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Tesis sobre el tema "Silicalita"

Autor: Grafiati

Publicado: 4 de junio de 2021

Última modificación: 15 de febrero de 2022

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1

Rigo, Reus Tiago. "S?ntese e caracteriza??o de membranas zeol?ticas tipo mfi e aplica??o em separa??o de arom?ticos." Universidade Federal do Rio Grande do Norte, 2013. http://repositorio.ufrn.br:8080/jspui/handle/123456789/17704.

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Made available in DSpace on 2014-12-17T15:42:06Z (GMT). No. of bitstreams: 1 ReusTR_DISSERT.pdf: 4094188 bytes, checksum: 4969fc6bf4243a6e241302a399783473 (MD5) Previous issue date: 2013-07-22<br>Coordena??o de Aperfei?oamento de Pessoal de N?vel Superior<br>The synthesis of MFI-type zeolite membranes was carried by the process in situ or hydrothermal crystallization. We studied the homogenization time of the room temperature and gel filtration just before the crystallization step performed out in an oven, thus obtaining a more uniform zeolite film. The powder synthesized zeolite (structure

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2

Prieto, Arnal Alejandro. "Producción de óxido de propileno a partir de H2O2 generada in situ con el empleo de sistemas catalíticos bifuncionales." Doctoral thesis, Universitat Politècnica de València, 2017. http://hdl.handle.net/10251/83482.

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Propylene oxide (PO), one of the most important intermediate reagent from the industrial point of view, has been historically obtained through non environmentally-friendly processes. Fortunately, the increasing worldwide environmental awareness during the last decades has motivated a willingness to change these processes for more environmentally-friendly ones. Among all the alternative processes that could substitute the traditional methodologies, the epoxidation of propylene by means of titanium silicalite-1 zeolite seems to be one of the most promising. Discovered in the beginning of 80s,

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3

Halhead, Michael David. "Characterisation of silicalite and post synthesis modified silicalite using adsorption." Master's thesis, University of Cape Town, 2001. http://hdl.handle.net/11427/13894.

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Bibliography: leaves 89-96.<br>The study of adsorption on microporous materials such as zeolites is of tremendous scientific and industrial interest. The effective development and design of both equipment and processes is reliant on the availability of accurate information on the processes of adsorption in these materials. Zeolites, of the type studied in this thesis, are becoming increasingly important in a wide range of fields such as ion-exchange, purification, separations particularly of close boiling compounds and catalytic processes. The work presented had two primary objectives. The fir

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4

Morell, Heiko. "Analyse der Gast-Wirt-Wechselwirkungen von n-Alkanen C6 - C12 im Kanalsystem von Silicalit-I." [S.l. : s.n.], 2001. http://deposit.ddb.de/cgi-bin/dokserv?idn=961810912.

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5

Sowerby, Beverley. "Drying of organic vapours by adsorption." Thesis, University of Bath, 1988. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.284567.

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6

Hargreaves, S. M. "Hydrocarbon adsorption in silicalite : experimental and numerical studies." Thesis, University of Cambridge, 2000. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.603712.

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The work contained in this thesis addresses the single and multicomponent adsorption of hydrocarbons in silicalite. Both experimental and numerical work is presented. Experimental measurements are made using a volumetric technique and many equilibrium adsorption studies are reported for the first time. Multicomponent adsorption studies have revealed several novel adsorption phenomena. Intermolecular interaction within silicalite has been probed using deuterium nuclear magnetic resonance (<SUP>2</SUP>H NMR) experiments. For the first time data are presented for both single and multicomponent ad

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7

Lee, Seung Ju. "Morphological control of silicalite-1 crystals using microemulsion mediated growth." Diss., Texas A&M University, 2005. http://hdl.handle.net/1969.1/2535.

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Zeolites are crystalline, microporous aluminosilicates that have been extensively used in heterogeneous catalysis, separations, and ion-exchange operations. It has long been understood that particle size and morphology play a central role in the successful application of zeolites. This dissertation reports on controlling the morphology of all-silica zeolite, silicalite-1, made in nonionic/ionic microemulsions under conventional synthesis conditions. Silicalite-1 materials formed in microemulsion-mediated syntheses possess different morphological properties as compared to samples grown using th

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8

Flynn, Tracey Karen. "Some sorption and salt occlusion properties of silicalite-1." Thesis, University of Edinburgh, 1987. http://hdl.handle.net/1842/14868.

