Gotowe bibliografie tematyczne / RP-HPLC Techniques for Stability Testing

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Gotowa bibliografia na temat „RP-HPLC Techniques for Stability Testing”

Autor: Grafiati

Data publikacji: 2 czerwca 2025

Data aktualizacji: 31 lipca 2025

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Artykuły w czasopismach na temat "RP-HPLC Techniques for Stability Testing"

Abhijit, Pawane* Dr. Vishwas Bhagat Dr. Deepak Kardile M. M. Karne Dr. Rajkumar Shete. "A Review on RP-HPLC Techniques for Stability Testing in Drug Formulations." International Journal of Pharmaceutical Sciences 3, no. 5 (2025): 3474–97. https://doi.org/10.5281/zenodo.15476001.

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RP-HPLC is one advanced analytical technique, usually for&ensp;drug analysis, can make separation, identification and quantification of drug compounds. The wide range of analyzable compounds and its adaptability to a variety of&ensp;detection methods makes it especially useful for the stability testing of a drug formulation. The purpose of stability&ensp;testing in drug development is to promote the safety, efficacy and quality of the drug product during its shelf life. RP-HPLC is one of the methods that is widely used because of its higher&ensp;resolution, greater sensitivity, specificity, an

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Swapnil, Khopade* Dr. Deepak Kardile Aniket Mohite Dr. Vishwas Bhagat Tushar Shinde Dr. Rajkumar Shete Vaibhavi Kunjir. "The Role of Stability-Indicating RP-HPLC In Ensuring Drug Product Quality and Shelf Life." International Journal of Pharmaceutical Sciences 3, no. 3 (2025): 3509–31. https://doi.org/10.5281/zenodo.15115168.

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Reverse-phase high-performance liquid&ensp;chromatography (RP-HPLC) is commonly employed in pharmaceutical analysis for the isolation and quantification of drugs, impurities, and degradation products. Ensuring the quality of drug products and the shelf life—determined by the potency, safety, and efficacy of a particular drug—is an important assessment that is carried out through stability studies, where environmental variables such&ensp;as temperature, humidity, and storage conditions are tested to see how they affect the drug over time. Stability-indicating RP-HPLC method is one o

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Jain, Neha, Amol Kakde, and Mohan Lal Kori. "Simultaneous Method Development for Pseudoephedrine Hydrochloride and Desloratadine." Journal of Drug Delivery and Therapeutics 15, no. 6 (2025): 6–13. https://doi.org/10.22270/jddt.v15i6.7157.

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Introduction: Chromatographic techniques are primarily used for the qualitative and quantitative analysis of pharmaceutical compounds, drug formulations, and raw materials throughout the drug development process, from the early research phase to the final release of therapeutic products. Objective: Simple, accurate, economical and reproducible RP-HPLC method for simultaneous estimation of two component drug mixture pseudoephedrine hydrochloride and desloratadine in combined tablet dosage form. Material and methods: Developed HPLC method is reversed phase chromatographic method using inertsil C

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Shrivas, Narayan, and S. K. Mishra. "Development and Validation of a Stability-Indicating HPLC Technique for Measuring Temozolomide in its Pharmaceutical Dose Form." Oriental Journal Of Chemistry 37, no. 4 (2021): 900–904. http://dx.doi.org/10.13005/ojc/370418.

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Using RP-HPLC, an accurate and precise technique for the measurement of Temozolomide in its pharmaceutical dose form was developed and validated. Chromatographic separation was achieved on an X Terra RP 18(250mm x 4.6mm), 5 µ column using a mobile phase consisting of methanol and buffer in the ratio of 10:990v/v. The flow rate was 1mL/min with the detection wavelength of 254 nm and retention time was found to be 20 min. The developed method was validated according to ICH guidelines. With a correlation coefficient of 0.9990, linearity was observed in the range of 50-150 percent. The %RSD of the

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Somase, Kanchan, and Dinesh Rishipathak. "Finerenone API Estimation Using RP-HPLC Technique and LC-MS Characterization of its Degradation Products." Oriental Journal Of Chemistry 41, no. 2 (2025): 528–40. https://doi.org/10.13005/ojc/410222.

