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Rozprawy doktorskie na temat „Organic compounds Synthesis”

Autor: Grafiati

Data publikacji: 4 czerwca 2021

Data aktualizacji: 30 lipca 2024

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1

Newington, Ian M. "Azo-anions in organic synthesis." Thesis, University of Oxford, 1985. http://ora.ox.ac.uk/objects/uuid:690ab891-be13-4582-a029-47974d20adac.

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Novel synthetic applications of ambident azo-anions derived from hindered hydrazones have been investigated. Reaction with electrophiles occurred predominantly at carbon as the N-addition pathway was sterically retarded. Trityl, diphenyl-4-pyridylmethyl (DPP) benzhydryl, and t-butyldiphenylmethyl (BDP) hydrazones of various aldehydes and ketones were prepared in good yields from the corresponding hydrazines and carbonyls in aqueous methanol. The lithium salts derived from trityl and DPP hydrazones, by treatment with methyl lithium at -55°C, reacted with aldehydes and ketones to generate azo-al

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2

Esfandiarfard, Keyhan. "Novel Organophosphorus Compounds for Materials and Organic Synthesis." Doctoral thesis, Uppsala universitet, Molekylär biomimetik, 2017. http://urn.kb.se/resolve?urn=urn:nbn:se:uu:diva-328295.

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This thesis is devoted to the development of new organophosphorus compounds for potential uses in material science and as reagents in Organic Chemistry. Organophosphorus compounds in a single molecule or organic electronics context are appealing as the phosphorous centers perturb the electronic properties of the π-conjugated systems while at the same time provide synthetic handles for subsequent synthetic modifications. As such, new synthetic methodology to such compounds and the exploration of new building blocks is of considerable interest. In a different study, novel organophosphorus compou

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3

Reynolds, Stephen J. "Carbamoylcobalt (III) compounds in organic synthesis." Thesis, University of Nottingham, 1991. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.280294.

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This thesis describes the development and use of organocobalt (III) compounds in the formation of carbon-carbon and carbon-heteroatom bonds and, in particular, details the application of this chemistry for the synthesis of functionalised amides and ~, 1" and 8-lactams. Organocobalt chemistry was born from the isolation and characterisation of the vitamin B12 coenzyme (2) in the 1950s and early 1960s. The introduction to this thesis covers the search for vitamin B12 and briefly describes its biological role. Next, the considerable development of the simple vitamin B12 analogues, i.e. organocoba

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4

Kim, Byeongmoon 1957. "Asymmetric organic synthesis using organoboron compounds." Thesis, Massachusetts Institute of Technology, 1987. http://hdl.handle.net/1721.1/14679.

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5

Sharma, Y. "Continuous flow synthesis of organic compounds." Thesis(Ph.D.), CSIR-National Chemical Laboratory, Pune, 2017. http://dspace.ncl.res.in:8080/xmlui/handle/20.500.12252/4520.

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6

Haughey, Simon Anthony. "Chemoenzymatic synthesis of organosulfur compounds." Thesis, Queen's University Belfast, 1996. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.318731.

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7

Kou, Xiaodi. "Synthesis, characterization and reactivity of organic bismuth compounds." Fort Worth, Tex. : Texas Christian University, 2007. http://etd.tcu.edu/etdfiles/available/etd-07312007-125631/unrestricted/kou.pdf.

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8

Wallner, Olov. "Palladium-Catalyzed Synthesis and Transformations of Organometallic Compounds." Doctoral thesis, Stockholm : Dept. of Organic Chemistry, Stockholm University, 2006. http://urn.kb.se/resolve?urn=urn:nbn:se:su:diva-804.

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9

Wang, Haofan. "Synthesis and reactions of organoiron compounds." Diss., The University of Arizona, 2003. http://hdl.handle.net/10150/289994.

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The multistep synthesis of the redox active adenine analog [e]-ferrocenyl-4-aminopyrimidine is reported. The redox active system will be incorporated into oligonucleotides to study the electron transfer through the molecular pi-system of DNA in future studies. Attempts were made to synthesize a cyclopenta-4-aminopyrimidine derivative which possesses an endocyclic double bond in the cyclopentane ring. This intermediate can be subsequently coupled with cyclopentadienyl iron dicarbonyl (Fp) group and, after thermal decarbonylation, form the desired ferrocene ring. Many double bond precursors are

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10

Buckley, Anne Margaret. "Inorganic-organic layer compounds : synthesis and properties." Thesis, University of Oxford, 1988. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.253398.

