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Journal articles on the topic 'Hydroxyaceto'

Author: Grafiati

Published: 5 June 2025

Last updated: 1 August 2025

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1

H., B. SUTHAR, and R. SHAH J. "Possible Different Behaviour of 4,4'-(4,4'-Biphenylylenebisazo)-di(2-hydroxyaceto- phenone) in its Copper(II), Zinc(II) lron(II), lron(III) and Dioxouranium(VI) Chelates." Journal of Indian Chemical Society Vol. 65, Jun 1988 (1988): 445–46. https://doi.org/10.5281/zenodo.6303463.

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Department of Chemistry, Sardar Patel University, Vallabh Vidyanagar-388 120 <em>Manuscript received 15 November 1983, revised 2 December 1986, accepted  22 April 1987</em> Possible Different Behaviour of 4,4'-(4,4'-Biphenylylenebisazo)-di(2-hydroxyaceto- phenone) in its Copper(II), Zinc(II) lron(II), lron(III) and Dioxouranium(VI) Chelates.

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2

A., K. D. MAZUMDAR, K. KARMAKAR P., K. TIWARI S., P. BANERJEE K., and D. BANERJI K. "Syntheses of some 2-(2' -Methoxyphenyl)-chromones." Journal of Indian Chemical Society Vol. 67, Oct. 1990 (1990): 845–47. https://doi.org/10.5281/zenodo.6257426.

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Chemical Laboratory, Bhagalpur University, Bhagalpur-812 007 <em>Manuscript received 13 June 1989, revised 27 June 1990, accepted 10 July 1990</em> Syntheses of some 2-(2’-Methoxyphenyl)-chromones

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3

R.N., PRASAD, and JINDAL MITHLESH. "Mixed Ligand Complexes of Alkaline Earth Metals. Part-IV. Magnesium(II) and Calcium(II) Complexes with 1,3-Diphenylpropane- 1,3-dione and Salicylaldehyde, 2-Hydroxyaceto- phenone, Pentane-2,4-dione or 1-Phenylbutane-1,3-dione." Journal of Indian Chemical Society Vol. 66, Mar 1989 (1989): 188–89. https://doi.org/10.5281/zenodo.6132220.

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Chemistry Department, University of Rajasthan, Jaipur-802 004 <em>Manuscript received 18 April 1988, revised 4 August 1988, accepted 14 December 1988</em> WE have already reported<sup>1</sup> the mixed ligand complexes of alkaline earth metals of the type MLL<em>'</em>. The present paper describes the mixed ligand complexes of the type MLL<em>' </em>(H<sub>2</sub>O)<sub>2</sub> , where M=Mg<sup>II </sup>and Ca<sup>II</sup> ; HL= 1,3-diphenylpropane-1,3-dione; and HL<em>'</em> = salicylaldehyde, 2-hydroxyacetophenone, pentane-2,4-dione or 1-phenylbutane-1 ,3-dion

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4

Commodari, Fernando, and Brian K. Hunter. "Production and interconversion of 1,2-propanediol and hydroxyacetone by Escherichia coli." Biochemistry and Cell Biology 67, no. 8 (1989): 468–72. http://dx.doi.org/10.1139/o89-074.

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The anaerobic metabolism of marginally lethal levels of [13C]formaldehyde by Escherichia coli (K12, MU352, CRB, and CR63) was followed in vivo by 13C NMR. The products include 1, 2-propanediol. Under aeration, the 1, 2-propanediol is converted to hydroxyacetone. The hydroxyacetone is reconverted to 1, 2-propanediol when aeration is stopped. The process can be cycled by varying the rate of aeration.Key words: hydroxyacetone, 1, 2-propanediol, Escherichia coli, production.

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5

Dicus, Christopher W., Kevin J. Burnham, M. Judith Charles, and Michael H. Nantz. "Synthesis of13C3-hydroxyacetone." Journal of Labelled Compounds and Radiopharmaceuticals 46, no. 9 (2003): 793–98. http://dx.doi.org/10.1002/jlcr.719.

