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1

Shpekina, Varvara I., Vasiliy A. Korotkov, and Nina D. Solovyova. "Electrodeposition of lead dioxide on titanium substrate." Electrochemical Energetics 21, no. 4 (2021): 191–96. http://dx.doi.org/10.18500/1608-4039-2021-21-4-191-196.

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Modern technology causes the renewal of the interest to physical and chemical properties of solid oxide electrodes. Among these, PbO2/substrate has attracted considerable attention due to its application as an electrode in backup current sources. It was shown that the stable and active lead dioxide coating can be produced by appropriate pretreatment of the titanium substrate, including the coating of the substrate with colloidal graphite.
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2

Greco, Giuseppe, Alessandra Moncada, Carmelo Sunseri, and Rosalinda Inguanta. "Behavior Modification of Nanostructured PbO2 Electrodes in Lead Acid Batteries Changing Electrolyte Concentration and Separator." Journal of Nanoscience and Nanotechnology 19, no. 11 (2019): 7398–403. http://dx.doi.org/10.1166/jnn.2019.16603.

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Currently, lead acid battery is extensively investigated owing to its prevalent use as a startinglighting and ignition device. An essential role for electrochemical reactions is played by the surface area available for conversion reactions and a possible approach is the use of nanostructured electrodes. In this work, lead dioxide nanostructured electrodes were tested in order to investigate the dependence of the charge and discharge behaviour on some parameters such as electrolyte concentration, and a new type of thin separator. In this last case, it is possible to reduce the size of the cell
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3

Bernardi, Dawn M. "Nucleation of Lead Sulfate in Porous Lead‐Dioxide Electrodes." Journal of The Electrochemical Society 137, no. 6 (1990): 1670–81. http://dx.doi.org/10.1149/1.2086769.

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4

LEE, Joon-Woo, Yoon Sun LEE, and In-Hyeong YEO. "Analytical Applications of Modified Lead Dioxide Electrodes." Analytical Sciences 13, Supplement (1997): 273–78. http://dx.doi.org/10.2116/analsci.13.supplement_273.

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5

Yang, Xiao Yong, Pei Xian Zhu, and Yun Sen Si. "Preparation and Application of Lead Dioxide Electrode for Zinc Electrolysis." Advanced Materials Research 785-786 (September 2013): 1125–29. http://dx.doi.org/10.4028/www.scientific.net/amr.785-786.1125.

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According to the process of anodic oxygen evolution in sulfate system for zinc electrolysis,Ti-base lead dioxide electrode can be prepared to use in this case.The surface characterization of the electrode was studied by Scanning electron microscopy(SEM) and X-ray diffraction(XRD).The electrode lifetime was tested in 1mol/L H2SO4solution at 60°C,and the electro-catalytic properties was examined by polarization curves.Then these samples was enlarged and simulation test was conducted at Mengzi marriage zinc smelter in Yunnan.The results show that the electro-catalytic properties is better and the
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6

Cheraghveisi, Meysam, Bozorgmehr Maddah, and Mostafa Najafi. "Electrosynthesis of perchlorate using neodymium-doped PbO 2 electrode: application of experimental design methodology for optimization of the effective parameters." Materials Research Express 9, no. 2 (2022): 025801. http://dx.doi.org/10.1088/2053-1591/ac5551.

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Abstract In recent decades, extensive research has been done on substrates (i.e., titanium and carbon) with lead dioxide coating to design a cheap anode in electrochemical systems instead of a platinized (Pt) electrode. Various factors can affect the structure and catalytic activity of lead dioxide coating. The most important of them are the type of substrate, how to prepare the substrate for the coating process and the types of lead dioxide additives. In this work, the effective factors in the preparation of the substrate were first investigated. Subsequently, the effect of neodymium as an ad
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7

Amadelli, Rossano, and A. B. Velichenko. "Lead dioxide electrodes for high potential anodic processes." Journal of the Serbian Chemical Society 66, no. 11-12 (2001): 835–45. http://dx.doi.org/10.2298/jsc0112835a.

