Artículos de revistas: "Fluorofor"

1

Champion, J. P. y G. Graner. "Fluoroform". Molecular Physics 58, n.º 3 (20 de junio de 1986): 475–84. http://dx.doi.org/10.1080/00268978600101301.

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2

Chai, Jin Young, Hyojin Cha, Sung-Sik Lee, Young-Ho Oh, Sungyul Lee y Dae Yoon Chi. "Mechanistic study of nucleophilic fluorination for the synthesis of fluorine-18 labeled fluoroform with high molar activity from N-difluoromethyltriazolium triflate". RSC Advances 11, n.º 11 (2021): 6099–106. http://dx.doi.org/10.1039/d0ra09827b.

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Route a: desired S_N2 reaction of fluoride to form fluoroform with high molar activity; route b: side reaction to form methyl fluoride; route c: side reaction to form difluorocarbene to give fluoroform with lower molar activity.

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3

Kyasa, ShivaKumar. "Fluoroform (CHF3)". Synlett 26, n.º 13 (11 de junio de 2015): 1911–12. http://dx.doi.org/10.1055/s-0034-1380924.

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4

Punna, Nagender, Takuya Saito, Mikhail Kosobokov, Etsuko Tokunaga, Yuji Sumii y Norio Shibata. "Stereodivergent trifluoromethylation of N-sulfinylimines by fluoroform with either organic-superbase or organometallic-base". Chemical Communications 54, n.º 34 (2018): 4294–97. http://dx.doi.org/10.1039/c8cc01526k.

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5

Miloserdov, Fedor M. y Vladimir V. Grushin. "Alcoholysis of fluoroform". Journal of Fluorine Chemistry 167 (noviembre de 2014): 105–9. http://dx.doi.org/10.1016/j.jfluchem.2014.06.006.

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6

Fujihira, Yamato, Yumeng Liang, Makoto Ono, Kazuki Hirano, Takumi Kagawa y Norio Shibata. "Synthesis of trifluoromethyl ketones by nucleophilic trifluoromethylation of esters under a fluoroform/KHMDS/triglyme system". Beilstein Journal of Organic Chemistry 17 (12 de febrero de 2021): 431–38. http://dx.doi.org/10.3762/bjoc.17.39.

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A straightforward method that enables the formation of biologically attractive trifluoromethyl ketones from readily available methyl esters using the potent greenhouse gas fluoroform (HCF3, HFC-23) was developed. The combination of fluoroform and KHMDS in triglyme at −40 °C was effective for this transformation, with good yields as high as 92%. Substrate scope of the trifluoromethylation procedure was explored for aromatic, aliphatic, and conjugated methyl esters. This study presents a straightforward trifluoromethylation process of various methyl esters that convert well to the corresponding trifluoromethyl ketones. The tolerance of various pharmacophores under the reaction conditions was also explored.

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7

Carbonnel, Elodie, Tatiana Besset, Thomas Poisson, Daniel Labar, Xavier Pannecoucke y Philippe Jubault. "18F-Fluoroform: a 18F-trifluoromethylating agent for the synthesis of SCF218F-aromatic derivatives". Chemical Communications 53, n.º 42 (2017): 5706–9. http://dx.doi.org/10.1039/c7cc02652h.

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8

Berdybaeva, Sh T., E. N. Telminov, T. A. Solodova y E. N. Nikonova. "Influence of solvents on generational characteristics and sensitivity of optical integral chemical sesnors". Izvestiya vysshikh uchebnykh zavedenii. Fizika, n.º 11 (2021): 151–54. http://dx.doi.org/10.17223/00213411/64/11/151.

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Sensor properties poly[9,9-dioctylfluorenyl-2,7-diyl] - end capped with dimethylphenyl - (ADS129) on the nitrotoluens vapor were studied. Sensor properties of the fluorophor dissolved in the different solvents were investigated in the laser mode due to complex formation between fluorophor and nitrotoluene molecules.