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6

Garden, Simon J., Marilza B. Corrêa, Angelo C. Pinto, James L. Wardell, John N. Low, and Christopher Glidewell. "EthylN-[2-(hydroxyacetyl)phenyl]carbamate, ethylN-[2-(hydroxyacetyl)-4-iodophenyl]carbamate and ethylN-[2-(hydroxyacetyl)-4-methylphenyl]carbamate." Acta Crystallographica Section C Crystal Structure Communications 63, no. 4 (2007): o234—o238. http://dx.doi.org/10.1107/s0108270107008682.

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7

Choi, Il-Ho, Hye-Jin Lee, and Kyung-Ran Hwang. "Understanding the effect of co-reactants on ketonization of carboxylic acids in the aqueous-phase pyrolysis oil of wood." Wood Science and Technology 55, no. 6 (2021): 1745–64. http://dx.doi.org/10.1007/s00226-021-01333-2.

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AbstractKetonization of carboxylic acids is one of the crucial reactions to produce sustainable bio-fuel and bio-chemicals from the pyrolysis oil of wood. Ketonization using different mixed solutions of carboxylic acids, furfural, and hydroxyacetone has been explored to understand the influence of co-feed reactants on the performance of ketonization of carboxylic acid over the selected CeZrOx catalyst. Furfural (7% in water) inhibited the catalytic activity for ketonization of acetic acid (20% solution) with reversible blocking of active sites, but for a mixed solution of hydroxyacetone (7%) a

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8

Ullah, Nisar, Clara Nanfe Fali, and Ian D. Spenser. "3-Amino-1-hydroxyacetone." Canadian Journal of Chemistry 82, no. 5 (2004): 579–82. http://dx.doi.org/10.1139/v04-010.

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3-Amino-1-hydroxypropan-2-one (3-amino-1-hydroxyacetone) was prepared in an overall yield of 52% in 6 steps starting with N-phthaloylglycine. This synthesis is readily adaptable for the preparation of bond-labeled samples, i.e., samples that are labeled intramolecularly at contiguous sites.Key words: 3-amino-1-hydroxyacetone, 3-amino-1-hydroxypropan-2-one.

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9

Wolf, Eckardt, Isaac A. Kennedy, Klaus Himmeldirk, and Ian D. Spenser. "5-Hydroxypentane-2,3-dione and 3-amino-1-hydroxypropan-2-one, putative precursors of vitamin B6." Canadian Journal of Chemistry 75, no. 7 (1997): 942–48. http://dx.doi.org/10.1139/v97-113.

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New syntheses are described of 5-hydroxypentane-2,3-dione (7) (i.e., laurencione [Formula: see text]) and of 3-amino-1-hydroxypropan-2-one (3-amino-1-hydroxyacetone) (5) hydrochloride, putative precursors of the C5 unit, C-2′,2,3,4,4′, and of the C3N unit, N-1,C-6,5,5′, respectively, of pyridoxine (6). Keywords: 3-amino-1-hydroxyacetone, 3-amino-1-hydroxypropanone, 5-hydroxypentane-2,3-dione, laurencione, vitamin B6.

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10

Spencer, K. M., M. R. Beaver, J. M. St Clair, J. D. Crounse, F. Paulot, and P. O. Wennberg. "Quantification of hydroxyacetone and glycolaldehyde using chemical ionization mass spectrometry." Atmospheric Chemistry and Physics Discussions 11, no. 8 (2011): 23619–53. http://dx.doi.org/10.5194/acpd-11-23619-2011.

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Abstract. Chemical ionization mass spectrometry (CIMS) enables online, fast, in situ detection and quantification of hydroxyacetone and glycolaldehyde. Two different CIMS approaches are demonstrated employing the strengths of single quadrupole mass spectrometry and triple quadrupole (tandem) mass spectrometry. Both methods are capable of the measurement of hydroxyacetone, an analyte with minimal isobaric interferences. Tandem mass spectrometry provides direct separation of the isobaric compounds glycolaldehyde and acetic acid using distinct, collision-induced dissociation daughter ions. Measur

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11

Mohaček-Grošev, Vlasta. "Vibrational analysis of hydroxyacetone." Spectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy 61, no. 3 (2005): 477–84. http://dx.doi.org/10.1016/j.saa.2004.05.007.