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9

Boulicaut, Ludovic. "Sorption and diffusion in silicalite crystals studied by HPLC." Thesis, National Library of Canada = Bibliothèque nationale du Canada, 1997. http://www.collectionscanada.ca/obj/s4/f2/dsk2/ftp04/mq23781.pdf.

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10

Simon, Jean-Marc, Nicole Floquet, Jean-Pierre Bellata, and Guy Weber. "Commensurate diffusion effects of n-heptane in silicalite-1." Universitätsbibliothek Leipzig, 2015. http://nbn-resolving.de/urn:nbn:de:bsz:15-qucosa-185690.

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11

Van-Den-Begin, Neil Graham. "A study on diffusion of hydrocarbons in silicalite-1." Thesis, Imperial College London, 1990. http://hdl.handle.net/10044/1/46591.

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12

Carter, David, Boguslaw Kruczek, and F. Handan Tezel. "Application of Maxwell Stefan equations to characterize silicalite membranes." Diffusion fundamentals 24 (2015) 8, S. 1, 2015. https://ul.qucosa.de/id/qucosa%3A14522.

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13

Simon, Jean-Marc, Nicole Floquet, Jean-Pierre Bellata, and Guy Weber. "Commensurate diffusion effects of n-heptane in silicalite-1." Diffusion fundamentals 16 (2011) 73, S. 1-2, 2011. https://ul.qucosa.de/id/qucosa%3A13816.

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14

Carter, David, Boguslaw Kruczek, and F. Handan Tezel. "Application of Maxwell Stefan equations to characterize silicalite membranes." Universitätsbibliothek Leipzig, 2016. http://nbn-resolving.de/urn:nbn:de:bsz:15-qucosa-198056.

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15

Zhang, Baojian. "Template-directed construction of hierarchically ordered zeolite materials." Thesis, University of Bristol, 2001. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.364867.

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16

Fernandez, Moisés, André Pampel, Jörg Kärger, Dieter Freude, Baten Jasper M. van, and Rajamani Krishna. "Mixture diffusion in silicalite-1 studied by MAS PFG NMR." Universitätsbibliothek Leipzig, 2016. http://nbn-resolving.de/urn:nbn:de:bsz:15-qucosa-193984.

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17

Tawalbeh, Muhammad. "Silicalite-1 Membranes Synthesis, Characterization, CO2/N2 Separation and Modeling." Thèse, Université d'Ottawa / University of Ottawa, 2013. http://hdl.handle.net/10393/30330.

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Zeolite membranes are considered to be a promising alternative to polymeric membranes and they have the potential to separate gases under harsh conditions. Silicalite-1 membranes in particular are easy to prepare and suitable for several industrial applications. In this research project, silicalite-1/ceramic composite membranes were prepared using the pore plugging hydrothermal synthesis method and supports with zirconium oxide and/or titanium oxide as active layers. The effect of the support’s pore size on the morphology and permeation performance of the prepared membranes was investigated us

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18

Du, Zhimei. "Computer simulation and theoretical studies of hydrocarbon adsorption in silicalite." Thesis, London South Bank University, 2000. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.342841.

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19

Fernandez, Moisés, André Pampel, Jörg Kärger, Dieter Freude, Baten Jasper M. van, and Rajamani Krishna. "Mixture diffusion in silicalite-1 studied by MAS PFG NMR." Diffusion fundamentals 6 (2007) 61, S. 1-2, 2007. https://ul.qucosa.de/id/qucosa%3A13189.

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20

Vaidya, Prahar S. "PURE AND BINARY ADSORPTION OF METHANE AND NITROGEN ON SILICALITE." Cleveland State University / OhioLINK, 2016. http://rave.ohiolink.edu/etdc/view?acc_num=csu1463751121.

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21

Zhou, Qianqian. "Pure Component Adsorption of Methane, Ethylene, Propylene and Carbon Dioxide in Silicalite." Cleveland State University / OhioLINK, 2013. http://rave.ohiolink.edu/etdc/view?acc_num=csu1369150380.

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22

Chafin, Raymond William II. "Torlon® and Silicalite Mixed Matrix Membranes for Xylene Isomer Purification." Diss., Georgia Institute of Technology, 2007. http://hdl.handle.net/1853/14562.