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9

Bao, Junwei Lucas, Xin Zhang y Donald G. Truhlar. "Predicting pressure-dependent unimolecular rate constants using variational transition state theory with multidimensional tunneling combined with system-specific quantum RRK theory: a definitive test for fluoroform dissociation". Physical Chemistry Chemical Physics 18, n.º 25 (2016): 16659–70. http://dx.doi.org/10.1039/c6cp02765b.

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10

Ma, Qiao y Gavin Chit Tsui. "Trifluoromethylation of α-diazoesters and α-diazoketones with fluoroform-derived CuCF3: synergistic effects of co-solvent and pyridine as a promoter". Organic Chemistry Frontiers 6, n.º 1 (2019): 27–31. http://dx.doi.org/10.1039/c8qo00834e.

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11

Ramos-Torres, Karla M., Yu-Peng Zhou, Bo Yeun Yang, Nicolas J. Guehl, Moon Sung-Hyun, Sanjay Telu, Marc D. Normandin, Victor W. Pike y Pedro Brugarolas. "Syntheses of [11C]2- and [11C]3-trifluoromethyl-4-aminopyridine: potential PET radioligands for demyelinating diseases". RSC Medicinal Chemistry 11, n.º 10 (2020): 1161–67. http://dx.doi.org/10.1039/d0md00190b.

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12

Zanardi, Alessandro, Maxim A. Novikov, Eddy Martin, Jordi Benet-Buchholz y Vladimir V. Grushin. "Direct Cupration of Fluoroform". Journal of the American Chemical Society 133, n.º 51 (28 de diciembre de 2011): 20901–13. http://dx.doi.org/10.1021/ja2081026.

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13

Torrie, B. H., O. S. Binbrek y B. M. Powell. "Structure of solid fluoroform". Molecular Physics 87, n.º 5 (10 de abril de 1996): 1007–13. http://dx.doi.org/10.1080/00268979600100691.

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14

Köckinger, Manuel, Tanja Ciaglia, Michael Bersier, Paul Hanselmann, Bernhard Gutmann y C. Oliver Kappe. "Utilization of fluoroform for difluoromethylation in continuous flow: a concise synthesis of α-difluoromethyl-amino acids". Green Chemistry 20, n.º 1 (2018): 108–12. http://dx.doi.org/10.1039/c7gc02913f.

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Difluoromethylated esters, malonates and amino acids (including the drug eflornithine) are obtained by a gas–liquid continuous flow protocol employing the abundant waste product fluoroform as an atom-efficient reagent.

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15

Geri, Jacob B. y Nathaniel K. Szymczak. "Recyclable Trifluoromethylation Reagents from Fluoroform". Journal of the American Chemical Society 139, n.º 29 (13 de julio de 2017): 9811–14. http://dx.doi.org/10.1021/jacs.7b05408.

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16

Bocquet, R., D. Boucher, W. D. Chen, J. Cosleou y J. Demaison. "The Submillimeterwave Spectrum of Fluoroform". Journal of Molecular Spectroscopy 158, n.º 2 (abril de 1993): 494–96. http://dx.doi.org/10.1006/jmsp.1993.1096.

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17

Kohls, Emilija, Anastas Mishev y Ljupčo Pejov. "Solvation of fluoroform and fluoroform–dimethylether dimer in liquid krypton: A theoretical cryospectroscopic study". Journal of Chemical Physics 139, n.º 5 (7 de agosto de 2013): 054504. http://dx.doi.org/10.1063/1.4816282.

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18

Lang, E. W., F. X. Prielmeier, H. Radkowitsch y H. D. Lüdemann. "High Pressure NMR Study of the Molecular Dynamics of Liquid Fluoroform and Deutero-Fluoroform". Berichte der Bunsengesellschaft für physikalische Chemie 91, n.º 10 (octubre de 1987): 1025–33. http://dx.doi.org/10.1002/bbpc.19870911010.

