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Rozprawy doktorskie na temat „Neutron diffraction”

Autor: Grafiati

Data publikacji: 4 czerwca 2021

Data aktualizacji: 25 lipca 2025

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1

Wang, Duan Qiang. "Strain measurement using neutron diffraction." Thesis, Open University, 1996. http://oro.open.ac.uk/57651/.

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This thesis contains a study of improvement and application of strain measurement technique using neutron diffraction. A dedicated neutron strain scanner - ENGIN, funded by Ee. has been developed at ISIS. It has two radial collimators, allowing for the first time, measurements taken simultaneously at two orthogonal directions; uses Pawley refinement permitting both whole pattern and individual peak profile analysis and its positioner allow's specimens weighing 250 kg to be placed with an accuracy of 100 um. Strain measurement using neutron diffraction has been investigated under two extreme ci

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2

Lobban, Colin. "Neutron diffraction studies of ices." Thesis, University College London (University of London), 1998. http://discovery.ucl.ac.uk/10065569/.

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This thesis reports on a series of neutron diffraction measurements on ices in the medium-pressure range of the phase diagram in order to address several outstanding issues. The structure of ice II under its thermodynamic conditions of stability is unknown. Previous studies have used helium gas as the pressurising medium, which is included within the ice structure. Argon gas has been used in this work as the pressure medium, and the detailed structure of ice II is presented and discussed. Similarly, the structure of ice V under its conditions of stability is established for the first time by t

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3

Tait, Kimberly. "Inelastic Neutron Scattering and Neutron Diffraction Studies of Gas Hydrates." Diss., The University of Arizona, 2007. http://hdl.handle.net/10150/194926.

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Gas hydrates (clathrates) are elevated-pressure (P) and low-temperature (T) solid phases in which gas molecule guests are physically incorporated into hydrogen-bonded, cage-like ice host frameworks. Natural clathrates have been found worldwide in permafrost and in ocean floor sediments, as well as in the outer solar system (comets, Mars, satellites of the gas giant planets). Diffraction patterns have been collected of gas hydrates at various methane and ethane compositions by preparing samples in an ex situ gas hydrate synthesis apparatus, and CO₂ gas hydrates were prepared in situ to look at

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4

Morrell, Jonathan T. "Experimental evaluation of polychromatic neutron diffraction." Thesis, Massachusetts Institute of Technology, 2017. http://hdl.handle.net/1721.1/112368.

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Thesis: S.B., Massachusetts Institute of Technology, Department of Nuclear Science and Engineering, 2017.<br>This electronic version was submitted by the student author. The certified thesis is available in the Institute Archives and Special Collections.<br>Cataloged from student-submitted PDF version of thesis.<br>Includes bibliographical references (pages 57-58).<br>Neutron diffraction is a technique that allows scientists to measure the arrangement and motions of atoms in a crystalline lattice by observing neutrons scattering at angles that are characteristic of the interatomic distances o

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5

Dashjav, Enkhtsetseg, Raphael Hermann, and Frank Tietz. "High-temperature Neutron Diffraction of Li1.2Al0.2Ti1.8P3O12." Diffusion fundamentals 21 (2014) 21, S.1-2, 2014. https://ul.qucosa.de/id/qucosa%3A32431.

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6

Reynolds, John Melton. "Neutron diffraction and reflection studies of superconductors." Thesis, University of Oxford, 1998. http://ora.ox.ac.uk/objects/uuid:bab01bde-f42e-41ca-830e-655d41499408.

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I have studied two magnetic properties of superconductors using different neutron scattering techniques. Due to their magnetic moment and lack of electrical charge, neutrons can provide an extremely sensitive probe into magnetism on a small scale. Unusual magnetic structures have previously been observed in the non-superconducting PrBa<sub>2</sub>Cu<sub>3</sub>O<sub>6</sub>+<sub>δ</sub>, in particular showing a coupling between the rare-earth and the Cu-O<sub>2</sub> planes. For comparison, I have used elastic neutron scattering to measure the temperature dependent magnetic structure of the hi

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7

Ibberson, Richard M. "Neutron power diffraction studies of molecular crystals." Thesis, University of Reading, 1993. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.357200.

