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Journal articles on the topic 'Silanized silica gel'

Author: Grafiati

Published: 5 June 2025

Last updated: 1 August 2025

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1

Parys, Wioletta, and Alina Pyka-Pająk. "Influence of Chromatographic Conditions on LOD and LOQ of Fluoxetine and Sertraline Analyzed by TLC-Densitometric Method." Processes 10, no. 5 (2022): 971. http://dx.doi.org/10.3390/pr10050971.

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This research introduces the analysis of fluoxetine and sertraline by means of the TLC-densitometric method. They provide information on LOD and LOQ under various chromatographic conditions. The study used adsorption (NPTLC) and partition (RPTLC) thin-layer chromatography in combination with a densitometric analysis. Four types of chromatographic plates precoated with: silica gel 60 F254, silica gel 60, silanized silica gel 60 F254 (RP-2), and a mixture of silica gel 60 and kieselguhr F254, as well as three mobile phases: chloroform + methanol + ammonia (9:1:0.4, v/v/v), chloroform + methanol

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2

Goworek, J. "Adsorption from binary solutions on silanized silica gel." Colloids and Surfaces 47 (January 1990): 167–77. http://dx.doi.org/10.1016/0166-6622(90)80070-k.

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3

Xie, Yi Hui, Yan Hua Ding, Wen Qin Liu, Wen Ting Bai, and Li Ping Huang. "Microwave Assisted Synthesis of Quercetin-Selective MIPs Grafted on Silica Gel Surface." Advanced Materials Research 1120-1121 (July 2015): 608–14. http://dx.doi.org/10.4028/www.scientific.net/amr.1120-1121.608.

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The silica gel surface was alkylated by silane coupling agent KH-570 under the microwave assisted and orthogonal experiment was adopted to optimize the silica gel surface silanized experimental conditions with synthetic yield as index. With quercetin as the template molecule, 4 - vinyl pyridine as the functional monomer, ethylene glycol dimethyl acrylate as the cross linking agent, azodiisobutyronitrile as initiator, under the microwave assisted in silane silicone surface quercetin molecularly imprinted polymer was successfully synthesized. Take selected quercetin as index, another orthogonal

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4

Boczkaj, Grzegorz, Malwina Momotko, Andrzej Przyjazny, and Marian Kamiński. "Studies of the separation performance of silanized silica gel for simulated distillation." Journal of Separation Science 39, no. 4 (2016): 748–55. http://dx.doi.org/10.1002/jssc.201501127.

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5

Kowalczuk, Dorota, and Hanna Hopkała. "Separation of fluoroquinolone antibiotics by TLC on silica gel, cellulose and silanized layers." Journal of Planar Chromatography – Modern TLC 19, no. 109 (2006): 216–22. http://dx.doi.org/10.1556/jpc.19.2006.3.9.

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6

Berlin, Matt, Jesse Allen, Varadharajan Kailasam, David Rosenberg, and Edward Rosenberg. "Nanoporous Silica Polyamine Composites for Metal Ion Capture From Rice Hull Ash." Eurasian Chemico-Technological Journal 12, no. 2 (2010): 123. http://dx.doi.org/10.18321/ectj34.

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Rice Hull Ash (RHA) was converted to amorphous silica gel using a modified version of published literature procedures. The gels were characterized by a comparison of their CPMAS [29] Si NMR and Scanning Electron Microscopy (SEM) images with commercial silica gels. The resulting gels were silanized with a 7.5:1 mixture of methyltrichlorosilane and chloropropyltrichlorosilane and then reacted with poly(allylamine) (PAA) to produce the silica polyamine composite (SPC) BP-1. The BP-1 was then further modified with pyridine-2-carboxaldehyde to form the copper selective SPC, CuSELECT. This procedure

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7

Bhabatosh, Mandai, Chowdhury Pranesh, and K. Pandit Susanta. "Extraction chromatographic studies of uranium(VI) with crosslinked poly(acrylic acid) coated on silica gel." Journal of Indian Chemical Society Vol. 85, Sep 2008 (2008): 930–35. https://doi.org/10.5281/zenodo.5820255.