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Doping of PbO2 by cations (Fe3+, Co2+ and Ni2+), by F- and by cations and F- simultaneously is discussed as a way of improving the stability and electrochemical activity in processes occurring at high potentials. Doping allows the control of the amount of structural water in an oxide. Radiotracer experiments showed that high electrodeposition current densities favour the segregation of incorporated tritium (protons) at the surface. On the other hand, fluorine doping results in a marked decrease in the amount of surface oxygen species. The influence of doping with metal cations strongly depends
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8

Kadnikova, N. V., M. M. Burashnikova, I. V. Zotova, M. A. Shishova, T. A. Lutskova, and I. A. Kazarinov. "Oxygen and hydrogen ionization on the working electrodes of the lead-acid battery." Electrochemical Energetics 9, no. 4 (2009): 199–208. http://dx.doi.org/10.18500/1608-4039-2009-9-4-199-208.

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Some useful characteristics of the separators from glass-absorptive matrices produced by several manufacturers and intended for valve-regulated lead-acid batteries were studied, namely, compressibility, electrolyte capacity, capillary rise speed, oxygen absorption rate on the lead electrode, and hydrogen absorption rate on the lead-dioxide one. The usage of these separators provides forced pumping of the gases released (oxygen and hydrogen) to the absorptive electrode's pores and allows the oxygen and hydrogen ionization rates to be raised.
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9

Pablos, C., R. van Grieken, J. Marugán, C. Adán, M. Osuna, and J. Palma. "Photoelectrocatalytic study and scaling up of titanium dioxide electrodes for wastewater treatment." Water Science and Technology 68, no. 5 (2013): 999–1003. http://dx.doi.org/10.2166/wst.2013.307.

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Different TiO2 photoelectrodes have been characterized and tested for the photoelectrocatalytic oxidation of methanol. Particulate electrodes (TiO2/Ti and TiO2/ITO) have been shown to notably favour charge-carrier transfer at the electrolyte interface while a thermal electrode (Ti) has been shown to favour charge-carrier separation when applying an electric potential bias according to cyclic voltammetry technique, as a consequence of differences in TiO2 surface between particulate and thermal electrodes. Particulate electrodes lead to a higher photoelectrocatalytic activity for methanol oxidat
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10

Verlotskii, A. A., I. P. Rublevskii, V. P. Frolova, et al. "Action of lead-glass melts on tin-dioxide electrodes." Glass and Ceramics 44, no. 2 (1987): 57–60. http://dx.doi.org/10.1007/bf00701104.

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11

Landfors, Johan. "Cycle life test of lead dioxide electrodes in compressed Lead/acid cells." Journal of Power Sources 52, no. 1 (1994): 99–108. http://dx.doi.org/10.1016/0378-7753(94)01944-4.

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12

Douard, Camille, Laurence Athouël, David Brown, et al. "Electrode Design for MnO2-Based Aqueous Electrochemical Capacitors: Influence of Porosity and Mass Loading." Materials 14, no. 11 (2021): 2990. http://dx.doi.org/10.3390/ma14112990.

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The purpose of this study is to highlight the influence of some fabrication parameters, such as mass loading and porosity, which are not really elucidated and standardized during the realization of electrodes for supercapacitors, especially when using metal oxides as electrode materials. Electrode calendering, as one stage during the fabrication of electrodes, was carried out step-by-step on manganese dioxide electrodes to study the decreasing porosity effect on the electrochemical performance of a MnO2 symmetric device. One other crucial parameter, the mass loading, which has to be understood
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13

Menon, Sananth H., G. Madhu, and J. Mathew. "Compact Flow-Through Electrochemical Cell - A Novel Perspective in Industrial Manufacture of Perchlorates." Open Chemical Engineering Journal 13, no. 1 (2019): 23–32. http://dx.doi.org/10.2174/1874123101913010023.

