De Cai Fu. "Chiral Separation of Amlodipine and its Enantiomer on a Molecularly Imprinted Polymer-Based Stationary Phase." Advanced Materials Research 706-708 (June 2013): 36–39. http://dx.doi.org/10.4028/www.scientific.net/amr.706-708.36.

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A new chiral stationary phase for amlodipine (3-ethyl 5-methyl-2 -[(-2-(aminoethoxymethyl)-4-(2-chlorophenyl)-1,4-dihydro-6-methyl-3,5-pyridinedicarboxylate) based on a molecularly imprinted polymer has been prepared by radiation polymerization method and used for chromatographic separation of the chiral enantiomers. The effects on the separation of mobile phase and flow rate were investigated, and the optimum conditions for HPLC were shown to be: mobile phase, chloroform; flow rate, 0.3 ml min-1; at room temperature. The results has shown that the amlodipine-imprinted polymer was capable of r

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Zhang, Ping, Sheng Wang, Dongmei Shi, et al. "Direct Enantiomeric Separation and Determination of Hexythiazox Enantiomers in Environment and Vegetable by Reverse-Phase High-Performance Liquid Chromatography." International Journal of Environmental Research and Public Health 17, no. 10 (2020): 3453. http://dx.doi.org/10.3390/ijerph17103453.

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In the present study, the direct enantiomeric separation of hexythiazox enantiomers on Lux cellulose-1, Lux cellulose-2, Lux cellulose-3, Lux cellulose-4, Lux amylose-1 and Chirapak IC chiral columns were carefully investigated by reverse-phase high-performance liquid chromatography (RP-HPLC). Acetonitrile/water and methanol/water were used as mobile phase at a flow rate of 0.8 mL·min−1. The effects of chiral stationary phase, temperature, thermodynamic parameters, mobile phase component and mobile phase ratio on hexythiazox enantiomers separation were fully evaluated. Hexythiazox enantiomers

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Kant, Ravi, Ramesh Babu Bodla, Rubina Bhutani, and Garima Kapoor. "Enantioselective Box Behenken Optimized HPLC-DAD Method for the Simultaneous Estimation of Alogliptin Enantiomorphs in Pharmaceutical For mulations and their Pharmacokinetic Study in Rat Plasma." Advanced Pharmaceutical Bulletin 9, no. 1 (2019): 147–58. http://dx.doi.org/10.15171/apb.2019.018.

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Purpose: A stereoselective high performance liquid chromatographic analytical method withphotodiode array detector was developed and validated as per the International Conferenceon Harmonization (ICH) guidelines for the determination of alogliptin (ALO) enantiomers informulations and rat plasma.Methods: Enantiomeric separation was performed on a Phenomenex Lux Cellulose-2 chiralcolumn. Box-Behnken design was used to identify the optimum conditions of the threeindependent variables for the desired output responses.Results: The HPLC peaks of ALO enantiomers and the internal standard pioglitazone

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Fang, Ying Ying, Xiao Ling Zha, Hui Li, and Wei Fang Yu. "Determination of Henry Constants of Azelnidipine Enantiomers on Chiralpak AD Column at Different Temperatures." Advanced Materials Research 1078 (December 2014): 78–81. http://dx.doi.org/10.4028/www.scientific.net/amr.1078.78.

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Simulated moving bed (SMB) chromatographic separation has become a highly promising method for chiral separation due to the less solvent consumption and efficient utilization of stationary phase. As reported, Azelnidipine exists two isomeric forms, it is necessary to product azelnidipine single enantiomer for medical safety and drug developmen. However, the separation of azelnidipine enantiomers on SMB is complex, requiring many operating parameters. And the SMB processes with temperature gradient (non-isotherm) mode may have significant advantages over the traditional isothermal mode. In this

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Lankhorst, Peter, Jozef van Rijn, and Alexander Duchateau. "One-Dimensional 13C NMR Is a Simple and Highly Quantitative Method for Enantiodiscrimination." Molecules 23, no. 7 (2018): 1785. http://dx.doi.org/10.3390/molecules23071785.

