Relevant bibliographies by topics / Organotin compounds X-ray crystallography

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Academic literature on the topic 'Organotin compounds X-ray crystallography'

Author: Grafiati
Published: 4 June 2021
Last updated: 1 February 2022

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Journal articles on the topic "Organotin compounds X-ray crystallography"

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Yusof, Enis Nadia Md, Muhammad A. M. Latif, Mohamed I. M. Tahir, et al. "o-Vanillin Derived Schiff Bases and Their Organotin(IV) Compounds: Synthesis, Structural Characterisation, In-Silico Studies and Cytotoxicity." International Journal of Molecular Sciences 20, no. 4 (2019): 854. http://dx.doi.org/10.3390/ijms20040854.

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Six new organotin(IV) compounds of Schiff bases derived from S-R-dithiocarbazate [R = benzyl (B), 2- or 4-methylbenzyl (2M and 4M, respectively)] condensed with 2-hydroxy-3-methoxybenzaldehyde (oVa) were synthesised and characterised by elemental analysis, various spectroscopic techniques including infrared, UV-vis, multinuclear (1H, 13C, 119Sn) NMR and mass spectrometry, and single crystal X-ray diffraction. The organotin(IV) compounds were synthesised from the reaction of Ph2SnCl2 or Me2SnCl2 with the Schiff bases (S2MoVaH/S4MoVaH/SBoVaH) to form a total of six new organotin(IV) compounds th
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Uhlig, Frank, Christian Kayser, Ralph Klassen, et al. "Synthese und Reaktionsverhalten von Stannyloligosilanen, I. Kettenförmige Stannyloligosilane mit SiMe2-Einheiten/Synthesis and Reactivity of Stannyloligosilanes, I. Stannyloligosilane Chains Containing SiMe2 Moieties." Zeitschrift für Naturforschung B 54, no. 2 (1999): 278–87. http://dx.doi.org/10.1515/znb-1999-0217.

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Stannyloligosilanes 1 and 2 with terminal organotin groups are available by reacting alkali metal tri- or diorganostannides with α,ω-dichloro- or difluorosilanes, or by treatment of organochlorostannanes with α,ω-difluorosilanes in the presence of magnesium . Attempts to functionalize the triorganotin derivatives 2 by halogenation reagents did not result in the halogen compounds 5; instead cleavage of silicon-tin bonds is observed. In contrast, reactions of the hydridotin derivatives 1 with CHX3 (X = Cl, Br) lead to the quantitative formation of the bis(chloro- or bromostannyl)oligosilanes 5.
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Hazani, Nur Nadira, Nur Nadia Dzulkifli, Sheikh Ahmad Izaddin Sheikh Mohd Ghazali, Yusairie Mohd, Yang Farina, and Mohammad Fadzlee Ngatiman. "Synthesis, Characterisation, Crystal Structure and Anti-corrosion Studies of an Organotin(IV) Complex of 2-acetylpyridine 4-ethyl-3-thiosemicarbazone (LH): n-BuSn(L)Cl2." ASM Science Journal 12 (July 22, 2019): 1–15. http://dx.doi.org/10.32802/asmscj.2019.271.

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This study explored the possibility of Schiff-base ligand compound, 2-acetylpyridine 4-ethyl-3-thiosemicarbazone (LH) and its organotin(IV) complex (BuSn(L)Cl2) as a corrosion inhibitor for mild steel in 1M hydrochloric acid (HCl) medium. The chemical structures of the synthesised compounds were confirmed by performing elemental analysis, FT-IR, UV-Vis, NMR spectroscopy, and X-ray crystallography diffraction study. The structure showed the LH served as a tridentate (N, N’, S) donor to tin through its pyridyl, azomethine nitrogen, and thiolate sulphur. The corrosion inhibition characteristics o
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Ma, Chunlin, Qin Jiang та Rufen Zhang. "Synthesis and characterization of a linked, π-π stacked organotin compound of 2-mercapto-6-nitrobenzothiazolyl diphenyltin chloride with 2-ethoxyl-6-nitrobenzothiazole". Canadian Journal of Chemistry 81, № 7 (2003): 825–31. http://dx.doi.org/10.1139/v03-087.