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12

Guthrie, J. Peter, and John Cossar. "The chlorination of acetone: a complete kinetic analysis." Canadian Journal of Chemistry 64, no. 6 (1986): 1250–66. http://dx.doi.org/10.1139/v86-208.

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Rate constants are reported for all of the major steps followed in the chlorination of acetone, including the chlorination of mono- and 1,1-dichloroacetone, the chlorination of hydroxyacetone, the chlorination and hydroxide-catalyzed rearrangement of 1,1-dihydroxyacetone, and the haloform cleavage of trichloroacetone. pKa values are reported for hydroxyacetone and monochloroacetone. Rate constants for the hydrolyses of chloroacetone and 1,1-dichloroacetone are reported; these reactions are probably not SN2 displacements but proceed by addition of hydroxide and intramolecular displacement.

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13

Clair, J. M. St, K. M. Spencer, M. R. Beaver, J. D. Crounse, F. Paulot, and P. O. Wennberg. "Quantification of hydroxyacetone and glycolaldehyde using chemical ionization mass spectrometry." Atmospheric Chemistry and Physics 14, no. 8 (2014): 4251–62. http://dx.doi.org/10.5194/acp-14-4251-2014.

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Chemical ionization mass spectrometry (CIMS) enables online, rapid, in situ detection and quantification of hydroxyacetone and glycolaldehyde. Two different CIMS approaches are demonstrated employing the strengths of single quadrupole mass spectrometry and triple quadrupole (tandem) mass spectrometry. Both methods are generally capable of the measurement of hydroxyacetone, an analyte with known but minimal isobaric interferences. Tandem mass spectrometry provides direct separation of the isobaric compounds glycolaldehyde and acetic acid using distinct, collision-induced dissociation daughter i

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14

Albuquerque, Elise M., Luiz E. P. Borges, and Marco A. Fraga. "Lactic acid production from hydroxyacetone on dual metal/base heterogeneous catalytic systems." Green Chemistry 17, no. 7 (2015): 3889–99. http://dx.doi.org/10.1039/c5gc00736d.

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15

Bergem, Håkon, Run Xu, Robert C. Brown, and George W. Huber. "Low temperature aqueous phase hydrogenation of the light oxygenate fraction of bio-oil over supported ruthenium catalysts." Green Chemistry 19, no. 14 (2017): 3252–62. http://dx.doi.org/10.1039/c7gc00367f.

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16

Han, Depeng, Wang Yin, Ali Arslan, Tongrui Liu, Yan Zheng, and Shuqian Xia. "Stabilization of Fast Pyrolysis Liquids from Biomass by Mild Catalytic Hydrotreatment: Model Compound Study." Catalysts 10, no. 4 (2020): 402. http://dx.doi.org/10.3390/catal10040402.

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Repolymerization is a huge problem in the storage and processing of biomass pyrolysis liquid (PL). Herein, to solve the problem of repolymerization, mild catalytic hydrotreatment of PL was conducted to convert unstable PL model compounds (hydroxyacetone, furfural, and phenol) into stable alcohols. An Ni/SiO2 catalyst was synthesized by the deposition-precipitation method and used in a mild hydrotreatment process. The mild hydrotreatment of the single model compound was studied to determine the reaction pathways, which provided guidance for improving the selectivity of stable intermediate alcoh

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17

Taatjes, Craig A., Fang Liu, Brandon Rotavera, et al. "Hydroxyacetone Production From C3 Criegee Intermediates." Journal of Physical Chemistry A 121, no. 1 (2016): 16–23. http://dx.doi.org/10.1021/acs.jpca.6b07712.

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18

Huang, Ru-Jin, Junji Cao, Yang Chen, et al. "Organosulfates in atmospheric aerosol: synthesis and quantitative analysis of PM<sub>2.5</sub> from Xi'an, northwestern China." Atmospheric Measurement Techniques 11, no. 6 (2018): 3447–56. http://dx.doi.org/10.5194/amt-11-3447-2018.

