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Journal articles on the topic 'N-benzoyl thiourea'

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Published: 5 June 2025

Last updated: 1 August 2025

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1

Abosadiya, Hamza Milad, Bohari M. Yamin, and Nurziana Ngah. "N-Benzoyl-N′-(3-hydroxyphenyl)thiourea." Acta Crystallographica Section E Structure Reports Online 63, no. 5 (2007): o2403—o2404. http://dx.doi.org/10.1107/s1600536807016509.

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2

Usman, Anwar, Ibrahim Abdul Razak, Suhana Satar, Maisara Abdul Kadir, Bohari M. Yamin, and Hoong-Kun Fun. "N-Benzoyl-N′-(2,6-dimethylphenyl)thiourea." Acta Crystallographica Section E Structure Reports Online 58, no. 6 (2002): o656—o658. http://dx.doi.org/10.1107/s1600536802008450.

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3

Yusof, M. Sukeri M., and Bohari M. Yamin. "N-Benzoyl-N'-(2-chlorophenyl)thiourea." Acta Crystallographica Section E Structure Reports Online 60, no. 8 (2004): o1403—o1404. http://dx.doi.org/10.1107/s1600536804017544.

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4

Dong, Wen-Kui, Xiao-Qing Yang, and Jian-Hua Feng. "N-Benzoyl-N′-(3-pyridyl)thiourea." Acta Crystallographica Section E Structure Reports Online 62, no. 8 (2006): o3459—o3460. http://dx.doi.org/10.1107/s1600536806027516.

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5

Zhang, Bin, Bi-Quan Su, and Liang Xian. "N-Benzoyl-N′-(2-methylphenyl)thiourea." Acta Crystallographica Section E Structure Reports Online 62, no. 9 (2006): o4024—o4026. http://dx.doi.org/10.1107/s1600536806032740.

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6

Sun, Chuan-Wen, and Xiao-Dong Zhang. "N-Benzoyl-N′-(tert-butylaminocarbonyl)thiourea." Acta Crystallographica Section E Structure Reports Online 62, no. 7 (2006): o2700—o2701. http://dx.doi.org/10.1107/s1600536806019799.

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The asymmetric unit of the title compound, C13H17N3O2, contains two molecules and neither of them adopts a planar conformation. The crystal structure is stabilized by the intermolecular N—H...O and intramolecular N—H...O and N—H...S hydrogen bonds. The intermolecular hydrogen bonds link the molecules to form infinite chains along the b axis.

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7

Zhang, You-Ming, Liang Xian, Tai-Bao Wei, and Li-Xiang Cai. "N-Benzoyl-N′-(2-hydroxyethyl)thiourea." Acta Crystallographica Section E Structure Reports Online 59, no. 6 (2003): o817—o819. http://dx.doi.org/10.1107/s1600536803010213.

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8

Gaber, Abd El-Aal M., Morsy M. Aly, and Ahmed A. Atalla. "Thermolysis of some thiourea derivatives." Collection of Czechoslovak Chemical Communications 56, no. 10 (1991): 2183–87. http://dx.doi.org/10.1135/cccc19912183.

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Thermolysis of N/benzoyl-N’,N’-diphenylthiourea (BDTU)(I) at 250°C gives NH3, H2S, H2O, benzaldehyde, benzil, benzonitrile, diphenylamine, diphenylcyanamide, 2-phenylbenzimidazole, benzoyl isothiocyanate, carbazole and 2-phenylbenzthiazole, whereas, thermolysis of N-benzoyl-N'-o-tolylthiourea (BTTU) (II) under the same conditions afford NH3, H2S, H2O, benzaldehyde, benzil, benzonitrile, o-toluidine, o-tolyl isothiocyanate, o-tolylcyanamide, benzoyl isothiocyanate and N,N’-di-o-tolylthiourea. The main feature of these thermolyses is homolysis of the amide and thioamide bonds providing free radi

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9

Binzet, Gün, Gülten Kavak, Nevzat Külcü, Süheyla Özbey, Ulrich Flörke, and Hakan Arslan. "Synthesis and Characterization of Novel Thiourea Derivatives and Their Nickel and Copper Complexes." Journal of Chemistry 2013 (2013): 1–9. http://dx.doi.org/10.1155/2013/536562.

