Relevant bibliographies by topics / Organic synthesis optimization

Contents

  1. Journal articles
  2. Dissertations / Theses
  3. Books
  4. Book chapters
  5. Conference papers
  6. Reports

Academic literature on the topic 'Organic synthesis optimization'

Author: Grafiati
Published: 4 June 2025
Last updated: 1 August 2025

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Journal articles on the topic "Organic synthesis optimization"

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Snieckus, Victor. "Optimization in organic synthesis." Medicinal Research Reviews 19, no. 5 (1999): 342–47. http://dx.doi.org/10.1002/(sici)1098-1128(199909)19:5<342::aid-med2>3.0.co;2-e.

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Emptage, Michael R., and Rolf Carlson. "Design and Optimization in Organic Synthesis." Technometrics 39, no. 2 (1997): 231. http://dx.doi.org/10.2307/1270918.

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Fajdek-Bieda, Anna, and Andrzej Perec. "Optimization of the organic compounds synthesis." Procedia Computer Science 207 (2022): 819–28. http://dx.doi.org/10.1016/j.procs.2022.09.137.

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Snieckus, Victor. "ChemInform Abstract: Optimization in Organic Synthesis." ChemInform 32, no. 44 (2010): no. http://dx.doi.org/10.1002/chin.200144282.

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Meyer, Elazar. "Optimization of MOF Synthesis." Technium: Romanian Journal of Applied Sciences and Technology 4, no. 10 (2022): 53–61. http://dx.doi.org/10.47577/technium.v4i10.7730.

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Synthesis optimization of the metal organic framework (MOF) UiO-66 has been carried out using 2-aminoterephthalic acid functional group, a zirconium salt and a modulator grafted into the UiO-66 framework. Reaction parameters such as the effects of temperature, reaction time, the nature of the zirconium salt and the ligand, the molar ratio between the zirconium salt and the ligand, the quantity of the modulator, the solvent and the effect of added water have been investigated. The synthesized MOFs have demonstrated excellent chemical and thermal stability, which ensured them to be used as carri
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Bubyrev, A. I., A. S. Tsarkova, and Z. M. Kaskova. "Optimization of Fungal Luciferin Synthesis." Russian Journal of Bioorganic Chemistry 45, no. 2 (2019): 183–85. http://dx.doi.org/10.1134/s106816201902002x.

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Elguero, José. "Design and optimization in organic synthesis, by Rolf Carlson." Chemometrics and Intelligent Laboratory Systems 19, no. 2 (1993): 271. http://dx.doi.org/10.1016/0169-7439(93)80113-v.

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Jaiswar, Rahul. "Base Catalysed One Pot Multicomponent Synthesis of Novel 6-(3-Nitrophenyl)-7, 9- Dihydro-1H-Purine-2, 8 (3H,6H)-Dithione via a Three-Component Biginelli Type Condensation Derivatives under Microwave Irradiation." Der Pharma Chemica 14, no. 10 (2022): 4. https://doi.org/10.4172/0975-413X.14.10.43-46.

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An efficient one-pot synthesis of novel 6-(3-nitrophenyl)-7, 9-dihydro-1H-purine-2,8 (3H,6H)-dithione via a three-component biginelli type condensation of 2-thiohydantoin, aldehyde and urea/thiourea in the presence of fused Sodium acetate and acetic acid as a solvent using microwave irradiation was carried out. The use of microwave irradiation in organic synthesis has become increasingly popular within the pharmaceutical and academic arenas, because it is new enabling technology for drug discovery and development. By taking advantage of his efficient source of energy compound libraries for lea
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Schwarz, A., D. Steinke, MR Kula, and C. Wandrey. "Optimization of enzyme‐mediated peptide bond formation." Biotechnology and Applied Biochemistry 12, no. 2 (1990): 188–95. http://dx.doi.org/10.1111/j.1470-8744.1990.tb00091.x.