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Analytical Laboratory, Department of Chemistry, Visva-Bharati, Santiniketan-731 235, West Bengal, India <em>E-mail:</em> bhabatosh_mandal@yahoo.co.in <em>Manuscript received 16 October 2007, revised 12 May 2008, accepted 25 June 2008</em> A selective method has been developed for extraction and separation of U<sup>VI</sup> with the chemically synthesized high molecular mass crosslinked poly(acrylic acid) coated on silanized silica gel. The coated materials act as a stationary phase for the extraction chromatographic studies. The structure and thermal stability of crosslinked poly(acrylic acid)

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8

Xu, Ling, Jian Sun, and Long Zhao. "Co-grafting of acrylamide and vinyl imidazole onto EB pre-irradiated silanized silica gel." Radiation Physics and Chemistry 80, no. 11 (2011): 1268–74. http://dx.doi.org/10.1016/j.radphyschem.2011.03.024.

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9

Lepri, L., P. G. Desideri, and V. Coas. "High-performance thin-layer chromatography of dinitropyridyl-amino acids and sulphonamides on silanized silica gel." Journal of Chromatography A 405 (January 1987): 394–400. http://dx.doi.org/10.1016/s0021-9673(01)81783-0.

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10

Ovari, Tamara-Rita, Timea Toth, Gabriel Katona, Gabriella Stefánia Szabó, and Liana Maria Muresan. "Epoxy Coatings Doped with (3-Aminopropyl)triethoxysilane-Modified Silica Nanoparticles for Anti-Corrosion Protection of Zinc." Coatings 13, no. 11 (2023): 1844. http://dx.doi.org/10.3390/coatings13111844.

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Epoxy (EP) coatings containing silica (SiO2) and (3-Aminopropyl)triethoxysilane-modified silica (SiO2-APTES) nanoparticles were prepared via the dip-coating technique on a zinc substrate. A detailed study was performed regarding their incorporation into the matrix, followed by the investigation of the newly obtained organic–inorganic hybrid coatings’ anti-corrosive properties. The two methods of embedding the nanoparticles were (I) modification of the silica nanoparticles with APTES followed by their introduction into the epoxy resin, and (II) functionalization of the silica nanoparticles in t

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11

Sousa Júnior, Lenivaldo Valério de, Thaís Regina Silva Ribeiro, Bruno José Barros da Silva, et al. "Different approaches to the synthesis of ZSM-22 zeolite with application in n-heptane cracking." Research, Society and Development 11, no. 3 (2022): e6411326070. http://dx.doi.org/10.33448/rsd-v11i3.26070.

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The synthesis of ZSM-22 zeolite has been extensively studied due to its properties of form selectivity, acidity and hydrothermal stability, which is applied in important reactions in the areas of petroleum refining and petrochemicals. In view of this, the present work studied different approaches of synthesis of ZSM-22 using: 1-diaminohexane as a structure directing agent, (ii) methanol and seed crystals, (iii) aging of the synthesis gel with addition of polymer, surfactant and silane and (iv) starch, calcium carbonate and silanized silica with subsequent desilication. Thus, the effects of the

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12

Chomicki, Adam, and Tadeusz H. Dzido. "Pressurized planar electrochromatography of DNS amino acids derivatives in silica gel and silanized silica gel systems with formic acid addition to the water mobile phase." JPC – Journal of Planar Chromatography – Modern TLC 34, no. 2 (2021): 105–11. http://dx.doi.org/10.1007/s00764-021-00099-4.

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AbstractPressurized planar electrochromatography (PPEC) of dansyl (DNS) derivatives of amino acids in normal- and reversed-phase systems is presented. The results have been obtained for mobile phases with different acetonitrile (ACN) concentrations (0–85%). The data obtained show differences in separation selectivity between high-performance thin-layer chromatography (HPTLC) and PPEC systems. These differences originate from the electrophoretic effect which is involved in the PPEC system, contrary to the HPTLC one.

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13

Pranesh, Chowdhury, K. Pandit Susanta, and Mandal Bhabatosh. "Solid phase extraction of Hgll ions with cross-linked poly(acrylic acid), coated on silanized silica gel." Journal of Indian Chemical Society Vol. 86, Apr 2009 (2009): 377–82. https://doi.org/10.5281/zenodo.5809971.

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Analytical Laboratory, Department of Chemistry, Visva-Bharati, Santiniketan-731 235, West Bengal, India <em>E-mail</em> : pranesh_02@yahoo.co.in <em>Manuscript received 15 December 2008, accepted 24 December 2008</em> A selective and reliable method has been developed for the extraction and separation of Hg<sup>II </sup>with high molecular mass cross-linked poly(acrylic acid) coated on silanized silica gel. The coated material acts as stationary phase for the extraction. Ion exchange and break-through capacity of the exchanger have been measured. The optimum pH range for the quantitative

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14

Rosace, G., E. Guido, C. Colleoni, and G. Barigozzi. "Influence of Textile Structure and Silica Based Finishing on Thermal Insulation Properties of Cotton Fabrics." International Journal of Polymer Science 2016 (2016): 1–10. http://dx.doi.org/10.1155/2016/1726475.