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The new organotin compound, Ph2Sn(Cl)[S(C7H3N2O2S)]·[(C7H3N2O2S)OEt], assembled by an intermolecular aromatic benzothiazole–benzothiazole π-π stacking interaction, has been synthesized by the reaction of diphenyltin dichloride with 2-mercapto-6-nitrobenzothiazole. The title compound was characterized by elemental, IR, 1H NMR, and X-ray crystallography analyses. Single-crystal X-ray diffraction data reveals that the title compound has two different molecular components. The component Ph2Sn(Cl)[S(C7H3N2O2S)] has a pentacoordinate tin, which further forms an infinite one-dimensional chain by inte
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Plasseraud, Laurent. "CO2 Derivatives of Molecular Tin Compounds. Part 2: Carbamato, Formato, Phosphinoformato and Metallocarboxylato Complexes." Inorganics 9, no. 3 (2021): 18. http://dx.doi.org/10.3390/inorganics9030018.

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Single-crystal X-ray diffraction structures of organotin compounds bearing hemicarbonate and carbonate ligands were recently reviewed by us—“CO2 Derivatives of Molecular Tin Compounds. Part 1: Hemicarbonato and Carbonato Complexes”, Inorganics 2020, 8, 31—based on crystallographic data available from the Cambridge Structural Database. Interestingly, this first collection revealed that most of the compounds listed were isolated in the context of studies devoted to the reactivity of tin precursors towards carbon dioxide, at atmospheric pressure or under pressure, thus highlighting the suitable d
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Wahba, Haytham, Ahmed Mansour, Julien Vanasse, et al. "The organomercurial lyase Merb possesses unique metal-binding properties." Acta Crystallographica Section A Foundations and Advances 70, a1 (2014): C1680. http://dx.doi.org/10.1107/s2053273314083193.

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Select bacterial strains survive in mercury-contaminated environments due to acquisition of a transferable genetic element known as the mer operon. The mer operon typically encodes for a series of proteins that includes two enzymes, MerA and MerB. The organomercurial lyase (MerB) cleaves carbon-mercury bonds of organomercurial compounds yielding ionic mercury Hg (II) and a reduced-carbon compound. The Hg (II) ion product remains bounds until it is shuttled directly to the mercuric ion reductase (MerA) to be reduced. Based on NMR spectroscopy and X-ray crystallography studies1, we have determin
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Jana, Surajit, Roland Fröhlich, and Norbert W. Mitzel. "Organozinc Siloxide-Hydrazide Aggregates [(RZn)4(NHNMe2)x(OSiMe3)(4 – x)]." Zeitschrift für Naturforschung B 61, no. 7 (2006): 838–45. http://dx.doi.org/10.1515/znb-2006-0711.

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The reaction of dialkylzinc compounds R2Zn (R = Me, Et) with N,N-dimethylhydrazine and trimethylsilanol in a 4 : 2 : 2 ratio leads to the formation of tetra(alkylzinc) tris-siloxide monohydrazide aggregates, [(RZn)4(NHNMe2)(OSiMe3)3] [R = Me (1) and Et (2)]. These compounds are aggregates of mirror symmetry, containing the novel Zn4N2O3 core. Both compounds have been characterised by 1H, 13C and 29Si NMR and IR spectroscopy, by mass spectrometry and by elemental analysis, and 2 also by X-ray crystallography. The structure can be derived from a heterocubane, in which one anionic vertex is repla
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Balas, Vasilis I., Christina N. Banti, Nikolaos Kourkoumelis, et al. "Structural and In Vitro Biological Studies of Organotin(IV) Precursors; Selective Inhibitory Activity Against Human Breast Cancer Cells, Positive to Estrogen Receptors." Australian Journal of Chemistry 65, no. 12 (2012): 1625. http://dx.doi.org/10.1071/ch12448.

