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Artykuły w czasopismach na temat „Organic eutectics”

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Data publikacji: 6 września 2023

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1

Rai, Uma Shanker, Manjeet Singh, and Rama Nand Rai. "Crystal growth and some physicochemical studies on an organic intermolecular compound of anthranilic acid and N,N-dimethylamino benzaldehyde." European Journal of Chemistry 9, no. 4 (2018): 303–10. http://dx.doi.org/10.5155/eurjchem.9.4.303-310.1720.

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The phase diagram of anthranilic acid and N,N-dimethylaminobenzaldehyde system gives two eutectics (E1 and E2) and a 1:1 intermolecular compound with congruent melting point. The mole fractions of anthranilic acid at E1 and E2 are 0.10 and 0.95, respectively. The negative values of heat of mixing of eutectics suggest that there is clustering of molecules in their eutectic liquid melt. The positive values of excess free energy for eutectics indicate that the interactions between the like molecules are stronger than those of unlike molecules. It can be inferred from single crystal X-ray analysis

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2

Yoshikawa, Shinichi, Shimpei Watanabe, Yoshinori Yamamoto, and Fumitoshi Kaneko. "Binary Phase Behavior of 1,3-Distearoyl-2-oleoyl-sn-glycerol (SOS) and Trilaurin (LLL)." Molecules 25, no. 22 (2020): 5313. http://dx.doi.org/10.3390/molecules25225313.

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This paper reports the precise analysis of the eutectic mixing behavior of 1,3-distearoyl-2-oleoyl-sn-glycerol (SOS) and trilaurin (LLL), as a typical model case of the mixture of cocoa butter (CB) and cocoa butter substitute (CBS). SOS was mixed with LLL at several mass fractions of LLL (wLLL); the mixtures obtained were analyzed for polymorphic phase behavior using differential scanning calorimetry (DSC) and synchrotron radiation X-ray diffractometry (SR-XRD). In melt crystallization with constant-rate cooling, SOS and LLL formed eutectics in their metastable polymorphs, allowing the occurre

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3

Araya-Sibaja, Andrea, José Vega-Baudrit, Teodolito Guillén-Girón, Mirtha Navarro-Hoyos, and Silvia Cuffini. "Drug Solubility Enhancement through the Preparation of Multicomponent Organic Materials: Eutectics of Lovastatin with Carboxylic Acids." Pharmaceutics 11, no. 3 (2019): 112. http://dx.doi.org/10.3390/pharmaceutics11030112.

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Lovastatin (LOV) is a drug used to treat hypercholesterolemia. Recent studies have identified its antioxidant effects and potential use in the treatment of some types of cancer. However, the low bioavailability related to its poor water solubility limits its use in solid oral dosage forms. Therefore, to improve the solubility of LOV three eutectic systems of LOV with the carboxylic acids benzoic (BEN), salicylic (SAL) and cinnamic (CIN) were obtained. Both binary phase and Tammann diagrams were constructed using differential scanning calorimetry (DSC) data of mixtures prepared from 0.1 to 1.0

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4

Gupta, R. K., S. K. Singh, and R. A. Singh. "Some physicochemical studies on organic eutectics." Journal of Crystal Growth 300, no. 2 (2007): 415–20. http://dx.doi.org/10.1016/j.jcrysgro.2006.12.017.

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5

Rai, U. S., and K. D. Mandal. "Some physicochemical studies on organic eutectics and 1:1 addition compound; p-phenylenediamine – benzoic acid system." Canadian Journal of Chemistry 67, no. 2 (1989): 239–44. http://dx.doi.org/10.1139/v89-039.

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The phase diagram of p-phenylenediamine – benzoic acid system, determined by the thaw–melt method, shows the formation of two eutectics and a 1:1 addition compound. The linear velocity of crystallization of pure components, eutectics and addition compound, determined by measuring the movement of growth front in a capillary, suggests that crystallization data obey the Hillig–Turnbull equation. Using experimental values of heats of fusion, entropy of fusion and excess thermodynamic functions were calculated and the results are explained on the basis of cluster formation in the melts. X-ray diffr

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6

Nahar, Yeasmin, and Stuart C. Thickett. "Greener, Faster, Stronger: The Benefits of Deep Eutectic Solvents in Polymer and Materials Science." Polymers 13, no. 3 (2021): 447. http://dx.doi.org/10.3390/polym13030447.