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Organic/inorganic materials have a high potential to enable major advances in membrane performance. It has previously been impossible to develop polymeric systems with adequate transport properties for xylene purification. Zeolite membranes have been created with the appropriate selectivities; however low productivity, low mechanical durability, and high capital costs have kept these materials from being utilized. So-called mixed matrix hybrid organic/inorganic membranes combine the mechanical durability and cost effectiveness of polymeric membranes with the enhanced performance of zeolitic

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23

Inzoli, Isabella, Signe Kjelstrup, Dick Bedeaux, and Jean-Marc Simon. "The coupled transport of heat and mass across a silicalite surface." Universitätsbibliothek Leipzig, 2015. http://nbn-resolving.de/urn:nbn:de:bsz:15-qucosa-189575.

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24

Inzoli, Isabella, Jean Marc Simon, and Signe Kjelstrup. "Surface resistance to heat and mass transfer in a silicalite membrane." Universitätsbibliothek Leipzig, 2016. http://nbn-resolving.de/urn:nbn:de:bsz:15-qucosa-193396.

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25

Loisruangsin, Arthorn, Siegfried Fritzsche, and Supot Hannongbua. "Potential calculations and MD simulations of n-pentane in silicalite-1." Universitätsbibliothek Leipzig, 2016. http://nbn-resolving.de/urn:nbn:de:bsz:15-qucosa-195428.

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26

Loisruangsin, Arthorn, Siegfried Fritzsche, and Supot Hannongbua. "Potential calculations and MD simulations of n-pentane in silicalite-1." Diffusion fundamentals 2 (2005) 29, S. 1-2, 2005. https://ul.qucosa.de/id/qucosa%3A14359.

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27

Chmelik, Christian, Lars Heinke, Jörg Kärger, Baten Jasper M. van, and Rajamani Krishna. "Diffusion of n-butane/iso-butane mixtures in silicalite-1 investigated using infrared microscopy: Diffusion of n-butane/iso-butane mixtures in silicalite-1investigated using infrared microscopy." Diffusion fundamentals 11 (2009) 25, S. 1-2, 2009. https://ul.qucosa.de/id/qucosa%3A13966.

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28

Pellenq, Roland Jean-Marc Gabriel. "Theory and computer simulation of absorption of simple molecules in silicalite-1." Thesis, Imperial College London, 1994. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.339443.

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29

Fryčová, Marie, Petr Sysel, Pavel Hrabánek, et al. "Helium permeation through mixed matrix membranes based on polyimides and silicalite-1." Universitätsbibliothek Leipzig, 2015. http://nbn-resolving.de/urn:nbn:de:bsz:15-qucosa-188833.

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30

Jalili, S. E. "Monte Carlo simulation and statistical mechanics modelling of mixture adsorption in silicalite." Thesis, University College London (University of London), 2011. http://discovery.ucl.ac.uk/1318086/.

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Adsorption in zeolites is widely and increasingly used in many industrial processes. For the design of new processes and improvement of the performance of existing ones, basic adsorption data is needed but due to the difficulties of experimentation it is lacking. In this thesis, different methods have been used to calculate the adsorption isotherms of benzene, methane, ethane and CO, mixtures as well as Propane, i-butane and n-butane and their binary and ternary mixtures in zeolites. Firstly, Lattice Model has been used to calculate benzene adsorption isotherms in silicalite zeolite whose expe

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31

Fryčová, Marie, Petr Sysel, Pavel Hrabánek, et al. "Helium permeation through mixed matrix membranes based on polyimides and silicalite-1." Universitätsbibliothek Leipzig, 2015. http://nbn-resolving.de/urn:nbn:de:bsz:15-qucosa-191331.

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Mixed matrix membranes based on modified polyimides and silicalite-1 were prepared and studied. The novel preparation approach consists in improvement of the interfacial adhesion by employment of the coupling agent 3-aminopropyltriethoxysilane in such a way which leads to forming of chemical bonds between polyimide and silicalite-1. Firstly polyimide chains were endcapped by this agent which subsequently enabled their reaction with groups naturally present on silicalite-1 surface. Membranes with silicalite-1 content up to 60 wt. % were prepared and characterized by SEM, light microscopy and pe

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32

Fryčová, Marie, Petr Sysel, Pavel Hrabánek, et al. "Helium permeation through mixed matrix membranes based on polyimides and silicalite-1." Diffusion fundamentals 11 (2009) 6, S. 1-2, 2009. https://ul.qucosa.de/id/qucosa%3A13926.

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33

Fryčová, Marie, Petr Sysel, Pavel Hrabánek, et al. "Helium permeation through mixed matrix membranes based on polyimides and silicalite-1." Diffusion fundamentals 11 (2009) 90, S. 1-17, 2009. https://ul.qucosa.de/id/qucosa%3A14063.

