Letteratura scientifica selezionata sul tema "Crystallization"

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Articoli di riviste sul tema "Crystallization"

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Frolova, S., and O. Sobol. "Dynamics of cluster structure change in melts that forms a continuous series of solid solutions during equilibrium and nonequilibrium crystallization." BULLETIN of the L.N. Gumilyov Eurasian National University. Chemistry. Geography. Ecology Series 143, no. 2 (2023): 45–51. http://dx.doi.org/10.32523/2616-6771-2023-143-2-45-51.

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The article describes the dynamics of changes in the melt structure during cooling of solid substitution solutions in the process of quasi-equilibrium (CRC) and non-equilibrium explosive crystallization (NRCC), taking into account clustering processes. The boundaries of the transition to the solid state are determined as the structure of clusters changes during crystallizations of the KRK and NRK types. The boundaries are determined taking into account the critical overheating and pre-crystallization supercooling relative to the liquidus line . It is determined that during quasi–equilibrium cr
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Florence, Alastair J., Andrea Johnston, Philippe Fernandes, Norman Shankland, and Kenneth Shankland. "An automated platform for parallel crystallization of small organic molecules." Journal of Applied Crystallography 39, no. 6 (2006): 922–24. http://dx.doi.org/10.1107/s0021889806040921.

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An automated platform for parallel crystallization of small organic molecules from solution is described. The principal gain over manual crystallization lies in the automated sequencing of crystallization steps, including computer-controlled dosing of liquids and solids. The platform is designed to conduct 32 crystallizations per day, from solution volumes up to 10 ml, allowing a search for physical forms to be conducted over a finer grid than might be accessible manually and thereby increasing the probability of success.
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Semjonova, Aina, and Agris Bērziņš. "Surfactant Provided Control of Crystallization Polymorphic Outcome and Stabilization of Metastable Polymorphs of 2,6-Dimethoxyphenylboronic Acid." Crystals 12, no. 12 (2022): 1738. http://dx.doi.org/10.3390/cryst12121738.

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2,6-Dimethoxyphenylboronic acid was used as a model substance to investigate the additive crystallization approach for polymorph control in phenylboronic acids. It was crystallized under different conditions by performing evaporation and cooling crystallization from different solvents. Most of the crystallizations from pure solvents produced the thermodynamically stable Form I, but in evaporation crystallization from alcohols, Form II or even a new polymorph, Form III, could be obtained. Structurally related substances, polymers, and surfactants with diverse intermolecular interaction possibil
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Roy, Pritish Kumar, and Shibendra Shekher Sikder. "Study of Nanocrystallization Kinetics in Fe 73.5 Cu 1 Nb 3 Si 13.5 B 9 Finemet Type Alloy by Differential Thermal Analysis and Using Different Models." BL College Journal 4, no. 1 (2022): 140–55. http://dx.doi.org/10.62106/blc2022v4i1e3.

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The study of the crystallization processes in the FINEMET type nanocrystalline amorphous alloy is interesting not only from the fundamental aspect of establishing reaction mechanism of crystal nucleation and growth, but also from a technological point of view. The process and nature of crystallization phase constitution of nanocrystalline amorphous alloy of composition Fe 73.5 Cu 1 Nb 3 Si 13.5 B 9 prepared by rapid quenching method is investigated in the present study. The amorphous nature of the alloy has been verified by x-ray diffraction (XRD). The differential thermal analysis (DTA) exper
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Qin, Hong Wu, Xiao Xue Xing, and Xian Zhang. "The Analysis for Crystallization of Sn-Pb Alloys Using Acoustic Emission Testing about Wind Turbine Root Materials." Applied Mechanics and Materials 668-669 (October 2014): 83–86. http://dx.doi.org/10.4028/www.scientific.net/amm.668-669.83.