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New benzoyl thiourea derivatives and their nickel and copper complexes were synthesized. The structure of the synthesized compounds were confirmed by elemental analysis, FT-IR, and1H NMR techniques. Four of the synthesized compounds are analyzed by X-ray single crystal diffraction technique. WhereasN,N-dimethyl-N′-(4-fluorobenzoyl)thiourea,N,N-diethyl-N′-(4-fluorobenzoyl)thiourea, andN,N-di-n-butyl-N′-(4-fluorobenzoyl) thiourea crystallize in the monoclinic system,bis(N,N-di-n-propyl-N′-(4-fluorobenzoyl)thioureato) nickel(II) complex crystallizes in the triclinic system. These ligand molecules

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10

Li, Ru Lin, Lin Wang, and Gang Xue. "Study on Preparation, Biological Activity and Thermal Decomposition of N-Benzoyl-N＇-(4-Chlorobenzamido) Thiourea." Advanced Materials Research 236-238 (May 2011): 1914–18. http://dx.doi.org/10.4028/www.scientific.net/amr.236-238.1914.

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A novel compound N-benzoyl-N＇-(4-chlorobenzamido) thiourea was prepared from benzoyl isothiocyanate which was obtained from benzoyl chloride and potassium thiocyanate, and 4-chlorobenzoyl hydrazine which was obtained from ethyl 4-chlorobenzoate and hydrazine hydrate. IR,1H NMR,13C NMR and elemental analysis were utilized to determine the structure of the thiourea. The biological tests indicated that the target compound had antibacterial activity against bacillus subtilis and taphylo-coccus aurers. Meanwhile, the thermal stability was investigated by thermogrativity（TG） and differential thermog

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11

Al-Riyahee, Ali A. A. "First Row Transition Metal Complexes Derived from N, Nʹ-Substituted Thiourea: Synthesis, Geometrical Structures and Cyclic Voltammetry Probe: A Review". BASRA JOURNAL OF SCIENCE 39, № 1 (2021): 96–118. http://dx.doi.org/10.29072/basjs.202117.

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Thioureas or thiourea derivatives as organosulfur compounds are one of the most widely used ligands in different applications as we are going to discuss it extensively such as in coordination chemistry by involving them to rich sources of N, O and S atoms coordinating through S atom, S and O atoms in benzoyl derivatives or S, O and N atoms in pyridyl hetrocylic benzoyl derivatives. These hard and soft donor sites facilitate the bonding between thiourea free ligand and metal ion through one or more to make ligands behave as mono, bi or multidentate ligands to form huge and stable series of the

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12

Journal, Baghdad Science. "Synthesis of New Amide and ThioUrease Compounds." Baghdad Science Journal 4, no. 3 (2007): 430–37. http://dx.doi.org/10.21123/bsj.4.3.430-437.

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The reaction of some new Schiff bases ( 2-[(2-Amino – ethylimino)-methyl]-R , 2-({2-[(R-benzylidene)-amino]-ethylimino}-methyl)-R with Benzoyl chloride or Acetyl chloride were carried out. Subsequent reactions of these products N-(2-Amino-ethyl)-N-[Chloro-(R) –methyl]-benzamide or N-(2-{?-[chloro-(R) –methyl]-amino}-ethyl)-N-[chloro-(R) –methyl]- benzamide with thiourea afforded thioureas compounds. The synthesized compounds were confirmed by their IR,UV,spectra and C.H.N. analysis.

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13

Ding, Yu-Jie, Jian Yao, Jian-Chao Wu, Wen-Kui Dong, and Jun-Feng Tong. "N-Benzoyl-N′-(2-chloro-3-pyridyl)thiourea." Acta Crystallographica Section E Structure Reports Online 65, no. 8 (2009): o1903. http://dx.doi.org/10.1107/s1600536809027081.

