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Artykuły w czasopismach na temat „MPEG Lysinol Ring opening polymerization”

Autor: Grafiati

Data publikacji: 2 czerwca 2025

Data aktualizacji: 31 lipca 2025

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1

Geng, Dian Guang, Yong Ming Chuan, Li Li Li, and Ming Long Yuan. "The Preparation and Characterization of ABC-Shaped Star Copolymer of MPEG-PCL-PBLG." Advanced Materials Research 750-752 (August 2013): 1358–62. http://dx.doi.org/10.4028/www.scientific.net/amr.750-752.1358.

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A novel biodegradable ABC-shaped star copolymer, poly (ethylene glycol)(PEG)-b-poly (ε-caprolactone)(PCL)-poly-c-poly (ɤ-benzyl-L-glutamic acid)(PBLG)(MPEG-PCL-PBLG), was synthesized by the graft polymerization of MPEG-NH2with the core of Boc-LYSZ-COOH and the twice ring-opening polymerization (ROP) of ε-caprolactone (CL) and N-carboxyanhydride of ɤ-benzyl-L-glutamate (BLGNCA) with centrally amino-functionalized lysine as a initiator. The ABC-shaped star copolymer and its precursors were characterized by1H NMR, GPC, and DSC-TG measurements.

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2

Cheng, Yu-En, I.-En Wu, Yi-Chen Chen, and I.-Ming Chu. "Thermo-Sensitive mPEG-PA-PLL Hydrogel for Drug Release of Calcitonin." Gels 8, no. 5 (2022): 282. http://dx.doi.org/10.3390/gels8050282.

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The oral route is the most popular way of drug administration because of good patient compliance and ease of use. However, the oral delivery of peptides and proteins is difficult, mainly due to poor oral bioavailability. In past decades, researchers have developed several strategies to improve oral bioavailability by avoiding losing activity in the gastrointestinal (GI) tract and enhancing the intestinal permeability of these drugs. Methoxy poly(ethylene glycol)-poly(l-alanine) (mPEG-PA) is a thermo-sensitive hydrogel exhibiting a sol-to-gel phase transition property. This characteristic is ap

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3

Efthimiadou, Eleni. "New approach in synthesis, characterization and release study of pH-sensitive polymeric micelles, based on PLA-Lys-b-PEGm, conjugated with doxorubicin." Journal of nanoparticle research 13, no. 12 (2011): 6725–36. https://doi.org/10.1007/s11051-011-0579-5.

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Amphiphilic block copolymers are well established as building blocks for the preparation of micellar drug carriers. The functional polymer micelles possess several advantages, such as high drug efficiency, targeted delivery, and minimized cytotoxicity. The synthesis of block copolymers using nanostructured templates has emerged as a useful and versatile approach for preparing drug carriers. Here, we report the synthesis of a smart polymeric compound of a diblock PLA-Lys-b-PEG copolymer containing doxorubicin. We have synthesized functionalized diblock copolymers, with lysinol, poly(lactide) an

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4

Qi, Yanxin, Bin Li, Yupeng Wang, and Yubin Huang. "Synthesis and sequence-controlled self-assembly of amphiphilic triblock copolymers based on functional poly(ethylene glycol)." Polymer Chemistry 8, no. 45 (2017): 6964–71. http://dx.doi.org/10.1039/c7py01680h.

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Given the increasing prosperity of multifunctional poly(ethylene glycol) (mf-PEG), an amphiphilic triblock copolymer, poly(ethylene glycol)-block-poly(ε-caprolactone)-block-poly(allyl glycidyl ether) (mPEG-PCL-PAGE), was synthesized by a combination of living ring-opening polymerization (ROP) and click chemistry.

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5

Wu, Wenjing, Weixin Wu, Mingwei Guo, Ruizhe Wang, Xuanxuan Wang, and Qinwei Gao. "Synthesis of MPEG-b-PLLA Diblock Copolymers and Their Crystallization Performance with PDLA and PLLA Composite Films." Materials 17, no. 9 (2024): 2105. http://dx.doi.org/10.3390/ma17092105.