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19

Yoo, Wesley J. y Larry T. Taylor. "Supercritical Fluid Extraction of Polychlorinated Biphenyls and Organochlorine Pesticides from Freeze-Dried Tissue of Marine Mussel, Mytilus eduli". Journal of AOAC INTERNATIONAL 80, n.º 6 (1 de noviembre de 1997): 1336–46. http://dx.doi.org/10.1093/jaoac/80.6.1336.

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Abstract Supercritical fluid extractions (SFEs) of 21 polychlorinated biphenyls (PCBs) and 8 organochlorine pesticides (OCPs) from freeze-dried mussel tissue are compared with traditional Soxhlet extractions. The aim was to determine the efficacy of supercritical CO2 to extract these 2 classes of lipophilic compounds. A spike study to determine the feasibility of on-line cleanup by inclusion of an inert matrix (activated alumina) in the extraction vessel showed that the chemical integrity of the PCBs was not compromised, whereas some DDTs were decomposed to their respective metabolites. Relatively long static extraction time, higher density, and lower temperature yielded quantitative recoveries of PCBs from freeze-dried mussel tissue with good reproducibilities. Recoveries of OCPs were nonquantitative and highly variable. Finally, the efficacy of fluoroform (CHF3) as an alternative supercritical fluid to selectively extract PCBs and OCPs was studied. Fluoroform yielded nonquantitative and variable recoveries of PCBs and OCPs, but its use eliminated the need for in situ alumina to retain coextracted lipids from the matrix.

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20

Chen, Zhan, Xiao-Ke Liu, Cai-Jun Zheng, Jun Ye, Xin-Yang Li, Fan Li, Xue-Mei Ou y Xiao-Hong Zhang. "A high-efficiency hybrid white organic light-emitting diode enabled by a new blue fluorophor". Journal of Materials Chemistry C 3, n.º 17 (2015): 4283–89. http://dx.doi.org/10.1039/c5tc00285k.

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21

Okusu, Satoshi, Etsuko Tokunaga y Norio Shibata. "Difluoromethylation of Terminal Alkynes by Fluoroform". Organic Letters 17, n.º 15 (16 de julio de 2015): 3802–5. http://dx.doi.org/10.1021/acs.orglett.5b01778.

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22

Zhang, Yuan, Motohiro Fujiu, Hiroki Serizawa y Koichi Mikami. "Organocatalysis approach to trifluoromethylation with fluoroform". Journal of Fluorine Chemistry 156 (diciembre de 2013): 367–71. http://dx.doi.org/10.1016/j.jfluchem.2013.07.018.

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23

Mori, Toshiaki, Yuri Tsuchiya y Yoshio Okahata. "Polymerizations of Tetrafluoroethylene in Homogeneous Supercritical Fluoroform and in Detergent-Free Heterogeneous Emulsion of Supercritical Fluoroform/Water". Macromolecules 39, n.º 2 (enero de 2006): 604–8. http://dx.doi.org/10.1021/ma051930b.

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24

Maruyama, Kenichi, Daichi Saito y Koichi Mikami. "(Sila)Difluoromethylation of Fluorenyllithium with CF3H and CF3TMS". SynOpen 02, n.º 03 (julio de 2018): 0234–39. http://dx.doi.org/10.1055/s-0037-1610361.

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Difluoromethylation of the C9-H site of the fluorene ring using lithium base and fluoroform (CF3H), which is one of the most cost-effective difluoromethylating reagents, is attained to give difluoromethylated fluorenes with an all-carbon quaternary center. The Ruppert–Prakash reagent (CF3TMS) can also be applied to the present reaction system, providing siladifluoromethylated fluorenes that can be utilized for sequential carbon–carbon bond-forming reactions through activation of the silyl group.

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25

Yang, Xinkan, Lisi He y Gavin Chit Tsui. "Hydroxytrifluoromethylation of Alkenes Using Fluoroform-Derived CuCF3". Organic Letters 19, n.º 9 (25 de abril de 2017): 2446–49. http://dx.doi.org/10.1021/acs.orglett.7b01085.