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Deep eutectic solvents (DESs) represent an emergent class of green designer solvents that find numerous applications in different aspects of chemical synthesis. A particularly appealing aspect of DES systems is their simplicity of preparation, combined with inexpensive, readily available starting materials to yield solvents with appealing properties (negligible volatility, non-flammability and high solvation capacity). In the context of polymer science, DES systems not only offer an appealing route towards replacing hazardous volatile organic solvents (VOCs), but can serve multiple roles inclu

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7

Pramanik, Titas, Ashish Anand, Janaky Sunil, et al. "Organic eutectics: characterization, microstructural evolution and properties." Acta Crystallographica Section A Foundations and Advances 77, a2 (2021): C121. http://dx.doi.org/10.1107/s0108767321095593.

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8

Rai, U. S., and H. Shekhar. "Some physicochemical studies on binary organic eutectics." Thermochimica Acta 175, no. 2 (1991): 215–27. http://dx.doi.org/10.1016/0040-6031(91)80068-t.

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9

Rai, U. S., and Santhi George. "A physicochemical study on organic eutectics and addition compound; benzidine–pyrogallol system." Canadian Journal of Chemistry 70, no. 12 (1992): 2869–74. http://dx.doi.org/10.1139/v92-366.

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The phase diagrams of the binary organic system of benzidine–pyrogallol was determined by the thaw–melt method. The solidification behaviour of the pure components, their eutectics, and the addition compound were studied by measuring the movement of growth front in a capillary. From the data on X-ray diffraction, thermal and microscopic investigations it can be inferred that the eutectics are not simple mechanical mixtures of the components involved. The IR and NMR spectral investigations were carried out to throw light on the nature of bonding between the two components forming the addition c

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10

Alhadid, Ahmad, Liudmila Mokrushina, and Mirjana Minceva. "Design of Deep Eutectic Systems: A Simple Approach for Preselecting Eutectic Mixture Constituents." Molecules 25, no. 5 (2020): 1077. http://dx.doi.org/10.3390/molecules25051077.

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Eutectic systems offer a wide range of new (green) designer solvents for diverse applications. However, due to the large pool of possible compounds, selecting compounds that form eutectic systems is not straightforward. In this study, a simple approach for preselecting possible candidates from a pool of substances sharing the same chemical functionality was presented. First, the melting entropy of single compounds was correlated with their molecular structure to calculate their melting enthalpy. Subsequently, the eutectic temperature of the screened binary systems was qualitatively predicted,

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11

Rai, U. S., and K. D. Mandal. "Solidification Behaviour of Organic Eutectics and Addition Compounds." Materials Science Forum 50 (January 1991): 117–28. http://dx.doi.org/10.4028/www.scientific.net/msf.50.117.

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12

Rai, U. S., K. D. Mandal, and N. P. Singh. "Thermochemical studies on organic eutectics and molecular complexes." Journal of Thermal Analysis 35, no. 5 (1989): 1687–97. http://dx.doi.org/10.1007/bf01912943.

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13

Sharma, Krishna, Prakash Ghimire, and Umesh Neupane. "Solid-Liquid Equilibrium Study for Binary System Forming Intermolecular Compound: Phase Diagram, Thermal, Physicochemical and Powder XRD study." Journal of Nepal Chemical Society 43, no. 1 (2022): 1–3. http://dx.doi.org/10.3126/jncs.v43i1.46956.

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The phase diagram study of the binary organic system has been investigated by the thaw melt method using 4-hydroxy- 3 methoxybenzaldehyde (HMB) and 4-nitroaniline (NA). The temperature-composition plot showed that the intermolecular compound (IMC) has formed at 1:1 molar ratio with two eutectics on either side of IMC. The melting points of eutectics and IMC along with parents are verified by the DSC method. The different phases of the systems which are in equilibrium and their physicochemical properties are estimated using the enthalpy of fusion values obtained from DSC. The higher melting tem

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14

Rai, U. S., and R. N. Rai. "Some Physicochemical Studies on Organic Eutectics and Molecular Complex: Urea – p-nitrophenol System." Journal of Materials Research 14, no. 4 (1999): 1299–305. http://dx.doi.org/10.1557/jmr.1999.0177.