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The discrimination of enantiomers of mandelonitrile by means of 1D 13C NMR and with the aid of the chiral solvating agent (S)-(+)-1-(9-anthryl)-2,2,2-trifluoroethanol (TFAE) is presented. 1H NMR fails for this specific compound because proton signals either overlap with the signals of the chiral solvating agent or do not show separation between the (S)-enantiomer and the (R)-enantiomer. The 13C NMR method is validated by preparing artificial mixtures of the (R)-enantiomer and the racemate, and it is shown that with only 4 mg of mandelonitrile a detection limit of the minor enantiomer of 0.5% i

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Gandhi, Karan, Umang Shah, and Sandip Patel. "Drug Stereochemistry: A Prodigy For Pharmacology and Drug Development." Current Drug Discovery Technologies 17, no. 5 (2020): 565–73. http://dx.doi.org/10.2174/1570163816666190502101803.

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Stereochemistry has evinced the importance of many chiral drugs with respect to drug designing and development. A literature review was conducted for several chiral drugs involving pharmacokinetic and pharmacodynamic parameters of their enantiomers along with their uses in certain diseased conditions. This article mainly includes the pharmacological profile review of some chiral drugs and the aspects due to which the single enantiomer is of importance as compared to the racemic mixture of the drug. This was achieved by moderating the side effects or toxic effects; or by the potentiated activit

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Pisaneschi, Lin, Leonard, et al. "The 3S Enantiomer Drives Enolase Inhibitory Activity in SF2312 and Its Analogues." Molecules 24, no. 13 (2019): 2510. http://dx.doi.org/10.3390/molecules24132510.

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We recently reported that SF2312 ((1,5-dihydroxy-2-oxopyrrolidin-3-yl)phosphonic acid), a phosphonate antibiotic with a previously unknown mode of action, is a potent inhibitor of the glycolytic enzyme, Enolase. SF2312 can only be synthesized as a racemic-diastereomeric mixture. However, co-crystal structures with Enolase 2 (ENO2) have consistently shown that only the (3S,5S)-enantiomer binds to the active site. The acidity of the alpha proton at C-3, which deprotonates under mildly alkaline conditions, results in racemization; thus while the separation of four enantiomeric intermediates was a

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Dissertations / Theses on the topic "Enantiomer separation"

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Fraunholz, Thomas [Verfasser], and R. H. W. [Akademischer Betreuer] Hoppe. "Transport at Interfaces in Lipid Membranes and Enantiomer Separation / Thomas Fraunholz. Betreuer: R. H. W. Hoppe." Augsburg : Universität Augsburg, 2015. http://d-nb.info/1077705638/34.

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Bao, Ye. "Enantiomeric separations and microorganism studies with analytical separation techniques." [Ames, Iowa : Iowa State University], 2008.

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Wildervanck, Alexander Franciscus. "Separation of enantiomers of Baclofen." Master's thesis, University of Cape Town, 1996. http://hdl.handle.net/11427/20462.

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(3-(Aminomethyl)-4-chlorobenzenepropanoic acid (Baclofen), 3-(p-chlorophenyl)pyrrolidone (Baclofen lactam) and 3-(p-Chlorophenyl)glutaramide (baclofen's synthetic precursor) were individually used as substrates in co-crystallisation experiments with several resolving agents. Experiments were conducted in the solid state and in solution. The (-) enantiomer of the lactam and the ( +) enantiomer of the glutaramide were found to cocrystallise selectively with (2R,3R)-( +)-tartaric acid and (S)-(-)-a.-Methylbenzylamine respectively. Both these dissociable diastereomers Vere analysed by X-ray crysta

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Oliveira, Elder Gonçalves de. "Desenvolvimento e validação de métodos analíticos para a análise enantiomérica da duloxetina e de sua impureza quiral em formulação farmacêutica." reponame:Biblioteca Digital de Teses e Dissertações da UFRGS, 2012. http://hdl.handle.net/10183/139442.