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Abstract. The sources, formation mechanism and amount of organosulfates (OS) in atmospheric aerosol are not yet well understood, partly due to the lack of authentic standards for quantification. In this study, we report an improved robust procedure for the synthesis of organosulfates with different functional groups. Nine authentic organosulfate standards were synthesized and four standards (benzyl sulfate, phenyl sulfate, glycolic acid sulfate, and hydroxyacetone sulfate) were used to quantify their ambient concentrations. The authentic standards and ambient aerosol samples were analyzed usin

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19

Georgescu, Vasile, Casen Panaitescu, Mihaela Bombos, and Dorin Bombos. "Hydrogenolysis of Glycerol in Gas Phase on Cu-Cr Mixed Oxide Catalyst Doped with Ni." Revista de Chimie 68, no. 5 (2017): 1118–21. http://dx.doi.org/10.37358/rc.17.5.5624.

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Hydrogenolysis of glycerol was conducted on catalyst of the type mixed oxide of Cu-Cr doped with NiO on g-Al2O3. The prepared catalyst was analyzed by XRD, IR and TPR. Catalytic tests were carried out on a laboratory plant in continuous flow system on a reactor equipped with heating mantle, at molar ratio of glycerol / hydrogen of 1/300, glycerol volume hourly space velocities 1000s-1, temperatures 200-220oC and pressures 3-5 bar. The main reaction products identified were propylene glycol and hydroxyacetone. Glycerol conversion increases with temperature and pressure on ranges of parameters s

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20

Zhou, Yu-Hao, Yu-Zu Zhang, Zhu-Lian Wu, Tian Cai, Wei Wen, and Qi-Xiang Guo. "Organocatalytic Asymmetric Aldol Reaction of Arylglyoxals and Hydroxyacetone: Enantioselective Synthesis of 2,3-Dihydroxy-1,4-diones." Molecules 25, no. 3 (2020): 648. http://dx.doi.org/10.3390/molecules25030648.

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A highly efficient quinine-derived primary-amine-catalyzed asymmetric aldol addition of hydroxyacetone to arylglyoxals is described. Structurally diverse anti-2,3-dihydroxy-1,4-diones were generated in high yields, with good diastereoselectivities and enantioselectivities.

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21

Galloway, M. M., A. J. Huisman, L. D. Yee, et al. "Yields of oxidized volatile organic compounds during the OH radical initiated oxidation of isoprene, methyl vinyl ketone, and methacrolein under high–NO<sub>x</sub> conditions." Atmospheric Chemistry and Physics Discussions 11, no. 4 (2011): 10693–720. http://dx.doi.org/10.5194/acpd-11-10693-2011.

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Abstract. We present first-generation and total production yields of glyoxal, methylglyoxal, glycolaldehyde, and hydroxyacetone from the oxidation of isoprene, methyl vinyl ketone (MVK), and methacrolein (MACR) with OH under high NOx conditions. Several of these first-generation yields are not included in commonly used chemical mechanisms, such as the Leeds Master Chemical Mechanism (MCM) v. 3.1. Inclusion of first-generation production of glyoxal, glycolaldehyde and hydroxyacetone from isoprene and methylglyoxal from MACR greatly improves performance of an MCM based model during the initial p

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22

Li, Bao-Lin, Zhen-Guo Zhang, Wei Wang, Jin Li, and Chou-Wen Wang. "Solvent-free Friedel-Crafts Reaction for Regioselective Synthesis of Ethyl (9-Anthryl)glyoxylate and Chiral Resolution of (±)-(9-Anthryl)hydroxyacetic Acid." Zeitschrift für Naturforschung B 63, no. 1 (2008): 77–82. http://dx.doi.org/10.1515/znb-2008-0111.

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A green chemistry-based highly regioselective synthesis of ethyl (9-anthryl)glyoxylate was achieved by solvent-free Friedel-Crafts reaction at r. t. Several derivatives of ethyl (9-anthryl)glyoxylate were also synthesized. Ethyl (9-anthryl)hydroxyacetate was obtained almost quantitatively by reduction of ethyl (9-anthryl)glyoxylate with NaBH4, and (9-anthryl)methoxyacetic acid was prepared by methylation of ethyl (9-anthryl)hydroxyacetate with CH3I in the presence of Ag2O and hydrolysis of ethyl (9-anthryl)methoxyacetate. The hydrolysis of ethyl (9-anthryl)hydroxyacetate gave racemic (9-anthry

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23

Rodigast, M., A. Mutzel, J. Schindelka, and H. Herrmann. "A new source of methyl glyoxal in the aqueous phase." Atmospheric Chemistry and Physics Discussions 15, no. 21 (2015): 31891–924. http://dx.doi.org/10.5194/acpd-15-31891-2015.