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Regular researches of system Sn-Pb alloys with use AE are carried out in various crystallization conditions. In the given researches the technique has been used, which allow to divide the signals radiated with plastic deformation and crack's formation and development from each process. In the metals and alloys majority radiation of AE signals begins in the middle of crystallization's area and comes to an end at the moment of the crystallization termination However in a number of materials AE signals have been registered below an excess point on a cooling curve in a firm condition. Essential in
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Bosq, Nicolas, Nathanaël Guigo, and Nicolas Sbirrazzuoli. "Crystallization Behaviour of Polytetrafluoroethylene over very Large Cooling Rate Domains." Advanced Materials Research 747 (August 2013): 201–4. http://dx.doi.org/10.4028/www.scientific.net/amr.747.201.

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Polytetrafluoroethylene (PTFE) is a semi-crystalline polymer that demonstrates a very fast crystallization process on cooling. This study investigates the nonisothermal PTFE ultra-fast crystallization over a wide range of cooling rates via conventional Differential Scanning Calorimetry (DSC), Fast Scanning Calorimetry (FSC) and Ultra-Fast Scanning Calorimetry (UFSC). A new knowledge about crystallization kinetics of PTFE is obtained from the data obtained under very fast cooling rates. The shift of the melting peak to lower temperature shows that the crystals formed under fast cooling rates ar
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Grant, D., W. F. Long, and F. B. Williamson. "Inhibition by glycosaminoglycans of CaCO3 (calcite) crystallization." Biochemical Journal 259, no. 1 (1989): 41–45. http://dx.doi.org/10.1042/bj2590041.

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Of a range of glycosaminoglycans, heparin and heparan sulphate were the most effective inhibitors in vitro of CaCO3 (calcite) crystallization as assayed by conductimetric measurements. The possible role of such glycosaminoglycans in modulating calcium-salt crystallizations in vivo is discussed.
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Aversa, Raffaella, Francesco Tamburrino, Daniela Parcesepe, and Antonio Apicella. "Cold Crystallization Behaviour of a Commercial Zr44-Ti11-Cu10-Ni10-Be25 Metal Glassy Alloy." Advanced Materials Research 1088 (February 2015): 206–12. http://dx.doi.org/10.4028/www.scientific.net/amr.1088.206.

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Isothermal crystallizations in the supercooled liquid metal metastable state at progressively increasing temperatures above the Glass Transition of the Zr44-Ti11-Cu10-Ni10-Be25 metal glass Alloy (cold crystallization attained by heating the samples from the glassy state) have been investigated in this study.Complex crystallization behaviours showing multiple exothermic peaks and selective crystallization of the alloy higher mobility atoms induced by the isothermal annealing, has been observed to lead to experimentally observed increase of the temperature needed to induce the glassy metal relax
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Xiuju, Z., S. Juncai, Y. Huajun, L. Zhidan, and T. Shaozao. "Mechanical Properties, Morphology, Thermal Performance, Crystallization Behavior, and Kinetics of PP/Microcrystal Cellulose Composites Compatibilized by Two Different Compatibilizers." Journal of Thermoplastic Composite Materials 24, no. 6 (2011): 735–54. http://dx.doi.org/10.1177/0892705711403527.

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Polypropylene (PP)/microcrystalline cellulose (MCC) composites and PP/MCC composites modified by maleic anhydride grafted PP (PP-g-MA) and methyl acrylic acid glycidyl ester grafted PP (PP-g-GMA) respectively were prepared in a twin-screw extruder. The mechanical properties, morphology, and thermal performance were investigated. The nonisothermal crystallization, melting behavior, and nonisothermal crystallization kinetics were investigated by DSC. The results indicated that the addition of MCC had led to the increase of the tensile strength, impact strength, and flexural strength of PP. PP-g-
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Carugo, Oliviero, and Kristina Djinović-Carugo. "Packing bridges in protein crystal structures." Journal of Applied Crystallography 47, no. 1 (2013): 458–61. http://dx.doi.org/10.1107/s160057671302880x.

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On the basis of a statistical analysis of the data deposited in the Protein Data Bank [Bermanet al.(2000).Nucleic Acids Res.28, 235–242; Bernsteinet al.(1977).J. Mol. Biol.112, 535–542], it is shown that two symmetry-related protein molecules are frequently bridged by a small molecule/monoatomic ion, which was used in the crystallization medium despite the fact that it is not a physiological ligand of the macromolecule. It is therefore sensible to suppose that some of the solutes used in crystallizations can favour the nucleation process by bridging and opportunely orienting adjacent protein m
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Tesi sul tema "Crystallization"

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Sweed, Muhamed. "Co-crystallization in polyolefin blends studied by various crystallization analysis techniques." Thesis, Link to the online version, 2006. http://hdl.handle.net/10019.1/2733.