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Researchers developed an RP-HPLC method to measure finerenone (FIN) which exhibits specificity, accuracy, precision and sensitivity. The RP-HPLC instrument functioned through an Isocratic method using a 250 mm X 4.6 mm i.d., 5μm i.d. Phenomenex C18 reversed-phase column as its component. At 252 nm wavelength the detector selected Acetonitrile: water (50:50 v/v) for operation in its analytical procedures using the mobile phase. The programmed mobile phase moved at 1mL/min through the system. The time for FIN to retain in the system under examination amounting to 4.62. Between 80–120 μg/mL conce

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Sumit, Wakchaure* Sonali Waghmare Pradyumna Ige. "A Review Analytical Advances and Challenges in Quality Control Techniques for Corticosteroid Ophthalmic Suspensions." International Journal of Pharmaceutical Sciences 2, no. 12 (2024): 1261–69. https://doi.org/10.5281/zenodo.14365890.

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Ophthalmic suspensions, particularly corticosteroid formulations, require stringent quality control (QC) measures to ensure their stability, therapeutic efficacy, and safety for patient use. Key physicochemical parameters, such as viscosity, rheological properties, pH, and osmolality, are vital in maintaining the desired characteristics of the suspension. Particle size distribution (PSD) is particularly critical, influencing both the stability and bioavailability of the active pharmaceutical ingredient (API). In addition, chemical parameters such as the assay of the API using High-Performance

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Kalyani, Ashok Patil*1 Shailesh B. Patil2. "To Develop And Validate Stability Indicating Assay Of Diloxanide Furoate By Using UV And HPLC And HPTLC Method For Pharmaceutical Dosage Form." International Journal in Pharmaceutical Sciences 2, no. 6 (2024): 498–517. https://doi.org/10.5281/zenodo.11543189.

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The study aimed to establish stability assays for Diloxanide Furoate using both High-Performance Liquid Chromatography (HPLC) and High-Performance Thin-Layer Chromatography (HPTLC) methods, covering crucial aspects of method development and validation. Detailed specifications were provided for the HPLC and HPTLC systems to ensure proper setup and functioning. Chromatographic conditions were optimized, including parameters like stationary phase, mobile phase composition, flow rate, and detection wavelength, to achieve optimal separation and detection of Diloxanide Furoate. The identity of pure

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Jeličić, Mario-Livio, Edvin Brusač, Daniela Amidžić Klarić, Biljana Nigović, Sabina Keser, and Ana Mornar. "Physicochemical Compatibility Investigation of Mesalazine and Folic Acid Using Chromatographic and Thermoanalytical Techniques." Pharmaceuticals 13, no. 8 (2020): 187. http://dx.doi.org/10.3390/ph13080187.

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Inflammatory bowel disease is a common name for Crohn’s disease and ulcerative colitis. These inflammatory states cause damage in the sidewalls of the gastrointestinal tract, resulting in malabsorption of food and vitamins. Folic acid (Vitamin B9) is often associated with inflammatory bowel diseases since reduced overall folate concentration in the human body may lead to the development of colorectal cancer and megaloblastic anaemia. However, its deficiency is easily compensated by taking an additional folic acid pill during regular therapy. At the moment, there are no studies that have examin

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Collie, Jake T. B., Ronda F. Greaves, Oliver A. H. Jones, Glenn Eastwood, and Rinaldo Bellomo. "Vitamin C measurement in critical illness: challenges, methodologies and quality improvements." Clinical Chemistry and Laboratory Medicine (CCLM) 58, no. 4 (2020): 460–70. http://dx.doi.org/10.1515/cclm-2019-0912.

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AbstractBackgroundThere is renewed interest in high-dose vitamin C interventions in clinical medicine due to its antioxidant properties, safe use and cost-effectiveness. Yet, randomised control trials (RCTs) employing these interventions are failing to include robust analytical methodology and proper sample handling and processing techniques. Consequently, comparisons between studies becomes impossible as there is no metrological traceability and results may be prone to pre-analytical errors.ContentThrough published vitamin C stability studies, method comparison papers and data from vitamin C

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Bhanja, Mrutyunjaya, and Aayush Vaishnaw. "Development and validation of a pediatric dosage form for a commonly used medication." Journal of Neonatal Surgery 14, no. 1S (2025): 72–78. https://doi.org/10.52783/jns.v14.1498.