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Enzyme‐catalyzed peptide bond formation requires thorough examination and optimization of each coupling step. In order to identify factors influencing the selectivity between aminolysis and hydrolysis, a systematic study was carried out for the kinetically controlled peptide synthesis. The reaction temperature, the type of C‐terminal protecting group, and different organic cosolvents showed little influence on the selectivity. The enzyme, excess nucleophile, pH, N‐terminal protecting group, and ionic strength of the solution were identified as major factors controlling the selectivity and, the
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Somani, R. R., G. J. Sanap, and P. K. Chaskar. "USE OF FACTORIAL DESIGN IN OPTIMIZATION OF MICROWAVE ASSISTED ORGANIC SYNTHESIS OF SOME AZOLES." INDIAN DRUGS 55, no. 10 (2018): 24–33. http://dx.doi.org/10.53879/id.55.10.11401.

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In the era of environment friendly chemistry, Microwave Assisted Organic Synthesis (MAOS) has proved to be an effective tool to achieve maximum yield in minimum time without compromising on quality. The present work focuses on synthesis of some bioactive heterocyclic azoles using MAOS. However, the synthetic reactions are optimized using a known technique of factorial designing. Here, 32 factorial design approach is used to achieve the set targets of yields and purity. The outcome has been very promising and opens up new avenues for organic chemists who face challenges in optimizing organic re
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Dissertations / Theses on the topic "Organic synthesis optimization"

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Murphy, Edward R. "Microchemical systems for rapid optimization of organic synthesis." Thesis, Massachusetts Institute of Technology, 2006. http://hdl.handle.net/1721.1/36912.

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Thesis (Ph. D.)--Massachusetts Institute of Technology, Dept. of Chemical Engineering, 2006.<br>This electronic version was submitted by the student author. The certified thesis is available in the Institute Archives and Special Collections.<br>Includes bibliographical references (leaves 111-119).<br>In the chemistry laboratory, the desire to use smaller quantities of material to minimize both reagent cost and waste generation has driven chemists to develop new experimental techniques. The current approach to small scale experimentation has mostly been a simple reduction in the size of batch
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Gholamipour-Shirazi, Azarmidokht. "Organic reactivity : kinetics studies and synthesis optimization, using microfluidic devices." Thesis, Lille 1, 2011. http://www.theses.fr/2011LIL10160/document.

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Les microsystèmes sont des réacteurs extraordinaires pour mettre en œuvre des réactions chimiques car ils apportent un rapport de contact entre phases très supérieur à celui en ballon, la possibilité d’hypertrempe thermique tant au chauffage qu’au refroidissement et enfin l’absence d’interaction des réactifs avec les produits. Les dimensions micro-ou nanométriques de ces réacteurs sont très largement compensées par la possibilité de parallélisation à grande échelle de ces réacteurs qui permet une montée en échelle de la production sans nouveau développement. Nous avons choisi comme réaction te
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Trivedi-Parmar, Vinay. "Synthesis and Optimization of Non-Phenolic Inhibitors of Macrophage Migration Inhibitory Factor." Thesis, Yale University, 2019. http://pqdtopen.proquest.com/#viewpdf?dispub=13851921.

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<p> Macrophage migration inhibitory factor (MIF) is a pleiotropic cytokine and an upstream regulator of inflammation and cell proliferation. Interestingly, MIF is also an enzyme that functions as a keto-enol tautomerase, though this function is believed to be vestigial in humans. Implicated in the pathogenesis of multiple infectious and autoimmune diseases, including rheumatoid arthritis and cancer, MIF has emerged as an attractive drug target, with the tautomerase active site serving as a convenient binding pocket for small molecule inhibitors. Most MIF inhibitors include a phenol ring, which
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Bonaretti, Edoardo <1986&gt. "Optimization of purification procedures in organic semiconductor synthesis for improving the performances of organic field-effect transistors." Doctoral thesis, Alma Mater Studiorum - Università di Bologna, 2015. http://amsdottorato.unibo.it/6841/1/Bonaretti_Edoardo_tesi.pdf.