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14

Binzet, Gun, Bülent Zeybek, Esma Kılıç, Nevzat Külcü, and Hakan Arslan. "Determination of the Ionization Constants of Some Benzoyl Thiourea Derivatives in Dioxane-Water Mixture." Journal of Chemistry 2013 (2013): 1–7. http://dx.doi.org/10.1155/2013/201238.

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The stoichiometric ionization constants ofN,N-dialkyl-N′-(4-substituted benzoyl) thiourea (Substitutes: H, Cl, and Br; alkyl groups: ethyl,n-propyl,n-butyl, and phenyl) derivatives have been determined potentiometrically in dioxane-water (v:v, 50:50) mixture at ionic strength of 0.1 M and25.0±0.1°C. The ionization constants were calculated with the BEST computer program and the formation curves using the data obtained from the potentiometric titrations. The effects of substituents and alkyl groups on the ionization constants of the benzoyl thiourea derivatives have been investigated. A compari

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15

Rauf, M. Khawar, Masahiro Ebihara, Amin Badshah, and Imtiaz-ud-Din. "1-Benzoyl-3-(4-n-butylphenyl)thiourea." Acta Crystallographica Section E Structure Reports Online 68, no. 1 (2011): o120. http://dx.doi.org/10.1107/s1600536811051774.

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16

ROSU, Tudor, VioreL CARCU, Maria NEGOIU, Ovidiu MAIOR, and Niculina BADICU. "SOME NEW N-BENZOYL-N-SUBSTITUTED PHENYL THIOUREA COMPLEXES OF COPPER(II)." SOUTHERN BRAZILIAN JOURNAL OF CHEMISTRY 5, no. 5 (1997): 43–49. http://dx.doi.org/10.48141/sbjchem.v5.n5.1997.45_1997.pdf.

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The new N-benzoyl-N-substituted phenyl thiourea ligands have been used to p1·cpare copper(ll) complexes [Cu(L)2Cl2]. The novel complexes were characterized by ESR, IR, NIR, electronic spectroscopy and conductivity measurements, Tentative geometry of the complexes involves four-coordinate environments (tetrahedral distorted D2d) for the copper ion and a monodentate behavior for ligands. In all these complexes N, N-substituted thiourea is sulphur-bonded to the copper ion.

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17

Milosavljevic, Milutin, Ivan Vukicevic, Veis Serifi, et al. "Optimization of the synthesis of N-alkyl and N,N-dialkyl thioureas from waste water containing ammonium thiocyanate." Chemical Industry and Chemical Engineering Quarterly 21, no. 4 (2015): 501–10. http://dx.doi.org/10.2298/ciceq141221006m.

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The optimized methods for N-alkyl and N,N-dialkyl substituted thioureas synthesis starting from ammonium thiocyanates, waste water constituent from the production of tetramethylthiuram monosulfide (TMTS), and alkyl amine, are presented in this work. Therefore, thioureas synthesis was developed in two ways: Method I - reaction of the thiocyanate and alkylamine in the presence of hydrochloric acid; Method II - reaction of the thiocyanate with benzoyl chloride following by amine addition in the first step, and base hydrolysis in the second step. The structure of the synthesized compounds was conf

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18

Rosiak, Damian, Andrzej Okuniewski, and Jarosław Chojnacki. "Copper(I) iodide ribbons coordinated with thiourea derivatives." Acta Crystallographica Section C Structural Chemistry 74, no. 12 (2018): 1650–55. http://dx.doi.org/10.1107/s2053229618015620.

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Two products of the reactions of CuI with 1-benzoyl-3-(4-bromophenyl)thiourea and with 1-benzoyl-3-(2-iodophenyl)thiourea have been obtained and characterized, namely poly[[[1-benzoyl-3-(4-bromophenyl)thiourea-κS]-μ3-iodido-copper(I)] acetone hemisolvate], {[CuI(C14H11BrN2OS)]·0.5C3H6O} n , and poly[μ4-iodido-μ3-iodido-[N-(benzo[d]thiazol-2-yl)benzamide-κN]dicopper(I)], [Cu2I2(C14H10N2OS)] n . Their structures, determined by single-crystal X-ray diffraction analysis, exhibit different stoichiometries and molecular organizations; however, both compounds are polymeric and possess close Cu...Cu c

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19

Hritzová, Oľga, and Dušan Koščík. "Hydrogen bonds in derivatives of N-substituted N’-benzoyl- and N’-(2-chlorobenzoyl)thiourea." Collection of Czechoslovak Chemical Communications 56, no. 4 (1991): 880–85. http://dx.doi.org/10.1135/cccc19910880.