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Mixed matrix membranes based on modified polyimides and silicalite-1 were prepared and studied. The novel preparation approach consists in improvement of the interfacial adhesion by employment of the coupling agent 3-aminopropyltriethoxysilane in such a way which leads to forming of chemical bonds between polyimide and silicalite-1. Firstly polyimide chains were endcapped by this agent which subsequently enabled their reaction with groups naturally present on silicalite-1 surface. Membranes with silicalite-1 content up to 60 wt. % were prepared and characterized by SEM, light microscopy and pe

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34

Al-Akwaa, Shaaima. "Synthesis and New Characterization Method of Silicalite-1 Membranes for Gas Separation." Thesis, Université d'Ottawa / University of Ottawa, 2020. http://hdl.handle.net/10393/41577.

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Zeolite membranes have great potential in gas separation applications because of their unique selective properties. The main challenge is in synthesizing defect-free zeolite membranes. In this study, we synthesized silicalite-1 zeolite membranes on ceramic supports composed of Al2O3 and TiO2 using the pore-plugging method. We investigated the effect of the fill-level in the autoclave during the synthesis on the membrane performance. In particular, we were interested in determining the conditions at which the defects' contribution to the total transport is minimized. We adopted and furthe

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35

Carter, David. "Fabrication and Characterization of Silicalite-1 Membranes for the Separation of the Greenhouse Gases." Thesis, Université d'Ottawa / University of Ottawa, 2019. http://hdl.handle.net/10393/39524.

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Membranes composed of zeolite crystals, in which gas molecules are transported by surface diffusion, are promising for gas separation applications. Since this mode of mass transfer mechanism is controlled by synergistic adsorption and diffusion phenomena, the separation of gas mixtures is not solely dependent on molecular size. However, undesirable defect pathways in zeolite membranes are often present due to factors such as incomplete crystal growth and/or thermal stresses during membrane synthesis and calcination. These pathways cause molecules to bypass the selective zeolite crystal layer a

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36

Gueudré, Laurent, Christian Chmelik, and Jörg Kärger. "Diffusion anisotropy in a single crystal of silicalite-1 studied by interference microscopy." Universitätsbibliothek Leipzig, 2015. http://nbn-resolving.de/urn:nbn:de:bsz:15-qucosa-185041.

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37

Robinson, Denis Joseph. "Catalytic oxidation reactions using titanium silicalite (TS-1) in conjunction with hydrogen peroxide." Thesis, University of Liverpool, 1998. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.367129.

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38

Carleen, Bradford J. "Hydrothermal Synthesis Process for the Production of Silicalite-1 Crystal Aggregate Packing Particles." Digital WPI, 2010. https://digitalcommons.wpi.edu/etd-theses/137.

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Methyl Tertiary-Butyl Ether (MTBE) contamination of groundwater and surface waters has become a relevant environmental and public safety concern in recent years. This anthropogenic compound is now persistent at low concentrations in several valuable ground and surface water locations within the United States due largely to the widespread production of MTBE for use as a fuel oxygenate in conjunction with negligent underground storage practices during the 1980's and 1990's. Though there are several treatment strategies for the remediation of MTBE spill sites, the most efficient strategy may be

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39

Gabry, Thomas Jacques Andre. "Simulation of the diffusion of endocrine disrupting compounds in silicalite by molecular dynamics." Digital WPI, 2012. https://digitalcommons.wpi.edu/etd-theses/341.

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In this thesis we investigated the separation of two endocrine disrupting chemicals (EDC), bisphenol-A (BPA) and nonylphenol (NP) from water over the defect free silicalite zeolite. Two force-fields were investigated, the OPLS-AA force-field which is an all-atom one, and the OPLS-UA force-field which is a united atom one. In order to be able to simulate BPA, we simulated and studied the diffusion of different molecules in silicalite. We compared two famous bulk water models, the non-rigid TIP3P modified for CHARMM model and the rigid SPC model, to literature and simulated the diffusion of th

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40

Gueudré, Laurent, Christian Chmelik, and Jörg Kärger. "Diffusion anisotropy in a single crystal of silicalite-1 studied by interference microscopy." Diffusion fundamentals 16 (2011) 45, S. 1-2, 2011. https://ul.qucosa.de/id/qucosa%3A13781.

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41

Li, Qinghua. "Crystallization of colloidal TPA-silicalite-1 by a two-stage varying-temperature synthesis." Licentiate thesis, Luleå tekniska universitet, 2000. http://urn.kb.se/resolve?urn=urn:nbn:se:ltu:diva-17472.