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The aim of the research activity focused on the investigation of the correlation between the degree of purity in terms of chemical dopants in organic small molecule semiconductors and their electrical and optoelectronic performances once introduced as active material in devices. The first step of the work was addressed to the study of the electrical performances variation of two commercial organic semiconductors after being processed by means of thermal sublimation process. In particular, the p-type 2,2′′′-Dihexyl-2,2′:5′,2′′:5′′,2′′′-quaterthiophene (DH4T) semiconductor and the n-type 2,2′′
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Bonaretti, Edoardo <1986&gt. "Optimization of purification procedures in organic semiconductor synthesis for improving the performances of organic field-effect transistors." Doctoral thesis, Alma Mater Studiorum - Università di Bologna, 2015. http://amsdottorato.unibo.it/6841/.

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The aim of the research activity focused on the investigation of the correlation between the degree of purity in terms of chemical dopants in organic small molecule semiconductors and their electrical and optoelectronic performances once introduced as active material in devices. The first step of the work was addressed to the study of the electrical performances variation of two commercial organic semiconductors after being processed by means of thermal sublimation process. In particular, the p-type 2,2′′′-Dihexyl-2,2′:5′,2′′:5′′,2′′′-quaterthiophene (DH4T) semiconductor and the n-type 2,2′′
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Woodard, John Lewis IV. "SYNTHESIS AND STRUCTURAL OPTIMIZATION OF THE NATURAL PRODUCTS SILVESTROL AND PHYLLANTHUSMIN C." The Ohio State University, 2015. http://rave.ohiolink.edu/etdc/view?acc_num=osu1424384284.

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Huntsman, Andrew C. "Development of Phyllanthusmin Derivatives as Anticancer Agents: Pharmacological Optimization and Mechanistic Insight." The Ohio State University, 2019. http://rave.ohiolink.edu/etdc/view?acc_num=osu156338449662965.

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Kulkarni, Sameer Shamrao. "Development and Optimization of Kinetic Target-Guided Synthesis Approaches Targeting Protein-Protein Interactions of the Bcl-2 Family." Scholar Commons, 2012. http://scholarcommons.usf.edu/etd/4351.

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Kinetic target-guided synthesis (TGS) and in situ click chemistry are among unconventional discovery strategies having the potential to streamline the development of protein-protein interaction modulators (PPIMs). In kinetic TGS and in situ click chemistry, the target is directly involved in the assembly of its own potent, bidentate ligand from a pool of reactive fragments. Herein, we report the use and validation of kinetic TGS based on the sulfo-click reaction between thio acids and sulfonyl azides as a screening and synthesis platform for the identification of high-quality PPIMs. Starting f
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Hansson, Lars. "Optimering i organisk syntes : betingelser, system, syntesvägar." Doctoral thesis, Umeå universitet, Kemiska institutionen, 1990. http://urn.kb.se/resolve?urn=urn:nbn:se:umu:diva-131575.

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This thesis deals with different optimization problems encountered in organic synthesis. The use of response surface, sequential simplex and PLS techniques, for simultanious optimization of yield and suppression of side reactions is investigated. This is illustrated by an example of enamine synthesis, were a side reaction was a serious problem. The problem of efficient screening to find suitable catalysts and solvents in new reactions is also investigated. Here, the use of principal properties as selection criterion, is demonstrated with a new process for the silylation of a,ß-unsaturated keto
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Scaduto, Ryan. "A Natural Product and High-Throughput Screening Synthetic Approach Towards the Discovery of Antileishmanial Agents." Ohio Dominican University Honors Theses / OhioLINK, 2021. http://rave.ohiolink.edu/etdc/view?acc_num=oduhonors1620081955401195.

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Books on the topic "Organic synthesis optimization"

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Carlson, Rolf. Design and optimization in organic synthesis. Elsevier, 1992.

