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Artykuły w czasopismach na temat „Physical properties of 1-2-4-triazole”

Autor: Grafiati

Data publikacji: 3 czerwca 2025

Data aktualizacji: 31 lipca 2025

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1

Dovbnya, Dmitro V., Andriy H. Kaplaushenko, Yuliia S. Frolova, and Evheniy S. Pruglo. "Synthesis and antioxidant properties of new (2,4- and 3,4-dimethoxyphenyl)-1,2,4-triazoles." Pharmacia 69, no. (1) (2022): 135–42. https://doi.org/10.3897/pharmacia.69.e74107.

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The purpose of the work is to develop preparative methods for the synthesis of ((5-(2,4- and 3,4-dimethoxyphenyl)-3H-1,2,4-triazole-3-yl)thio)aceto(propano-, butano-, benzo)nitriles, to investigate the reaction of acid hydrolysis, to receive the physical-chemical properties of the synthesized compounds, and to study antioxidant activity of new compounds. Preparative methods for the synthesis of (5-(2,4- and 3,4-dimethoxyphenyl)-3H-1,2,4-triazole-3-yl)thio)aceto(propano-, butano-, benzo)nitriles have been developed for which studied the reaction of acid hydrolysis, resulting in the production o

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2

Journal, Baghdad Science. "Synthesis of Some New 1,2,4-Triazoles Derived from 2-Mercaptobenzimidazole." Baghdad Science Journal 6, no. 1 (2009): 200–208. http://dx.doi.org/10.21123/bsj.6.1.200-208.

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New 1,2,4-triazole derivatives of 2-mercaptobenzimidazole (MB) are reported. Ethyl (benzimidazole-2-yl thio) acetate (1) has been prepared by condensing 2-mercaptobenzimidazole with ethylchloroacetate. The ester (1) on reacting with hydrazine hydrate gave the corresponding acetohydrazide(2)which was reacted separately with phenylisocyanate and phenylisothiocyanate, followed by ring closure in an alkaline medium giving 3-[(benzimidazole-2-yl thio) methyl]-4-phenyl-1,2,4-triazole-5-ol and 3-[(benzimidazole-2-yl thio) methyl]-4-phenyl-1,2,4-triazole-5-thiol respectively (6,7). Reaction of acetohy

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3

Al-Messri, Zainab, A. K. "Synthesis of Some New 1,2,4-Triazoles Derived from 2-Mercaptobenzimidazole." Baghdad Science Journal 6, no. 1 (2009): 200–208. http://dx.doi.org/10.21123/bsj.2009.6.1.200-208.

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New 1,2,4-triazole derivatives of 2-mercaptobenzimidazole (MB) are reported. Ethyl (benzimidazole-2-yl thio) acetate (1) has been prepared by condensing 2-mercaptobenzimidazole with ethylchloroacetate. The ester (1) on reacting with hydrazine hydrate gave the corresponding acetohydrazide(2)which was reacted separately with phenylisocyanate and phenylisothiocyanate, followed by ring closure in an alkaline medium giving 3-[(benzimidazole-2-yl thio) methyl]-4-phenyl-1,2,4-triazole-5-ol and 3-[(benzimidazole-2-yl thio) methyl]-4-phenyl-1,2,4-triazole-5-thiol respectively (6,7). Reaction of acetohy

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4

Yevgean, Pruglo. "Synthesis, physical and chemical properties and anxiolytic activity OF 2-(4-(R-arylidenamino)-5-methyl-4H-1,2,4-triazole-3-YL)thio)acetic acids and their salts." ScienceRise: Pharmaceutical Science, no. 3(13) (June 29, 2018): 19–25. https://doi.org/10.15587/2519-4852.2018.135786.

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It is estimated that 50% of all molecules of medicinal products used in drug therapy are administered as salts. This fact indicates that formation of a medicinal substance salt is an important stage in the development of a medicinal remedy. Therefore, we believe that the combinatorial synthesis of organic and inorganic salts of derivatives of 1,2,4-triazole has not only theoretical but also practical significance. <strong>The aim of the work </strong>is to synthesize and establish the structure of new 2-((4-(R-arylidenamino)-5-methyl-4H-1,2,4-triazole-3-yl)thio)acetic acids and their salt

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5

Blokhin, Andrey V., Sviataslau V. Kohut, Gennady J. Kabo, Elena N. Stepurko, Yauheni U. Paulechka, and Olga V. Voitkevich. "Thermodynamic properties of 1-ethyl-4-nitro-1,2,3-triazole." Thermochimica Acta 565 (August 2013): 221–26. http://dx.doi.org/10.1016/j.tca.2013.05.011.