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A duloxetina é um potente inibidor duplo da recaptação de serotonina e norepinefrina, disponível como enantiômero puro, sob a forma S-duloxetina e comercializado como pellets em cápsulas. O R enantiômero da duloxetina é também um inibidor da recaptação, no entanto, este é menos potente que seu isômero, sendo considerado como impureza enantiomérica. Este trabalho teve como objetivos o desenvolvimento e a validação de métodos analíticos para o controle de qualidade da duloxetina e de sua respectiva impureza enantiomérica por cromatografia líquida de alta eficiência (CLAE), e por eletroforese cap

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Barros, Georgia de Oliveira Figueiredo. "Resolução de misturas racemicas por acoplamento de cristalização a cromatografia em leito movel simulado : estudos fundamentais para a produção de S-cetamina." [s.n.], 2005. http://repositorio.unicamp.br/jspui/handle/REPOSIP/267314.

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Orientador: Everson Alves Miranda<br>Dissertação (mestrado) - Universidade Estadual de Campinas, Faculdade de Engenharia Quimica<br>Made available in DSpace on 2018-08-04T07:13:28Z (GMT). No. of bitstreams: 1 Barros_GeorgiadeOliveiraFigueiredo_M.pdf: 2282903 bytes, checksum: b104323f697a813ec6af57b15ba7b95b (MD5) Previous issue date: 2005<br>Resumo: A separação de enantiômetros em altos níveis de pureza enantiomérica é atualmente um requerimento da industria farmacêutica. No entanto, altas purezas estão sendo alcançadas neste sistema com comprometimento da produtividade. O acoplamento do lei

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Chatah, Nour-El-Houda. "Apports de la cristallisation aux dédoublements d'espèces chirales." Rouen, 1996. http://www.theses.fr/1996ROUES032.

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Le comportement stéréospécifique des espèces organiques chirales impose le dédoublement du mélange racémique. La cristallisation fractionnée de sels diastéréoisomères est un protocole qui concerne près de 65 % des produits pharmaceutiques. L'intervention de l'agent chiral de dédoublement vérifiant la stoechiométrie pastorienne peut être fortement limitée en opérant en présence d'un agent achiral et réduisant ainsi le coût de la production. Le mélange en milieu éthanolique conduit à un système thermodynamique relevant d'un quaternaire réciproque. Le système met en jeu les (1R, 3S)-(+)-camphorat

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Elgarhy, Karim. "The separation of the enantiomers of asparagine by crystallization /." Thesis, McGill University, 2005. http://digitool.Library.McGill.CA:80/R/?func=dbin-jump-full&object_id=100356.

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Enantiomers are chiral molecules (i.e. they are mirror-images of each other). They have identical physical properties except for the rotation of polarized light. However their chemical properties are different when reacting with other chiral molecules. The majority of biological processes involve the reaction of two or more chiral molecules. There is therefore a strong interest coming from the pharmaceutical, food and agricultural industry for the separation of enantiomers.<br>Separation methods such as chromatography exist but are generally expensive and limited in scale. Stereosynthesis ofte

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Meeson, Stephen Russell. "The separation of enantiomers by high performance liquid chromatography." Thesis, University of Newcastle Upon Tyne, 1990. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.278414.

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Rocco, Anna. "Separation of Enantiomers by Means of NanoO-Liquid Chromatography." Doctoral thesis, Lithuanian Academic Libraries Network (LABT), 2013. http://vddb.library.lt/obj/LT-eLABa-0001:E.02~2013~D_20130122_144808-59559.

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Nano-liquid chromatography (nano-LC) was selected as analytical tool to develop different methods for chiral separations. Nano-LC offers several advantages over conventional LC, e.g., low sample requirement, short analysis time, easy coupling with mass spectrometer, and use of small amount of reagents, with a consequent low environmental pollution. In case of chiral separations, where expensive chiral stationary phases or chiral mobile phase additives (CMPA) have to be employed, nano-LC results very useful since it allows to perform analysis with small amount of this costly material. Initiall

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Haglöf, Jakob. "Enantiomeric Separations using Chiral Counter-Ions." Doctoral thesis, Uppsala universitet, Avdelningen för analytisk farmaceutisk kemi, 2010. http://urn.kb.se/resolve?urn=urn:nbn:se:uu:diva-130049.