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A novel synthesis method called a two-stage varying-temperature synthesis was developed for the investigation of kinetics and mechanism of the crystallization of discrete colloidal crystals of TPA-silicalite-1. Briefly, this method involves a rapid change in treatment temperature at some point during the crystallization. By extending the duration of the period at the initial synthesis temperature, the crystal concentration and final crystal size varied until they were approximately equal to those obtained for a complete synthesis at the initial temperature. At this point in the crystallization

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42

Petry, David P. "Silicalite Clear Sol Precursors Studied by NMR, Mass Spectrometry and Dynamic Light Scattering." Thesis, University of Manchester, 2010. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.525295.

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43

Cheng, Chil-Hung. "High-silica zeolite nucleation from clear solutions." Texas A&M University, 2005. http://hdl.handle.net/1969.1/3273.

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Understanding the mechanism of zeolite nucleation and crystallization will enable the zeolite science community to tune zeolite properties during synthesis in order to accommodate the purposes of various applications. Thus there has been considerable research effort in "deciphering" the mechanism by studying the growth course of tetrapropylammonium (TPA)-mediated silicalite-1 using several techniques, such as dynamic light scattering (DLS), small-angle X-ray/neutron scattering (SAXS/SANS), and nuclear magnetic resonance (NMR). While these studies have generated a more comprehensive picture on

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44

Gueudré, Laurent. "Diffusion du cyclohexane dans la Silicalite-1 : Origine et caractérisation de la résistance de surface." Lyon, Ecole normale supérieure, 2010. http://www.theses.fr/2010ENSL0580.

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L’objectif de ce travail est d’étudier plus en détail la résistance au transfert de matière à la surface des solides microporeux, en mesurant les cinétiques d’adsorption sur le système cyclohexane/Silicalite-1 par thermogravimétrie. Afin de réaliser cette thèse, un soin particulier a été accordé à la synthèse de cristaux de Silicalite-1 de différentes tailles afin de dissocier la résistance de surface de la résistance diffusionnelle intracristalline. Ces synthèses ont été réalisées de manière à obtenir des cristaux de géométrie quasi sphérique et possédant une répartition de taille homogène. L

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45

Chmelik, Christian, Lars Heinke, Jörg Kärger, Baten Jasper M. van, and Rajamani Krishna. "Diffusion of n-butane/iso-butane mixtures in silicalite-1 investigated using infrared microscopy." Universitätsbibliothek Leipzig, 2015. http://nbn-resolving.de/urn:nbn:de:bsz:15-qucosa-189481.

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46

Yip, Chi Kin. "A catalytic architecture composed of titanium silicalite-1 and nanostructured support for oxime synthesis /." View abstract or full-text, 2009. http://library.ust.hk/cgi/db/thesis.pl?CBME%202009%20YIP.

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47

Shin, Sang Baek. "Catalytic reaction engineering of propene epoxidation with hydrogen peroxide over titanium silicalite (TS-1)." Thesis, Imperial College London, 2011. http://hdl.handle.net/10044/1/6951.

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Propene oxide is an important chemical intermediate in the chemical industry. The propene oxide industry has employed two different types of commercial processes for several decades: the chlorohydrin process and the hydroperoxidation process. However, direct epoxidation of propene with hydrogen peroxide has recently attracted much attention as a more environmentally benign and profitable process. This thesis presents the catalytic reaction engineering of the epoxidation of propene to propene oxide using hydrogen peroxide as the oxidant and titanium silicalite (TS-1) as the catalyst under mild

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48

Rimer, Jeffrey D. "Self-assembly of silica nanoparticles and their role in the mechanism of silicalite-1 crystallization." Access to citation, abstract and download form provided by ProQuest Information and Learning Company; downloadable PDF file, 302 p, 2007. http://proquest.umi.com/pqdlink?did=1253510461&Fmt=7&clientId=79356&RQT=309&VName=PQD.

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49

Chalhoub, Elie, and Dhananjai B. Shah. "Measurement of diffusivities of helium and argon in silicalite by static single crystal membrane technique." Universitätsbibliothek Leipzig, 2016. http://nbn-resolving.de/urn:nbn:de:bsz:15-qucosa-196430.

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50

Laloué, Nicolas, Catherine Laroche, and Hervé Jobic. "Concentration dependence of transport and corrected diffusivities of n-Hexane in silicalite measured by QENS." Universitätsbibliothek Leipzig, 2016. http://nbn-resolving.de/urn:nbn:de:bsz:15-qucosa-196598.

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