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Background: Sodium Perchlorate is one of the major starting intermediate product for the manufacture of various Perchlorates viz, Ammonium perchlorate as solid oxidizer and Strontium Perchlorate as Secondary Injection Thrust Vector Control (SITVC) in launch vehicles. This critical product is manufactured industrially by electrochemical oxidation of Sodium Chlorate solution at the anodic surface. Lead dioxide is preferred in various perchlorate cells because of its low cost. Infrequent detachment of Lead dioxide deposits from the substrate during electrolysis is a grave issue confronted by asso
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14

Shmychkova, Olesia, Tatiana Luk’yanenko, Larisa Dmirtikova, and Alexander Velichenko. "Modified lead dioxide for organic wastewater treatment: Physicochemical properties and electrocatalytic activity." Journal of the Serbian Chemical Society 84, no. 2 (2019): 187–98. http://dx.doi.org/10.2298/jsc180712091s.

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An investigation is reported on lead dioxide electrodeposition from methanesulfonate electrolytes additionally containing Ni2+ ions. It is shown that lead dioxide electrodes micromodified by nickel have different physico-chemical properties vs. nonmodified PbO2-anodes that are formed during the deposition. Electrocatalytical reactivity of electrodes involved in comparison to both the oxygen evolution, as well as to the electrooxidation of 2,4- dichlorophenoxyacetic (2,4-D) acid is investigated. Processes of electrochemical oxidation of 2,4-D on various materials occur qualitatively with the sa
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15

Sivasubramanian, M., J. Vignesh, V. Senthil kumar, et al. "An Innovative Solution for Battery Draining in 5G Devices Using Alternate Routing Model." International Transactions on Electrical Energy Systems 2022 (September 29, 2022): 1–8. http://dx.doi.org/10.1155/2022/8924801.

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When the electrolyte is layered, excessively large and prolonged charging and exhaust currents lead to the random tendency of reactions in different parts of the electrodes. This was leading to mechanical stresses and the warming of the plates of the battery. The presence of nitric and acetic acid contaminants in the electrolyte improves the oxidation of the deeper layers of positive electrodes. Because lead dioxide has a larger volume than lead, electrodes expand and curve. Positive electrodes are subject to war and growth. The negative electrode curve is mainly caused by the nearby distracte
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16

Chen, Lu, Qibin Tao, Lin Wang, Hao Lan, and Qizhou Dai. "CMS and Nd Co-Modified PbO2 Electrodes with Enhanced Lifetime and Electrochemical Activity for the Degradation of Bisphenol S." Journal of The Electrochemical Society 170, no. 10 (2023): 103504. http://dx.doi.org/10.1149/1945-7111/acfcdc.

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In this study, a lead dioxide electrode co-modified with carbon microspheres and neodymium (CMS-Nd-PbO2) was prepared. The structural morphology and electrochemical properties of the four electrodes, PbO2, CMS-PbO2, Nd-PbO2, and CMS-Nd-PbO2, were compared by field emission scanning electron microscopy, X-ray diffractometer, X-ray photoelectron spectroscopy, cyclic voltammetry, and electrochemical impedance, respectively. The results showed that the prepared CMS-Nd-PbO2 electrode had higher surface denseness and higher electrode activity. Based on the accelerated lifetime experiment, the actual
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17

Vorobets, Vera, Gennadii Kolbasov, Sergii Karpenko, and Svitlana Oblovatna. "DETERMINATION OF LEAD (II) AND OXYGEN CONTENT IN LIQUID MEDIUM ON TITANIUM DIOXIDE ELECTRODES MODIFIED WITH YTTRIUM." Ukrainian Chemistry Journal 90, no. 3 (2024): 33–47. https://doi.org/10.33609/2708-129x.90.3.2024.33-47.

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This work demonstrates the possibility of using the anodic stripping voltammetry me­thod on electrodes based on nanocrystalline thin films of yttrium-modified titanium dioxi­de to determine the content of lead (II) and, at the same time, oxygen in their joint presence in liquids, which is an urgent task in the development of multisensors toxic substances and oxygen in liquid media. Lead was determined by anodic potential scanning after preliminary electroconcentration of the electrode in the electrolyte solution containing Pb(II) ions; oxygen was determined by cathodic potential scanning. The
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18

Das, Kaushik, and Aparesh Mondal. "Studies on a lead–acid cell with electrodeposited lead and lead dioxide electrodes on carbon." Journal of Power Sources 89, no. 1 (2000): 112–16. http://dx.doi.org/10.1016/s0378-7753(00)00384-0.