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The aim of this work is to investigate the influence of weave structures and silica coatings obtained via sol-gel process on the thermal insulation properties of cotton samples. For this reason three main weave structures (plain, satin, and piqué) of cotton fabric were selected with different yarn count, threads per cm, and mass per square meter values. Thereafter, only for the plain weave, the samples were padded using silica sol formed by hydrolysis and subsequent condensation of 3-glycidoxypropyltrimethoxysilane under acidic conditions. The silanized plain weave samples were characterized b

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15

Heimler, Daniela. "High-performance thin-layer chromatography of selected flavonoid aglycones on ready-for-use layers of silanized silica gel." Journal of Chromatography A 366 (January 1986): 407–11. http://dx.doi.org/10.1016/s0021-9673(01)93492-2.

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16

Fujinuma, Kenji, Kazuo Saito, Mitsuo Nakazato, Yoko Kikuchi, Akihiro Ibe, and Taichiro Nishima. "Thin Layer Chromatographic Detection and Liquid Chromatographic Determination of Stevioside and Rebaudioside A in Beverages and Foods Following Reverse Phase Column Chromatography." Journal of AOAC INTERNATIONAL 69, no. 5 (1986): 799–802. http://dx.doi.org/10.1093/jaoac/69.5.799.

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Abstract A method for the detection and determination of stevioside and rebaudioside A in beverages and foods by thin layer chromatography (TLC) and liquid chromatography (LC) is presented. Stevioside and rebaudioside A are extracted with water from a sample and purified by a reverse phase column chromatographic procedure using a silica gel 60 silanized column. The eluate from the column is concentrated to dryness, and the resulting residue is dissolved in 80% ethanol. For the detection, TLC is used, and spots of stevioside and rebaudioside A are visualized with anisaldehyde sulfuric acid reag

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17

Goworek, J., and W. Stefaniak. "Some aspects of the adsorption properties of silanized silica gel at the solid/liquid interface part 1. Adsorption isotherms." Colloids and Surfaces 54 (January 1991): 321–26. http://dx.doi.org/10.1016/0166-6622(91)80070-5.

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18

Goworek, J., and W. Stefaniak. "Some aspects of the adsorption properties of silanized silica gel at the solid/liquid interface part 2. Thermogravimetric nalysis." Colloids and Surfaces 54 (January 1991): 327–30. http://dx.doi.org/10.1016/0166-6622(91)80071-u.

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19

Ren, Xianjie, Yang Geng, Alfred B. O. Soboyejo, and Katrina Cornish. "REINFORCED MECHANICAL PROPERTIES OF FUNCTIONALIZED SILICA AND EGGSHELL FILLED GUAYULE NATURAL RUBBER COMPOSITES." Rubber Chemistry and Technology 92, no. 4 (2019): 687–708. http://dx.doi.org/10.5254/rct.19.81485.

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ABSTRACT Replacing synthetic fillers, which are commonly used to reinforce rubber, with bio-fillers has potential to improve the sustainability of rubber products. Eggshell (ES) (a powder with a maximum particle diameter of 9.4 μm and a median of 1.1 μm) was added to guayule natural rubber (GNR) composites to partially or fully replace bifunctionally silanized, high surface area, precipitated silica (BSS). The mixing energy consumption, mechanical properties, cross-link density, filler dispersion and final particle size, fracture surface morphology, and dyeability of GNR composites were charac

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20

Chowdhury, P., S. K. Pandit, and B. Mandal. "Preparation and characterization of silanized silica gel-supported poly(acrylic acid) network polymer and study of its analytical application as selective extractor for lead ion." Journal of Applied Polymer Science 110, no. 1 (2008): 475–80. http://dx.doi.org/10.1002/app.28664.

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21

Marmiy, N. V., and D. S. Esipov. "METHOD OF PREPARATIVE SYNTHESIS OF 8-OXO-2'-DEOXYGUANOSINE FOR LABORATORY USING." Fine Chemical Technologies 12, no. 4 (2017): 58–64. http://dx.doi.org/10.32362/2410-6593-2017-12-4-58-64.