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Methoxy poly(ethylene glycol)-block-poly(L-lactide) (MPEG-b-PLLA) has a wide range of applications in pharmaceuticals and biology, and its structure and morphology have been thoroughly studied. In the experiment, we synthesized MPEG-b-PLLA with different block lengths using the principle of ring-opening polymerization by controlling the amount of lactic acid added. The thermodynamic properties of copolymers and the crystallization properties of blends were studied separately. The crystallization kinetics of PDLA/MPEG-b-PLA and PLLA/MPEG-b-PLA composite films were studied using differential sca

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6

Ko, Youn Kyung, Soon Hee Kim, Hyun Jung Ha, et al. "Hybrid Type of Tissue Engineered Biodisc Using Annulus Fibrosus Seeded PLGA Scaffold and Nucleus Pulposus Seeded MPEG-PCL Hydrogel: Preliminary Study." Key Engineering Materials 342-343 (July 2007): 173–76. http://dx.doi.org/10.4028/www.scientific.net/kem.342-343.173.

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Recently, it has been studied tissue engineered technique as novel approaches for treatment of the degenerative intervertebral disc (IVD). We designed the hybrid type of IVD mimicked scaffolds with poly(lactide-co-glycolide) (PLGA) and methoxypoly(ethyleneglycol)- poly(-caprolactone) (MPEG-PCL) diblock copolymers in order to application for the tissue engineered IVD. The MPEG-PCL solutions formed a gel-to-sol phase transitions as the temperature was increasesd. MPEG-PCL diblock copolymers were prepared by ring opening polymerization, and then nucleus pulposus (NP) cell was impregnated. Also, i

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7

Shang, Pei, Jie Wu, Xiaoyu Shi, Zhidan Wang, Fei Song, and Shouxin Liu. "Synthesis of Thermo-Responsive Block-Graft Copolymer Based on PCL and PEG Analogs, and Preparation of Hydrogel via Click Chemistry." Polymers 11, no. 5 (2019): 765. http://dx.doi.org/10.3390/polym11050765.

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Thermo-responsive cross-linkable mPEG-b-[PCL-g-(MEO2MA-co-OEGMA)]-b-mPEG was synthesized by ring-opening polymerization (ROP) and atom transfer radical polymerization (ATRP). Then, the cross-linkable block-graft copolymer was used to prepare hydrogel via a copper-catalyzed 1,3-dipolar azide-alkyne cycloaddition reaction. The chemical structure and composition of copolymer were characterized by proton nuclear magnetic resonance (1H NMR), Fourier-transform infrared (FT-IR) and gel permeation chromatography (GPC). The self-assembly behaviors of the copolymer in aqueous solution were studied by UV

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8

Tapdiqov, Shamo Zokhrab. "Encapsulation and In Vitro Controlled Release of Doxycycline in Temperature-Sensitive Hydrogel Composed of Polyethyleneglycol–polypeptide (L-Alanine-co-L-Aspartate)." Journal of Biomimetics, Biomaterials and Biomedical Engineering 49 (February 2021): 119–29. http://dx.doi.org/10.4028/www.scientific.net/jbbbe.49.119.

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Doxycycline was loaded with synthesized micelles composed of methyl Poly (ethylene glycol-block-poly (L-alanine–co–L-aspartate), or mPEG–Ala–Asp, and then characterized as a drug delivery carrier. The synthesis of the temperature-sensitive mPEG–Ala–Asp block copolymer was carried out by two-step ring-opening polymerization: firstly, the mPEG reacts with L-alanine N-carboxylic anhydride, and secondly the resulting mPEG–Ala reacts with benzyl aspartate N-carboxylic anhydride. The molecular structure of the copolymers obtained was determined by FT-IR and NMR spectroscopy methods and the micelles

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9

Luo, Chunhui, Chongyi Chen, and Zhibo Li. "Efficient synthesis and self-assembly of hetero-grafted amphiphilic polypepide bottlebrushes." Pure and Applied Chemistry 84, no. 12 (2012): 2569–78. http://dx.doi.org/10.1351/pac-con-12-02-07.

