Academic literature on the topic 'Solvotermal synthesis'

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Journal articles on the topic "Solvotermal synthesis"

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Gutierrez, Angel, M. Felisa Perpiñán, Ana E. Sánchez, and M. Carmen Torralba. "Solvotermal Synthesis of NiO, Ni and NiS Nanoparticles." Journal of Nanoscience and Nanotechnology 13, no. 1 (2013): 461–66. http://dx.doi.org/10.1166/jnn.2013.6717.

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Moklyak, V. V., V. О. Kotsyubynsky, A. B. Hrubiak, and L. Z. Zbihlei. "Morphological and Structural Characteristics of the Iron Fluoride Preparated by Solvotermal Synthesis." Фізика і хімія твердого тіла 17, no. 3 (2016): 356–62. http://dx.doi.org/10.15330/pcss.17.3.356-362.

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In this communication we demonstrate the fast and facile preparation of nanoparticles hydrated and anhydrous iron trifluoride by solvotermal synthesis using the surface active substances. The iron fluoride/acytelen black composites were prepared by ultrasonic treatment. The analysis of the crystal microstructure and morphological properties of the material received.
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Zherebtsov, D., S. Naifert, M. Polozov, et al. "The Choice of Solvents for Solvotermal Synthesis of Single-Crystal Polycyclic Aromatic Compounds." «Bulletin of the South Ural State University series "Chemistry"» 9, no. 4 (2017): 29–34. http://dx.doi.org/10.14529/chem170404.

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Nadjib, Muhammad, Ratna Ediati, Yudi Aris Sulistiyo, and Lutfiatun Nadifah. "Synthesis zeolitic Imidazolate Framework-8 (Zif-8) In Solvothermal: The Effect Comparison of Metal-Ligand." Jurnal ILMU DASAR 17, no. 1 (2017): 53. http://dx.doi.org/10.19184/jid.v17i1.2674.

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Synthesis of ZIF-8 (zeolitic Imidazolate Frameworks-8) have been successfully carried out by the reaction of zinc nitrate and 2-methylimidazolate in DMF (N'N-dimethylformamide) solvent at a temperature of 120 °C for 24 hours. Synthesis of ZIF-8 has been conducted five times with variations molar ratio of metal (Zn2+):ligand (MeIM) consecutive 1:1; 1:1.5; 1:2; 1:2.5 and 1:3 to study the influence of metal-ligand ratio of the crystallinity and morphology of ZIF-8 that was produced. The results of characterization by X-ray diffraction, FTIR and SEM show that ZIF-8 is synthesized with a ratio of m
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Nasution, Erika Linda Yani. "ANALISIS KARAKTERISASI XRD SINTESIS GADOLINIUM KARBONAT (Gd2(CO3)3@PEG DENGAN METODE SOLVOTERMAL." JOURNAL ONLINE OF PHYSICS 5, no. 1 (2019): 29–32. http://dx.doi.org/10.22437/jop.v5i1.8213.

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Abstrak
 Telah dilakukan sintesis partikel pegilasi gadolinium karbonat dengan metode solvotermal menggunakan prekursor polietilen glikol (PEG-1000) dan gadolinium asetat hidrat (Gd(CH3CO3)3) pada suhu 180oC dengan waktu pemanasan selama 3 jam, 5 jam, dan 7 Jam. Partikel pegilasi gadolinium karbonat (Gd2(CO3)3@PEG tersebut selanjutnya dianalisis pola difraksi dan bentuk struktur dengan menggunakan X-Ray Diffraction (XRD). Hasil karakterisasi spektrum XRD terhadap partikel Gd2(CO3)3 menunjukkan pila difraksi dengan posisi puncak-puncak difraksi bersesuaian dengan JCPDS No. 37-0559 dengan p
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Putri, Yulia Eka, Merida Saputri, Rahmadhini Anwar, et al. "Peran Capping Agent terhadap Morfologi SrTiO3 Bulat Berongga yang Terbentuk dari Susunan Nanokubus melalui Metode Solvotermal." Jurnal Kimia Valensi 5, no. 1 (2019): 124–32. http://dx.doi.org/10.15408/jkv.v5i1.9972.