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19

Yeo, In‐Hyeong, Yoon Sun Lee, Sun Mho, and Dennis C. Johnson. "Electrocatalytic Oxidation of Fe/EDTA Complexes at Lead Dioxide Electrodes." Journal of The Electrochemical Society 139, no. 5 (1992): L49—L50. http://dx.doi.org/10.1149/1.2069441.

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20

Amadelli, R., L. Armelao, A. B. Velichenko, et al. "Oxygen and ozone evolution at fluoride modified lead dioxide electrodes." Electrochimica Acta 45, no. 4-5 (1999): 713–20. http://dx.doi.org/10.1016/s0013-4686(99)00250-9.

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21

Oury, Alexandre, Angel Kirchev, and Yann Bultel. "Oxygen evolution on alpha-lead dioxide electrodes in methanesulfonic acid." Electrochimica Acta 63 (February 2012): 28–36. http://dx.doi.org/10.1016/j.electacta.2011.12.028.

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22

Kabbara, Hiba, Jaafar Ghanbaja, Abdelkrim Redjaïmia та Thierry Belmonte. "Crystal structure, morphology and formation mechanism of a novel polymorph of lead dioxide, γ-PbO2". Journal of Applied Crystallography 52, № 2 (2019): 304–11. http://dx.doi.org/10.1107/s1600576719001079.

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Nanosecond-pulsed spark discharge between two lead electrodes in liquid nitrogen has been used to synthesize hexagonal lead nanosheets. These original nanostructures are collected on a substrate located under the electrodes. After the full evaporation of the liquid nitrogen, the nanosheets are oxidized in air and transform into a lead dioxide. The resulting hexagonal sheets have typical widths of around 1 µm and typical thicknesses of around 10 nm. Investigations by energy dispersive spectroscopy microanalysis, transmission electron microscopy, high-angle annular dark-field scanning transmissi
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23

Hao, Xu, Guo Wuqi, Wu Jia, Feng Jiangtao, Yang Honghui, and Yan Wei. "Preparation and characterization of titanium-based PbO2electrodes modified by ethylene glycol." RSC Advances 6, no. 9 (2016): 7610–17. http://dx.doi.org/10.1039/c5ra21195f.

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24

Thomas, J. D. R. "Ion-selective electrode and enzyme sensors for flow-type environmental analysis." Collection of Czechoslovak Chemical Communications 56, no. 1 (1991): 178–91. http://dx.doi.org/10.1135/cccc19910178.

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Illustrative examples from researches in the author’s laboratories are given of potentiometric ion-selective electrodes (ISEs) and catalytic membrane amperometric electrodes suitable for environmental analysis. The uses of sulphide ISEs are demonstrated for monitoring the activities of sulphate-reducing bacteria, in effluent analysis for sulphide, and in process/effluent analysis for sulphide, thiols and polysulphides. Diquat and paraquat ISEs are discussed in relation to their optimisation in terms of appropriate crown ether and ion-pairing agents, together with prospects of their uses. Catal
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25

Hsiao, Yun‐Lin, and Dennis C. Johnson. "Electrocatalysis of Anodic Oxygen‐Transfer Reactions: Chloride‐Doped Lead Dioxide Electrodes." Journal of The Electrochemical Society 136, no. 12 (1989): 3704–11. http://dx.doi.org/10.1149/1.2096534.

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26

Lihua, Yu, Xue Juanqin, Wang Lei, Tang Changbin, and Li Guoping. "Preparation and Characterization of [Emim]BF 4 Modified Lead Dioxide Electrodes." Rare Metal Materials and Engineering 46, no. 7 (2017): 1833–38. http://dx.doi.org/10.1016/s1875-5372(17)30175-3.

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27

Wabner, Dietrich, and Clemens Grambow. "Reactive intermediates during oxindation of water lead dioxide and platinum electrodes." Journal of Electroanalytical Chemistry and Interfacial Electrochemistry 195, no. 1 (1985): 95–108. http://dx.doi.org/10.1016/0022-0728(85)80008-5.