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Crystals of Ph3SnCl (1) were grown from a methanol/acetonitrile solution. Compounds [Ph3SnOH]n (2) and [(Ph2Sn)4Cl2O2(OH)2] (3) were crystallized from diethyl ether/methanol/acetonitrile and hot acetone/water solutions respectively, of the white precipitation, formed by adding KOH to solutions of 1 and [Ph2SnCl2] in 1 : 1 and 1 : 2 molar ratios respectively. Complex 1 was characterized by X-ray crystallography. X-ray structure determination of compounds 2 and 3 confirmed the previously reported identities. The molecular structure of 1, reported here, is a new polymorphic form of the known one
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Wiecek, Joanna, Dimitra Kovala-Demertzi, Zbigniew Ciunik, Joanna Wietrzyk, Maria Zervou, and Mavroudis A. Demertzis. "Organotin Compound Derived from 3-Hydroxy-2-formylpyridine Semicarbazone: Synthesis, Crystal Structure, and Antiproliferative Activity." Bioinorganic Chemistry and Applications 2010 (2010): 1–7. http://dx.doi.org/10.1155/2010/718606.

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The novel diphenyltin(IV) compound (2), where (1) is 3-hydroxy-2-formylpyridine semicarbazone, was prepared and characterized by vibrational and NMR (1H,13C) spectroscopy. The structure of [P(HyFoSc)Sn] was confirmed by single-crystal X-ray crystallography. The doubly deprotonated ligand is coordinated to the tin atom through the enolic-oxygen, the azomethine-nitrogen, and phenolic-oxygen, and so acts as an anionic tridentate ligand with the ONO donors. Two carbon atoms complete the fivefold coordination at the tin(IV) center. Intermolecular hydrogen bonding, , and interactions combine to stab
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Latsis, George, Christina Banti, Nikolaos Kourkoumelis, et al. "Poly Organotin Acetates against DNA with Possible Implementation on Human Breast Cancer." International Journal of Molecular Sciences 19, no. 7 (2018): 2055. http://dx.doi.org/10.3390/ijms19072055.

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Two known tin-based polymers of formula {[R3Sn(CH3COO)]n} where R = n-Bu– (1) and R = Ph– (2),were evaluated for their in vitro biological properties. The compounds were characterized via their physical properties and FT-IR, 119Sn Mössbauer, and 1H NMR spectroscopic data. The molecular structures were confirmed by single-crystal X-Ray diffraction crystallography. The geometry around the tin(IV) ion is trigonal bi-pyramidal. Variations in O–Sn–O···Sn′ torsion angles lead to zig-zag and helical supramolecular assemblies for 1 and 2, respectively. The in vitro cell viability against human breast
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Dissertations / Theses on the topic "Organotin compounds X-ray crystallography"

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Stem, Joseph Michelle R. "Computational modeling studies of the structures and properties of organotin(IV) and stannyl-thioether systems with comparisons to X-ray crystallography." To access this resource online via ProQuest Dissertations and Theses @ UTEP, 2009. http://0-proquest.umi.com.lib.utep.edu/login?COPT=REJTPTU0YmImSU5UPTAmVkVSPTI=&clientId=2515.

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Athukorala, Arachchige Kasun S. "Synthesis and crystallographic studies of novel organotin acenaphthene compounds." Thesis, University of St Andrews, 2014. http://hdl.handle.net/10023/6363.

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Organic frameworks with rigid backbones, such as acenaphthene, are highly suitable for the study of interatomic interactions. The short “natural” peri-distance (2.44 Å) and the rigidity of the aromatic system causes considerable steric strain between peri-substituted heteroatoms. As a consequence, substitution at both peri-positions leads to in- and out-of-plane distortions, which often result in buckling of the ring system. In order to relax this geometric strain, weak bonding interactions can also exist between the peri-substituents. This thesis focuses on the synthesis, structural character
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Doidge-Harrison, Solange Maria Silva Veloso. "X-ray and spectroscopic studies of organotin compounds." Thesis, Robert Gordon University, 1992. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.304984.