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Patki, Rahul P. "Quench Crystallization of Linear Polyethylene: Crystallization Kinetics, Morphology and Structure Investigation." Cincinnati, Ohio : University of Cincinnati, 2008. http://rave.ohiolink.edu/etdc/view.cgi?acc_num=ucin1227282696.

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Núñez, Eugenia. "Crystallization in Constrained Polymer Structures : Approaching the Unsolved Problems in Polymer Crystallization." Doctoral thesis, KTH, Fiber- och polymerteknik, 2006. http://urn.kb.se/resolve?urn=urn:nbn:se:kth:diva-4041.

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The knowledge regarding certain issues in polymer crystallization e.g. the possible existence of short–lived mesophases remains inconclusive due to experimental limitations. Polymers undergo chain folding upon crystallization, which introduces some complications that are not found in crystallization of low molar mass materials. Chain–folded crystals are far from their equilibrium shape and they rearrange rapidly at the crystallization temperature. This, together with the slow experimental techniques traditionally used, impedes the observation of the originally formed structures. To approach th
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Suzuki, Yasuhito [Verfasser]. "How different is water crystallization from polymer crystallization under confinement? / Yasuhito Suzuki." Mainz : Universitätsbibliothek Mainz, 2015. http://d-nb.info/1078386684/34.

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Robertson, Divann. "Studying crystallization kinetics using solution crystallization analysis by laser light scattering (Scalls)." Thesis, Stellenbosch : Stellenbosch University, 2012. http://hdl.handle.net/10019.1/20112.

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Thesis (MSc)--Stellenbosch University, 2012.<br>ENGLISH ABSTRACT: This study involved the analysis of crystallization kinetics by means of a unique and newly developed Solution crystallization analysis by laser light scattering (Scalls) technique. In the main study we compared two commercial linear low-density polyethylene (LLDPE) polymers (PE-1- octene and PE-1-hexene) and studied the effect of short-chain branching on the solution crystallization of these complex polymer systems. Characterization of the polymers was done by nuclear magnetic resonance spectroscopy (NMR) and high-tempera
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Walter, Thomas S. "Methodology for macromolecular crystallization." Thesis, University of Oxford, 2010. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.542989.

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Pridmore, Derik A. (Derik Arnold) 1978. "Online polymer crystallization experiment." Thesis, Massachusetts Institute of Technology, 2005. http://hdl.handle.net/1721.1/33335.

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Thesis (M. Eng.)--Massachusetts Institute of Technology, Dept. of Electrical Engineering and Computer Science, 2005.<br>Includes bibliographical references (leaves 119-120).<br>An architecture for online remote operation of a polymer crystallization experiment was refined, beta tested in actual use conditions, and extended based on feedback from those tests. In addition, an application for graphically simulating macroscopic crystal spherulite growth was developed for use as an educational tool. Finally, the experiment was used in the design process for modifying the generic iLab framework to i
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Yang, Li-yin 1952. "Crystallization kinetics of diphenylhydantoin." Thesis, The University of Arizona, 1989. http://hdl.handle.net/10150/277190.

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The crystallization kinetics of diphenylhydantoin (DPH) has been studied at constant conditions in a small mixed suspension mixed product removal (MSMPR) crystallizer. Supersaturation is created by changing the pH of a DPH solution in the crystallization vessel. Crystal size distributions (CSD's) are measured by an in situ zone sensing method. Effects of pH and supersaturation on crystallization kinetics and CSD are summarized. The effect of an additive on the crystal growth of DPH has been studied in a batch system. Avoidance of nucleation in the early stages of crystallization is essential t
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Jana, Sarbojeet. "Crystallization behavior of waxes." Thesis, Utah State University, 2016. http://pqdtopen.proquest.com/#viewpdf?dispub=10239292.