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28

Samet, Youssef, Lamia Agengui, and Ridha Abdelhédi. "Anodic oxidation of chlorpyrifos in aqueous solution at lead dioxide electrodes." Journal of Electroanalytical Chemistry 650, no. 1 (2010): 152–58. http://dx.doi.org/10.1016/j.jelechem.2010.08.008.

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29

Ai, Shiyun, Mengnan Gao, Wen Zhang, Zhengdong Sun, and Litong Jin. "Preparation of Fluorine-Doped Lead Dioxide Modified Electrodes for Electroanalytical Applications." Electroanalysis 15, no. 17 (2003): 1403–9. http://dx.doi.org/10.1002/elan.200302667.

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30

Aljashaam, Samiya, and Zainab T. Y. Alabdullah. "Synthesis, Characterization of Titanium Dioxide Nanotubes, and their Application as an Adsorbent for Removing of Heavy Elements." European Journal of Advanced Chemistry Research 4, no. 3 (2023): 40–44. http://dx.doi.org/10.24018/ejchem.2023.4.3.142.

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The nanotubes were prepared by anodizing method. The anodization process was carried out using 60 volts between two titanium plates as electrodes, leaving a distance between the two electrodes 6.5 cm. The electrolyte contains (0.5 w/w NH4F, 2 w/w H2O, 5 w/w ethylene glycol). A scanning electron microscope (SEM) was used to examine the surface morphology of titanium dioxide nanotubes (TiO2). The SEM image shows that the prepared tubes are in the range (80-90 nm) in diameter. titanium dioxide nanotubes (TiO2) are used as effective adsorbents for water treatment. Titanium dioxide nanotubes (TiO2)
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31

Malkar, Ashok Shankar, Mayur Anil Jaiswal, Akash Gajanan Bhagat, and Prof. Pallavi Patthe. "Design and Implementation of Lead Carbon Battery Storage System." International Journal of Ingenious Research, Invention and Development (IJIRID) 3, no. 2 (2024): 127–36. https://doi.org/10.5281/zenodo.11078923.

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<em>The lead acid battery has been a dominant device in large-scale energy storage systems since its invention in 1859. It has been the most successful commercialised aqueous electrochemical energy storage system ever since. In addition, this type of battery has witnessed the emergence and development of modern electricity-powered society. Nevertheless, lead acid batteries have technologically evolved since their invention. Over the past two decades, engineers and scientists have been exploring the applications of lead-acid batteries in emerging devices such as hybrid electric vehicles and ren
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32

LaCourse, William R., Yun‐Lin Hsiao, Dennis C. Johnson, and W. H. Weber. "Electrocatalytic Oxidations at Electrodeposited Bismuth (III)‐Doped Beta‐Lead Dioxide Film Electrodes." Journal of The Electrochemical Society 136, no. 12 (1989): 3714–19. http://dx.doi.org/10.1149/1.2096536.

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33

LIU, M., Y. TANG, L. WANG, Y. HU, X. JIAO, and W. HUANG. "Degradation of Phenol by Hydroxyl Radicals on Different Coating Lead Dioxide Electrodes." Chemical Research in Chinese Universities 24, no. 3 (2008): 285–90. http://dx.doi.org/10.1016/s1005-9040(08)60061-6.

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34

Das, Kaushik, and Aparesh Mondal. "Discharge behaviour of electro-deposited lead and lead dioxide electrodes on carbon in aqueous sulfuric acid." Journal of Power Sources 55, no. 2 (1995): 251–54. http://dx.doi.org/10.1016/0378-7753(95)02191-i.

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35

Velayutham, D., and M. Noel. "Comparative evaluation of electrodeposition of polypyrrole on lead-dioxide-coated glassy carbon and of lead dioxide on polypyrrole-coated glassy carbon electrodes." Journal of Electroanalytical Chemistry 353, no. 1-2 (1993): 101–12. http://dx.doi.org/10.1016/0022-0728(93)80289-t.