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6

Stepurko, Elena N., Andrey V. Blokhin, Sviataslau V. Kohut, and Gennady J. Kabo. "Thermodynamic Properties of 1-Methyl-4-nitro-1,2,3-triazole." Thermochimica Acta 686 (April 2020): 178534. http://dx.doi.org/10.1016/j.tca.2020.178534.

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7

HAN, Xue, Jin YANG, Yingying LIU, and Jianfang MA. "Syntheses and Luminescent Properties of Coordination Polymers Based on 1, 2, 4-Triazole-Substituted Resorcin[4]arene." Acta Physico-Chimica Sinica 34, no. 5 (2018): 476–82. http://dx.doi.org/10.3866/pku.whxb201709151.

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8

Martynyshyn, V. P., V. M. Hunchak, B. V. Gutyj, and O. P. Rudenko. "Prediction of biological activity of 4-(3,4 dimethoxybenzylidene)amino)-5-(2-fluorophenyl)-4H-1,2,4 triazole-3-thiol." Scientific Messenger of LNU of Veterinary Medicine and Biotechnologies 26, no. 116 (2024): 255–59. https://doi.org/10.32718/nvlvet11637.

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Among the various heterocyclic systems, 1,2,4-triazole derivatives occupy a leading position due to a whole range of unique and valuable properties. 1,2,4-triazole derivatives exhibit a wide range of pharmacological activity, affecting various biochemical processes while having minimal toxicity. Due to their unique chemical structure, these heterocyclic compounds exhibit different biological properties, making them promising for developing new drugs. The work aimed to study new types of activity of 4-(3,4-dimethoxybenzylidene)amino)-5-(2-fluorophenyl)-4Н-1,2,4-triazole-3-thiol using in silico

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9

Slyvka, Yurii I., Evgeny A. Goreshnik, Andrii M. Fedko, and Marian G. Mys’kiv. "3-Phenyl-4-(prop-2-en-1-yl)-5-[(prop-2-en-1-yl)sulfanyl]-4H-1,2,4-triazole." Molbank 2022, no. 3 (2022): M1405. http://dx.doi.org/10.3390/m1405.

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1,2,4-Triazoles appear to be attractive substances due to their wide range of applications. Previously 3-phenyl-4-(prop-2-en-1-yl)-5-[(prop-2-en-1-yl)sulfanyl]-4H-1,2,4-triazole (Atr) has proven to be an effective precursor for us to prepare Cu(I)-π,σ-coordination compounds with nonlinear optical and magnetic properties. In this study, we present the structural characterization of Atr by a single-crystal X-ray diffraction method. The crystals are monoclinic, Sp.gr. P21, Z = 2, unit cell dimensions: a = 5.6967(3), b = 7.8045(3), c = 14.9327(7) Å, β = 91.113(4)°, V = 663.78(5) Å3 at 150 K. To an

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10

Kucheryavyi, Yu M., and A. G. Kaplaushenko. "Synthesis, physical and chemical properties of 5-(phenoxymethylene)-4-R-1,2,4-triazol-3-thiones derivatives, which contain alkyl- and arylnitrile fragments." Farmatsevtychnyi zhurnal, no. 4 (September 4, 2018): 52–58. http://dx.doi.org/10.32352/0367-3057.4.15.01.

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Ukraine takes the second place in Europe for the dissemination of cancer. Ukrainian pharmaceutical market practically doesn’t have domestic anti-tumor drugs. That’s why, many scientists of pharmaceutical industry work in this direction. The searching of biologically active substances among derivatives of 1,2,4-triazole is actually for today. Anastrozole and Letrozole are enough known like anti-tumor drugs which contain in their structures the core of 1,2,4-triazole and nitrile groups. The aim of our work is purposeful synthesis a number of new highly effective compounds 2-((5-(phenoxymet

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11

Kalpana, Venkatesan, Kannan Rajavelu, and Perumal Rajakumar. "Synthesis, Photo-physical and Electrochemical Properties of Dendrimers with (S)-BINOL Core and Benzothiazole Surface Unit." Australian Journal of Chemistry 68, no. 1 (2015): 93. http://dx.doi.org/10.1071/ch13693.