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Carlson, Rolf. Design and optimization in organic synthesis. Elsevier, 1992.

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1973-, Carlson Johan E., ed. Design and optimization in organic synthesis. 2nd ed. Elsevier, 2005.

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Carlson, R. Design and Optimization in Organic Synthesis. Elsevier Science & Technology Books, 1991.

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Design and Optimization in Organic Synthesis. Elsevier, 1992. http://dx.doi.org/10.1016/s0922-3487(08)x7011-x.

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Carlson, Johan E., and Rolf Carlson. Design and Optimization in Organic Synthesis, Volume 24: Second Revised and Enlarged Edition (Data Handling in Science and Technology). Elsevier Science, 2005.

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Andraos, John. Algebra of Organic Synthesis: Green Metrics, Design Strategy, Route Selection, and Optimization. Taylor & Francis Group, 2016.

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Andraos, John. Algebra of Organic Synthesis: Green Metrics, Design Strategy, Route Selection, and Optimization. Taylor & Francis Group, 2016.

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Andraos, John. Algebra of Organic Synthesis: Green Metrics, Design Strategy, Route Selection, and Optimization. Taylor & Francis Group, 2013.

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Carlson, Johan E., and Rolf Carlson. Design and Optimization in Organic Synthesis: Second Revised and Enlarged Edition. Elsevier Science & Technology Books, 2005.

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Book chapters on the topic "Organic synthesis optimization"

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Yan, Bing. "Vibrational Spectroscopy for Optimization of Solid-Phase Organic Syntheses." In Solid-Phase Organic Synthesis. John Wiley & Sons, Inc., 2002. http://dx.doi.org/10.1002/0471228249.ch7.

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Mason, Timothy J., and Eric Cordemans de Meulenaer. "Practical Considerations for Process Optimization." In Synthetic Organic Sonochemistry. Springer US, 1998. http://dx.doi.org/10.1007/978-1-4899-1910-6_8.

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"Optimization." In The Algebra of Organic Synthesis. CRC Press, 2011. http://dx.doi.org/10.1201/b11442-7.

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"Protein Sources and Optimization of Biocatalyst Performance." In Hydrolases in Organic Synthesis. Wiley-VCH Verlag GmbH & Co. KGaA, 2006. http://dx.doi.org/10.1002/3527607544.ch4.

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Taber, Douglass F. "Alkaloid Synthesis: (−)-α-Kainic Acid (Ohshima), Serpentine (Scheidt), (−)-Galanthamine ( Jia), (+)-Trigolutes B (Gong), Sarain A (Yokoshima/Fukuyama), DZ-2384 (Harran)." In Organic Synthesis. Oxford University Press, 2017. http://dx.doi.org/10.1093/oso/9780190646165.003.0060.

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(−)-α-Kainic acid 3 is widely used in neuropharmacological studies. En route to 3, Takashi Ohshima of Kyushu University found (Chem. Eur. J. 2015, 21, 3937) that the intramolecular ene cyclization of 1 delivered 2 with high diastereocontrol. Karl A. Scheidt of Northwestern University set (Angew. Chem. Int. Ed. 2015, 54, 6900) the absolute configuration of 5 and so of serpentine 6 by the organocatalyzed cyclization of 4. This is the first total synthesis of that alkaloid. Yanxing Jia of Peking University prepared (Angew. Chem. Int. Ed. 2015, 54, 6255) the benzofuran 8 by the Pd-mediated cycliza
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Taber, Douglass F. "The Smith Synthesis of (−)-Nodulisporic Acid D." In Organic Synthesis. Oxford University Press, 2017. http://dx.doi.org/10.1093/oso/9780190646165.003.0103.

