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Journal articles on the topic 'MADIX controlled radical polymerization'

Author: Grafiati

Published: 25 May 2024

Last updated: 31 July 2025

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1

Etchenausia, Laura, Abdel Khoukh, Elise Deniau Lejeune, and Maud Save. "RAFT/MADIX emulsion copolymerization of vinyl acetate and N-vinylcaprolactam: towards waterborne physically crosslinked thermoresponsive particles." Polymer Chemistry 8, no. 14 (2017): 2244–56. http://dx.doi.org/10.1039/c7py00221a.

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2

Destarac, Mathias, Wojciech Bzducha, Daniel Taton, Isabelle Gauthier-Gillaizeau, and Samir Z. Zard. "Xanthates as Chain-Transfer Agents in Controlled Radical Polymerization (MADIX): Structural Effect of the O-Alkyl Group." Macromolecular Rapid Communications 23, no. 17 (2002): 1049–54. http://dx.doi.org/10.1002/marc.200290002.

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3

Destarac, Mathias, Juliette Ruchmann-Sternchuss, Eric Van Gramberen, Xavier Vila та Samir Z. Zard. "α-Amido Trifluoromethyl Xanthates: A New Class of RAFT/MADIX Agents". Molecules 29, № 10 (2024): 2174. http://dx.doi.org/10.3390/molecules29102174.

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Xanthates have long been described as poor RAFT/MADIX agents for styrene polymerization. Through the determination of chain transfer constants to xanthates, this work demonstrated beneficial capto-dative substituent effects for the leaving group of a new series of α-amido trifluoromethyl xanthates, with the best effect observed with trifluoroacetyl group. The previously observed Z-group activation with a O-trifluoroethyl group compared to the O-ethyl counterpart was quantitatively established with Cex = 2.7 (3–4 fold increase) using the SEC peak resolution method. This study further confirmed

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4

Seiler, Lucie, Julien Loiseau, Frédéric Leising, Pascal Boustingorry, Simon Harrisson, and Mathias Destarac. "Acceleration and improved control of aqueous RAFT/MADIX polymerization of vinylphosphonic acid in the presence of alkali hydroxides." Polymer Chemistry 8, no. 25 (2017): 3825–32. http://dx.doi.org/10.1039/c7py00747g.

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5

Wang, Pucheng, Jingwen Dai, Lei Liu, Qibao Dong, Hu Wang та Ruke Bai. "Synthesis and properties of a well-defined copolymer of chlorotrifluoroethylene and N-vinylpyrrolidone by xanthate-mediated radical copolymerization under 60Co γ-ray irradiation". Polym. Chem. 5, № 21 (2014): 6358–64. http://dx.doi.org/10.1039/c4py00902a.

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6

Theis, Alexander, Thomas P. Davis, Martina H. Stenzel, and Christopher Barner-Kowollik. "Probing the reaction kinetics of vinyl acetate free radical polymerization via living free radical polymerization (MADIX)." Polymer 47, no. 4 (2006): 999–1010. http://dx.doi.org/10.1016/j.polymer.2005.12.054.

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7

Zard, Samir Z. "The Genesis of the Reversible Radical Addition–Fragmentation–Transfer of Thiocarbonylthio Derivatives from the Barton–McCombie Deoxygenation: A Brief Account and Some Mechanistic Observations." Australian Journal of Chemistry 59, no. 10 (2006): 663. http://dx.doi.org/10.1071/ch06263.

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The observations and reasoning leading to the discovery of the degenerative transfer of xanthates and related thiocarbonylthio derivatives are briefly described. A few synthetic applications are presented, and the consequences on the emergence of the RAFT and MADIX polymerization technologies as well as some mechanistic aspects are briefly discussed.

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8

Matyjaszewski, Krzysztof. "Controlled radical polymerization." Current Opinion in Solid State and Materials Science 1, no. 6 (1996): 769–76. http://dx.doi.org/10.1016/s1359-0286(96)80101-x.