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The phase diagram of urea–p-nitrophenol system, in the form of a temperature-composition curve, shows the formation of a 1: 1 molecular complex surrounded by two eutectics containing 0.216 and 0.777 mole fraction of p-nitrophenol. Data on growth velocity (v), obtained by measuring the rate of movement of the interface at different undercoolings (ΔT), suggest that they obey the Hillig–Turnbull equation, i.e., v = u (ΔT)n, where u and n are constants depending on the nature of materials involved. From the heat of fusion values, determined by the differential scanning calorimetry (DSC) method, he

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15

Rai, U. S., Manjeet Singh, and R. N. Rai. "Some physicochemical studies on organic eutectics and inter-molecular compounds." Journal of Thermal Analysis and Calorimetry 130, no. 2 (2017): 967–74. http://dx.doi.org/10.1007/s10973-017-6429-7.

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16

Gupta, R. K., and R. A. Singh. "Thermochemical and microstructural studies on binary organic eutectics and complexes." Journal of Crystal Growth 267, no. 1-2 (2004): 340–47. http://dx.doi.org/10.1016/j.jcrysgro.2004.03.025.

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17

Reddi, R. S. B., V. S. A. Kumar Satuluri, and R. N. Rai. "Solid–liquid equilibrium, thermal and physicochemical studies of organic eutectics." Journal of Thermal Analysis and Calorimetry 107, no. 1 (2011): 183–88. http://dx.doi.org/10.1007/s10973-011-1634-2.

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18

Rai, U. S., and R. N. Rai. "Some Physicochemical Studies on Organic Analog of Metal-Nonmetal Eutectics." Crystal Research and Technology 32, no. 6 (1997): 821–29. http://dx.doi.org/10.1002/crat.2170320614.

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19

Rai, U. S., and K. D. Mandal. "Some Physicochemical Studies on Organic Eutectics and 1:2 Addition Compounds." Molecular Crystals and Liquid Crystals 182, no. 1 (1990): 387–404. http://dx.doi.org/10.1080/00268949008035768.

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20

Chapman, Robert D., and John W. Fronabarger. "A Convenient Correlation for Prediction of Binary Eutectics Involving Organic Explosives." Propellants, Explosives, Pyrotechnics 23, no. 1 (1998): 50–55. http://dx.doi.org/10.1002/(sici)1521-4087(199802)23:1<50::aid-prep50>3.0.co;2-e.

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21

Kaur, Ramanpreet, Raj Gautam, Suryanarayan Cherukuvada, and Tayur N. Guru Row. "Do carboximide–carboxylic acid combinations form co-crystals? The role of hydroxyl substitution on the formation of co-crystals and eutectics." IUCrJ 2, no. 3 (2015): 341–51. http://dx.doi.org/10.1107/s2052252515002651.

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Carboxylic acids, amides and imides are key organic systems which provide understanding of molecular recognition and binding phenomena important in biological and pharmaceutical settings. In this context, studies of their mutual interactions and compatibility through co-crystallization may pave the way for greater understanding and new applications of their combinations. Extensive co-crystallization studies are available for carboxylic acid/amide combinations, but only a few examples of carboxylic acid/imide co-crystals are currently observed in the literature. The non-formation of co-crystals

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22

Dorset, Douglas L. "Crystal structure of lamellar paraffin eutectics." Macromolecules 19, no. 12 (1986): 2965–73. http://dx.doi.org/10.1021/ma00166a015.

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23

Dolotko, Oleksandr, Jerzy W. Wiench, Kevin W. Dennis, Vitalij K. Pecharsky, and Viktor P. Balema. "Mechanically induced reactions in organic solids: liquid eutectics or solid-state processes?" New J. Chem. 34, no. 1 (2010): 25–28. http://dx.doi.org/10.1039/b9nj00588a.