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Abstract. Carbonyl compounds are ubiquitous in atmospheric multiphase system participating in gas, particle, and aqueous-phase chemistry. One important compound is methyl ethyl ketone (MEK), as it is detected in significant amounts in the gas phase as well as in cloud water, ice, and rain. Consequently, it can be expected that MEK influences the liquid phase chemistry. Therefore, the oxidation of MEK and the formation of corresponding oxidation products were investigated in the aqueous phase. Several oxidation products were identified from the oxidation with OH radicals, including 2,3-butanedi

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24

Rodigast, Maria, Anke Mutzel, Janine Schindelka, and Hartmut Herrmann. "A new source of methylglyoxal in the aqueous phase." Atmospheric Chemistry and Physics 16, no. 4 (2016): 2689–702. http://dx.doi.org/10.5194/acp-16-2689-2016.

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Abstract. Carbonyl compounds are ubiquitous in atmospheric multiphase system participating in gas, particle, and aqueous-phase chemistry. One important compound is methyl ethyl ketone (MEK), as it is detected in significant amounts in the gas phase as well as in cloud water, ice, and rain. Consequently, it can be expected that MEK influences the liquid-phase chemistry. Therefore, the oxidation of MEK and the formation of corresponding oxidation products were investigated in the aqueous phase. Several oxidation products were identified from the oxidation with OH radicals, including 2,3-butanedi

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25

Galloway, M. M., A. J. Huisman, L. D. Yee, et al. "Yields of oxidized volatile organic compounds during the OH radical initiated oxidation of isoprene, methyl vinyl ketone, and methacrolein under high-NO<sub>x</sub> conditions." Atmospheric Chemistry and Physics 11, no. 21 (2011): 10779–90. http://dx.doi.org/10.5194/acp-11-10779-2011.

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Abstract. We present first-generation and total production yields of glyoxal, methylglyoxal, glycolaldehyde, and hydroxyacetone from the oxidation of isoprene, methyl vinyl ketone (MVK), and methacrolein (MACR) with OH under high NOx conditions. Several of these first-generation yields are not included in commonly used chemical mechanisms, such as the Leeds Master Chemical Mechanism (MCM) v. 3.2. The first-generation yield of glyoxal from isoprene was determined to be 2.1 (±0.6)%. Inclusion of first-generation production of glyoxal, glycolaldehyde and hydroxyacetone from isoprene greatly impro

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26

Arakawa, Ryuichi. "Mass Spectral Study of Ionized-Hydroxyacetone Dissociation." Bulletin of the Chemical Society of Japan 64, no. 3 (1991): 1022–24. http://dx.doi.org/10.1246/bcsj.64.1022.

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27

Zhou, Xianliang, Gu Huang, Kevin Civerolo, and James Schwab. "Measurement of Atmospheric Hydroxyacetone, Glycolaldehyde, and Formaldehyde." Environmental Science & Technology 43, no. 8 (2009): 2753–59. http://dx.doi.org/10.1021/es803025g.

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28

Liu, Wen-Jing, Zhi-Qiang Wei та Shan-Tang Yue. "Tetraaqua(2-hydroxyacetato-κ2O1,O2)magnesium nitrate". Acta Crystallographica Section E Structure Reports Online 67, № 3 (2011): m374. http://dx.doi.org/10.1107/s1600536811006611.

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29

Petitjean, Mélanie, Maria Darvas, Sylvain Picaud, Pál Jedlovszky, and Stéphane Le Calvé. "Adsorption of Hydroxyacetone on Pure Ice Surfaces." ChemPhysChem 11, no. 18 (2010): 3921–27. http://dx.doi.org/10.1002/cphc.201000629.

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30

Guella, G., I. Mancini, D. Duhet, B. Richer de Forges, and F. Pietra. "Ethyl 6-Bromo-3-indolcarboxylate and 3-Hydroxyacetal-6-bromoindole, Novel Bromoindoles from the Sponge Pleroma menoui of the Coral Sea." Zeitschrift für Naturforschung C 44, no. 11-12 (1989): 914–16. http://dx.doi.org/10.1515/znc-1989-11-1206.