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36

Kim, Hong-Won, and Nam-Yong Chung. "Effectiveness of the Sensor using Lead Dioxide Electrodes for the Electrochemical Oxygen Demand." Journal of manufacturing engineering & technology 21, no. 4 (2012): 575–81. http://dx.doi.org/10.7735/ksmte.2012.21.4.575.

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37

K.R., Adithya Maurya, Bipin S. Chikkatti, Ashok M. Sajjan, Nagaraj R. Banapurmath, T. M. Yunus Khan, and C. Ahamed Saleel. "Facile development of flexible cellulose acetate-lead dioxide membrane electrodes for supercapacitor applications." Next Energy 5 (October 2024): 100178. http://dx.doi.org/10.1016/j.nxener.2024.100178.

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38

Yao, Yingwu, Xin Chen, Naichuan Yu, Feng Wei, and Huailiang Feng. "Preparation and Supercapacitive Performance of Lead Dioxide Electrodes with Three-Dimensional Porous Structure." Russian Journal of Electrochemistry 54, no. 7 (2018): 585–91. http://dx.doi.org/10.1134/s1023193518070078.

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39

Petersson, Ingela, Bo Berghult, and Elisabet Ahlberg. "Thin lead dioxide electrodes for high current density applications in semi-bipolar batteries." Journal of Power Sources 74, no. 1 (1998): 68–76. http://dx.doi.org/10.1016/s0378-7753(98)00035-4.

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40

Butt, Shahid Bilal, Aqsa Hassan Ansari, Mohammad Ali, and Safeer Ahmed. "Electrochemical fabrication and preliminary examination of modified lead dioxide bulk and analytical electrodes." Monatshefte für Chemie - Chemical Monthly 144, no. 9 (2013): 1261–69. http://dx.doi.org/10.1007/s00706-013-1002-y.

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41

González-García, Jose´, Jesús Iniesta, Antonio Aldaz, and Vicente Montiel. "Effects of ultrasound on the electrodeposition of lead dioxide on glassy carbon electrodes." New Journal of Chemistry 22, no. 4 (1998): 343–49. http://dx.doi.org/10.1039/a708754c.

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42

Huang, Zih-Jhong, Daniel Kabtamu, and Chen-Hao Wang. "LTO/TiO2 Nanowire-Decorated on Graphite Felt As Electrode for High-Performance Vanadium Redox Flow Battery." ECS Meeting Abstracts MA2023-01, no. 55 (2023): 2670. http://dx.doi.org/10.1149/ma2023-01552670mtgabs.

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Vanadium redox flow battery(VRFB) is one of the most promising large-scale energy storage systems. However, the graphite electrode materials employed for VRFB often have shortcomings such as poor electrochemical activity and insufficient conductivity, which will lead to poor performance of VRFB. To modify the graphite electrode, in this study, lithium titanate/titanium dioxide(LTO/TiO2) composite catalyst with the nanowire morphology was directly grown on the surface of the heat treatment graphite felt(HGF). The graphite felt electrode through the nanowire morphology, the reaction area between
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43

Pierpaoli, Mattia, Michał Rycewicz, Aneta Łuczkiewicz, Sylwia Fudala-Ksiązek, Robert Bogdanowicz, and Maria Letizia Ruello. "Electrodes criticality: the impact of CRMs in the leachate electrochemical oxidation." Manufacturing Review 7 (2020): 7. http://dx.doi.org/10.1051/mfreview/2020006.

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Landfill leachate possesses high concentrations of ammonia, micropollutants, and heavy metals, and are characterised for low biodegradability. For this reason, conventional treatment technologies may result ineffective for complete pollutant removal. Electrochemical oxidation allows most of the of recalcitrant pollutants to be oxidised effectively within an easy operational and acceptable retention time, without the need to provide additional chemicals, and without producing waste materials. The mineralisation efficiency and electrode durability depend on the nature of the electrode material.
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44

Abbas, Fatima, and Hatem Asel. "The Electrochemical removal of Oil and COD from petroleum wastewater." Wasit Journal of Engineering Sciences 11, no. 1 (2023): 134–49. http://dx.doi.org/10.31185/ejuow.vol11.iss1.433.