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24

Rai, U. S., and H. Shekhar. "Chemistry of Binary Organic Eutectics and Molecular Complexes: Phenanthrenem. Nitrobenzoic Acid System." Molecular Crystals and Liquid Crystals Science and Technology. Section A. Molecular Crystals and Liquid Crystals 220, no. 1 (1992): 217–30. http://dx.doi.org/10.1080/10587259208033442.

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25

Rai, U. S., and H. Shekhar. "Chemistry of organic eutectics: Phenanthrene — benzoic acid and phenanthrene — cinnamic acid systems." Crystal Research and Technology 25, no. 7 (1990): 771–79. http://dx.doi.org/10.1002/crat.2170250708.

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26

Rai, U. S., and Santhi George. "Some Physicochemical Studies on Binary Organic Eutectics and 1:2 Molecular Complexes." Crystal Research and Technology 26, no. 4 (1991): 511–19. http://dx.doi.org/10.1002/crat.2170260426.

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27

Dorset, Douglas L., James Hanlon, and Gail Karet. "Epitaxy and structure of paraffin-diluent eutectics." Macromolecules 22, no. 5 (1989): 2169–76. http://dx.doi.org/10.1021/ma00195a029.

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28

Rai, U. S., and K. D. Mandal. "Chemistry of organic eutectics and 1:1 addition compound: p-phenylenediamine-catechol system." Thermochimica Acta 138, no. 2 (1989): 219–31. http://dx.doi.org/10.1016/0040-6031(89)87258-2.

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29

Rai, U. S., and Pinky Pandey. "Solidification behaviour of binary organic eutectics and monotectics; 1,2,4,5-tetrachlorobenzene–m-aminophenol system." Materials Letters 39, no. 3 (1999): 166–72. http://dx.doi.org/10.1016/s0167-577x(98)00235-3.

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30

Kaul, Michael J., Diab Qadah, Victoria Mandella, and Mark L. Dietz. "Systematic evaluation of hydrophobic deep-melting eutectics as alternative solvents for the extraction of organic solutes from aqueous solution." RSC Advances 9, no. 28 (2019): 15798–804. http://dx.doi.org/10.1039/c9ra01596e.

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31

Pandey, Saurabh, Abhishek Anand, Dharam Buddhi, and Atul Sharma. "Development and thermophysical analysis of binary eutectics phase change materials for solar drying application." F1000Research 11 (November 9, 2022): 1277. http://dx.doi.org/10.12688/f1000research.127268.1.

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Background: In the past 30–40 years, conflicts over limited conventional energy sources and the negative climate change caused by them have attracted researchers and analysts to new, clean, and green energy technologies. Thereby reducing the consumption of conventional fuel and the negative impact on the climate. The production of alternative energy in the form of thermal energy storage using phase change materials (PCMs) is one of the techniques that not only reduces the gap between the supply and demand of energy but also increases the stability of the energy supply. The tendency of PCMs to

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32

Rai, U. S., and K. D. Mandal. "Solidification behaviour of organic eutectics and 1:1 addition compound: p-Phenylenediamine-resorcinol system." Crystal Research and Technology 23, no. 7 (1988): 871–80. http://dx.doi.org/10.1002/crat.2170230706.

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33

Rai, U. S., та Santhi George. "Some physicochemical studies on organic eutectics and 1:2 addition compound; benzidine-β-naphthol system". Thermochimica Acta 191, № 2 (1991): 271–84. http://dx.doi.org/10.1016/0040-6031(91)87219-m.

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34

Rai, U. S., та Santhi George. "Physicochemical studies on organic eutectics and the 1:1 addition compound: benzidine-α-naphthol system". Journal of Materials Science 27, № 3 (1992): 711–18. http://dx.doi.org/10.1007/bf02403884.

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35

Adeel Hassan, Hafiz Muhammad, and Ivar Lund. "Inorganic PCMs applications in passive cooling of buildings - A review." Journal of Physics: Conference Series 2116, no. 1 (2021): 012103. http://dx.doi.org/10.1088/1742-6596/2116/1/012103.