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Intramolecular hydrogen bonds of the N-H···O=C type have been detected in the derivatives of N-substituted N’-benzoyl- and N’-(2-chlorobenzoyl)thiourea on the basis of IR spectral studies. The title compounds can exist in two tautomeric forms.

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20

Shanmuga Sundara Raj, S., K. Puviarasan, D. Velmurugan, G. Jayanthi, and H. K. Fun. "N—H...S hydrogen bonding inN-benzoyl-N'-methyl-N'-phenylthiourea andN-benzoyl-N'-(3,4-dimethylphenyl)thiourea." Acta Crystallographica Section C Crystal Structure Communications 55, no. 8 (1999): 1318–20. http://dx.doi.org/10.1107/s0108270199005788.

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21

Bhattacharjee, Tirtha, Prasanta Gogoi, Vedavati G. Puranik, Rupesh L. Gawade, and Pranjit Barman. "1-Benzoyl-3-[(2-benzylsulfanyl)phenyl]thiourea." Acta Crystallographica Section C Crystal Structure Communications 68, no. 12 (2012): o485—o487. http://dx.doi.org/10.1107/s0108270112045167.

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In the title compound, C21H18N2OS2, a strong intramolecular N—H...O hydrogen bond [N...O = 2.642 (3) Å] between the amide N atom and the benzoyl O atom forms an almost planar six-membered ring in the central part of the molecule. In the crystal, molecules are packed through weak N—H...S interactions. Intra- and intermolecular hydrogen bonds and van der Waals interactions are the stabilizing forces for the crystal structure.

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22

Khawar Rauf, M., Amin Badshah, and Michael Bolte. "1-(2,3-Dimethylphenyl)-3-(2-methylbenzoyl)thiourea." Acta Crystallographica Section E Structure Reports Online 63, no. 3 (2007): o1256—o1257. http://dx.doi.org/10.1107/s1600536807005582.

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The benzoyl and dimethylphenyl groups in the title compound, C17H18N2OS, are cis and trans, respectively, with respect to the C=S bond. The crystal packing is characterized by N—H...O and N—H...S hydrogen bonds.

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23

Kaminsky, Werner, Karen I. Goldberg, and Douglas X. West. "Synthesis and structures of two N,N′-bis(2-pyridinyl)thioureas and N-(2-pyridinyl)-N′-(benzoyl)thiourea." Journal of Molecular Structure 605, no. 1 (2002): 9–15. http://dx.doi.org/10.1016/s0022-2860(01)00655-x.

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24

Jin, Zong-ming, Weiqun Zhou, and Zheng Jin. "X-ray powder diffraction analysis of a nonlinear optical material 1-benzoyl-3-(4-benzyl)thiourea [N-benzoyl-N′-(4-benzyl)thiourea]." Powder Diffraction 13, no. 1 (1998): 41–43. http://dx.doi.org/10.1017/s088571560000974x.

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A nonlinear optical material, 1-benzoyl-3-(4-benzyl)thiourea (C15H14N2OS), has been characterized by X-ray powder diffraction. Experimental values of 2θ corrected for systematic errors, relative peak intensities, values of d, and the Miller indices of 82 observed reflections with 2θ up to 80° are reported. The powder diffraction data have been evaluated, and the figures-of-merit are reported. The least-squares refined unit cell parameters are a=22.0243(6)Å, b=10.9795(7)Å, c=13.0322(8)Å, β=116.88(2)°, V=2810.8(9)Å3, Z=8, Dx=1.278 g/cm3, space group Pn.