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9

Gaynor, Scott, Dorota Greszta, Daniela Mardare, Mircea Teodorescu, and Krzysztof Matyjaszewski. "Controlled Radical Polymerization." Journal of Macromolecular Science, Part A 31, no. 11 (1994): 1561–78. http://dx.doi.org/10.1080/10601329408545868.

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10

Bertin, Denis, and Bernard Boutevin. "Controlled radical polymerization." Polymer Bulletin 37, no. 3 (1996): 337–44. http://dx.doi.org/10.1007/bf00318066.

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11

Lou, Yu, Dong Jian Shi, Wei Fu Dong, and Ming Qing Chen. "Synthesis and Self-Assemble Behavior of Block Copolymerization of Vinyl Acetate and N-Vinylacetamide." Advanced Materials Research 645 (January 2013): 10–14. http://dx.doi.org/10.4028/www.scientific.net/amr.645.10.

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Polymerizations of VAc was carried out using AIBN as the initiator and DIP as the MADIX agent precursor. Then, block copolymer PVAc-b-PNVA had been synthesized by RAFT radical polymerization in the presence of PVAc-DIP as macro CTA. The length of blocks could be tuned by changing the molar ratio of NVA and VAc. Block copolymer PVAc-b-PNVA self-assembled into micelles in solution, and underwent microphase separation in bulk state.

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12

Severin, K., M. Haas, E. Solari, O. Nguyen, S. Gautier, and R. Scopelliti. "RT-Controlled Radical Polymerization." Synfacts 2006, no. 5 (2006): 0446. http://dx.doi.org/10.1055/s-2006-934385.

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13

Matyjaszewski, Krzysztof, and James Spanswick. "Controlled/living radical polymerization." Materials Today 8, no. 3 (2005): 26–33. http://dx.doi.org/10.1016/s1369-7021(05)00745-5.

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14

Pan, Xiangcheng, Mehmet Atilla Tasdelen, Joachim Laun, Thomas Junkers, Yusuf Yagci, and Krzysztof Matyjaszewski. "Photomediated controlled radical polymerization." Progress in Polymer Science 62 (November 2016): 73–125. http://dx.doi.org/10.1016/j.progpolymsci.2016.06.005.

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15

Tasdelen, Mehmet Atilla, Mustafa Uygun, and Yusuf Yagci. "Photoinduced Controlled Radical Polymerization." Macromolecular Rapid Communications 32, no. 1 (2010): 58–62. http://dx.doi.org/10.1002/marc.201000351.

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16

Bon, Stefan A. F., Michiel Bosveld, Bert Klumperman, and Anton L. German. "Controlled Radical Polymerization in Emulsion." Macromolecules 30, no. 2 (1997): 324–26. http://dx.doi.org/10.1021/ma961003s.

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17

Matyjaszewski, Krzysztof, Scott Gaynor, Dorota Greszta, Daniela Mardare, and Takeo Shigemoto. "?Living? and controlled radical polymerization." Journal of Physical Organic Chemistry 8, no. 4 (1995): 306–15. http://dx.doi.org/10.1002/poc.610080414.

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18

Whitfield, Richard, Nghia P. Truong, and Athina Anastasaki. "Sequence-controlled Polymers via Controlled Radical Polymerization." CHIMIA International Journal for Chemistry 73, no. 4 (2019): 331. http://dx.doi.org/10.2533/chimia.2019.331.

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19

Caille, Jean-Raphaël, Antoine Debuigne, and Robert Jérôme. "Controlled Radical Polymerization of Styrene by Quinone Transfer Radical Polymerization (QTRP)." Macromolecules 38, no. 1 (2005): 27–32. http://dx.doi.org/10.1021/ma048561o.

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20

Matyjaszewski, Krzysztof. "Transition Metal Catalysis in Controlled Radical Polymerization: Atom Transfer Radical Polymerization." Chemistry - A European Journal 5, no. 11 (1999): 3095–102. http://dx.doi.org/10.1002/(sici)1521-3765(19991105)5:11<3095::aid-chem3095>3.0.co;2-#.