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A preparative method for the synthesis of 8-oxo-2'-deoxyguanosine (8-oxo-dG) giving a high yield up to 80% and suitable for laboratory use is suggested. The urgency of the development of this method is associated with the need to obtain large quantities of 8-oxo-dG for the study of biological and pharmaceutical activity. Evidence of this need was obtained in the last decades, when the mechanisms of the interface of DNA repair with intracellular signaling through 8-oxo-dG were discovered and its anti-inflammatory and protective effects were revealed. The suggested method is based on the scheme

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22

Dymek, Aleksandra, Jarosław Widelski, Krzysztof Kamil Wojtanowski, Vladyslav Vivcharenko, Agata Przekora, and Tomasz Mroczek. "Fractionation of Lycopodiaceae Alkaloids and Evaluation of Their Anticholinesterase and Cytotoxic Activities." Molecules 26, no. 21 (2021): 6379. http://dx.doi.org/10.3390/molecules26216379.

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In view of the abundant evidence that Lycopodiaceae alkaloids, including the well-known huperzine A (HupA), are among the potent acetylcholinesterase (AChE) inhibitors, an attempt was made to search for new compounds responsible for this property. For this purpose, three plant species belonging to the Lycopodiaceae family, commonly found in the Euro-Asia region, were subjected to the isolation of bioactive compounds, their identification and subsequent evaluation of their anticholinesterase and cytotoxic activities. Methanolic extracts of two Lycopodium and one Hupezia species were obtained vi

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23

Mandal, Bhabatosh, Dipika Roy, Mousumi Chatterjee, et al. "n-Capric acid-anchored silanized silica gel: its application to sample clean-up of Th(iv) sorbed as a dinuclear species in quantified H-bonded dimeric metal-trapping cores." New Journal of Chemistry 41, no. 13 (2017): 5542–54. http://dx.doi.org/10.1039/c7nj00694b.

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nCA anchored to SSG surface generates 121 μM g<sup>−1</sup> H-bonded metal-trapping cores with 10-fold increase in surface area for selective uptake of {Th<sub>2</sub>(OH)<sub>2</sub>(H<sub>2</sub>O)<sub>2</sub>}<sup>6+</sup>.

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24

B., Mandal, Narayan Datta Dip, and Roy U.S. "Extraction chromatographic studies of cadmium(II) with SRS-100, a high molecular mass carboxylic acid." Journal of Indian Chemical Society Vol. 85, June 2008 (2008): 632–34. https://doi.org/10.5281/zenodo.5816786.

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Department of Chemistry. Visva-Bharati, Santiniketan-731 235. West BengaL India <em>E-mail : </em>bhabatosh_mandal@yahoo.co.in <em>Manuscript received 9 March 2007. revised 18 March 2008. accepted 20 March 2008</em> A selective method has been developed for the extraction chromatographic separation of Cd<sup>II</sup> with SRS-100 (liquid cation exchanger) coated on silanised silica gel. Quantitative extraction of Cd<sup>II</sup> has been achieved from acetate buffer at the pH range 6.5-7.5. The effects of pH, stripping agents, flow-rate, on extraction and elution have been investigated. Exchan

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25

B., Mandal, K. Patra P., and Chakrabarti S. "Extraction chromatographic method of preconcentration and separation of fluoride with high molecular mass liquid anion exchanger, Aliquat-336." Journal of Indian Chemical Society Vol. 86, Nov 2009 (2009): 1166–72. https://doi.org/10.5281/zenodo.5820731.

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Department of Chemistry, be entre for Environmental Studies, Visva-Bharati, Santiniketan-731 235, West Bengal, India <em>E-mail</em> : bhabatosh_mandal@yahoo.co.in <em>Manuscript received 1 April 2009, revised 25 June 2009, accepted 26 June 2009</em> A selective method has been developed for the extraction chromatographic separation of fluoride with Aliquat 336 (liquid cation exchanger) coated on silanised silica gel. Its quantitative extraction has been achieved in HCl medium at 0.1-0.3 <em>M</em> range. The effects of acid with different concentrations, flow-rate, stripping agents on extract

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26

B., Mandal, Ghosh N., and Roy U.S. "Solid phase extraction, preconcentration of Cull and its separation from environmentally toxic metal ions with high molecular mass liquid cation exchanger, Versatic 9." Journal of Indian Chemical Society Vol. 86, Dec 2009 (2009): 1303–14. https://doi.org/10.5281/zenodo.5823884.