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Abstract Buildings consume around 40% of total world energy and are responsible for 30-35% greenhouse gas emissions globally. Latent heat thermal energy storage is one of the most promising techniques being investigated currently to reduce the thermal load of buildings. Different types of phase change materials (PCMs) i.e. organic, inorganic and eutectics with different thermophysical properties have been investigated for passive cooling of buildings showing great potential for saving energy. Due to their higher thermal conductivity and high heat storage capacity per unit volume, inorganic pha

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36

Rai, U. S., and R. N. Rai. "Chemistry and characterization of binary organic eutectics and molecular complexes. The urea-m-nitrobenzoic acid system." Materials Letters 34, no. 1-2 (1998): 67–75. http://dx.doi.org/10.1016/s0167-577x(97)00147-x.

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37

Rai, U. S. "Some physicochemical studies on binary organic eutectics and 1:1 addition compound; benzidine-p-nitrophenol system." Journal of Crystal Growth 144, no. 3-4 (1994): 291–96. http://dx.doi.org/10.1016/0022-0248(94)90469-3.

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38

Corset, D. L. "Crystal Structure Analysis of Organic Solid Solutions and Eutectics in the Electron Microscope: Paraffins, Polymers and Lipids." Solid State Phenomena 5 (January 1989): 185–0. http://dx.doi.org/10.4028/www.scientific.net/ssp.5.185.

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39

Fernandes, Richard Perosa, Ana Carina Sobral de Carvalho, Bruno Ekawa, et al. "Synthesis and characterization of meloxicam eutectics with mandelic acid and saccharin for enhanced solubility." Drug Development and Industrial Pharmacy 46, no. 7 (2020): 1092–99. http://dx.doi.org/10.1080/03639045.2020.1775633.

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40

Cysewski, Piotr, Tomasz Jeliński, Patryk Cymerman, and Maciej Przybyłek. "Solvent Screening for Solubility Enhancement of Theophylline in Neat, Binary and Ternary NADES Solvents: New Measurements and Ensemble Machine Learning." International Journal of Molecular Sciences 22, no. 14 (2021): 7347. http://dx.doi.org/10.3390/ijms22147347.

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Theophylline, a typical representative of active pharmaceutical ingredients, was selected to study the characteristics of experimental and theoretical solubility measured at 25 °C in a broad range of solvents, including neat, binary mixtures and ternary natural deep eutectics (NADES) prepared with choline chloride, polyols and water. There was a strong synergistic effect of organic solvents mixed with water, and among the experimentally studied binary systems, the one containing DMSO with water in unimolar proportions was found to be the most effective in theophylline dissolution. Likewise, fo

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41

Zhang, W. P., and D. L. Dorset. "Direct lattice imaging of domain boundaries in N-paraffin binary eutectics formed from the vapor phase." Proceedings, annual meeting, Electron Microscopy Society of America 47 (August 6, 1989): 702–3. http://dx.doi.org/10.1017/s0424820100155487.

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In the past few years, we have been studying the crystal structures of binary paraffin solids in the continuum of states from the stable solid solution through the eutectoid to the fully fractionated eutectic. While electron diffraction data have been very useful to detect microstructures, direct lattice images are needed to depict domain separation.As an example of an eutectic, C30H62/C40H82 thin films were prepared epitaxially on the (100) cleavage face of KCl substrates kept at room temperature under a vacuum of 10−5 torr using the method described by Ueda and Ashida and in our study of pal

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42

Singh, N. P., B. M. Shukla, Namwar Singh, and Narsingh Bahadur Singh. "Structure of melts in binary organic eutectics and molecular complexes. Phenanthrene-picric acid and anthracene-picric acid systems." Journal of Chemical & Engineering Data 30, no. 1 (1985): 49–50. http://dx.doi.org/10.1021/je00039a016.

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Matsumoto, Shogen, Shunsuke Kurosawa, Daisaku Yokoe, Teiichi Kimura, and Akihiko Ito. "Growth and scintillation properties of Ce 3+:LuAG–Al2O3 chemically deposited eutectics." Optical Materials 138 (April 2023): 113674. http://dx.doi.org/10.1016/j.optmat.2023.113674.