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Chiral dendritic architectures with benzothiazole as surface group, 1,2,3-triazole as a bridging unit, and (S)-BINOL (1,1-bi-2-naphthol) as a core unit were synthesised in good yields via a convergent synthetic strategy. The chiroptical properties of the dendrimers revealed that the specific rotation increased in the order of dendrimers 4 > 3 > 2 > 1. All the dendrimers showed excellent optical and electrochemical response, and hence would find application in dye-sensitised solar cells.

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12

Yun, Xiaoyun, Yuhan Xie, Jerome P. L. Ng, Betty Yuen Kwan Law, Vincent Kam Wai Wong, and Paolo Coghi. "2-Bromo-3-((1-(7-chloroquinolin-4-yl)-1H-1,2,3-triazol-4-yl)-methoxy)-benzaldehyde." Molbank 2022, no. 1 (2022): M1351. http://dx.doi.org/10.3390/m1351.

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The 1,2,3-triazole ring system can be easily obtained by copper-catalyzed click reaction of azides with alkynes. 1,2,3-Triazole exhibits a myriad of biological activities, including antimalarial, antibacterial, and antiviral activities. We herein reported the synthesis of quinoline-based [1,2,3]-triazole hybrid via Cu(I)-catalyzed click reaction of 4-azido-7-chloroquinoline with alkyne derivative of 2-bromobenzaldehyde. The compound was fully characterized by proton nuclear magnetic resonance (1H-NMR), carbon-13 nuclear magnetic resonance (13C-NMR), heteronuclear single quantum coherence (HSQC

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13

Frolova, Yuliia, Andrii Kaplaushenko, Sameliuk Yurii, Daria Romanina, and Liubov Morozova. "nvestigation of the antimicrobial and antifungal activities of some 1,2,4-triazole derivatives." Česká a slovenská farmacie 71, no. 3 (2022): 149–58. http://dx.doi.org/10.5817/csf2022-4-149.

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This article presents the results of the study of the antimicrobial and antifungal properties among 1,2,4-triazole derivatives synthesized at the Department of Physical and Colloidal Chemistry of the Zaporizhzhia State Medical University. Previous studies have established the antimicrobial and antifungal activity of 1,2,4-triazole derivatives. Therefore, it was reasonable to investigate highly effective substances with antimicrobial and antifungal properties among synthesized compounds. In the first stage of our research, acute toxicity prediction was performed. The antimicrobial and antifunga

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14

Khan, Ayad Kareem. "Facile Synthesis, Characterization of New Quinazolinones with Different Azo Compounds, 1,2,3-Triazole Moieties and Evaluation Their Anti-bacterial Activity." Al-Mustansiriyah Journal of Science 28, no. 3 (2018): 122. http://dx.doi.org/10.23851/mjs.v28i3.180.

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In the present research, a series of some azo compounds (5-9) and 1,2,3-triazoles derived from 2-methyl quinazolin-4(3H)-one were synthesized successfully by stepwise routes includes the following: 3-amino-2-methylquinazolin-4(3H)-one (3) prepared firstly by conversion of 2-aminobenzoic acid into methyl 2-aminobenzoate (1) followed by reaction with acetic anhydride to form methyl -2-acetamidobenzoate (2). The amide then allowed reacting with hydrazine hydrate to give compound (3). Diazotization reaction with sodium nitrite in the presence of hydrochloric acid yield the 3-(chlorodiazenyl)-2-met

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15

Majed Jari Mohammed, Majed Jari Mohammed, Abdul Amir H. Kadhum Abdul Amir H Kadhum, and Adnan Ibrahim Mohammed and Sameer H. Abbood Al Rekabi Adnan Ibrahim Mohammed and Sameer H Abbood Al Rekabi. "Synthesis of One New Sugar Imine Molecule." Journal of the chemical society of pakistan 42, no. 1 (2020): 103. http://dx.doi.org/10.52568/000622.

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In this research, the molecule Nand#39;-((E)-5-methoxy-2-((1-((2R,3R,4S,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)tetrahydro-2H-pyran-2-yl)-4,5-dihydro-1H-1,2,3-triazol-4-yl)methoxy) benzylidene)-4-methyl-1,2,3-thiadiazole-5-carbohydrazide were synthesized and characterized by several conventional analysis methods. Its physical properties and thermal stability was studied. The synthesis was conducted based on D-glucose using concept of click chemistry reaction mechanism. Some of the reaction was conducted using microwave irradiation. The synthesis steps initiated by adding propargyl bromide to

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Majed Jari Mohammed, Majed Jari Mohammed, Abdul Amir H. Kadhum Abdul Amir H Kadhum, and Adnan Ibrahim Mohammed and Sameer H. Abbood Al Rekabi Adnan Ibrahim Mohammed and Sameer H Abbood Al Rekabi. "Synthesis of One New Sugar Imine Molecule." Journal of the chemical society of pakistan 42, no. 1 (2020): 103. http://dx.doi.org/10.52568/000622/jcsp/42.01.2020.