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Cheung, Eugene. "Solid state photochemistry and x-ray crystallography of carbonyl-containing compounds." Thesis, National Library of Canada = Bibliothèque nationale du Canada, 2000. http://www.collectionscanada.ca/obj/s4/f2/dsk1/tape3/PQDD_0017/NQ56659.pdf.

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Lane, S. E. "Structure determination by X-ray crystallography of some Group IIIB compounds." Thesis, Lancaster University, 1985. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.355338.

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Du, Junyi. "X-ray crystallographic studies of sulfur/selenium heteroatom compounds." Thesis, University of St Andrews, 2016. http://hdl.handle.net/10023/8984.

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The major aim of research reported on this thesis uses X-ray crystallography to investigate the structural features of a series of pentafluorosulfuranyl (SF₅) containing aromatic compounds, chalcogen amides, 2,4-diaryl-1,3-selenazoles and 2,4-diaryl-1,3-chalcogen azoles bearing SF₅ group and organo phosphorus-chalcogen macrocycles incorporationg double OP(S)SC[sub]n or OP(Se)SeC[sub]n scaffolds. The basic theory of crystallography is introduced in Chapter 1, followed by a general discussion on pentafluorosulfuranyl (SF₅) containing heteroatom compounds and sulfur/selenium heterocycles in Chapt
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Hodgson, Susan Marie. "Structural studies of lithium compounds." Thesis, University of Newcastle Upon Tyne, 1989. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.244863.

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Williams, Steven Andrew. "Synthesis, structural characterisation and dynamic behaviour of heteronuclear Group IB metal cluster compounds." Thesis, University of Exeter, 1998. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.245930.

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唐偉方 and Wai-fong Tong. "X-ray crystallographic studies of osmium and ruthenium complexes of multianionic, polypyridyl and tertiary amine ligands." Thesis, The University of Hong Kong (Pokfulam, Hong Kong), 1991. http://hub.hku.hk/bib/B31210016.

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Tong, Wai-fong. "X-ray crystallographic studies of osmium and ruthenium complexes of multianionic, polypyridyl and tertiary amine ligands /." [Hong Kong : University of Hong Kong], 1991. http://sunzi.lib.hku.hk/hkuto/record.jsp?B13019272.

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Books on the topic "Organotin compounds X-ray crystallography"

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Mutikainen, Ilpo. X-ray structural studies on metal complexes of uracil and orotic acid: A survey of coordination induced changes in the uracil fragment. Suomalainen Tiedeakatemia, 1988.

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Habermehl, Gerhard, and Halvor Jaeger. Röntgenstrukturanalyse organischer Verbindungen: Eine Einführung. Springer, 2011.

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Yin, Yaobo. New solid-state fluorides: Synthesis, crystal chemistry, and optical properties. 1993.

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Yin, Yaobo. New solid-state fluorides: Synthesis, crystal chemistry, and optical properties. 1993.

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Book chapters on the topic "Organotin compounds X-ray crystallography"

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Wagner, Ulrike, and Christoph Kratky. "Structure Elucidation of Natural Compounds by X-Ray Crystallography." In Progress in the Chemistry of Organic Natural Products 100. Springer International Publishing, 2014. http://dx.doi.org/10.1007/978-3-319-05275-5_1.

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Alvarez-Larena, Angel, Joan Farran, and Joan F. "Supramolecular Arrangements in Organotellurium Compounds via Te···Halogen Contacts." In Current Trends in X-Ray Crystallography. InTech, 2011. http://dx.doi.org/10.5772/30097.

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Niepötter, Benedikt, and Dietmar Stalke. "X-Ray Crystallography of Organosilicon Compounds (Electron Density and Chemical Bonding in Organosilicon Compounds)." In Organosilicon Compounds. Elsevier, 2017. http://dx.doi.org/10.1016/b978-0-12-814213-4.00001-0.