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Ahmad, Naveed, Xingyu Lin, Xiaoxiao Wang, Jian Xu, and Xia Xu. "Understanding the CO2 capture performance by MDEA-based deep eutectics solvents with excellent cyclic capacity." Fuel 293 (June 2021): 120466. http://dx.doi.org/10.1016/j.fuel.2021.120466.

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45

Sudheer, R., and K. Narayan Prabhu. "Characterization of Metal-PCMs for Thermal Energy Storage Applications." Materials Science Forum 830-831 (September 2015): 505–8. http://dx.doi.org/10.4028/www.scientific.net/msf.830-831.505.

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In recent years phase change materials have emerged to be ideal energy storage materials for their higher energy density over sensible heat storing materials. Use of phase change materials (PCM) have been successfully implemented at lower temperature applications with various organic compounds. On the other hand, high temperature applications have been solely dominated by various salts, their eutectics and mixtures as phase change materials. This work discusses the suitability of metals and alloys for thermal energy storage applications as the phase change material. Metals offer superior therm

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46

Alkhawaja, Bayan, Faisal Al-Akayleh, Ashraf Al-Khateeb, et al. "Deep Eutectic Liquids as a Topical Vehicle for Tadalafil: Characterisation and Potential Wound Healing and Antimicrobial Activity." Molecules 28, no. 5 (2023): 2402. http://dx.doi.org/10.3390/molecules28052402.

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Deep eutectic solvents (DESs) and ionic liquids (ILs) offer novel opportunities for several pharmaceutical applications. Their tunable properties offer control over their design and applications. Choline chloride (CC)-based DESs (referred to as Type III eutectics) offer superior advantages for various pharmaceutical and therapeutic applications. Here, CC-based DESs of tadalafil (TDF), a selective phosphodiesterase type 5 (PDE-5) enzyme inhibitor, were designed for implementation in wound healing. The adopted approach provides formulations for the topical application of TDF, hence avoiding syst

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47

Saeed, Zeinab M., Bhausaheb Dhokale, Abeer F. Shunnar, et al. "Crystal Engineering of Binary Organic Eutectics: Significant Improvement in the Physicochemical Properties of Polycyclic Aromatic Hydrocarbons via the Computational and Mechanochemical Discovery of Composite Materials." Crystal Growth & Design 21, no. 7 (2021): 4151–61. http://dx.doi.org/10.1021/acs.cgd.1c00420.

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48

BRUNET, L., J. CAILLARD, and P. ANDRÉ. "THERMODYNAMIC CALCULATION OF n-COMPONENT EUTECTIC MIXTURES." International Journal of Modern Physics C 15, no. 05 (2004): 675–87. http://dx.doi.org/10.1142/s0129183104006121.

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This paper presents a simple numerical method to calculate the eutectic mixture composition and melting temperature. Using a Newton–Raphson method to solve the nonlinear problem, the calculation is possible for n-component eutectic. We tested this algorithm on inorganic and organic mixtures. A better correlation between experimental and numerical results has been found for organic compound.

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49

Podolinsky, V. V., Yu N. Taran, and V. G. Drykin. "Eutectic solidification in organic systems." Journal of Crystal Growth 74, no. 1 (1986): 57–66. http://dx.doi.org/10.1016/0022-0248(86)90248-4.

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Thakur, Ajay, Monika Verma, Ruchi Bharti, and Renu Sharma. "Recent Advances in Utilization of Deep Eutectic Solvents: An Environmentally Friendly Pathway for Multi-component Synthesis." Current Organic Chemistry 26, no. 3 (2022): 299–323. http://dx.doi.org/10.2174/1385272826666220126165925.

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Abstract: With the increasing analysis of saving the environment, the researchers demonstrated much effort to replace toxic chemicals with environmentally benign ones. Eutectic mixtures are those solvents that fulfill the criteria of green solvents. The synthesis of organic compounds in the chemical and pharmaceutical industries makes it necessary to find unconventional solvents that cause no harmful impact on health parameters. This review showed that using deep eutectic mixture-based solvents to overcome the hazardous effects of harmful volatile organic solvents over the past few years has g

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