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11

Hamilton, A. L. "Applications of lithium compounds in organic synthesis." Thesis, Swansea University, 1998. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.637209.

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The lithiation and subsequent condensation with an electrophile is a useful reaction in many 'total' syntheses. This study was undertaken to investigate the lithiation reactions of several organic molecules. In Chapters 2 and 3, the lithiation of a range of <I>N-</I>pivaloyl-<I>o</I>-toluidines was studied, with the resultant formation of indoles (Chapter 2) and reaction with carbon monoxide to form a carbonylated product (Chapter 3). The lithiation reaction was then applied to 2,5-dimethyl-1,4-phenylene-di-<I>N</I>-pivaloylamine as an attempt to effect quadruple lithiation. However, only doub

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12

Adiraju, Kiran A. V. "Synthesis and characterization of organic-inorganic colorants." To access this resource online via ProQuest Dissertations and Theses @ UTEP, 2009. http://0-proquest.umi.com.lib.utep.edu/login?COPT=REJTPTU0YmImSU5UPTAmVkVSPTI=&clientId=2515.

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13

Mantell, Simon J. "Synthesis of highly functionalised homochiral compounds." Thesis, University of Oxford, 1993. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.334895.

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14

King, Alistair William Thomas. "Chemoenzymatic synthesis of chiral organosulfur compounds." Thesis, Queen's University Belfast, 2002. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.396118.

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15

Ducept, Pascal. "Synthesis of heterocycles using silyldiazocarbonyl compounds." Thesis, Imperial College London, 2002. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.271307.

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16

Lee, Danny Ka Ming. "Unsaturated sulfinates and sulfoxides in organic synthesis." HKBU Institutional Repository, 1995. http://repository.hkbu.edu.hk/etd_ra/47.

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17

Ikegami, Toru. "Hypervalent Organobismuth Compounds : Synthesis, Reaction, and Applications to Organic Synthesis." 京都大学 (Kyoto University), 1997. http://hdl.handle.net/2433/86484.

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18

BERTON, GIACOMO. "SYNTHESIS OF TRIPHENYLENES FOR SUPRAMOLECULAR APPLICATIONS." Doctoral thesis, Università degli Studi di Trieste, 2020. http://hdl.handle.net/11368/2969361.

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In this Doctoral Thesis, through several examples of new chemical modifications characterized by high yields and selectivities and new supramolecular structures, held together by a wide range of intermolecular forces forming several new host systems, we reached our target to revamp triphenylene and derivatives as a new molecular scaffold in supramolecular chemistry. More specifically, the introduction in our triphenylenic scaffold of alkyl thiol chains allowed the formation of sulphide and disulphide covalent cages, while by insertion of pyridine moieties through Mannich reaction it was possib

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19

Frankowski, Kevin J. "Carbenes and carbenoids as powerful tools in organic synthesis." Access to citation, abstract and download form provided by ProQuest Information and Learning Company; downloadable PDF file 2.18 Mb., 94 p, 2006. http://gateway.proquest.com/openurl?url_ver=Z39.88-2004&res_dat=xri:pqdiss&rft_val_fmt=info:ofi/fmt:kev:mtx:dissertation&rft_dat=xri:pqdiss:3205422.

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20

Guertin, Kevin Richard. "The synthesis of highly oxygenated decalin compounds." Thesis, McGill University, 1992. http://digitool.Library.McGill.CA:80/R/?func=dbin-jump-full&object_id=39396.

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The Lewis acid catalysed tandem Michael-Claisen (4C + 2C) annelation reaction of 1-trimethylsiloxy-1-methoxy-3-phenylthio-1,3-butadiene and 4,4-dimethyl-2-cyclohexen-1-one has been reexamined. The intermediate E and Z Michael adducts were cyclized under basic conditions to give the $ beta$-diketone 3-phenylthio-5,6,4a,8a-tetrahydro-5,5-dimethyl-(4H,7H)-naphthalen-1,8-dione. Angular methylation of this $ beta$-diketone under basic conditions was examined in detail, providing the cis angularly methylated product stereoselectively.<br>The cis ring junction stereochemistry of the $ beta$-diketone

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21

Stessman, Nhu Y. Tran. "Synthesis, structures and studies of organoiron compounds." Diss., The University of Arizona, 1999. http://hdl.handle.net/10150/283985.