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26

Ingrosso, Francesca, Branka M. Ladanyi, Benedetta Mennucci y Giovanni Scalmani. "Solvation of Coumarin 153 in Supercritical Fluoroform". Journal of Physical Chemistry B 110, n.º 10 (marzo de 2006): 4953–62. http://dx.doi.org/10.1021/jp056226b.

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27

Carlotti, M., G. Di Lonardo, L. Fusina, A. Trombetti y B. Carli. "The far-infrared spectrum of fluoroform (CHF3)". Journal of Molecular Spectroscopy 123, n.º 1 (mayo de 1987): 135–44. http://dx.doi.org/10.1016/0022-2852(87)90266-9.

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28

Silva, Kélio Garcia, Denise Pedrini, Alberto Carlos Botazzo Delbem y Mark Cannon. "Microhardness and fluoride release of restorative materials in different storage media". Brazilian Dental Journal 18, n.º 4 (2007): 309–13. http://dx.doi.org/10.1590/s0103-64402007000400007.

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This study evaluated the surface microhardness and fluoride release of 5 restorative materials - Ketac-Fil Plus, Vitremer, Fuji II LC, Freedom and Fluorofil - in two storage media: distilled/deionized water and a pH-cycling (pH 4.6). Twelve specimens of each material, were fabricated and the initial surface microhardness (ISM) was determined in a Shimadzu HMV-2000 microhardness tester (static load Knoop). The specimens were submitted to 6- or 18-h cycles in the tested media. The solutions were refreshed at the end of each cycle. All solutions were stored for further analysis. After 15-day storage, the final surface microhardness (FSM) and fluoride release were measured. Fluoride dose was measured with a fluoride-specific electrode (Orion 9609-BN) and digital ion analyzer (Orion 720 A). The variables ISM, FSM and fluoride release were analyzed statistically by analysis of variance and Tukey's test (p<0.05). There was significant difference in FSM between the storage media for Vitremer (pH 4.6 = 40.2 ± 1.5; water = 42.6 ± 1.4), Ketac-Fil Plus (pH 4.6 = 73.4 ± 2.7; water = 58.2 ± 1.3) and Fluorofil (pH 4.6 = 44.3 ± 1.8; water = 38.4 ± 1.0). Ketac-Fil Plus (9.9 ± 18.0) and Fluorofil (4.4 ± 1.3) presented higher fluoride release in water, whereas Vitremer (7.4 ± 7.1), Fuji II LC (5.7 ± 4.7) and Freedom (2.1 ± 1.7) had higher fluoride release at pH 4.6. Microhardness and fluoride release of the tested restorative materials varied according to the storage medium.

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29

Zhang, Cai. "Application of fluoroform in trifluoromethylation and diﬂuoromethylation reactions". Arkivoc 2017, n.º 1 (12 de marzo de 2017): 67–83. http://dx.doi.org/10.24820/ark.5550190.p009.884.

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30

Song, W., N. Patel y M. Maroncelli. "A 2-Site Model for Simulating Supercritical Fluoroform". Journal of Physical Chemistry B 106, n.º 34 (agosto de 2002): 8783–89. http://dx.doi.org/10.1021/jp021079s.

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31

Närger, U., J. R. de Bruyn, M. Stein y D. A. Balzarini. "Coexistence curve of fluoroform near its critical point". Physical Review B 39, n.º 16 (1 de junio de 1989): 11914–19. http://dx.doi.org/10.1103/physrevb.39.11914.

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32

Russell, Jamie y Nicolas Roques. "Effective nucleophilic trifluoromethylation with fluoroform and common base". Tetrahedron 54, n.º 45 (noviembre de 1998): 13771–82. http://dx.doi.org/10.1016/s0040-4020(98)00846-1.