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Dutko, Frank J., Guy D. Diana, Daniel C. Pevear, M. Patricia Fox, and Mark A. McKinlay. "Quantitative Structure–Activity Relationships and Biological Consequences of Picornavirus Capsid-Binding Compounds." In Use of X-Ray Crystallography in the Design of Antiviral Agents. Elsevier, 1990. http://dx.doi.org/10.1016/b978-0-12-438745-4.50019-7.

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MILES, EDITH WILSON, S. ASHRAF AHMED, and ARVIND M. KAYASTHA. "Exploring the Tryptophan Synthase α2β2 Multienzyme Complex by X-Ray Crystallography and Site-Directed Mutagensis." In Enzymes Dependent on Pyridoxal Phosphate and Other Carbonyl Compounds As Cofactors. Elsevier, 1991. http://dx.doi.org/10.1016/b978-0-08-040820-0.50054-6.

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Giacovazzo, Carmelo. "Phasing via electron and neutron diffraction data." In Phasing in Crystallography. Oxford University Press, 2013. http://dx.doi.org/10.1093/oso/9780199686995.003.0016.

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Among the statistics freely available on the webpage of the Cambridge Structural Database, there is a detail of interest for this chapter: of the 596 910 crystal structures deposited up to 1 January 2012, only 1534 were solved by neutron data (see Table 1.11). No information is provided on the number of structures solved by electron data because it is negligible (organic samples are soon damaged by the electron beams). A statistical search of the Inorganic Crystal Structure Database (ICSD, Ver. 2012–1, about 150 000 entries; by courtesy of Thomas Weirich) on structures that have been solved by means of electron diffraction, eventually in combination with other techniques, indicates a total of about 0.7%. In spite of limited impact on the databases, electron and neutron diffraction play a fundamental role in materials science and in crystallography. The main reason is that they provide alternative techniques to X-rays. Let us first consider electron diffraction (ED) techniques. The study of crystalline samples at the nanometer scale is mandatory for many industrial applications; indeed, physical properties depend on the crystal structure. Unfortunately it is not unusual for compounds to only exist in the nanocrystalline state; then, traditional X-ray diffraction techniques for atomic structure determination cannot be applied, because of the weak interactions between X-rays and matter. As a consequence, such structures remain unknown, in spite of their technological importance. This limits the contribution of X-ray crystallography to nanoscience, a growing scientific area, crucial to many fields, from semiconductors to pharmaceuticals and proteins. The result is a lack of knowledge on the underlying structure–property relationships, which often retards further research and development. Structure analysis by electron diffraction began as early as the 1930s (in particular, by Rigamonti, in 1936), but the interest of the crystallographic community in such a technique soon faded, mostly because electron diffraction intensities are not routinely transferable into kinematical |F|2. In spite of this limitation, the technique has been used for investigating the structure of many inorganic, organic, and metallo-organic crystals, biological structures, and various minerals, especially layer silicates.
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Patrick, Graham. "3. The synthesis and analysis of organic compounds." In Organic Chemistry: A Very Short Introduction. Oxford University Press, 2017. http://dx.doi.org/10.1093/actrade/9780198759775.003.0003.

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The design of novel medicines, insecticides, perfumes, flavourings, or polymeric materials relies crucially on organic chemists. ‘The synthesis and analysis of organic compounds’ outlines how the synthesis of an organic compound is devised to ensure that each atom is in the correct position within the molecule. It explains retrosynthesis and how reactions are carried out and monitored using chromatography and infrared spectroscopy. Once a reaction has been carried out, it is necessary to isolate and purify the reaction product. The structure of the end product needs to be analysed by elemental analysis, mass spectrometry, X-ray crystallography, or nuclear magnetic resonance spectroscopy. Another important part of organic chemistry is understanding how reactions take place.
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Harada, Nobuyuki. "Chiral Molecular Tools Powerful for the Preparation of Enantiopure Compounds and Unambiguous Determination of Their Absolute Configurations by X-Ray Crystallography and/or 1H NMR Diamagnetic Anisotropy." In Chiral Analysis. Elsevier, 2018. http://dx.doi.org/10.1016/b978-0-444-64027-7.00007-0.

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