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Abstract The demosponge Pleroma menoui (order Lithistida, suborder Trienosina (= Desmophorina), family Pleromidae), collected in the Coral Sea south-east of Noum ea at a depth of 500 m, is proven here to contain the novel alkaloids ethyl 6-brom o-3-indolcarboxylate and 3-hydroxyacetyl-6-brom oindole.

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31

Hettiyadura, A. P. S., E. A. Stone, S. Kundu, et al. "Determination of atmospheric organosulfates using HILIC chromatography with MS detection." Atmospheric Measurement Techniques 8, no. 6 (2015): 2347–58. http://dx.doi.org/10.5194/amt-8-2347-2015.

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Abstract. Measurements of organosulfates in ambient aerosols provide insight to the extent of secondary organic aerosol (SOA) formation from mixtures of biogenic gases and anthropogenic pollutants. Organosulfates have, however, proved analytically challenging to quantify, due to lack of authentic standards and the complex sample matrix in which organosulfates are observed. This study presents a sensitive and accurate new analytical method for the quantification of organosulfates based upon ultra-performance liquid chromatography (UPLC) with negative electrospray ionization mass spectrometry (M

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32

Luciani, Giuseppina, Giovanna Ruoppolo, Gianluca Landi, Valentina Gargiulo, Michela Alfè, and Almerinda Di Benedetto. "Glycerol Hydrogenolysis to 1,2-Propanediol over Novel Cu/ZrO2 Catalysts." Catalysts 12, no. 1 (2022): 72. http://dx.doi.org/10.3390/catal12010072.

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Glycerol is the main by-product of biodiesel production; its upgrading to more valuable products is a demanding issue. Hydrogenolysis to 1,2-propanediol is one of the most interesting processes among the possible upgrading routes. In this study, we propose novel copper/zirconia catalysts prepared by advanced preparation methods, including copper deposition via metal–organic framework (MOF) and support preparation via the sol–gel route. The catalysts were characterized by N2 physisorption, X-ray diffraction, Scanning Electron Microscopy, H2-TPR and NH3-TPD analyses and tested in a commercial ba

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33

Prudius, S. V., V. M. Sontsev, and V. V. Brei. "Hydroxyacetone oxidation with hydrogen peroxide over acid catalysts." Himia, Fizika ta Tehnologia Poverhni 6, no. 4 (2015): 498–503. http://dx.doi.org/10.15407/hftp06.04.498.

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34

Chowdhury, Pradyot K., Hari P. Upadhyaya, Prakash D. Naik, and Jai P. Mittal. "Direct observation of OH photofragment from triplet hydroxyacetone." Chemical Physics Letters 356, no. 5-6 (2002): 476–82. http://dx.doi.org/10.1016/s0009-2614(02)00391-3.

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35

Bigovic, Miljan, Veselin Maslak, Zorana Tokic-Vujosevic, Vladimir Divjakovic, and Radomir N. Saicic. "A Useful Synthetic Equivalent of a Hydroxyacetone Enolate." Organic Letters 13, no. 17 (2011): 4720–23. http://dx.doi.org/10.1021/ol2019357.

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36

Daliacker, Franz, Hans-Joachim Schieuter, and Petra Schneider. "Darstellung und Reaktionen von 1,3-Benzdioxol-biscarbaldehyden. Ein Beitrag zur Strukturaufklärung des Nepenthons A / Synthesis and Reactions of 1,3-Benzodioxoledicarboxaldehydes. A Contribution to the Structure Elucidation of Nepenthone-A." Zeitschrift für Naturforschung B 41, no. 10 (1986): 1273–80. http://dx.doi.org/10.1515/znb-1986-1014.

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We describe the preparation o f 1,3-Benzodioxole-5,6-dicarboxaldehyde (1d) and 1,3-Benzdioxole- 4,5-dicarboxaldehyde (3h). Under especially mild conditions also the synthesis of 4,7- Dimethoxy-1,3-benzodioxole-5,6-dicarboxaldehyde (4g) can be achieved. Its reaction with Hydroxyacetone leads to quinone 9a, which after methylation can be identified with the dim ethylether of Nepenthone-A .