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21

Wang, Lu, Wang, and Bai. "A New Strategy for the Synthesis of Fluorinated Polyurethane." Polymers 11, no. 9 (2019): 1440. http://dx.doi.org/10.3390/polym11091440.

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An alternating fluorinated copolymer based on chlorotrifluoroethylene (CTFE) and butyl vinyl ether (BVE) was synthesized by RAFT/MADIX living/controlled polymerization in the presence of S-benzyl O-ethyl dithiocarbonate (BEDTC). Then, using the obtained poly(CTFE-alt-BVE) as a macro chain transfer agent (macro-CTA), a block copolymer was prepared by chain extension polymerization of vinyl acetate (VAc). After a basic methanolysis process, the poly(vinyl acetate) (PVAc) block was transferred into poly(vinyl alcohol) (PVA). Finally, a novel fluorinated polyurethane with good surface properties d

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22

Jenkins, Aubrey D., Richard G. Jones, and Graeme Moad. "Terminology for reversible-deactivation radical polymerization previously called "controlled" radical or "living" radical polymerization (IUPAC Recommendations 2010)." Pure and Applied Chemistry 82, no. 2 (2009): 483–91. http://dx.doi.org/10.1351/pac-rep-08-04-03.

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This document defines terms related to modern methods of radical polymerization, in which certain additives react reversibly with the radicals, thus enabling the reactions to take on much of the character of living polymerizations, even though some termination inevitably takes place. In recent technical literature, these reactions have often been loosely referred to as, inter alia, "controlled", "controlled/living", or "living" polymerizations. The use of these terms is discouraged. The use of "controlled" is permitted as long as the type of control is defined at its first occurrence, but the

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23

Quiclet-Sire, Béatrice, and Samir Z. Zard. "Fun with radicals: Some new perspectives for organic synthesis." Pure and Applied Chemistry 83, no. 3 (2010): 519–51. http://dx.doi.org/10.1351/pac-con-10-08-07.

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The degenerative radical addition-transfer of xanthates onto alkenes allows the rapid assembly of richly functionalized structures. Various families of open-chain, cyclic, and polycyclic compounds can thus be readily accessed. Furthermore, the process can be extended to the synthesis or modification of aromatic and heteroaromatic derivatives by exploiting the possibility of using peroxides both as initiators and stoichiometric oxidants. The modification of existing polymers and the controlled synthesis of block polymers by what is now known as the RAFT/MADIX (reversible addition–fragmentation

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24

Grimaud, Thomas, and Krzysztof Matyjaszewski. "Controlled/“Living” Radical Polymerization of Methyl Methacrylate by Atom Transfer Radical Polymerization." Macromolecules 30, no. 7 (1997): 2216–18. http://dx.doi.org/10.1021/ma961796i.

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25

Xia, Jianhui, and Krzysztof Matyjaszewski. "Controlled/“Living” Radical Polymerization. Atom Transfer Radical Polymerization Using Multidentate Amine Ligands." Macromolecules 30, no. 25 (1997): 7697–700. http://dx.doi.org/10.1021/ma971009x.

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26

Higashimura, Hideyuki. "Radical-Controlled Oxidative Polymerization of Phenols." Journal of Synthetic Organic Chemistry, Japan 63, no. 10 (2005): 970–81. http://dx.doi.org/10.5059/yukigoseikyokaishi.63.970.

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27

UEDA, Naoki. "Controlled Radical Polymerization with Iodine Compounds." Kobunshi 48, no. 7 (1999): 513. http://dx.doi.org/10.1295/kobunshi.48.513.

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28

SHIGA, Akinobu. "“Radical -Controlled”Oxidative Polymerization of Phenols." Kobunshi 49, no. 4 (2000): 236. http://dx.doi.org/10.1295/kobunshi.49.236.