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33

Wynne, Dolores C. y Philip G. Jessop. "Cyclopropanation Enantioselectivity Is Pressure Dependent in Supercritical Fluoroform". Angewandte Chemie International Edition 38, n.º 8 (19 de abril de 1999): 1143–44. http://dx.doi.org/10.1002/(sici)1521-3773(19990419)38:8<1143::aid-anie1143>3.0.co;2-y.

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34

Zhang, Yuan, Motohiro Fujiu, Hiroki Serizawa y Koichi Mikami. "ChemInform Abstract: Organocatalysis Approach to Trifluoromethylation with Fluoroform." ChemInform 45, n.º 18 (17 de abril de 2014): no. http://dx.doi.org/10.1002/chin.201418042.

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35

Kometani, Noritsugu, Yuji Hoshihara, Yoshiro Yonezawa, Okitsugu Kajimoto, Kimihiko Hara y Naoki Ito. "Rotational Dynamics of Coumarin 153 in Supercritical Fluoroform". Journal of Physical Chemistry A 108, n.º 44 (noviembre de 2004): 9479–83. http://dx.doi.org/10.1021/jp047854g.

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36

Corbett, P., A. Tarr y E. Whittle. "The Vapour Phase Brominations of Fluoroform and Methane". Bulletin des Sociétés Chimiques Belges 71, n.º 11-12 (2 de septiembre de 2010): 778–79. http://dx.doi.org/10.1002/bscb.19620711127.

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37

Fourrier, M. y M. Redon. "A new CW FIR lasing medium: Methyl fluoroform". Optics Communications 64, n.º 6 (diciembre de 1987): 534–36. http://dx.doi.org/10.1016/0030-4018(87)90284-7.

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38

Okusu, Satoshi, Etsuko Tokunaga y Norio Shibata. "ChemInform Abstract: Difluoromethylation of Terminal Alkynes by Fluoroform." ChemInform 46, n.º 52 (diciembre de 2015): no. http://dx.doi.org/10.1002/chin.201552065.

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39

Sharma, Gitanjali, David Turton, Graham Smith, Philip Miller y Gabriela Kramer-Marek. "[18F]Fluoroform radiolabelling of the CHK1 inhibitor CCT245737". Nuclear Medicine and Biology 96-97 (mayo de 2021): S48—S49. http://dx.doi.org/10.1016/s0969-8051(21)00343-7.

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40

Rasu, Loorthuraja, Ben Rennie, Mark Miskolzie y Steven H. Bergens. "A Fortuitous, Mild Catalytic Carbon–Carbon Bond Hydrogenolysis by a Phosphine-Free Catalyst". Australian Journal of Chemistry 69, n.º 5 (2016): 561. http://dx.doi.org/10.1071/ch15792.

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The putative catalyst trans-[Ru((S,S)-skewphos)(H)2((R,R)-dpen)] (skewphos = 2,4-bis(diphenylphosphino)pentane; dpen = 1,2-diphenylethylenediamine) transforms the trifluoroacetyl amide 2,2,2-trifluoro-1-(piperidin-1-yl)ethanone under mild conditions (4 atm H2, room temperature, 4–24 h, 1 mol-% Ru, 15 mol-% KOtBu in tetrahydrofuran) to generate the formylated amine 1-formylpiperidine and fluoroform via C–C bond hydrogenolysis. Catalysts are also prepared by reacting cis-[Ru(η3-C3H5)(MeCN)2(COD)]BF4 (COD = 1,5-cyclooctadiene) with diamine ligands in situ. Low-temperature NMR studies provided insight into this reaction.

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41

Меликова, С. М., К. С. Рутковский, Д. Н. Щепкин, С. Махолл y В. Херребут. "Криоспектроскопическое исследование резонансных мультиплетов ν-=SUB=-s-=/SUB=- ~2ν-=SUB=-b-=/SUB=- в молекуле CHF-=SUB=-3-=/SUB=-". Оптика и спектроскопия 129, n.º 8 (2021): 1019. http://dx.doi.org/10.21883/os.2021.08.51197.2002-21.