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8

Criswell, Leah. "Neutron diffraction and quasielastic neutron scattering studies of films of N-alkanes and a branched alkane absorbed on graphite." Diss., Columbia, Mo. : University of Missouri-Columbia, 2007. http://hdl.handle.net/10355/6010.

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Thesis (Ph. D.)--University of Missouri-Columbia, 2007.<br>The entire dissertation/thesis text is included in the research.pdf file; the official abstract appears in the short.pdf file (which also appears in the research.pdf); a non-technical general description, or public abstract, appears in the public.pdf file. Title from title screen of research.pdf file (viewed on March 11, 2008) Includes bibliographical references.

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9

Unruh, Troy Casey. "Development of a neutron diffraction system and neutron imaging system for beamport characterization." Thesis, Manhattan, Kan. : Kansas State University, 2009. http://hdl.handle.net/2097/2324.

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10

Filippone, Roberto. "Martensite characterization in multiphase steels using neutron diffraction." Thesis, McGill University, 2001. http://digitool.Library.McGill.CA:80/R/?func=dbin-jump-full&object_id=32958.

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Previous use of the diffraction technique as a means of characterizing microstructure in multiphase steels has been generally limited to measurements of retained austenite. Other phases, specifically martensite, have not been examined in complex microstructures since there exists peak overlap with ferrite. This research looks at using neutron diffraction as a means to characterize martensite in a multiphase steel microstructure, thus providing a more complete characterization tool.<br>Three low carbon steels, comprised of a dual-phase, ferrite-martensite microstructure, were used in this study

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11

Clarke, Stuart James. "Neutron diffraction studies of silicate and borate glasses." Thesis, University of Reading, 2006. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.493994.

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Two systems of glasses have been studied: soda-lime-silica and alkali borate glasses. Vitreous boron oxide was included as a standard for comparison with alkali borates. Silica and irradiated vitreous silica were included for low Q diffraction studies as comparison with previous results.

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12

Dong, Bo. "Neutron diffraction studies of lithium-based battery materials." Thesis, University of Sheffield, 2018. http://etheses.whiterose.ac.uk/19190/.

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13

Donnelly, Mary-Ellen. "Neutron diffraction of hydrogen inclusion compounds under pressure." Thesis, University of Edinburgh, 2017. http://hdl.handle.net/1842/31471.

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When ice is compressed alongside a gas, crystalline 'host - guest' inclusion compounds known as gas clathrate hydrates form. These compounds are of interest not only for their environmental and possible technological impact as gas storage and separation materials, but also for their ability to probe networks not readily adopted by the pure `host' water molecules, and to study the interactions between water and gas molecules. Despite the pressure dependent crystal structures being fully determined for a large variety of `guest' gas species there is still relatively little known about the crysta

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14

Bianchini, Matteo. "In situ diffraction studies of electrode materials for Li-ion and Na-ion batteries." Thesis, Amiens, 2015. http://www.theses.fr/2015AMIE0022/document.

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Ce travail vise à étudier les matériaux d'électrodes pour batteries Li-ion et Na-ion lors qu’ils fonctionnent à l'intérieur des batteries. Afin de comprendre l'évolution structurelle des matériaux alors que les ions Li+ ou Na+ sont insérés/extraits de leur cadre, on utilise principalement la diffraction, exploitant neutrons, rayons X et le rayonnement synchrotron (SR). Nous avons adopté une approche combinée des mesures ex situ, in situ et operando. Au début, nous avons conçu une cellule électrochimique pour mesures in situ de diffraction de neutrons sur poudre (NPD), avec un alliage en (Ti,Zr

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15

Ye, Hong. "X-ray diffraction, neutron diffraction and circular dichroism studies of nucleic acids and proteins." Thesis, Keele University, 1998. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.245601.