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29

Matyjaszewski, K., and E. Chernikova. "New trends in controlled radical polymerization." Polymer Science Series C 57, no. 1 (2015): 1–2. http://dx.doi.org/10.1134/s1811238215010075.

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30

Pan, Xiangcheng, Marco Fantin, Fang Yuan, and Krzysztof Matyjaszewski. "Externally controlled atom transfer radical polymerization." Chemical Society Reviews 47, no. 14 (2018): 5457–90. http://dx.doi.org/10.1039/c8cs00259b.

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ATRP can be externally controlled by electrical current, light, mechanical forces and various chemical reducing agents. The mechanistic aspects and preparation of polymers with complex functional architectures and their applications are critically reviewed.

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31

Cuthbert, Julia, Anna C. Balazs, Tomasz Kowalewski, and Krzysztof Matyjaszewski. "STEM Gels by Controlled Radical Polymerization." Trends in Chemistry 2, no. 4 (2020): 341–53. http://dx.doi.org/10.1016/j.trechm.2020.02.002.

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32

Bruno, Ameduri. "Controlled Radical (Co)polymerization of Fluoromonomers." Macromolecules 43, no. 24 (2010): 10163–84. http://dx.doi.org/10.1021/ma1019297.

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33

Ameduri, Bruno. "Controlled Radical (Co)polymerization of Fluoromonomers." Macromolecules 44, no. 7 (2011): 2394. http://dx.doi.org/10.1021/ma2003536.

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34

Allen, Michael H., Sean T. Hemp, Adam E. Smith, and Timothy E. Long. "Controlled Radical Polymerization of 4-Vinylimidazole." Macromolecules 45, no. 9 (2012): 3669–76. http://dx.doi.org/10.1021/ma300543h.

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35

Ansong, Omari E., Susan Jansen, Yen Wei, et al. "Accelerated controlled radical polymerization of methacrylates." Polymer International 58, no. 1 (2008): 54–65. http://dx.doi.org/10.1002/pi.2492.

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36

Bohrisch, Jörg, Ulrich Wendler, and Werner Jaeger. "Controlled radical polymerization of 4-vinylpyridine." Macromolecular Rapid Communications 18, no. 11 (1997): 975–82. http://dx.doi.org/10.1002/marc.1997.030181104.

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37

Charmot, D., P. Corpart, H. Adam, S. Z. Zard, T. Biadatti, and G. Bouhadir. "Controlled radical polymerization in dispersed media." Macromolecular Symposia 150, no. 1 (2000): 23–32. http://dx.doi.org/10.1002/1521-3900(200002)150:1<23::aid-masy23>3.0.co;2-e.

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38

Matyjaszewski, Krzysztof. "Environmental aspects of controlled radical polymerization." Macromolecular Symposia 152, no. 1 (2000): 29–42. http://dx.doi.org/10.1002/1521-3900(200003)152:1<29::aid-masy29>3.0.co;2-c.

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39

Tamasi, Matthew, Shashank Kosuri, Jason DiStefano, Robert Chapman, and Adam J. Gormley. "Automation of Controlled/Living Radical Polymerization." Advanced Intelligent Systems 2, no. 2 (2020): 1900126. http://dx.doi.org/10.1002/aisy.201900126.

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40

Schmidt-Naake, Gudrun, Marco Drache, and Carsten Taube. "TEMPO-controlled free radical suspension polymerization." Die Angewandte Makromolekulare Chemie 265, no. 1 (1999): 62–68. http://dx.doi.org/10.1002/(sici)1522-9505(19990301)265:1<62::aid-apmc62>3.0.co;2-p.

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41

Steenbock, M., M. Klapper, and K. Müllen. "“Self-regulation” of controlled radical polymerization." Acta Polymerica 49, no. 7 (1998): 376–78. http://dx.doi.org/10.1002/(sici)1521-4044(199807)49:7<376::aid-apol376>3.0.co;2-e.

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42

Jin, Xin, Hongliang Kang, Ruigang Liu, and Yong Huang. "Controlled radical emulsion polymerization of polystyrene." Colloid and Polymer Science 291, no. 10 (2013): 2481–85. http://dx.doi.org/10.1007/s00396-013-2998-6.