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An A value of 3.7 kcal/mole was determined for the (η⁵-cyclopentadienyl) iron (II) dicarbonyl group by variable temperature ¹H NMR spectroscopic studies on cis-4-phenyl-1-(η⁵-cyclopentadienyl) iron (II) dicarbonyl cyclohexane. This is the first determination of the A value of a group with a transition metal directly attached to a cyclohexane ring. The energy of activation (-ΔG‡) for ring inversion of cis-4-phenyl-1-(η⁵-cyclopentadienyl) iron (II) dicarbonyl cyclohexane was calculated to be 9.4 kcal/mol. The stereospecific synthesis of cis- and trans-4-phenyl-1-(η⁵-cyclopentadienyl) iron (II) d

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22

Sacripante, Guerino. "Radical reactions in organic synthesis." Thesis, McGill University, 1986. http://digitool.Library.McGill.CA:80/R/?func=dbin-jump-full&object_id=75340.

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The 4-substituted glutarimide required for the synthesis of sesbanimide (53) was obtained by free radical addition of iodoacetamide onto the $ alpha, beta$-unsaturated ester (81) mediated by tributyltin; the lactol ring C was prepared by the analogous free radical cyclization of the $ alpha$-bromo-dipropargyl ketal 73.<br>The syntheses of tricyclic carbapenems involved appropriately substituted monocyclic azetidinone precursors. Free radical 5- exo cyclizations led to the relatively unstable benzo carbapenems 116, 119 and 120. The 6- exo mode, however, afforded stable benzo carbacephems 125, 1

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23

Ye, Xiangyang. "I. Enantioselective total synthesis of ( - )-triptolide : II. synthesis of triptolide analogs /." Hong Kong : University of Hong Kong, 1999. http://sunzi.lib.hku.hk/hkuto/record.jsp?B20896918.

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24

Rowley, Michael. "Some uses of tin compounds in organic synthesis." Thesis, University of Cambridge, 1986. https://www.repository.cam.ac.uk/handle/1810/265341.

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The work described in the dissertation is concerned mainly with organo-tin chemistry. In the first part, I describe the investigation of the stereochemistry of intramolecular electrophilic attack on a tin-carbon bond. The react ion of a number of cS - and � -s tanny 1 a lcoho 1 s and 0-stannyl acid chlorides was investigated, but stereochemical information was obtained only with the reaction of a 0-stannyl aldehyde to give a cyclopentanol, which proceeded largely with retention of configuration at the tin-bearing carbon, unlike the reaction of cS -stannyl alcohols, which give cyclopropanes wit

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25

Roper, Kimberley Ann. "New flow chemistry methods for organic synthesis." Thesis, University of Cambridge, 2013. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.607846.

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26

Saito, Yu. "Synthesis of bioactive compounds: Synthetic study of D-Lac-terminated peptidoglycan fragment structures." Thesis, KTH, Kemiteknik, 2021. http://urn.kb.se/resolve?urn=urn:nbn:se:kth:diva-300085.

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Peptidoglycan (PGN) är en bakteriecellväggskomponent och känd för att känna igen olika receptorer eller enzymer för att leda aktiveringsimmunsystemet. Den allmänna strukturen för PGN består av sockerkedjor inklusive N-acetylglutamin (GlcNAc), N-acetylmuraminsyra (MurNAc) och tvärbundna peptidkedjor. PGN-fragment med D-Lac-ändpeptider har hittats från vankomycinresistenta enterokocker men ett kemiskt syntetiserat PGN-fragment med en D-Lac-ändpeptid har inte undersökts i detalj. Således fokuserade vi på syntesen av PGN-fragmentstrukturer som inkluderar en D-Ala-D-Lac-rest vid den terminala delen

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27

Rujiwatra, Apinpus. "Synthesis and characterisation of novel framework compounds." Thesis, University of Oxford, 2001. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.365355.