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16

Rovira, Esteva Muriel. "Short-range order in disordered phases using neutron diffraction." Doctoral thesis, Universitat Politècnica de Catalunya, 2014. http://hdl.handle.net/10803/283110.

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Neutron diffraction is a powerful technique that allows to probe the structure of disordered phases across a variety of length scales. However, due to the inherent complexity of these disordered hases, the analysis of the information contained in the experimental data is not obvious. In this work, a few alternative methods are presented that allow to make the most of the neutron diffraction measurements as well as the molecular configurations obtained from molecular dynamics simulations or data modelling. They mainly consist in a Bayesian approach to fit the molecular structures measured with

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17

Cheyne, Simon M. "Total neutron diffraction studies of disordered cyanide crystal structures." Thesis, University of Reading, 2004. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.402196.

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18

Hall, Christopher David. "Neutron diffraction and molecular dynamics studies of fluid halocarbons." Thesis, University of Liverpool, 1992. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.316495.

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19

Bourke, Mark A. M. "Residual stress measurement in engineering components by neutron diffraction." Thesis, Imperial College London, 1990. http://hdl.handle.net/10044/1/47782.

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20

Williams, Anthony James. "Synthesis and neutron diffraction studies of manganese oxide perovskites." Thesis, University of Cambridge, 2004. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.615786.

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21

Guthrie, Malcolm. "Developments in single-crystal neutron diffraction at high pressure." Thesis, University of Edinburgh, 2002. http://hdl.handle.net/1842/13969.

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An in-depth analysis of neutron powder-diffraction data from a sample of ice VII is presented. This study involved an attempt to extract information about the detailed nature of atomic disorder present in the water molecule, information only accessible via neutron techniques. The resulting difficulties lead to an exploration of the fundamental limits of powder-diffraction. This investigation highlighted a need to extend the maximum accessible pressure for single-crystal techniques that, for structural neutron-diffraction, is currently limited to 25kbars. The majority of the work constituting t

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22

Hamacher, Klaus A. "Neutron diffraction studies of organic and magnetic layered structures /." free to MU campus, to others for purchase, 1998. http://wwwlib.umi.com/cr/mo/fullcit?p9901240.

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23

McKnight, Thomas Kevin. "An Improved Flexible Neutron Detector For Powder Diffraction Experiments." BYU ScholarsArchive, 2005. https://scholarsarchive.byu.edu/etd/463.

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Large amounts of money are being applied to the construction of the next generation of spallation sources for neutron scattering. Neutron powder diffraction instruments will be an important element of these facilities and the incorporation of detectors into these instruments with a high neutron capture efficiency is desirable. A new detector design named the Flexible Embedded Fiber Detector (FEFD) has been developed and tested for this thesis. This detector is based on wavelength shifting fibers embedded in a zinc-sulfide lithium-fluoride based scintillator. The virtue of this design is that t

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24

Pang, Judy Wai Lan. "A neutron diffraction study of intergranular strains and plastic deformation." Thesis, National Library of Canada = Bibliothèque nationale du Canada, 1999. http://www.collectionscanada.ca/obj/s4/f2/dsk1/tape9/PQDD_0006/NQ41267.pdf.

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25

Fowkes, Amelia Jane. "High resolution powder neutron diffraction in solid state inorganic chemistry." Thesis, University of Oxford, 1998. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.299525.

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26

Parrot, Ingrid Michele. "X-ray and neutron diffraction studies of fibrous biological molecules." Thesis, Keele University, 2004. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.423428.

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27

Wilson, Claire. "Structure-reactivity relationships through X-ray and neutron diffraction studies." Thesis, Durham University, 1995. http://etheses.dur.ac.uk/5314/.