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25

Cao, Cheng, Tai Xiao, Tai-Bao Wei, and You-Ming Zhang. "N-Benzoyl-N′-(2-{2-[2-(N-benzoylthioureido)phenoxy]ethoxy}phenyl)thiourea." Acta Crystallographica Section E Structure Reports Online 63, no. 5 (2007): o2699—o2701. http://dx.doi.org/10.1107/s1600536807018661.

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26

Li, Zhonghua, Yan Zhang, and Yangang Wang. "Synthesis and Characterization of N-benzoyl-N′-carboxyalkyl Substituted Thiourea Derivatives." Phosphorus, Sulfur, and Silicon and the Related Elements 178, no. 2 (2003): 293–97. http://dx.doi.org/10.1080/10426500307952.

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27

Mat Rashid, Fatisha Liyana, Lee Yook Heng, Jean-Claude Daran, and Mohammad B. Kassim. "N-Benzoyl-N′-(1,10-phenanthrolin-5-yl)thiourea dichloromethane hemisolvate monohydrate." Acta Crystallographica Section E Structure Reports Online 67, no. 6 (2011): o1397—o1398. http://dx.doi.org/10.1107/s160053681101734x.

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28

Jirman, Josef, and Antonín Lyčka. "15N, 13C, and 1H NMR spectra of acylated ureas and thioureas." Collection of Czechoslovak Chemical Communications 52, no. 10 (1987): 2474–81. http://dx.doi.org/10.1135/cccc19872474.

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A series of 1-acylated and 1,3-diacylated (acyl = acetyl or benzoyl) ureas and thioureas have been prepared and their proton-coupled and proton-decoupled 15N, 13C, and 1H NMR spectra have been measured. All the signals have been assigned. The 15N NMR chemical shifts in 1-acylated ureas and thioureas are shifted downfield as compared with δ(15N) of urea and thiourea, resp. This shift is greater for N-1 than for N-3 nitrogen atoms in both the series. When comparing acylureas and acylthioureas it is obvious from the Δδ(15N) differences that the CS group is better than CO group in transferring the

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29

Yusof, M. Sukeri M., S. Kamilah C. Soh, Nurziana Ngah, and Bohari M. Yamin. "1-Benzoyl-3-(6-methylpyridin-2-yl)thiourea." Acta Crystallographica Section E Structure Reports Online 62, no. 4 (2006): o1446—o1448. http://dx.doi.org/10.1107/s1600536806009366.

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The molecular structure of the title compound, C14H13N3OS, adopts a cis–trans configuration with respect to the positions of the benzoyl and 6-methylpyridin-2yl groups relative to the S atom across the thiourea C—N bonds. In the crystal structure, the molecules are linked by N—H...S, C—H...S and C—H...O interactions, forming a one-dimensional chain parallel to the b axis.

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30

Merdivan, M., R. S. Aygün, and N. Külcü. "Thermal behaviour of some metal complexes of N,N-diethyl-N′-benzoyl thiourea." Journal of Thermal Analysis 48, no. 6 (1997): 1423–29. http://dx.doi.org/10.1007/bf01983453.

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31

Okuniewski, Andrzej, Damian Rosiak, Jarosław Chojnacki, and Barbara Becker. "Crystallographic study of self-organization in the solid state including quasi-aromatic pseudo-ring stacking interactions in 1-benzoyl-3-(3,4-dimethoxyphenyl)thiourea and 1-benzoyl-3-(2-hydroxypropyl)thiourea." Acta Crystallographica Section C Structural Chemistry 73, no. 1 (2017): 52–56. http://dx.doi.org/10.1107/s2053229616019495.

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1-Benzoylthioureas contain both carbonyl and thiocarbonyl functional groups and are of interest for their biological activity, metal coordination ability and involvement in hydrogen-bond formation. Two novel 1-benzoylthiourea derivatives, namely 1-benzoyl-3-(3,4-dimethoxyphenyl)thiourea, C16H16N2O3S, (I), and 1-benzoyl-3-(2-hydroxypropyl)thiourea, C11H14N2O2S, (II), have been synthesized and characterized. Compound (I) crystallizes in the space group P\overline{1}, while (II) crystallizes in the space group P21/c. In both structures, intramolecular N—H...O hydrogen bonding is present. The resu

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32

Glotova, T. E., M. Yu Dvorko, A. I. Albanov, and N. I. Protsuk. "Reaction of N-(carbamimidoyl)thiourea with 1-benzoyl-2-phenylacetylene." Russian Journal of Organic Chemistry 43, no. 1 (2007): 121–25. http://dx.doi.org/10.1134/s1070428007010162.