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The nodulisporic acids, isolated from the endophytic fungus Nodulisporium sp., show promising insecticidal activity. Amos B. Smith III of the University of Pennsylvania envisioned (J. Am. Chem. Soc. 2015, 137, 7095) the construction of the central indole of nodulisporic acid D 4 by the convergent coupling of the chloroaniline 1 with the enol triflate 2. The preparation of 2 began (Org. Process Res. Dev. 2007, 11, 19) with the mono­ketal 5 of the Wieland–Miescher ketone, available in enantiomerically-pure form by organocatalyzed Robinson annulation. Condensation with thiophenol and formal­dehyd
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Taber, Douglass F. "The Thomson Synthesis of (–)-GB17." In Organic Synthesis. Oxford University Press, 2015. http://dx.doi.org/10.1093/oso/9780190200794.003.0096.

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(–)-GB17 3 is one of the Galbulimima alkaloids, a family that shows a wide range of interesting physiological activity. Regan J. Thomson of Northwestern University devised (Angew. Chem. Int. Ed. 2012, 51, 2481) a convergent assembly of 3, a key step of which was the intramolecular Michael cyclization of 1 to 2. The hydroxy aldehyde 6 was prepared by alkylation of the dithiane 4 with 5, followed by hydrolysis. The preparation of 9, by condensation of 8 with 7 followed by hydrogenation and protection, had been reported by Lhommet. Condensation of 9 with the linchpin reagent 10 gave an intermedia
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"Creation and Optimization of Artificial Enzymes for Abiological Reactions." In Biocatalysis in Organic Synthesis, edited by Faber, Fessner, and Turner. Georg Thieme Verlag, 2015. http://dx.doi.org/10.1055/sos-sd-216-00397.

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Taber, Douglass F. "The Nakada Synthesis of (+)-Ophiobolin A." In Organic Synthesis. Oxford University Press, 2017. http://dx.doi.org/10.1093/oso/9780190646165.003.0084.

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Ophiobolin A 3 shows nanomolar toxicity toward a range of cancer cell lines. A central feature of this sesterterpene, isolated from the rice fungus Ophiobolus miyabeanus, is the highly-substituted eight-membered ring. A key step in the synthesis of 3 described (Chem. Eur. J. 2013, 19, 5476; Angew. Chem. Int. Ed. 2011, 50, 9452) by Masahisa Nakada of Waseda University was the acid-mediated cyclization of 1 to 2. The preparation of 1 began with the enantioselective hydrolysis of 4 to the mono­ester 5. Selective reduction followed by protection gave 6, that was carried on via 7 to 8. The ethoxyet
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Taber, Douglass F. "C–O Ring Construction: The Georg Synthesis of Oximidine II." In Organic Synthesis. Oxford University Press, 2015. http://dx.doi.org/10.1093/oso/9780190200794.003.0047.

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Chun-Bao Miao and Hai-Tao Yang of Changzhou University constructed (J. Org. Chem. 2011, 76, 9809) the oxetane 2 by exposing the Michael adduct 1 to I2 and air. Huanfeng Jiang of the South China University of Science and Technology carboxylated (Org. Lett. 2011, 13, 5520) the alkyne 3 in the presence of a nitrile to give the three-component coupled product 4. Alois Fürstner of the Max-Planck-Institut Mülheim cyclized (Angew. Chem. Int. Ed. 2011, 50, 7829) 5 with a Mo catalyst, released in situ from a stable precursor, to give 6 in high ee. Hiromichi Fujioka of Osaka University rearranged (Chem.
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Conference papers on the topic "Organic synthesis optimization"

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Nocera, Nicola, Bozhena Tsyupa, Marco Bandiera, et al. "Optimizing Sol-Gel Coatings for Corrosion Protection of Braking Discs." In CONFERENCE 2023. AMPP, 2023. https://doi.org/10.5006/c2023-18872.