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This thesis is primarily concerned with the investigation of a structure-reactivity relationship in a series of pentacyclic Isodrin derivatives. These compounds undergo a two-hydrogen atom dyotropic rearrangement at vastly differing rates when apparently small structural changes are made. Two pairs of these isomers (with the formulas C(_16)H(_8)Cl(_10) and C(_16)H(_9)Cl(_9) ) have been investigated using both X-ray and neutron single crystal diffraction studies, at ambient and low temperatures. The experimental details of these studies are given for five experiments and the results of the leas

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28

Hayama, Shusaku. "Neutron and X ray diffraction studies of metal amine solutions." Thesis, University College London (University of London), 2001. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.249712.

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29

Xu, Xuelian. "X-ray and neutron diffraction studies of organic molecular crystals." Thesis, University of Strathclyde, 2005. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.416190.

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30

Van, Duijn Joost. "Powder neutron diffraction studies of some magnetic boron-containing compounds." Thesis, University of Cambridge, 2001. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.620967.

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31

Pope, Lisa Helen. "X-ray and neutron fibre diffraction studies of deoxyribonucleic acid." Thesis, Keele University, 1997. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.388355.

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32

Binns, Jack. "Development of high-pressure single-crystal neutron diffraction on KOALA." Thesis, University of Edinburgh, 2016. http://hdl.handle.net/1842/20416.

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This thesis project has focused on the development of high-pressure single-crystal diffraction experiments on the neutron Laue diffractometer KOALA at the OPAL reactor at ANSTO, Australia. Over the course of this project several candidate systems have been studied under conditions of high-pressure using X-ray diffraction with a view to their use in developmental experiments on KOALA. The results of two high-pressure KOALA experiments are presented as well as the notable results from X-ray diffraction on the candidate systems. The first experiment on hexamethylenetetramine provided valuable ins

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33

Alianelli, Lucia. "Characterization and modelling of imperfect crystals for thermal neutron diffraction." Université Joseph Fourier (Grenoble), 2002. http://www.theses.fr/2002GRE10170.

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34

Al-Hayalee, Yaseen Ahmed. "Neutron high angle fibre diffraction of biological and synthetic polymers." Thesis, Keele University, 1993. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.357084.

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35

Bachra, Bilber. "Studies of the structure of oxide glasses by neutron diffraction." Thesis, University of Reading, 1994. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.359050.

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36

Garawi, M. S. "Thermal neutron scattering by some molecular liquids." Thesis, University of Kent, 1987. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.378356.

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37

England, Roger D. "Measurement Of Residual Stresses in Diesel Components using X-ray, Synchrotron, and Neutron Diffraction." University of Cincinnati / OhioLINK, 2000. http://rave.ohiolink.edu/etdc/view?acc_num=ucin966625751.

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38

Lee, Jang Seob. "Solid-state NMR, X-ray diffraction and neutron diffraction studies on organic guest/zeolite ZSM-5 complexes." Thesis, University of British Columbia, 2007. http://hdl.handle.net/2429/31380.

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Zeolites are microcrystalline aluminosilicate materials that have intricate channel systems, into which molecules can be adsorbed. Important as industrial materials, they are used in gas separations, sorption and catalysis where the property of 'molecular sieving' is exhibited toward guest species. Thus, understanding the interactions between guest species and the host zeolite frameworks is central to predicting the syntheses and applications of zeolites, and this requires detailed structural information about the guest/zeolite complexes. For most zeolites, structure determination by single cr

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39

Boysen, Hans, Ines Kaiser-Bischoff, and Martin Lerch. "Anion diffusion processes in O- and N-mayenite investigated by neutron powder diffraction: Anion diffusion processes in O- and N-mayenite investigated by neutron powder diffraction." Diffusion fundamentals 8 (2008) 2, S. 1-7, 2008. https://ul.qucosa.de/id/qucosa%3A14148.