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<p> Crystallization behavior of different waxes such as beeswax (BW), paraffin wax (PW), ricebran wax (RBW), sunflower wax (SFW) was studied individually and in different oil solutions. Binary mixture at various proportions of the individual waxes was also explored in this study. Soybean oil is used in most of the study but olive, corn, sunflower, safflower, and canola oils were also explored. Lipid crystalline networks were characterized by several physical properties such as melting profile, solid fat content, viscoelastic parameters, cooling rate, phase behavior, crystal morphology. High in
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Taffs, Jade. "Local structure in crystallization." Thesis, University of Bristol, 2015. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.685975.

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In the work presented here, we use simulations of hard and nearly-hard spheres to examine the role of local structures in crystallisation. We are motivated by the work of Sir Charles Frank, who suggested that locally favoured structures, if incommensurate with crystalline ordering, could potentially suppress nucleation [1). Structural analysis is carried out using the topological cluster classification [2], which identifies those local arrangements of 5 < n < 13 particles which are structurally equivalent to the ground state structure for 11 particles considered in isolation. Initial work comp
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Libri sul tema "Crystallization"

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Beckmann, Wolfgang, ed. Crystallization. Wiley-VCH Verlag GmbH & Co. KGaA, 2013. http://dx.doi.org/10.1002/9783527650323.

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Mullin, J. W. Crystallization. 3rd ed. Butterworth-Heinemann, 1993.

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Reiter, Günter, and Jens-Uwe Sommer, eds. Polymer Crystallization. Springer Berlin Heidelberg, 2003. http://dx.doi.org/10.1007/3-540-45851-4.

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Tavare, Narayan S. Industrial Crystallization. Springer US, 1995. http://dx.doi.org/10.1007/978-1-4899-0233-7.

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M, Bergfors Terese, ed. Protein crystallization. International University Line, 2008.

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H, Ohtaki, ed. Crystallization processes. Wiley, 1998.

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Gupta, Baskar Sen, and Shaliza Ibrahim, eds. Mixing and Crystallization. Springer Netherlands, 2000. http://dx.doi.org/10.1007/978-94-017-2290-2.

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Auriemma, Finizia, Giovanni Carlo Alfonso, and Claudio de Rosa, eds. Polymer Crystallization I. Springer International Publishing, 2017. http://dx.doi.org/10.1007/978-3-319-49203-2.

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Dosière, Marcel, ed. Crystallization of Polymers. Springer Netherlands, 1993. http://dx.doi.org/10.1007/978-94-011-1950-4.

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Herlach, Dieter M., ed. Solidification and Crystallization. Wiley-VCH Verlag GmbH & Co. KGaA, 2004. http://dx.doi.org/10.1002/3527603506.

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Capitoli di libri sul tema "Crystallization"

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Beckmann, Wolfgang. "Crystallization: Introduction." In Crystallization. Wiley-VCH Verlag GmbH & Co. KGaA, 2013. http://dx.doi.org/10.1002/9783527650323.ch1.

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Wieckhusen, Dierk. "Development of Batch Crystallizations." In Crystallization. Wiley-VCH Verlag GmbH & Co. KGaA, 2013. http://dx.doi.org/10.1002/9783527650323.ch10.

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Hofmann, Günter, and Christian Melches. "Continuous Crystallization." In Crystallization. Wiley-VCH Verlag GmbH & Co. KGaA, 2013. http://dx.doi.org/10.1002/9783527650323.ch11.

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Beckmann, Wolfgang. "Precipitation." In Crystallization. Wiley-VCH Verlag GmbH & Co. KGaA, 2013. http://dx.doi.org/10.1002/9783527650323.ch12.

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Nienhaus, Bernd. "Mixing in Crystallization Processes." In Crystallization. Wiley-VCH Verlag GmbH & Co. KGaA, 2013. http://dx.doi.org/10.1002/9783527650323.ch13.

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Wieckhusen, Dierk, and Wolfgang Beckmann. "Downstream Processes." In Crystallization. Wiley-VCH Verlag GmbH & Co. KGaA, 2013. http://dx.doi.org/10.1002/9783527650323.ch14.