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A new type of hetero-grafted molecular bottlebrush with polypeptide as backbone was synthesized using graft-onto strategy. Poly(γ-propargyl-L-glutamate) (PPLG) as backbone was firstly synthesized via ring-opening polymerization (ROP) of γ-propargyl-L-glutamate (PLG) N-carboxyanhydride (NCA). Next, polystyrene-N3 (PS-N3) and monomethoxy poly(ethylene glycol)-N3 (mPEG-N3) as side chains were grafted onto the PPLG backbone using copper-catalyzed click reaction, which afforded good grafting density and efficiency. Two polypeptide bottlebrushes with PS-to-mPEG molar ratio at 70/30 and 30/70 were pr

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10

Liu, Lian, Pei Wang, Chao Qu, Zhi Yong Wei та Min Qi. "Synthesis, Characterization and Crystallization of Poly(Ethylene Glycol)-b-Poly(ε-Caprolactone)". Advanced Materials Research 152-153 (жовтень 2010): 1665–68. http://dx.doi.org/10.4028/www.scientific.net/amr.152-153.1665.

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A family of poly(ethylene glycol)-b-poly(ε-caprolactone) (PEG-PCL) were synthesized in high yields by the ring-opening polymerization of monomethoxy-terminated poly(ethylene glycol) (mPEG) with ε-caprolactone in the presence of stannous octoate (Sn(Oct)2). Their crystallization behaviors were studied by DSC, XRD. The results illustrated that crystallization behaviors of the copolymers depended on the copolymer composition and the relative length of each block in copolymers. The melting peak of PCL block appeared gradually in the XRD patterns and DSC curves in copolymers, with increasing of the

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11

Nifant’ev, Ilya, Andrei Siniavin, Eduard Karamov, et al. "A New Approach to Developing Long-Acting Injectable Formulations of Anti-HIV Drugs: Poly(Ethylene Phosphoric Acid) Block Copolymers Increase the Efficiency of Tenofovir against HIV-1 in MT-4 Cells." International Journal of Molecular Sciences 22, no. 1 (2020): 340. http://dx.doi.org/10.3390/ijms22010340.

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Despite the world’s combined efforts, human immunodeficiency virus (HIV), the causative agent of AIDS, remains one of the world’s most serious public health challenges. High genetic variability of HIV complicates the development of anti-HIV vaccine, and there is an actual clinical need for increasing the efficiency of anti-HIV drugs in terms of targeted delivery and controlled release. Tenofovir (TFV), a nucleotide-analog reverse transcriptase inhibitor, has gained wide acceptance as a drug for pre-exposure prophylaxis or treatment of HIV infection. In our study, we explored the potential of t

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12

Xiao, Yin, Hui Peng, Xueli Mao, Andrew K. Whittaker, and Ross Crawford. "Novel Synthetic Bio-Mimic Polymers for Cell Delivery." Advanced Materials Research 32 (February 2008): 215–22. http://dx.doi.org/10.4028/www.scientific.net/amr.32.215.

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Cell-based therapy is one of the major potential therapeutic strategies for cardiovascular, neuronal and degenerative diseases in recent years. The aims of this study is to develop a novel biomimic polymeric materials which will facilitate the delivery cells, control cell bioactivities and enhance the focal integration of graft cells with host tissues. We synthesized a novel tri-block copolymer, methoxy-terminated poly (ethylene glycol) (MPEG)-polyL-lactide (PLLA)-polylysine (PLL) via sequential polymerization of PLLA onto MPEG, followed by ring opening polymerization of PLL onto the functiona

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13

Brunzel, Michaela, Tobias Majdanski, Jürgen Vitz, Ivo Nischang, and Ulrich Schubert. "Fast Screening of Diol Impurities in Methoxy Poly(Ethylene Glycol)s (mPEG)s by Liquid Chromatography on Monolithic Silica Rods." Polymers 10, no. 12 (2018): 1395. http://dx.doi.org/10.3390/polym10121395.