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28

McMurray, Brian Thomas. "Chemical and enzymatic synthesis of organosulphur compounds." Thesis, Queen's University Belfast, 1993. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.359111.

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29

Hadjipavlidis, V. "Synthesis and reactions of some spiroheterocylic compounds." Thesis, Nottingham Trent University, 1985. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.354396.

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30

Tran, Chuong Hao. "Synthesis of pseudo-sugars and related compounds." Thesis, University of Warwick, 1995. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.308507.

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31

Edmondson, S. J. "Synthesis, properties and applications of phthalocyanine compounds." Thesis, University of Reading, 1987. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.378676.

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32

Shirtcliff, Laura Donnell. "'Coarctate' cyclizations : applications to heterocycle synthesis /." view abstract or download file of text, 2006. http://proquest.umi.com/pqdweb?did=1188876631&sid=1&Fmt=2&clientId=11238&RQT=309&VName=PQD.

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Thesis (Ph. D.)--University of Oregon, 2006.<br>Typescript. Includes vita and abstract. Includes bibliographical references (leaves 336-357). Also available for download via the World Wide Web; free to University of Oregon users.

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33

Hurley, Jeffrey S. "Synthesis of organic compounds exhibiting enhanced nonlinear optical effects." Thesis, Georgia Institute of Technology, 1990. http://hdl.handle.net/1853/27133.

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34

Dutta, Somnath. "Alkylzirconium alkoxides in organic synthesis reactions with sigma- and pi-bonded organic substrates /." Online access via UMI:, 2005.

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35

Fryling, James Allen 1959. "AN ENANTIOSELECTIVE SYNTHESIS OF BETA-EUDESMOL (DIASTEREOSELECTIVE, CYCLOPROPANATION)." Thesis, The University of Arizona, 1986. http://hdl.handle.net/10150/291680.

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36

Law, Ga-lai, and 羅嘉麗. "Synthesis and photophysical studies of organic lanthanide complexes." Thesis, The University of Hong Kong (Pokfulam, Hong Kong), 2007. http://hub.hku.hk/bib/B38308216.

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37

Tatebe, Caleb J. "Synthesis of Sugar-Derived Esters and Carbamate Compounds." Youngstown State University / OhioLINK, 2014. http://rave.ohiolink.edu/etdc/view?acc_num=ysu1409833972.

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38

Law, Ga-lai. "Synthesis and photophysical studies of organic lanthanide complexes." Click to view the E-thesis via HKUTO, 2007. http://sunzi.lib.hku.hk/hkuto/record/B38308216.

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39

Rhodes, J. B. "Synthesis of 1,6,6aLambdasup(4)-triheterapentalenes and related compounds." Thesis, University of St Andrews, 1985. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.373044.

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40

Gardner, Helen. "New methods for the synthesis of amino compounds." Thesis, University of Newcastle Upon Tyne, 1993. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.357640.

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41

Barrell, Juliet Kay. "The asymmetric synthesis of #alpha#-heterosubstituted carbonyl compounds." Thesis, University of Sheffield, 1999. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.312778.

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42

Walterson, George H. "Direct synthesis and stabilities of unsymmetrical triorganotin compounds." Thesis, University of Aberdeen, 1991. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.293488.

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The syntheses of a variety of triorganotin bromides of general formula RBu<sub>2</sub>SnBr were attempted by reaction of dibutyltin dibromide, an alkyl bromide (RBr), tin and tetrabutylammonium bromide. With the exception of tributyltin bromide which was prepared as a fairly pure compound where R was a butyl group, all other products were mixtures of organotin bromides. In order to identify the compounds of the type RBu<sub>2</sub>SnBr in these products, tetraorganotins of general formula, RBu<sub>2</sub>PeSn, were prepared as GLC standards by a sequence of selective dephenylation and alkylati

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43

goyal, Navneet. "Synthesis and biological evaluation of aeruginosin based compounds and self-assembly of glucosamine based compounds." ScholarWorks@UNO, 2011. http://scholarworks.uno.edu/td/1395.