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33

Mopari, Anuja M., and Gajanan V. Korpe. "Synthesis and Structural Studies of N-Maltosylated Aryl Thiobiurets." Asian Journal of Chemistry 34, no. 5 (2022): 1220–24. http://dx.doi.org/10.14233/ajchem.2022.23649.

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The derivatives of urea, thiourea and thiosemicarbazide play an important role in medicinal chemistry by influencing various pharmacological activities. The design and development of novel N-maltosides have emerged as an important class of organic compounds. A series of 1-hepta-O-benzoyl-β-D-Maltosyl- 5-aryl-2-4-thiobiurets are described in present work. By mixing hepta-O-benzoyl→D-maltosyl isocyanates with various aryl thiocarbamides, 1-hepta-O-benzoyl-β-D-maltosyl-5-aryl-2-4-thiobiurets have been synthesized. The identities of this newly synthesized 1-hepta-O-benzoyl-β-D-Maltosyl-5- aryl-2-4

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34

Li, Gang, Meng-Meng Zhao, Li Wang, Yu-Hua Yang, Yu-Jie Zhang, and Xiu-Yan Dong. "Synthesis and Crystal Structure of N-(p-Nitro)benzoyl-N'-(3-pyridyl)thiourea." Asian Journal of Chemistry 25, no. 8 (2013): 4334–36. http://dx.doi.org/10.14233/ajchem.2013.13968.

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35

Weiqun, Zhou, Li Baolong, Zhu liming, et al. "Structural and spectral studies on N-(4-chloro)benzoyl-N′-(4-tolyl)thiourea." Journal of Molecular Structure 690, no. 1-3 (2004): 145–50. http://dx.doi.org/10.1016/j.molstruc.2003.11.029.

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36

Marzi, M., K. Pourshamsian, F. Hatamjafari, A. Shiroudi, and A. R. Oliaey. "Synthesis of New N-Benzoyl-N'-Triazine Thiourea Derivatives and Their Antibacterial Activity." Russian Journal of Bioorganic Chemistry 45, no. 5 (2019): 391–97. http://dx.doi.org/10.1134/s106816201905008x.

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37

Balgar, Singh, Mahajan Simpy, N. Sheikh Haq, and L. Kalsotra Bansi. "Peroxo complexes of uranium(VI) with N-benzoyl urea and related ligands Synthesis, characterization and antifungal activity." Journal of Indian Chemical Society Vol. 89, Sep 2012 (2012): 1265–71. https://doi.org/10.5281/zenodo.5769659.

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Department of Chemistry, University of Jammu, Jammu-180 006, Jammu and Kashmir, India <em>E-mail </em>: hnsheikh@rediffmail.com <em>Manuscript received 19 July 2011, revised 13 December 2011, accepted 21 December 2011</em> The peroxouranium(VI) complexes containing N-benzoyl urea and related ligands having composition [UO(O<sub>2</sub>)L-L(NO<sub>3</sub>)<sub>2</sub>].H<sub>2</sub>O {where L-L =<em>N</em>-benzoyl urea (NBU), <em>N</em>-benzoyl thiourea (NBT), <em>N</em>-benzoyl hydrazine (NBH<sub>2</sub>> and <em>N</em>-bcnzoyl hydroxylamine (NBH<sub>A</sub>)} are reported. The synthesized

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38

Kim, Namhun, Haneol Kim, and Sung Kwon Kang. "A monoclinic polymorph of 1-benzoyl-4-thiobiuret." Acta Crystallographica Section E Structure Reports Online 69, no. 12 (2013): o1760. http://dx.doi.org/10.1107/s1600536813030250.