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The determination of diol impurities in methoxy poly(ethylene glycol)s (mPEG)s is of high importance, e.g., in the area of pharmaceutical applications, since mPEGs are considered the gold standard—based on properties of biocompatibility, stealth effect against the immune system, and well-established procedures used in PEGylation reactions. Herein, we communicate a straightforward and fast approach for the resolution of the PEGdiol impurities in mPEG products by liquid chromatography on reversed-phase monolithic silica-rods. Thus, we utilize fine, in-house prepared and narrow dispersity mPEGs (

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14

Chang, Jeong Ho, Kyung Ja Kim, and Young Kook Shin. "The Preparation of Pore-Size Controlled Mesoporous Silicas by Biodegradable Diblock Copolymers." Key Engineering Materials 287 (June 2005): 141–45. http://dx.doi.org/10.4028/www.scientific.net/kem.287.141.

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Selected MPEG-b-PDLLA block copolymers have been synthesized by ring-opening polymerization with systematic variation of the chain lengths of the resident hydrophilic and hydrophobic blocks. The size and shape of the micelles that spontaneously form in solution are then controlled by the characteristics of the block copolymer template. All the materials prepared in this study showed the tunable pore size of 20-80Å with the increase of hydrophobic chain lengths and up to 660m2/g of specific surface area. The formation mechanism of these nanoporous structures obtained by controlling the micelle

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15

Zhao, Guangkuo, Tongtong Ge, Yunfeng Yan, Qi Shuai, and Wei-Ke Su. "Highly Efficient Modular Construction of Functional Drug Delivery Platform Based on Amphiphilic Biodegradable Polymers via Click Chemistry." International Journal of Molecular Sciences 22, no. 19 (2021): 10407. http://dx.doi.org/10.3390/ijms221910407.

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Amphiphilic copolymers with pendant functional groups in polyester segments are widely used in nanomedicine. These enriched functionalities are designed to form covalent conjugates with payloads or provide additional stabilization effects for encapsulated drugs. A general method is successfully developed for the efficient preparation of functional biodegradable PEG-polyester copolymers via click chemistry. Firstly, in the presence of mPEG as initiator, Sn(Oct)2-catalyzed ring-opening polymerization of the α-alkynyl functionalized lactone with D,L-lactide or ε-caprolactone afforded linear mPEG-

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16

Lee, Ren-Shen, та Yi-Ting Huang. "Synthesis and characterization of amphiphilic block–graft MPEG-b-(PαN3CL-g-alkyne) degradable copolymers by ring-opening polymerization and click chemistry". Journal of Polymer Science Part A: Polymer Chemistry 46, № 13 (2008): 4320–31. http://dx.doi.org/10.1002/pola.22741.

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17

Fu, Tsai-Sheng, Yu-Hong Wei, Po-Yuan Cheng, I.-Ming Chu, and Wei-Chuan Chen. "A Novel Biodegradable and Thermosensitive Poly(Ester-Amide) Hydrogel for Cartilage Tissue Engineering." BioMed Research International 2018 (December 19, 2018): 1–12. http://dx.doi.org/10.1155/2018/2710892.

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Thermosensitive hydrogels are attractive alternative scaffolding materials for minimally invasive surgery through a simple injection and in situ gelling. In this study, a novel poly(ester-amide) polymer, methoxy poly(ethylene glycol)-poly(pyrrolidone-co-lactide) (mPDLA, P3L7) diblock copolymer, was synthesized and characterized for cartilage tissue engineering. A series of amphiphilic diblock copolymers was synthesized by ring-opening polymerization of mPEG 550, D,L-lactide, and 2-pyrrolidone. By dynamic light scattering analysis and tube-flipped-upside-down method, viscoelastic properties of

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18

Son, Young Ju, and Hyuk Sang Yoo. "pH-responsive microspheres encapsulated with iron oxide nanoaggregates for gastrointestinal delivery." Journal of Bioactive and Compatible Polymers 27, no. 1 (2012): 54–66. http://dx.doi.org/10.1177/0883911511430537.