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Ulrich, Joachim, and Torsten Stelzer. "Melt Crystallization." In Crystallization. Wiley-VCH Verlag GmbH & Co. KGaA, 2013. http://dx.doi.org/10.1002/9783527650323.ch15.

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Hofmann, Günter, and Christian Melches. "Examples of Realized Continuous Crystallization Processes." In Crystallization. Wiley-VCH Verlag GmbH & Co. KGaA, 2013. http://dx.doi.org/10.1002/9783527650323.ch16.

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Ulrich, Joachim, and Torsten Stelzer. "Design Examples of Melt Crystallization." In Crystallization. Wiley-VCH Verlag GmbH & Co. KGaA, 2013. http://dx.doi.org/10.1002/9783527650323.ch17.

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Beckmann, Wolfgang. "Mechanisms of Crystallization." In Crystallization. Wiley-VCH Verlag GmbH & Co. KGaA, 2013. http://dx.doi.org/10.1002/9783527650323.ch2.

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Atti di convegni sul tema "Crystallization"

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Trnka, Jan, and Franti�ek �tep�nek. "Modeling the Impact of Non-Ideal Mixing on Continuous Crystallization: A Non-Dimensional Approach." In The 35th European Symposium on Computer Aided Process Engineering. PSE Press, 2025. https://doi.org/10.69997/sct.194630.

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Mathematical modeling is essential for the effective control of many chemical engineering processes, including crystallization. However, most existing crystallization models used in industry and academia assume ideal mixing. As a result, the unclear effects of imperfect mixing on crystallization, reported in experimental studies, remain largely unexplained. In this work we aim to address this gap in understanding by examining antisolvent crystallization processes on a�general theoretical level, using a novel dimensionless model. To address the impact of mixing on crystallization, we employ the
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Barhate, Yash, Yung Shun Kang, Neda Nazemifard, et al. "Data-driven Digital Design of Pharmaceutical Crystallization Processes." In The 35th European Symposium on Computer Aided Process Engineering. PSE Press, 2025. https://doi.org/10.69997/sct.128994.

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Mechanistic population balance modeling (PBM) has advanced the design of pharmaceutical crystallization processes, enabling the production of active pharmaceutical ingredient (API) crystals with desired critical quality attributes (CQAs), such as purity and crystal size distribution. However, PBM development can sometimes be resource-intensive, requiring extensive design of experiments (DoE) and high-quality process data, making it impractical under fast-paced industrial development timelines. This study proposes a machine learning (ML)-based workflow for developing �fit-for-purpose� digital t
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Wohn, Donghee Yvette, and Brian J. Bowe. "Crystallization." In the companion publication of the 17th ACM conference. ACM Press, 2014. http://dx.doi.org/10.1145/2556420.2556509.

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Wallbank, M., and J. Jarvis. "Realizing Steady-State Microbunching with Optical Stochastic Crystallization." In Realizing Steady-State Microbunching with Optical Stochastic Crystallization. US DOE, 2024. http://dx.doi.org/10.2172/2440009.

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Forsberg, Kerstin. "Crystallization challenges in hydrometallurgy." In Proceedings of XVI International Mineral Processing and Recycling Conference, Belgrade, 28-30.05.2025. University of Belgrade, Technical Faculty, Bor, 2024. https://doi.org/10.5937/imprc25050f.

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Crystallization and precipitation processes are of key relevance in extractive metallurgy. In battery recycling eutectic freeze crystallization has recently emerged as an energy saving alternative to evaporative crystallization. Crystallization of Ni, Co, and Mn sulphate salts of high purity can be obtained by this technology. Antisolvent crystallization can also provide interesting advantaged within extractive metallurgy. In particular the crystallization of rare earth salts has shown promising results. This work will highlight challenges and opportunities connected to these 2 unit operations
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Goncharenko, О. P., and I. L. Lashina. "ENVIRONMENT OF POTASSIUM-MAGNESIUM SALT FORMATION IN THE UPPERPERMIAN KALININGRAD-GDANSK BLOCK OF THE CENTRAL EUROPEAN HALOGEN BASIN (FROMEXAMINATIONOFINCLUSIONSINMINERALS)." In Проблемы минералогии, петрографии и металлогении. Научные чтения памяти П. Н. Чирвинского. Пермский государственный национальный исследовательский университет, 2021. http://dx.doi.org/10.17072/chirvinsky.2021.25.