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The title compound, C9H9N3O2S, is a monoclinic (C2/c) polymorph of the previously reported triclinic structure [Kang (2013).Acta Cryst.E69, o1327]. The molecule is almost planar with an r.m.s. deviation of 0.069 Å from the mean plane of all non-H atoms. The benzoyl and terminal thiourea fragments adopt atransoidconformation with respect to the central carbonyl O atom. Two intramolecular N—H...O hydrogen bonds are present. In the crystal, N—H...O and N—H...S interactions link the molecules into zigzag chains extending along thec-axis direction.

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39

Arslan, Hakan, Nevzat Külcü, and Ulrich Flörke. "Normal coordinate analysis and crystal structure of N,N-dimethyl-N′-(2-chloro-benzoyl)thiourea." Spectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy 64, no. 4 (2006): 1065–71. http://dx.doi.org/10.1016/j.saa.2005.09.016.

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40

Li, Qianjin, Dan Wang, Min Chen, et al. "Dual Roles of N,N-Dimethylformamide in Benzothiazoles Synthesis from N-Benzoyl-N′-(2,4,6-trichlorophenyl)thiourea." Journal of Chemical Crystallography 50, no. 4 (2019): 287–94. http://dx.doi.org/10.1007/s10870-019-00796-3.

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41

Ameram, Nadiah, and Farook Adam. "Crystal structure of 2-methyl-N-{[2-(pyridin-2-yl)ethyl]carbamothioyl}benzamide." Acta Crystallographica Section E Crystallographic Communications 71, no. 9 (2015): o636. http://dx.doi.org/10.1107/s2056989015013559.

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In the title compound, C16H17N3OS, a benzoyl thiourea derivative, the planes of the pyridine and benzene rings are inclined to one another by 66.54 (9)°. There is an intramolecular N—H...O hydrogen bond present forming anS(6) ring motif. In the crystal, molecules are linkedviapairs of N—H...N hydrogen bonds, forming inversion dimers, which are reinforced by pairs of C—H...S hydrogen bonds. The dimers are linkedviaC—H...π interactions, forming ribbons along [010].

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42

Aydin, Fatma, and N. Burcu Arslan. "Synthesis, Crystal Structure and Cyclic Voltammetric Behavior of N-aroyl-N′-(4′-cyanophenyl)thioureas." Molbank 2022, no. 1 (2022): M1316. http://dx.doi.org/10.3390/m1316.

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Herein, two title compounds, N-benzoyl-N′-(4′-cyanophenyl)thiourea (1) and N-(4-nitrobenzoyl)-N′-(4′-cyanophenyl)thiourea (2) were synthesized in a high yield, via different applications of aroyl isocyanate and 4-aminobenzonitrile. The structure of the prepared compounds was characterized by elemental analysis and FT-IR, 1H, and 13C-NMR spectroscopic methods. The crystal structure of the title compound 1 was determined by an X-ray single-crystal technique and an intramolecular C=O…H-N hydrogen bond and intermolecular C=S…H-N and C=S…H-C hydrogen interactions, which were observed for the crysta

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43

Peng, Hao, and Hong-Wu He. "N-{3-[2-Chloro-4-(trifluoromethyl)phenoxy]benzoyl}-N′-(4,6-dimethylpyrimidin-2-yl)thiourea." Acta Crystallographica Section E Structure Reports Online 62, no. 12 (2006): o5371—o5372. http://dx.doi.org/10.1107/s1600536806045429.

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44

Glotova, T. E., M. Yu Dvorko, A. I. Albanov, and O. V. Gubaidullina. "N-(4,6-Diphenylpyrimidin-2-yl)thiourea from 1-Benzoyl-2-phenylacetylene and N-Carbamimidoylthiourea." Russian Journal of Organic Chemistry 41, no. 9 (2005): 1404–5. http://dx.doi.org/10.1007/s11178-005-0358-9.

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45

Samb, Issa, Nango Gaye, Rokhaya Sylla-Gueye, Elhadj Ibrahima Thiam, Mohamed Gaye, and Pascal Retailleau. "Crystal structure ofN,N′-[(ethane-1,2-diyl)bis(azanediylcarbonothioyl)]bis(benzamide)." Acta Crystallographica Section E Crystallographic Communications 75, no. 5 (2019): 642–45. http://dx.doi.org/10.1107/s205698901900495x.