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Block copolymer-stabilized iron oxide nanoaggregates were fabricated into pH-responsive polymeric microspheres for intestinal delivery of the magnetic nanoaggregates. A diblock copolymer consisted of methoxy poly(ethylene glycol) (mPEG) and poly(e-caprolactone) (PCL) was synthesized by ring-opening polymerization. Microspheres, consisted of Eudragit L100-55 encapsulate and stabilized magnetic nanoaggregates, were prepared by an oil-in-oil emulsification technique. The magnetization of the microspheres decreased, and the stability of the magnetic nanoaggregates in aqueous solutions increased as

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19

Khodir, Wan Khartini Wan Abdul, Mohamad Wafiuddin Ismail, Shafida Abd Hamid, et al. "Synthesis and Characterization of Ciprofloxacin Loaded Star-Shaped Polycaprolactone–Polyethylene Glycol Hydrogels for Oral Delivery." Micromachines 14, no. 7 (2023): 1382. http://dx.doi.org/10.3390/mi14071382.

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The administration of poorly water-soluble drugs represents a relevant problem due to the low body fluids transport efficiency through hydrophilic hydrogels. Star-shaped co-polymers, i.e., amphiphilic polymers such as those with a hydrophobic core and a hydrophilic outer shell, can be used to improve weak interactions with drugs, with relevant benefits in terms of administration and controlled delivery. In this work, two different co-polymers, four-arm star-shaped PCL–PEG and six-arm star-shaped PCL–PEG, were synthesized via ring-opening polymerization to be loaded with ciprofloxacin. 1H-NMR a

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20

Gharebaghi, Farhad, Naser Dalali, Ebrahim Ahmadi, and Hossein Danafar. "Preparation of wormlike polymeric nanoparticles coated with silica for delivery of methotrexate and evaluation of anticancer activity against MCF7 cells." Journal of Biomaterials Applications 31, no. 9 (2017): 1305–16. http://dx.doi.org/10.1177/0885328217698063.

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Methotrexate is one of the most effective drugs that is commonly used in the treatment of cancer. However, its application is limited due to low solubility, high toxicity and rapid metabolism. Therefore, in the present study, worm-like polymeric nanoparticles as carrier of methotrexate were prepared using biodegradable copolymers (mPEG–PCL). The impact of nanoparticles’ geometry on the loading, delivery and drug’s anti-cancer activity was investigated. The di-block copolymer mPEG–PCL was being synthesized by a ring opening polymerization of ɛ-caprolactone in the presence of mPEG as the initiat

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21

Xu, Jing, Benkai Qin, Shujuan Luan, et al. "Acid-labile poly(ethylene glycol) shell of hydrazone-containing biodegradable polymeric micelles facilitating anticancer drug delivery." Journal of Bioactive and Compatible Polymers 33, no. 2 (2018): 119–33. http://dx.doi.org/10.1177/0883911517715658.

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Biodegradable pH-sensitive amphiphilic block polymer (mPEG-Hyde-PLGA) was synthesized via ring-opening polymerization, initiated from a hydrazone-containing macro-initiator. In this way, a pH-sensitive hydrazone bond was inserted into the backbone of block copolymer, linking hydrophilic poly(ethylene glycol) segment and hydrophobic poly(lactic-co-glycolic acid) segment. The copolymer self-assembled to form stable micelles with mean diameters below 100 nm and served as a drug delivery system for doxorubicin, with drug loading content of 5.3%. pH sensitivity of the hydrazone-containing micelles

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22

Huang, Sai Xi, Zi Hao Wang, Min Lin, Xiao Hui Fu, and Jing Sun. "One-pot preparation of polypeptide nanogels in aqueous solution via ring-opening polymerization-induced nano-gelation." Polymer Chemistry, 2023. http://dx.doi.org/10.1039/d3py00206c.