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Examination of inclusions in minerals makes the basis for analyzing the peculiarities of salt crystallizationin the Kaliningrad-Gdansk halogen block of the Central- European evaporite basin. Most of the studied sections are composed of fine – medium- grained rock made of halite impregnated with polyhalite, kieserite, carnallite and kainite. Threesystemsofmicro-inclusionsmaybedistinguishedamongthe wide diversity of inclusions: 1) inclusions of mineral-forming mediums; 2) inclusions of surrounding mediums; 3) solid inclusions captured by minerals during their growth from marine solutions. Thedea
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Scherer, G. W. "Factors affecting crystallization pressure." In International RILEM Workshop on Internal Sulfate Attack and Delayed Ettringite Formation. RILEM Publications SARL, 2004. http://dx.doi.org/10.1617/2912143802.009.

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Oliveira, Vinícius, Willian Righi Assis, and Erick de Moraes Franklin. "Crystallization in Bidispersed Beds." In 19th Brazilian Congress of Thermal Sciences and Engineering. ABCM, 2022. http://dx.doi.org/10.26678/abcm.encit2022.cit22-0058.

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Boix, Pablo P. "Device-oriented perovskite crystallization." In International Conference on Hybrid and Organic Photovoltaics. FUNDACIO DE LA COMUNITAT VALENCIANA SCITO, 2024. http://dx.doi.org/10.29363/nanoge.hopv.2024.067.

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Zhou, Guofu, Herman J. Borg, J. C. N. Rijpers, Martijn H. R. Lankhorst, and J. J. L. Horikx. "Crystallization behavior of phase-change materials: comparison between nucleation- and growth-dominated crystallization." In Optical Data Storage, edited by Douglas G. Stinson and Ryuichi Katayama. SPIE, 2000. http://dx.doi.org/10.1117/12.399337.

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Rapporti di organizzazioni sul tema "Crystallization"

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Yepez, Jeffrey. Lattice-Gas Crystallization. Defense Technical Information Center, 1994. http://dx.doi.org/10.21236/ada421735.

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HERTING DL. FRACTIONAL CRYSTALLIZATION FEED ENVELOPE. Office of Scientific and Technical Information (OSTI), 2008. http://dx.doi.org/10.2172/926177.

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Schiffer, J. P. Summary talk on beam crystallization. Office of Scientific and Technical Information (OSTI), 1993. http://dx.doi.org/10.2172/10194766.

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Rosenberg, Marlene. Coulomb Crystallization in Dusty Plasmas. Defense Technical Information Center, 1998. http://dx.doi.org/10.21236/ada354822.

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Roland, C. M., and Gary S. Buckley. Thermal Crystallization of Polytetrahydrofuran Networks. Defense Technical Information Center, 1989. http://dx.doi.org/10.21236/ada215336.

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Orebaugh, E. G. Simulation of salt waste evaporation/crystallization. Office of Scientific and Technical Information (OSTI), 1993. http://dx.doi.org/10.2172/10142007.

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Cullinan, Timothy Edward. Crystallization dynamics in glass-forming systems. Office of Scientific and Technical Information (OSTI), 2016. http://dx.doi.org/10.2172/1342537.

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Skone, Timothy J. Marcellus Shale Water Treatment with Crystallization. Office of Scientific and Technical Information (OSTI), 2011. http://dx.doi.org/10.2172/1509082.

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PERSON, J. C. LITERATURE SURVEY FOR FRACTIONAL CRYSTALLIZATION STUDY. Office of Scientific and Technical Information (OSTI), 2004. http://dx.doi.org/10.2172/828250.

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Orebaugh, E. G. Simulation of salt waste evaporation/crystallization. Office of Scientific and Technical Information (OSTI), 1993. http://dx.doi.org/10.2172/6645352.

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