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Pediatric children often have difficulty administering their drugs due to a lack of age-appropriate dosage forms, which can result in inadequate therapeutic effects and poor compliance. The creation and validation of a pediatric dosage form for the regularly administered medications acetaminophen and ibuprofen for feverish conditions is the main focus of this study. By creating a kid-friendly dosage form, the study sought to address important formulation issues such as dose accuracy, taste acceptability, and excipient safety. Using a methodical approach, formulations such liquid suspensions an

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Części książek na temat "RP-HPLC Techniques for Stability Testing"

Konarachapalle, Nagalakshmi. "Chromatographic Techniques." In Analytical Methods for Drug Development. THINKPLUS PHARMA PUBLICATIONS, 2025. https://doi.org/10.69613/j49f3p67.

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Chromatographic methods separate complex pharmaceutical mixtures based on differential interactions between components, mobile phases, and stationary phases. HPLC techniques utilize diverse separation mechanisms, stationary phases, mobile phase compositions, and detection systems for pharmaceutical assays, impurity profiling, and stability studies. Gas chromatography analyzes volatile compounds, residual solvents, and headspace samples with temperature programming, specialized columns, and various detection systems. Ion chromatography quantifies counterions, ionic impurities, and ionic formula

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Segall, Adriana. "Preformulation: Active Pharmaceutical Ingredient-Excipient Compatibility Studies." In Advanced Pharmacy. BENTHAM SCIENCE PUBLISHERS, 2023. http://dx.doi.org/10.2174/9789815049428123010004.

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A relevant area of research in the preformulation phase for the development of new dosages is active pharmaceutical ingredient (API)-excipient compatibility. The possibilities of chemical and physical interaction of API and the excipients may affect how efficient and effective it is, while displaying an impact on the nature, stability and availability of API. The most common signs of deterioration of an API are changes in the color, taste, odor, polymorphic form, or crystallization (pharmaceutical incompatibility). These changes arise from chemical reactions with the excipient, leading to degr

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Jain, Paras, N. V. D. Prasad Ketha, and Buchi N. Nalluri. "A High-Performance Liquid Chromatographic Method for Dissolution Testing of Lurasidone Tablets." In Current Trends in Drug Discovery, Development and Delivery (CTD4-2022). Royal Society of Chemistry, 2023. http://dx.doi.org/10.1039/9781837671090-00296.

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A simple, rapid, selective, and reproducible HPLC method for Lurasidone Hydrochloride tablet release estimation has been developed and validated. An Agilent, X-Bridge column C18,150*4.6 mm, 3.5m was used to produce a symmetrical peak form at a regulated column temperature of 25°C with a flow rate of 1.5 mL/min, a mobile phase component of A and B in the ratio of 30:70, a run time of 14 minutes, and an isocratic elution. Mobile phase A is 0.2% ammonia in water with a pH of 8.5, and mobile phase B is 98:2 acetonitrile and water. At 232 nm, 25 μL sample solutions were injected. A two-stage acid-b

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Streszczenia konferencji na temat "RP-HPLC Techniques for Stability Testing"

Jadhav, Rahul, and Thomas Pisklak. "Liquid Strength Retrogression Control Additive." In SPE/IADC Middle East Drilling Technology Conference and Exhibition. SPE, 2021. http://dx.doi.org/10.2118/202104-ms.

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Abstract To mitigate strength retrogression at temperatures, higher than 230°F, well cement designs typically include strength retrogression control additives (SRCAs). Solid siliceous materials (e.g., silica flour, fume, and sized-sands) are commonly used SRCAs that are incorporated into cements using dry-blending techniques. This study highlights liquid silica compositions as alternative SRCAs to dry-blended silica for high-temperature cementing. Liquid additives can be managed easily, delivered accurately, and offer a reduced on-site footprint, thus making them particularly advantageous for

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Czuprat, Oliver, Kjetil Eriksen, Duncan Clinch, et al. "Systematic Selection of Drill-In and Completion Fluids for Development of the Dvalin HT Gas Field - Part II: Successful Clean-Up Validates Experimental Qualification Approach." In SPE/IADC International Drilling Conference and Exhibition. SPE, 2021. http://dx.doi.org/10.2118/204091-ms.

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Abstract Formation damage by the drill-in fluid has been identified as a major risk for the Dvalin HT gas field. To ensure the long-term stability and mobility of the mud even after an extended suspension time between drill-in and clean-up of the wells, a novel static aging test under downhole temperature and high pressure was conducted. Experiments have shown that the downhole stability is commonly underestimated when the surrounding pressure is lower than in the field. Thus, a high-pressure cylinder was used in vertical orientation in a heating oven with a pressure pump regulating the pressu

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