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In this work, polypeptide nanogels were prepared by an innovative strategy of ring-opening polymerization induced nano-gelation using α-amino-poly(ethylene oxide) (mPEG-NH2) as a macroinitiator in an aqueous solution.

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23

Baimark, Yodthong, Mangkorn Srisa-ard, Jirasak Threeprom, Robert Molloy та Winita Punyodom. "Synthesis and characterization of methoxy poly(ethylene glycol)-b-poly(DL-lactide-co-glycolide-co-ε-caprolactone) di block copolymers: Effects of block lengths and compositions". e-Polymers 7, № 1 (2007). http://dx.doi.org/10.1515/epoly.2007.7.1.1609.

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AbstractMethoxy poly(ethylene glycol)-b-poly(D,L-lactide-co-glycolide-co-ε- caprolactone) diblock copolymers, designated as MPEG-b-PDLLGCL, with different MPEG block lengths and DLL:G:CL ratios were synthesized via ring-opening polymerization in bulk using MPEG and stannous octoate as the initiating system. The diblock copolymers were characterized using a combination of FT-IR, 1HNMR, GPC and DSC. The percentage yields of the diblock copolymers were in excess of 90%. 1H-NMR analysis confirmed that the PDLLGCL blocks contained at least some random character. From their DSC curves, the diblock c

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24

Kim, D. K., M. Mikhaylova, M. Toprak, A. Guyou, Y. K. Jeong, and M. Muhammed. "Synthesis and Characterization of Magnetic Polymeric Nanospheres for Biomedical Applications." MRS Proceedings 750 (2002). http://dx.doi.org/10.1557/proc-750-y9.2.

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ABSTRACTEntrapment of proteins in biodegradable nanospheres has been widely investigated as a technique to produce sustained release formulations for protein or anti-cancer drugs administration. Amphiphilic PLLA-mPEG diblock copolymer was prepared by ring opening polymerization (ROP) to form polymeric nanoparticles with a core-shell structure. The main encapsulation technique done is a water-in-oil-in-water (w/o/w) solvent evaporation technique. Here, protein was encapsulated using a newly developed water-in-oil emulsion-solvent diffusion technique. This technique leads to the formation of an

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25

Ong, Pin Jin, Hui Yi Shuko Lee, Jayven Chee Chuan Yeo, et al. "A Copolymer of Monomethoxy Poly(ethylene glycol)‐Polycaprolactone as Form‐Stable Phase Change Materials for Thermal Energy Storage." ChemistrySelect 8, no. 39 (2023). http://dx.doi.org/10.1002/slct.202302997.

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AbstractIn this work, a series of monomethoxy poly(ethylene glycol)‐polycaprolactone (mPEG‐PCL) copolymers with different mass percentages of mPEG was chemically synthesized as form‐stable phase change materials (FSPCMs) for thermal energy storage (TES) application for the first time. Their chemical structures, surface morphology, and thermal properties were studied in terms of nuclear magnetic resonance (NMR), Fourier transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM), thermogravimetric analysis (TGA), and differential scanning calorimetry (DSC). 1H NMR, gel permeation

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Hua, Cong, Yi Zhang, and Yuanhao Liu. "Enhanced Anticancer Efficacy of Chemotherapy by Amphiphilic Y-Shaped Polypeptide Micelles." Frontiers in Bioengineering and Biotechnology 9 (December 31, 2021). http://dx.doi.org/10.3389/fbioe.2021.817143.

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Although the treatment modalities of cancers are developing rapidly, chemotherapy is still the primary treatment strategy for most solid cancers. The progress in nanotechnology provides an opportunity to upregulate the tumor suppression efficacy and decreases the systemic toxicities. As a promising nanoplatform, the polymer micelles are fascinating nanocarriers for the encapsulation and delivery of chemotherapeutic agents. The chemical and physical properties of amphiphilic co-polymers could significantly regulate the performances of the micellar self-assembly and affect the behaviors of contr

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