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SrTiO3 bulat berongga yang tersusun dari nano kubus telah disintesis dengan penambahan cetyltrimethylammonium bromide (CTAB) sebagai capping agent untuk mengontrol morfologi partikel. Kondisi sintesis pada suhu 220 °C selama 48 jam dengan perbandingan mol Sr:Ti = 1:1.25 dan perbandingan material awal dengan CTAB adalah 1:0.5 menghasilkan partikel dengan kristalinitas yang tinggi pada puncak spesifik 2θ = 32.41o bidang 110 yang merujuk pada struktur perovskit kubus. Penghalusan struktur kristal dengan metoda Rietveld menunjukkan bahwa struktur kristal hasil pengukuran memiliki kecocokan yang ti
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Alifah, Miratul, Vika Ayu Devianti, Amirul Mukminin, Yulia Rachmawati, Muhammad Ainul Fahmi, and Ratna Ediati. "The Effect of KOH Activation in Synthesis and Characterization of Zeolitic Imidazolate Frameworks-8 (ZIF-8) Templated Mesoporous Carbon." Advanced Materials Research 1123 (August 2015): 78–83. http://dx.doi.org/10.4028/www.scientific.net/amr.1123.78.

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ZIF - 8 material has been successfully synthesized through a reaction between zinc nitrate hexahydrate with 2 - metilimidazol in the dimethylformamide solvent in solvotermal condition. Synthesis process is carried out at 120oC for 24 hours . The results show that the characterization by XRD diffractogram synthesized ZIF - 8 has a characteristic peak at 2θ = 7.4o; 12.7o; 16.5oand 18.0ocorresponding to the characteristic peaks of ZIF - 8 standard . The results of ZIF - 8 templated carbon show the XRD pattern of amorphous carbon material, while the carbon activated KOH show peak K2CO3at 2θ = 31.6
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Oliveira, Roberta, Raphael Pereira, Rodrigo Viana, Severino Alves, and Mônica Belian. "UMA ROTA ALTERNATIVA PARA OBTENÇÃO DE REDES DE COORDENAÇÃO VIA SÍNTESE SOLVOTERMAL UTILIZANDO Eu2O3 E ÁCIDO 2,6-NAFTALENODICARBOXÍLICO." Química Nova, 2022. http://dx.doi.org/10.21577/0100-4042.20170863.

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AN ALTERNATIVE ROUTE TO OBTAIN METAL-ORGANIC FRAMEWORKS VIA SOLVOTHERMAL SYNTHESIS USING Eu2O3 AND 2,6-NAPHTHALENODICARBOXYLIC ACID. An alternative route to synthesis of metal-organic frameworks containing Eu(III) ion was proposed via solvothermal process in aqueous medium. The compounds of the minimal formulae [Ln2(NDC)3(H2O)4] were synthesized starting from the mixture of the 2,6-naphthalenedicarboxylic acid with europium(III) oxide. So far, this type of metalorganic framework based on the lanthanide ion synthetic route has not been investigated before as the main metal sources are nitrate a
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Dissertations / Theses on the topic "Solvotermal synthesis"

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Ivanisenko, V. V., and V. V. Sirota. "Structure and Properties of Ceramics Based on ZrO2, Synthesis by Solvotermal Method." Thesis, Sumy State University, 2012. http://essuir.sumdu.edu.ua/handle/123456789/35091.

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Nanosized powders ZrO2-NiO with a particle size of 10 – 20 nm were obtained by the method of solvotermal synthesis. It is shown that the processes of formation of nanoparticles of c(t)-ZrO2 and m-ZrO2 at the given parameters of solvotermal synthesis take place at different speeds. Ceramic material based on nanosized powders of ZrO2 was obtained by the cold isostatic pressing and further sintering. The microstructure, phase composition and strength properties of ceramics were determined by the scanning electron microscopy (SEM), transmission electron microscopy (TEM) with diffraction, X-ra
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Salimian, Maryam. "Advances in multifunctional nickel/reduced graphene oxide nanocomposites, synthesis and characterization." Doctoral thesis, Universidade de Aveiro, 2018. http://hdl.handle.net/10773/23709.

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Doutoramento em Engenharia Mecânica<br>O grafeno é constituído por uma monocamada de átomos de carbono dispostos numa espécie de rede hexagonal perfeita. Devido às suas propriedades extraordinárias, este nanomaterial tem suscitado um grande interesse tanto no setor científico como no industrial. A este respeito, a investigação em torno do grafeno mostrou um aumento exponencial em áreas tão diferentes como a energia, biomedicina, eletrónica, entre outras. O óxido de grafeno (GO), um dos derivados de grafeno, foi considerado como um substrato interessante para o desenvolvimento de nanocomposito
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