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The sequences of Fermi resonances vs~2vb in the IR spectrum of a solution of fluoroform (CHF3) in liquefied krypton are investigated. Here vs is the CH stretching vibration, vb is the bending vibration. It is shown that for a correct description of resonance multiplets (polyads) at a high degree of vibrational excitation, it is necessary to use an extended set of spectroscopic parameters. In particular, it is necessary to take into account the dependence of the anharmonic interaction constant asbb on the vibrational quantum numbers. The conclusions are generalized for the arbitrary case of the CH-chromophore CHX3.

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42

Folléas, Benoît, Ilan Marek, Jean-F. Normant y Laurent Saint Jalmes. "Fluoroform: an efficient precursor for the trifluoromethylation of aldehydes". Tetrahedron Letters 39, n.º 19 (mayo de 1998): 2973–76. http://dx.doi.org/10.1016/s0040-4039(98)00391-8.

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43

Parsons, Drew F., Bradley I. Boone, Philip G. Jessop y Susan C. Tucker. "Electrostriction effects on competing transition states in supercritical fluoroform". Journal of Supercritical Fluids 24, n.º 2 (noviembre de 2002): 173–81. http://dx.doi.org/10.1016/s0896-8446(02)00032-3.

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44

He, Lisi, Xinkan Yang y Gavin Chit Tsui. "Domino Hydroboration/Trifluoromethylation of Alkynes Using Fluoroform-Derived [CuCF3]". Journal of Organic Chemistry 82, n.º 12 (31 de mayo de 2017): 6192–201. http://dx.doi.org/10.1021/acs.joc.7b00755.

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45

Chabinyc, Michael L. y John I. Brauman. "Unusual Ionic Hydrogen Bonds: Complexes of Acetylides and Fluoroform". Journal of the American Chemical Society 122, n.º 36 (septiembre de 2000): 8739–45. http://dx.doi.org/10.1021/ja000806z.

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46

Potash, Shay y Shlomo Rozen. "General Synthesis of Trifluoromethyl Selenides Utilizing Selenocyanates and Fluoroform". Journal of Organic Chemistry 79, n.º 22 (12 de noviembre de 2014): 11205–8. http://dx.doi.org/10.1021/jo5022844.

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47

Folléas, Benoı̂t, Ilan Marek, Jean-F. Normant y Laurent Saint-Jalmes. "Fluoroform: an Efficient Precursor for the Trifluoromethylation of Aldehydes". Tetrahedron 56, n.º 2 (enero de 2000): 275–83. http://dx.doi.org/10.1016/s0040-4020(99)00951-5.

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48

Wynne, Dolores C. y Philip G. Jessop. "Druckabhängigkeit der Enantioselektivität bei der Cyclopropanierung in überkritischem Fluoroform". Angewandte Chemie 111, n.º 8 (19 de abril de 1999): 1213–15. http://dx.doi.org/10.1002/(sici)1521-3757(19990419)111:8<1213::aid-ange1213>3.0.co;2-c.

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49

Pees, Anna, Albert D. Windhorst, Maria J. W. D. Vosjan, Vincent Tadino y Danielle J. Vugts. "Synthesis of [18 F]Fluoroform with High Molar Activity". European Journal of Organic Chemistry 2020, n.º 9 (25 de febrero de 2020): 1177–85. http://dx.doi.org/10.1002/ejoc.202000056.

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50

Reimann, Bernd, Konstantin Buchhold, Sascha Vaupel, Bernhard Brutschy, Zdeněk Havlas, Vladimír Špirko y Pavel Hobza. "Improper, Blue-Shifting Hydrogen Bond between Fluorobenzene and Fluoroform†". Journal of Physical Chemistry A 105, n.º 23 (junio de 2001): 5560–66. http://dx.doi.org/10.1021/jp003726q.

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Artículos de revistas sobre el tema "Fluorofor"

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