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Department of Chemistry, Visva-Bharati, Santiniketan-731 235, West Bengal, India <em>E-mail</em>: bhabatosh_mandal@yahoo.co.in Fax : 91-3463-261526 <em>Manuscript received 3 April 2009, accepted 21 July 2009</em> A selective method has been developed for the extraction chromatographic trace level separation of Cu<sup>ll</sup> with Versatic 9 (liquid cation exchanger) coated on silanised silica gel. Cu<sup>ll</sup> has been extracted from 0.1 <em>M</em> acetate buffer at the range of pH 4.0-5.5. The effects of foreign ions, pH, flow-rate, stripping agents on extraction and elution have been inv

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27

PILIPAVICIUS, Jurgis, Ala CHODOSOVSKAJA, Aldona BEGANSKIENE, and Aivaras KAREIVA. "Formation of Silver Nanoplates Layer on Amino Group Grafted Silica Coatings." Materials Science 22, no. 2 (2017). https://doi.org/10.5755/j01.ms.22.2.8405.

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In this study the self-arrangement of Ag nanoplates on (3-Aminopropyl)triethoxysilane (APTES) silanized silica coatings was investigated. Silica coatings were made by sol-gel method and silanized in two different ways. The first one includes silanization in acidic 2-propanol solution, the other one – in dry toluene. Coatings were silanized by using different amounts of APTES in case of silanization in 2-propanol. Silver nanoplates layer of functionalized silica coatings was obtained via self-assembly. Coatings were investigated by atomic force microscopy (AFM), water contact angle measurements

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28

Chomicki, Adam, and Tadeusz H. Dzido. "Thin-layer chromatography of DNS amino acids derivatives in systems with silica gel and silanized silica gel plates." Current Issues in Pharmacy and Medical Sciences, July 28, 2022. http://dx.doi.org/10.2478/cipms-2022-0011.

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Abstract Investigations into separation selectivity of High-Performance Thin-layer chromatography (HPTLC) of dansyl (DNS) derivatives of amino acids in silica gel (Silica gel 60 F254s plates) and silanized silica gel (RP-18 W plates) systems are presented. The results have been obtained for mobile phases containing different concentrations of acetonitrile (ACN) in formic acid (FA) water solution (final concentration of FA in the mobile phase was equal to 265 mmol/dm3). The data obtained show differences in separation selectivity of the solutes between employment of HPTLC silica gel and RP-18 W

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29

Ghamarpoor, Reza, Masoud Jamshidi, and Majid Mohammadpour. "Achieving outstanding mechanical/bonding performances by epoxy nanocomposite as concrete–steel rebar adhesive using silane modification of nano SiO2." Scientific Reports 13, no. 1 (2023). http://dx.doi.org/10.1038/s41598-023-36462-0.

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AbstractAnchoring steel rebar in concrete structures is a common method in the building and construction industry. This research focuses on improving the mechanical/bonding properties of the prepared epoxy nanocomposite adhesive using surface treatment of SiO2 nano fillers by glycidoxypropyltrimethoxysilane (GPTMS). For this purpose, the nano silica particles were silanized via a facile sol–gel method at silane concentrations of 1, 5, 10 and 20X (i.e. X is stoichiometric silane concentration). The nanoparticles were characterized carefully by FTIR, TGA, XRD and XPS techniques. It was found tha

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30

Hadioui, Madjid, Med Mecherri, Rastislav Šípoš, Yan Yvon, and Patrick Sharrock. "Polyamine-substituted epoxy-grafted silica for aqueous metal recovery." Chemical Papers 65, no. 6 (2011). http://dx.doi.org/10.2478/s11696-011-0067-5.

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AbstractGlycidoxypropyltriethoxysilane (GPS) was used as a reactive silane to graft metal- complexing ligands onto silica gel in aqueous media under mild conditions. The synthesis entailed the reaction of GPS with silica gel, followed by grafting polyamine onto the epoxy functional group. GPS was added to silica gel in ethanol with 5 vol. % water and the mixture was air-dried for 24 h. Subsequently, excess amounts of polyamines: triethylenetetramine, tetraethylenepentamine, and pentaethylenehexamine were individually added to the silanised silica, followed by solvent evaporation and ovendrying

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31

sprotocols. "Biofunctionalization of PDMS-based microfluidic systems." January 18, 2015. https://doi.org/10.5281/zenodo.14013.

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Authors: Bergoi Ibarlucea, Cesar Fernández-Sánchez, Stefanie Demming, Stephanus Büttgenbach & Andreu Llobera ### Abstract Three simple approaches for the selective immobilization of biomolecules on the surface of poly(dimethylsiloxane) (PDMS) microfluidic systems that do not require any specific instrumentation, are described and compared. They are based in the introduction of hydroxyl groups on the PDMS surface by direct adsorption of either polyethylene glycol (PEG) or polyvinyl alcohol (PVA) as well as by a liquid-based oxidation step. The hydroxyl groups are then silanized using a sila

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