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37

Smith, Paul J., Louise Smith, Nicholas F. Dummer, et al. "Investigating the Influence of Reaction Conditions and the Properties of Ceria for the Valorisation of Glycerol." Energies 12, no. 7 (2019): 1359. http://dx.doi.org/10.3390/en12071359.

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The reaction of aqueous glycerol over a series of ceria catalysts is investigated, to produce bio-renewable methanol. Product distributions were greatly influenced by the reaction temperature and catalyst contact time. Glycerol conversion of 21% was achieved for a 50 wt.% glycerol solution, over CeO2 (8 m2 g−1) at 320 °C. The carbon mass balance was >99 % and the main product was hydroxyacetone. In contrast, at 440 °C the conversion and carbon mass balance were >99.9 % and 76 % respectively. Acetaldehyde and methanol were the major products at this higher temperature, as both can be form

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38

Kawamura, K., K. Okuzawa, S. G. Aggarwal, H. Irie, Y. Kanaya, and Z. Wang. "Determination of gaseous and particulate carbonyls (glycolaldehyde, hydroxyacetone, glyoxal, methylglyoxal, nonanal and decanal) in the atmosphere at Mt. Tai." Atmospheric Chemistry and Physics 13, no. 10 (2013): 5369–80. http://dx.doi.org/10.5194/acp-13-5369-2013.

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Abstract. Gaseous and particulate semi-volatile carbonyl compounds were determined every three hours in the atmosphere of Mount Tai (elevation, 1534 m) in the North China Plain during 2–5, 23–24 and 25 June 2006 under clear sky conditions. Using a two-step filter cartridge in a series, particulate carbonyls were first collected on a quartz filter and then gaseous carbonyls were collected on a quartz filter impregnated with O-benzylhydroxylamine (BHA). After the two-step derivatization with BHA and N,O-Bis(trimethylsilyl)trifluoroacetamide (BSTFA), carbonyl derivatives were measured using a gas

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39

White, Robert H. "Biochemical Origins of Lactaldehyde and Hydroxyacetone in Methanocaldococcus jannaschii†." Biochemistry 47, no. 17 (2008): 5037–46. http://dx.doi.org/10.1021/bi800069x.

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40

Braakman, Rogier, Brian J. Drouin, Susanna L. Widicus Weaver, and Geoffrey A. Blake. "Extended analysis of hydroxyacetone in the torsional ground state." Journal of Molecular Spectroscopy 264, no. 1 (2010): 43–49. http://dx.doi.org/10.1016/j.jms.2010.09.003.

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41

Liu, Huawei, Lizeng Peng, Tao Zhang, and Yulin Li. "l-Proline catalyzed asymmetric aldol reactions of protected hydroxyacetone." New Journal of Chemistry 27, no. 8 (2003): 1159. http://dx.doi.org/10.1039/b304019b.

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42

Zhou, Yan, Dong-Hui Quan, Xia Zhang, and Sheng-Li Qin. "Detection of hydroxyacetone in protostar IRAS 16293-2422 B." Research in Astronomy and Astrophysics 20, no. 8 (2020): 125. http://dx.doi.org/10.1088/1674-4527/20/8/125.

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43

Ye, Q. S., M. J. Xie, J. Yu, et al. "Crystal structures of tetrakis (hydroxyacetato)bis(dimethylsulfoxide) dirhodium(II)." Journal of Structural Chemistry 58, no. 3 (2017): 631–35. http://dx.doi.org/10.1134/s0022476617030313.

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44

Wu, Yong, Daiqian Xie, and Ying Xue. "Ab initio studies for the photodissociation mechanism of hydroxyacetone." Journal of Computational Chemistry 24, no. 8 (2003): 931–38. http://dx.doi.org/10.1002/jcc.10264.

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45

Buchcic, Aleksandra, Anna Zawisza, Stanisław Leśniak, Justyna Adamczyk, Adam Marek Pieczonka, and Michał Rachwalski. "Enantioselective Mannich Reaction Promoted by Chiral Phosphinoyl-Aziridines." Catalysts 9, no. 10 (2019): 837. http://dx.doi.org/10.3390/catal9100837.