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Recently, COD and oil concentrations in the water have increased, as a result of reduced water volumes and increased industrial waste being dumped into the river. Increased concentrations of these pollutants lead to health and environmental problems. As the water treatment plants use the usual methods of water treatment and could not reduce the concentration of oil and COD to the limit set by the World Health Organization, so an effective way to treat these pollutants became absolutely necessary. In this study, electrochemical method was used to treat water contaminated with oil and COD, using
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45

Yao, Yingwu, Lihua Cui, Chunmei Zhao, and Limiao Jiao. "Influences of Cerium on the Electrodeposition Process and Physicochemical Properties of Lead Dioxide Electrodes." Journal of The Electrochemical Society 161, no. 10 (2014): D528—D533. http://dx.doi.org/10.1149/2.0901410jes.

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46

Hmani, Emna, Youssef Samet, and Ridha Abdelhédi. "Electrochemical degradation of auramine-O dye at boron-doped diamond and lead dioxide electrodes." Diamond and Related Materials 30 (November 2012): 1–8. http://dx.doi.org/10.1016/j.diamond.2012.08.003.

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47

Shmychkova, Olesia, Tatiana Luk'yanenko, Valentina Knysh, and Alexander Velichenko. "The Influence of Fluorine-Containing Surfactants and Polymers on Regularities of Lead Dioxide Electrodeposition." ECS Meeting Abstracts MA2022-01, no. 24 (2022): 2474. http://dx.doi.org/10.1149/ma2022-01242474mtgabs.

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Electrochemical synthesis allows one to influence the composition and properties of materials by changing the conditions of electrolysis and electrolyte composition. Lead dioxide due to the simplicity of its electrochemical synthesis, high corrosion resistance and relatively low cost is widely used in electrocatalysis, electroplating, lead-acid batteries, etc. The inclusion of fluorine-containing compounds in the metal oxide matrix provides antistatic, anti-adhesive, anti-corrosion properties, and at the same time the materials retain the properties of metal oxide: high electrical conductivity
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48

Chen, Bu Ming, Zhong Cheng Guo та Hui Huang. "Anodic Synthesis of α-PbO2-CeO2-TiO2 Composite Materials from Colloidal Electrolyte: Morphology, Composition and Structure of PbO2-Matrix Composites". Advanced Materials Research 308-310 (серпень 2011): 728–33. http://dx.doi.org/10.4028/www.scientific.net/amr.308-310.728.

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During electrodepositing pure lead dioxide, the electrocatalytic activity of PbO2 electrodes, as well as their stability, can often be considerably enhanced by the incorporation of some fine particles added to the electrodeposition. The morphology, crystal phase, surface composition, microstructure, of the electrode were characterized by means of SEM, XRD and EDS. SEM-EDS analysis showed the addition of solid particles could inhibit the growth of α-PbO2 unit cells, improving the specific surface areas of coating surface.Under all condition, the matrix was highly oriented α-PbO2. The electrocat
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49

Шмычкова, О.Б., В.А. Кныш, Т.В. Лукьяненко, Р. Амаделли та А.Б. Величенко. "Электрокаталитические процессы на PbO2-электродах при высоких анодных потенциалах". Elektronnaya Obrabotka Materialov 53, № 3 (2017): 55–63. https://doi.org/10.5281/zenodo.1053531.

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The determination of the electrocatalytic activity and selectivity of electrodes with respect to the target process is considered to be of interest both, in the theoretical aspect, for the development of electrocatalysis theory and in application for efficient electrocatalysts, which can be used in electrochemical systems for wastewater treatment. The purpose of the given work was to identify the relationship between the chemical and phase composition of materials based on lead dioxide, their physical-chemical properties and electrocatalytic activity. The major research methods were: quasi-sta
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Hsiao, Yun‐Lin, Joseph E. Vitt, and Dennis C. Johnson. "Electrocatalysis of Anodic Oxygen‐Transfer Reactions: Acetate‐Doped Lead Dioxide Electrodes in Sulfuric Acid Media." Journal of The Electrochemical Society 139, no. 2 (1992): 377–80. http://dx.doi.org/10.1149/1.2069226.

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