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This thesis describes the use of chiral counter-ions for the enantiomeric separation of amines in non-aqueous capillary electrophoresis. The investigations have been concentrated on studies of the influence, of the chiral counter-ion, the solvent, the electrolyte and the analyte, on the enantioselective separation. Modified divalent dipeptides have been introduced in capillary electrophoresis for the separation of amino alcohols and chiral resolution of amines. Association constants for the ion-pair between dipeptide and amino alcohol could be utilized for development of separation systems wit

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Books on the topic "Enantiomer separation"

1

Toda, Fumio, ed. Enantiomer Separation. Springer Netherlands, 2004. http://dx.doi.org/10.1007/978-1-4020-2337-8.

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König, Wilfried A. Gas chromatographic enantiomer separation with modified cyclodextrins. Hüthig Buch, 1992.

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Briggs, David Andrew. Enantiomer separation by high performance liquid chromatography. University of East Anglia, 1990.

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König, Wilfried. The practice of enantiomer separation by capillary gas chromatography. A. Hüthig, 1987.

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Todd, Matthew, ed. Separation of Enantiomers. Wiley-VCH Verlag GmbH & Co. KGaA, 2014. http://dx.doi.org/10.1002/9783527650880.

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Chromatographic enantioseparation: Methods and applications. 2nd ed. E. Horwood, 1991.

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Allenmark, Stig G. Chromatographic enantioseparation: Methods and applications. E. Horwood, 1988.

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8

Wren, Stephen. The Separation of Enantiomers by Capillary Electrophoresis. Vieweg+Teubner Verlag, 2001.

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Wren, Stephen. The Separation of Enantiomers by Capillary Electrophoresis. Edited by T. A. Berger, K. S. Boos, H. Engelhardt, et al. Vieweg+Teubner Verlag, 2001. http://dx.doi.org/10.1007/978-3-322-83141-5.

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Chromatographic Society International Symposium on Chiral Separations (2nd 1989 University of Surrey). Recent advances in chiral separations. Plenum Press, 1990.

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Book chapters on the topic "Enantiomer separation"

1

Wren, Stephen, T. A. Berger, K. S. Boos, et al. "Modelling Enantiomer Separation by CE." In Chromatographia CE Series. Vieweg+Teubner Verlag, 2001. http://dx.doi.org/10.1007/978-3-322-83141-5_3.

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Okamoto, Yoshio. "Helical Polymers for Efficient Enantiomer Separation." In Hierarchical Macromolecular Structures: 60 Years after the Staudinger Nobel Prize I. Springer International Publishing, 2013. http://dx.doi.org/10.1007/12_2013_240.

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Bishop, Roger. "Enantiomer Ordering and Separation during Molecular Inclusion." In Separations and Reactions in Organic Supramolecular Chemistry. John Wiley & Sons, Ltd, 2004. http://dx.doi.org/10.1002/0470020261.ch2.

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Schleimer, Michael, and Volker Schurig. "Enantiomer Separation by Capillary Supercritical Fluid Chromatography." In Analysis with Supercritical Fluids: Extraction and Chromatography. Springer Berlin Heidelberg, 1992. http://dx.doi.org/10.1007/978-3-642-77474-4_8.

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Schurig, Volker, and Rainer Link. "Recent Developments in Enantiomer Separation by Complexation Gas Chromatography." In Chiral Separations. Springer US, 1988. http://dx.doi.org/10.1007/978-1-4615-6634-2_11.

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Boyarkin, Oleg, Stefan Burger, Thomas Franke, et al. "Transport at Interfaces in Lipid Membranes and Enantiomer Separation." In Transport Processes at Fluidic Interfaces. Springer International Publishing, 2017. http://dx.doi.org/10.1007/978-3-319-56602-3_17.

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Wall, Peter E. "High-Performance Thin-Layer Chromatography: A Quantitative Technique for Enantiomer Separation." In Recent Advances in Chiral Separations. Springer US, 1991. http://dx.doi.org/10.1007/978-1-4684-8282-9_20.

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Tanaka, Koichi. "Asymmetric Catalysis and Chromatographic Enantiomer Separation by Homochiral Metal–Organic Framework: Recent Advances." In Advances in Organic Crystal Chemistry. Springer Singapore, 2020. http://dx.doi.org/10.1007/978-981-15-5085-0_23.