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In this study, a set of enantiomerically pure aziridines bearing a phosphine oxide moiety were prepared in high yields and tested as chiral catalysts in the direct asymmetric Mannich reaction of hydroxyacetone, an amine (p-anisidine), and various aromatic aldehydes. The appropriate Mannich adducts were formed in chemical yields from moderate to good with a high level of enantio- and diastereoselectivity. The best results were obtained using the catalysts bearing a free NH-aziridine subunit.

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46

S., Kothari, Singhal M., Vijayvergia D., Vyas R., and L. Verma B. "Synthesis and biocidal activity of some new 2-amino-4,6-diarylsubstituted-pyrimidines." Journal of Indian Chemical Society Vol. 77, Jul 2000 (2000): 329–31. https://doi.org/10.5281/zenodo.5867166.

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Department of Chemistry, Faculty of Science, M. L. Sukhadia University, Udaipur-313 002, India <em>Manuscript received 17 November 1999, accepted 23 March 2000</em> The chalcones (3a-q), derived from 3,5-dibromo-4-hydroxyacetophenone (Ia), 3,5-dibromo-2-hydroxyacet!)phenone (1b), 3-bromo-5- chloro-/5-methyl-2-hydroxyacetophenones (1c,d) and 4-(4'-nitrophenoxy)acetophenone (1e) and prepared by Claisen-Schmidt condensation with different substituted aromatic aldehydes (2a-f) in presence of base, on treatment with guanidine nitrate in ethanol and base give new 2-amino-4,6-diaryl-sub

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47

Al-Taie, Zahraa S., Simon J. Coles, Aileen Congreve, et al. "C2-Symmetric Amino Acid Amide-Derived Organocatalysts." Reactions 5, no. 3 (2024): 567–86. http://dx.doi.org/10.3390/reactions5030027.

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N-alkylated C2-symmetric amino acid amide derivatives were shown to catalyse the Michael addition of 2-hydroxy-1,4-napthoquinone to β-nitrostyrene, achieving a maximum ee of 44%. The corresponding trifluoroacetic acid salts also catalysed the aldol reaction between 4-nitrobenzaldehyde and hydroxyacetone, leading to the formation of predominantly syn-aldol products in up to 55% ee. Aspects of the solvent dependence of the aldol reaction and the H-bonding of the catalyst were investigated.

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48

Zegota, Henryk, Man Nien Schuchmann, Dorothea Schulz, and Clemens von Sonntag. "Acetonylperoxyl Radicals, CH3COCH2O2: A Study on the y-Radiolysis and Pulse Radiolysis of Acetone in Oxygenated Aqueous Solutions." Zeitschrift für Naturforschung B 41, no. 8 (1986): 1015–22. http://dx.doi.org/10.1515/znb-1986-0815.

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Abstract Hydroxyl radicals from the radiolysis of N2O/O2 (4:1)-saturated aqueous solutions of acetone (10−3 mol dm −3) react with the solute by H-abstraction thereby forming acetonyl radicals. As shown by pulse radiolysis, the acetonyl radicals rapidly add oxygen (k = 3 x 109 dm3mol−1s−1) thereby forming acetonylperoxyl radicals which decay by second-order kinetics (2 k = 8 x 108 dm3mol−1s−1). Under steady-state radiolysis conditions (0.24 Gy s−1) the products (G values in parentheses) are methylglyoxal (2.5), hydroxyacetone (0.5), form aldehyde (1 .6), acids (1 .7), carbon dioxide (0 .5), org

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49

Gu, Qing, Ling-Xia Jiang, Kui Yuan, Lei Zhang, and Xin-Yan Wu. "Organocatalytic, Asymmetric, One-Pot, Three-Component Mannich Reaction of Hydroxyacetone." Synthetic Communications 38, no. 23 (2008): 4198–206. http://dx.doi.org/10.1080/00397910802323098.

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Bolm, Carsten, Andrey Kasyan, Peter Heider та ін. "Synthesis and Use of α-Silyl-Substituted α-Hydroxyacetic Acids†". Organic Letters 4, № 13 (2002): 2265–67. http://dx.doi.org/10.1021/ol025911n.

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