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Abstract This manuscript describes the development and optimization of sol-gel SiO2 -based Hybrid-Organic-Inorganic (HIO) coatings for application as corrosion protective layer on rotors employed in disc brake systems. The corrosion protection achieved with the coatings is optimized by tuning their water wettability, surface free energy (SFE), thickness and cross-linking degree, which strongly depend on sol chemical composition. Optimal film features are obtained modifying the silica network with organic components and accurately tailoring the deposition parameters. In particular, a Design of
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Afshar, Shahrara, Heshmatollah Najafabadi, and Mansoor Amani. "Optimization of synthesis of dioctyl phthalate using response surface methodology." In The 14th International Electronic Conference on Synthetic Organic Chemistry. MDPI, 2010. http://dx.doi.org/10.3390/ecsoc-14-00455.

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Kovács, Györgyi, Zoltán Timár, Zoltán Kele, and Lajos Kovács. "Optimization of peptide nucleic acid (PNA) oligomer synthesis using Fmoc/acyl-protected monomers." In The 4th International Electronic Conference on Synthetic Organic Chemistry. MDPI, 2000. http://dx.doi.org/10.3390/ecsoc-4-01883.

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Bartl, Johannes D., Martin Stutzmann, Anna Cattani-Scholz, and Marc Tornow. "Synthesis and optimization of organic sensing platforms for label-free DNA detection." In 2017 IEEE 12th International Conference on Nano/Micro Engineered and Molecular Systems (NEMS). IEEE, 2017. http://dx.doi.org/10.1109/nems.2017.8016987.

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Barham, Joshua Philip, Yasuo Norikane, Hiromichi Egami, and Yoshitaka Hamashima. "High Efficiency Microwave Flow Chemistry Towards Synthesis of Functional Materials and Pharmaceutical Cores." In Ampere 2019. Universitat Politècnica de València, 2019. http://dx.doi.org/10.4995/ampere2019.2019.9860.

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Microwave (MW) heating benefits organic synthesis by affording higher product yields in shorter time periods than conventional heating, yet it suffers from poor scalability and is limited to polar solvents in typical batch mode reactors. Herein, we report a microwave flow reactor using a solid-state semiconductor MW generator. The tunable, single-mode MW heating allows high efficiency, scalable organic synthesis, rapid reaction optimization and is applicable to non-polar solvents (o-Xylene and CPME can be rapidly heated to ca. 260 oC). Auto-frequency tuning compensates for changes in the micro
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Hayashi, Yamato, Kyosuke Fujita, Ichihito Narira, Masahiro Inoue, and Hirotsugu Takizawa. "Synthesis and optimization of silver nanowire transparent conductive film by organic needle-shaped precursor painting reduction method." In 2016 IEEE 16th International Conference on Nanotechnology (IEEE-NANO). IEEE, 2016. http://dx.doi.org/10.1109/nano.2016.7751502.

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Chiang, Jay, and K. Sharpless. "Automation in Reaction Optimization." In The 3rd International Electronic Conference on Synthetic Organic Chemistry. MDPI, 1999. http://dx.doi.org/10.3390/ecsoc-3-01762.

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Bohner, Tanja, and Andrea Vasella. "Optimization of the PdII/CuI-catalyzed Cross-Coupling of Alkynylglucopyranoses." In The 1st International Electronic Conference on Synthetic Organic Chemistry. MDPI, 1997. http://dx.doi.org/10.3390/ecsoc-1-02018.

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Benjamin, Ellis, Shannon Hutson, Tony James, et al. "Temperature and Time Optimization of Diels-Alder Reactions in the CEM Microwave." In The 12th International Electronic Conference on Synthetic Organic Chemistry. MDPI, 2008. http://dx.doi.org/10.3390/ecsoc-12-01265.

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Yan, Bing. "Single bead FTIR in the optimization of solid-phase combinatorial organic syntheses." In The 3rd International Electronic Conference on Synthetic Organic Chemistry. MDPI, 1999. http://dx.doi.org/10.3390/ecsoc-3-01754.

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Reports on the topic "Organic synthesis optimization"

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Sun, Ning. Process scale-up and optimization of the metal-organic framework synthesis. Office of Scientific and Technical Information (OSTI), 2020. http://dx.doi.org/10.2172/1618846.

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