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Kallenborn, Roland, Heinrich Hühnerfuss, Hassan Y. Aboul-Enein, and Imran Ali. "Quality Control and Evaluation Criteria for Enantiomer-Selective Separation Methods in Environmental Sciences." In Chiral Environmental Pollutants. Springer International Publishing, 2021. http://dx.doi.org/10.1007/978-3-030-62456-9_7.

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Schurig, Volker, and Martin Jung. "Enantiomer Separation on Dissolved Cyclodextrin Derivatives by High-Resolution Gas Chromatography: Thermodynamic Data of Chiral Recognition." In Recent Advances in Chiral Separations. Springer US, 1991. http://dx.doi.org/10.1007/978-1-4684-8282-9_17.

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Conference papers on the topic "Enantiomer separation"

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Golder, Francis J., Santhosh M. Baby, Ryan B. Gruber, et al. "Enantiomeric Separation Of Doxapram Reveals The (+)-Enantiomer (GAL-054) To Be A Superior Respiratory Stimulant With An Improved Therapeutic Index." In American Thoracic Society 2012 International Conference, May 18-23, 2012 • San Francisco, California. American Thoracic Society, 2012. http://dx.doi.org/10.1164/ajrccm-conference.2012.185.1_meetingabstracts.a3616.

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Bing, Nai-Ci, Zhen Tian, Sheng-Wen Chen, et al. "Analysis on Microstructure of Polymers for Selective Separation of Naproxen Enantiomers." In 2009 Symposium on Photonics and Optoelectronics. IEEE eXpress Conference Publishing, 2009. http://dx.doi.org/10.1109/sopo.2009.5230138.

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Kumar, Rakesh, Neha Yadav, Jyoti Arora, and Ashok K. Prasad. "Synthesis of chiral 4-pyrazolyl dihydropyridines and their enantiomeric separation." In 15th Brazilian Meeting on Organic Synthesis. Editora Edgard Blücher, 2013. http://dx.doi.org/10.5151/chempro-15bmos-bmos2013_2013101521523.

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Tao, Yugui, Qijin Wang, Qiang Wang, Hao Gu, and Changyun Qin. "Notice of Retraction: Optimization of Tryptophan Enantiomers Separation by Capillary Electrophoresis with Cyclodextrins." In 2011 5th International Conference on Bioinformatics and Biomedical Engineering. IEEE, 2011. http://dx.doi.org/10.1109/icbbe.2011.5779994.

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NG, S. C., L. CHEN, Y. C. PEH, et al. "SYNTHESIS AND CHROMATOGRAPHIC STUDY OF A NOVEL CSP FOR ENANTIOMERIC SEPARATION." In Proceedings of the Second Pacific Basin Conference. WORLD SCIENTIFIC, 2000. http://dx.doi.org/10.1142/9789812793331_0030.

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Weidong Li. "Enantiomeric separations of neonicotinoid insecticides on a Chirobiotic V column by high-performance liquid chromatography." In 2011 Second International Conference on Mechanic Automation and Control Engineering (MACE). IEEE, 2011. http://dx.doi.org/10.1109/mace.2011.5988524.

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Sázelová, Petra, Václav Kašička, Dušan Koval, and Zdeněk Prusík. "Separation of synthetic oligopeptides and terbutaline enantiomers by capillary zone electrophoresis with electroosmotic flow controlled by radial electric field." In IXth Conference Biologically Active Peptides. Institute of Organic Chemistry and Biochemistry, Academy of Sciences of the Czech Republic, 2005. http://dx.doi.org/10.1135/css200508073.

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Reports on the topic "Enantiomer separation"

1

Liu, Ying. Chromatographic Separations of Enantiomers and Underivatized Oligosaccharides. Office of Scientific and Technical Information (OSTI), 2004. http://dx.doi.org/10.2172/837283.

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Bae, Sue Y., and Mark D. Winemiller. Separation of VX, RVX and GB Enantiomers Using Liquid ChromatographyTime-of-Flight Mass Spectrometry. Defense Technical Information Center, 2016. http://dx.doi.org/10.21236/ad1002738.

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Ding, Wei Liang. Capillary electrophoresis separation of neutral organic compounds, pharmaceutical drugs, proteins and peptides, enantiomers, and anions. Office of Scientific and Technical Information (OSTI), 1999. http://dx.doi.org/10.2172/350830.

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