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Aeruginosins are a family of marine natural products containing mostly non-proteogenic amino acids. These compounds contain a common 2-carboxy-6-hydroxy-octaindole (Choi) rigid bicyclic structure. Many aeruginosins are inhibitors for enzymes involved in the blood coagulation cascade, such as thrombin and Factor VIIa. In order to understand the structure activity relationship (SAR) of the aeruginosins and to discover novel anticoagulants with potentially improved inhibitory and pharmacokinetic properties, in the first part of my thesis I have discussed, synthesis of a series of novel analogs of

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44

Mahanjana, Lungelwa. "Reactions towards the synthesis of the uncommon P57 cymarose moiety." Thesis, Nelson Mandela Metropolitan University, 2013. http://hdl.handle.net/10948/6711.

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The work described in this study aims to investigate methods that will improve a lengthy synthetic pathway in the synthesis of the P57 cymarose moiety, and to examine the conformational structure of certain glycosides in order to shed light on the problematic stereochemical issues surrounding the formation of the cymarose glycosyl donor. The cymarose moiety forms part of the trisaccharide derivative present in P57, an appetite suppressant molecule. Modification of reaction steps in the conversion of the stereochemistry at C-3 of a previously reported synthesis of the P57 cymarose moiety was ca

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45

Crump, Roger Adrian Neil Callow. "Enantio- and diastereocontrol with silicon compounds in organic synthesis." Thesis, University of Cambridge, 1993. https://www.repository.cam.ac.uk/handle/1810/272577.

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46

Zhou, Yi. "Organic synthesis and fungicidal activity of oxylipin-based compounds." Thesis, Aston University, 2011. http://publications.aston.ac.uk/13365/.

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Previous research has shown that the naturally occurring reactive electrophilic species (RES), 12-oxophytodienoic acid (OPDA), not only serves as a precursor for jasmonic acid but is also a potent antifungal compound. However, both the low amount present in plants and the multistep synthesis required to produce this compound on a scale viable for agrochemical use currently limits its practical value. The aim of this research was to generate a range of molecular mimics of OPDA with a minimum number of synthetic steps and screen for antifungal activity. Synthetic 4-octyl-cyclopentenone containin

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47

Kewley, Adam. "The synthesis and separation properties of organic cage compounds." Thesis, University of Liverpool, 2014. http://livrepository.liverpool.ac.uk/2010659/.

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Microporous materials play an important role in a variety of industrial and domestic applications. While a diverse range of microporous materials have been identified, this thesis focuses on porous organic cages (POCs) because they have received much attention as synthetically tunable, solution processable, microporous materials. After introducing the latest developments in POC synthesis and the general application of microporous materials as selective sorbents, this thesis presents three developments in organic cage chemistry: a high-throughput workflow for the discovery of POCs, which yielde

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48

Mitchell, Michael Anthony. "Synthesis and evaluation of new nonlinear optical organic compounds." Diss., The University of Arizona, 1991. http://hdl.handle.net/10150/185377.

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Nonlinear optical (NLO) materials are of current interest because of their potential applications in the development of optical computers, switches, and information storage devices, as well as laser attenuation. Organic molecules with a donor group and an acceptor group connected through a pi system exhibit a large second order NLO response, the NLO characteristic of the most interest. Previous studies have suggested that by having the NLO molecular units connected in series there is a synergistic enhancement of the NLO effect. In an effort to study this enhancement various p-aminophenyl sulfo

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49

Perez, Fuertes Yolanda. "New strategies using BINOL-boron compounds for organic synthesis." Thesis, University of Bath, 2005. https://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.414606.

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50

Long, Sha <1983&gt. "Design, Synthesis and Characterization of N-Containing Organic Compounds." Doctoral thesis, Alma Mater Studiorum - Università di Bologna, 2013. http://amsdottorato.unibo.it/5624/1/LONG_SHA_TESI.pdf.

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The needed of new intermediates/products for screening in the fields of drug discovery and material science is the driving force behind the development of new methodologies and technologies. Organic scaffolds are privileged targets for this scouting. Among them a priority place must be attributed to those including nitrogen functionalities in their scaffolds. It comes out that new methodologies, allowing the introduction of the nitrogen atom for the synthesis of an established target or for the curiosity driven researches, will always be welcome. The target of this PhD Thesis’ work is framed w

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