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The reaction of benzoyl chloride and ethylendiamine in the presence of potassium thiocyanate yielded a white solid, C18H18N4O2S2, which consists of two benzoylthioureido moieties connected by an ethylene chain. The asymmetric unit consists of one half of the molecule, the complete molecule being generated by crystallographic inversion symmetry. Both thiourea moieties are in atransconformation. An intramolecular N—H...O hydrogen bond occurs. In the crystal, C—H...S and C—H...O hydrogen bonds link the molecules, forming layers parallel to theacplane.

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46

Staicu, Teodora, Monica Iliş, Viorel Cîrcu, and Marin Micutz. "Influence of hydrocarbon moieties of partially fluorinated N -benzoyl thiourea compounds on their gelation properties. A detailed rheological study of complex viscoelastic behavior of decanol/ N -benzoyl thiourea mixtures." Journal of Molecular Liquids 255 (April 2018): 297–312. http://dx.doi.org/10.1016/j.molliq.2018.01.162.

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47

Nawar, Nagwa, Essam Ell-Sawaah, Nasser M. Hosny, and Mohsen M. Mostafa. "Synthesis and Spectral Characterization of Some Complexes Derived From N-Benzoyl-N′-Carboxylmethylthiopropylidine Thiourea (Bcmt)." Phosphorus, Sulfur, and Silicon and the Related Elements 187, no. 8 (2012): 976–89. http://dx.doi.org/10.1080/10426507.2012.658980.

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48

Zhou, Weiqun, Chao Xie, Zheng Jin, and Zong-ming Jin. "X-ray powder diffraction analysis of a nonlinear optical material N-(p-methoxy benzoyl)-N′-(p-methyl phenyl) thiourea." Powder Diffraction 17, no. 3 (2002): 238–40. http://dx.doi.org/10.1154/1.1348003.

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A nonlinear optical material, N-(p-methoxy benzoyl)-N′-(p-methyl phenyl) thiourea (C16H16N2O2S), has been characterized by X-ray powder diffraction. Experimental values of 2θ corrected for systematic errors, relative peak intensities, values of d, and the Miller indices of 94 observed reflections with 2θ up to 66° are reported. The powder diffraction data and the figure-of-merit are reported. The least-squares refined unit cell parameters are a=25.3291(3) Å, b=11.9478(1) Å, c=10.1407(4) Å, β=103.10(2)°, V=2988.97(6) Å3, Z=8, Dx=1.335(0) g/cm3, with space group P21(4).

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49

Zhou, Weiqun, Zhenjiang Zhang, Zheng Jin, and Zong-ming Jin. "X-ray powder diffraction analysis of a nonlinear optical material N-(p-methoxy benzoyl)-N′-(o-methyl phenyl) thiourea." Powder Diffraction 17, no. 3 (2002): 241–43. http://dx.doi.org/10.1154/1.1468228.

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A nonlinear optical material, N-(p-methoxy benzoyl)-N′(o-methyl phenyl) thiourea (C16H16N2O2S), has been characterized by X-ray powder diffraction. Experimental values of 2θ corrected for systematic errors, relative peak intensities, values of d, and the Miller indices of 90 observed reflections with 2θ up to 88° are reported. The powder diffraction data have been evaluated, and the figures-of-merit are reported. The least-squares refined unit cell parameters are a=26.7079(3) Å, b=6.7995(9) Å, c=19.2845(1) Å, β=121.39(4), V=2989.42(3) Å3, Z=8, Dx=1.334(8) g/cm3, space group P2(3).

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50

Mohamadou, Aminou, Isabelle Déchamps-Olivier, and Jean-Pierre Barbier. "Synthesis of N-morpholine or N,N-diethyl, N′-monosubstituted benzoyl thiourea copper complexes: characterization and electrochemical investigations." Polyhedron 13, no. 24 (1994): 3277–83. http://dx.doi.org/10.1016/s0277-5387(00)83108-3.

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