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43

Kavitha, Amalin A., Anusuya Choudhury, and Nikhil K. Singha. "Controlled Radical Polymerization of Furfuryl Methacrylate." Macromolecular Symposia 240, no. 1 (2006): 232–37. http://dx.doi.org/10.1002/masy.200650828.

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44

Özyürek, Zeynep, Hartmut Komber, Stefan Gramm, Dirk Schmaljohann, Axel H. E. Müller, and Brigitte Voit. "Thermoresponsive Glycopolymers via Controlled Radical Polymerization." Macromolecular Chemistry and Physics 208, no. 10 (2007): 1035–49. http://dx.doi.org/10.1002/macp.200600661.

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45

Tasdelen, Mehmet Atilla, Mustafa Uygun, and Yusuf Yagci. "Photoinduced Controlled Radical Polymerization in Methanol." Macromolecular Chemistry and Physics 211, no. 21 (2010): 2271–75. http://dx.doi.org/10.1002/macp.201000445.

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46

Save, Maud, Yohann Guillaneuf, and Robert G. Gilbert. "Controlled Radical Polymerization in Aqueous Dispersed Media." Australian Journal of Chemistry 59, no. 10 (2006): 693. http://dx.doi.org/10.1071/ch06308.

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Controlled radical polymerization (CRP), sometimes also termed ‘living’ radical polymerization, offers the potential to create a wide range of polymer architectures, and its implementation in aqueous dispersed media (e.g. emulsion polymerization, used on a vast scale industrially) opens the way to large-scale manufacture of products based on this technique. Until recently, implementing CRP in aqueous dispersed media was plagued with problems such as loss of ‘living’ character and loss of colloidal stability. This review examines the basic mechanistic processes in free-radical polymerization in

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47

Yaǧci, Yusuf, Ayşegül Başkan Düz, and Ayşen Önen. "Controlled radical polymerization initiated by stable radical terminated polytetrahydrofuran." Polymer 38, no. 11 (1997): 2861–63. http://dx.doi.org/10.1016/s0032-3861(97)85626-1.

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48

Chen, Mao, Honghong Gong, and Yu Gu. "Controlled/Living Radical Polymerization of Semifluorinated (Meth)acrylates." Synlett 29, no. 12 (2018): 1543–51. http://dx.doi.org/10.1055/s-0036-1591974.

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Fluorinated polymers are important materials for applications in many areas. This article summarizes the development of controlled/living radical polymerization (CRP) of semifluorinated (meth)acrylates, and briefly introduces their reaction mechanisms. While the classical CRP such as atom transfer radical polymerization (ATRP), reversible addition-fragmentation chain transfer (RAFT) polymerization and nitroxide-mediated radical polymerization (NMP) have promoted the preparation of semifluorinated polymers with tailor-designed architectures, recent development of photo-CRP has led to unpreceden

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49

Thurecht, Kristofer J., and Steven M. Howdle. "Controlled Dispersion Polymerization in Supercritical Carbon Dioxide." Australian Journal of Chemistry 62, no. 8 (2009): 786. http://dx.doi.org/10.1071/ch09081.

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Recent advances in controlled polymerization have led to increased activity in controlled free radical polymerization in unconventional solvents. This short report focuses on the renewed interest in dispersion polymerization in supercritical CO2 brought about by the application of controlled free radical polymerization techniques. The emergence of novel and industrially-applicable materials is discussed, as well as the dependence of material properties and morphology upon factors such as surfactant type and how it is employed during the polymerization.

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50

Xia, Jianhui, Scott G. Gaynor, and Krzysztof Matyjaszewski. "Controlled/“Living” Radical Polymerization. Atom Transfer Radical Polymerization of Acrylates at Ambient Temperature." Macromolecules 31, no. 17 (1998): 5958–59. http://dx.doi.org/10.1021/ma980725b.

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