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The crystal structure of mayenite (ideal composition: Ca12Al14O33) consists of a (disordered) calcium-aluminate framework comprising 32 of the 33 oxygen anions. It contains large open cages, 1/6 of them being filled randomly by the remaining “free” oxygen which is available for diffusion and very high ionic conductivities. This extraframework oxygen could be substituted by nitrogen, opening up possibilities for a pure nitrogen ionic conductor. From high temperature neutron powder diffraction experiments, data analysis employing difference Fourier methods and anharmonic Debye-Waller factors and

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40

Davies, Edward. "Neutron diffraction studies of amorphous ice and amorphous ice co-deposits." Thesis, University of Kent, 1992. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.305366.

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41

Dutta, Monojit. "Residual stress measurement in engineering materials and structures using neutron diffraction." Thesis, Open University, 1999. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.301945.

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42

Coates, Leighton. "Quasi laue neutron and atomic resolution x-ray diffraction of endothiapepsin." Thesis, University of Southampton, 2002. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.249945.

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43

Jupe, Andrew Charles. "Development of X-ray and neutron diffraction methods for cement research." Thesis, Birkbeck (University of London), 2000. https://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.392173.

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44

Payne, Stephen John. "Critical scattering and time resolved neutron diffraction studies of phase transitions." Thesis, Keele University, 1998. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.245355.

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45

Shotton, Mark William. "DNA structure investigated using complementary x-ray and neutron fibre diffraction." Thesis, Keele University, 1998. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.245356.

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46

Bianchi, Laurent. "The structure of molecular liquids : neutron diffraction and molecular dynamics simulations." Thesis, University of Dundee, 2000. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.312329.

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47

McNally, Graham Michael. "High pressure synthesis and neutron diffraction studies of new magnetic manganites." Thesis, University of Edinburgh, 2018. http://hdl.handle.net/1842/31185.

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With the discovery of appreciable room temperature magnetoresistance (MR) in high Curie temperature (Tc) ferrimagnetic double perovskites such as Sr2FeMoO6, research surrounding other materials of this type has expanded. Most ferrimagnetic double perovskites of the formula A2BB'O6 have non-magnetic A-site cations, such as Sr2+, Ca2+ or Ba2+. Replacing non-magnetic cations with magnetic variants offers further possibilities to tune magnetic effects. This thesis focuses on the substitution of non-magnetic A-site cations with relatively small magnetic Mn2+ cations. This substitution is made possi

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48

Noor, Faizani M. "Advanced techniques for extracting structural information from neutron diffraction of glasses." Thesis, University of Warwick, 2016. http://wrap.warwick.ac.uk/82169/.

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The structures of lithium and lead tellurite glasses (Li2O-TeO2 and PbO-TeO2) are studied using the combinations of neutron diffraction, isotope substitution neutron diffraction, and synchrotron X-ray diffraction. Additional complementary methods such as density measurement, thermal analysis and Raman spectroscopy show that the tellurite networks in lithium and lead tellurite glasses exhibit similar behaviour as a function of composition. From the diffraction data, real-space interatomic information on the glasses was extracted. The local environments of Te remain largely unchanged in both gla

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49

Badyal, Yaspal Singh. "The structure of binary molten salt mixtures : a neutron diffraction study." Thesis, University of Leicester, 1994. http://hdl.handle.net/2381/34931.

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Structural modification in a series of polyvalent metal chloride - alkali chloride binary molten salt mixtures has been investigated using the pulsed neutron diffraction technique. Structure factors have been measured for NiCl2- KCl, NiCl2-LiCl and ZnCl2-LiCl samples spanning the entire composition range. The key finding was that the degree of structural modification is dependent on the relative size and polarising power of the two cation species. The mixtures of NiCl2, and ZnCl2, with LiCl largely appear to be admixtures of the two pure salt structures, whereas adding KCl to NiCl2 results in

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50

Castellan, John-Paul Adrian Gaulin B. D. "X-ray and neutron diffraction studies of strongly correlated electron systems." *McMaster only, 2007.

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