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In this research, the molecule Nand#39;-((E)-5-methoxy-2-((1-((2R,3R,4S,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)tetrahydro-2H-pyran-2-yl)-4,5-dihydro-1H-1,2,3-triazol-4-yl)methoxy) benzylidene)-4-methyl-1,2,3-thiadiazole-5-carbohydrazide were synthesized and characterized by several conventional analysis methods. Its physical properties and thermal stability was studied. The synthesis was conducted based on D-glucose using concept of click chemistry reaction mechanism. Some of the reaction was conducted using microwave irradiation. The synthesis steps initiated by adding propargyl bromide to

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17

Pokhodylo, Nazariy T., and Mykola D. Obushak. "4-(Benzo[d]thiazol-2-yl)-1-(2-nitrophenyl)-1H-1,2,3-triazol-5-amine." Molbank 2022, no. 3 (2022): M1398. http://dx.doi.org/10.3390/m1398.

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The protocol for the reaction of 2-nitrophenyl azide with 2-(benzo[d]thiazol-2-yl)acetonitrile has been selected. It was found that an optimal condition under which the target 4-(benzo[d]thiazol-2-yl)-1-(2-nitrophenyl)-1H-1,2,3-triazol-5-amine could be formed in good yield is the triethylamine system as a base in the DMF solution. The synthesized triazole is promising both for the evaluation of its antiproliferative properties and for the study of the path to new ring annulation by transforming nitro and amino groups.

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18

Elhady, A. N. El-Sharabasy A. S. Kassab S. R. R. Soliman A. M. F. &. Ali A. A. E. "New anticorrosion and flame retardant coating compositions based on 4-amino triazole derivatives , their Schiffs' bases and epoxy varnish." International Journal of Applied Research 6, no. 1 (2020): 60–72. https://doi.org/10.5281/zenodo.4013369.

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In this study, some recently amino triazole derivatives mainly 4-amino-5-phenyl-2,4-dihydro-3H-1,2,4-triazole-3-thione(I),4-((furan-2-yl-methylene)amino)-5-phenyl-2,4-dihydro-3H-1,2,4-triazole-3-thione(II), 4-((4-nitrobenzyl- idene)amino)-5-phenyl-2,4-dihydro-3H-1,2,4-triazole-3-thione (III),4-((4-(dimethylamino)benzylidene)amino)-5-phenyl-2,4-dihydro-3H-1,2,4-triazole-3-thione (IV), 5-phenyl-4-((3-phenyl-4-((3-phenylallylidene) amino)-2,4-dihydro-3H-1,2,4-triazole-3-thione(V),4-(((3-phenyl-5-thioxo-1,5-dihydro-4H-1,2,4-triazole-4yl)imino)methyl)benzal-  dehyde(VI),and3-(((3-phenyl-5-thio

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19

Tm, Kaplaushenko, Panasenko Oi, and Kucheryavy Yu. "RESEARCH OF THE SYNTHETIC, PHYSICAL AND CHEMICAL PROPERTIES OF 3-ALKYLSULFONYL-5-(CHINOLINE-2-YL, 2-HYDROXYCHINOLINE-4-YL)-4-R -2,4-DIHYDRO3N-1,2,4-TRIAZOLES 1." Asian Journal of Pharmaceutical and Clinical Research 10, no. 1 (2016): 81. http://dx.doi.org/10.22159/ajpcr.2017.v10i1.14096.

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ABSTRACTObjective: Fundamental research in pharmacy and medicine have shown that drugs, which are based on nucleus of the 1,2,4-triazole, have a widerange of biological effects. Derivatives of this heterocyclic system have well-known Ukrainian clinicians and the world scientists due to its antifungal,antidepressant, anticancer, cardio- and hepatoprotective properties. The pharmacological activity of most organic compounds depends on severaldifferent factors, including bioavailability of the substance. Hence, it is very important to consider the results of the synthetic and biological researche

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20

Kucherenko, L. I., T. S. Brytanova, and A. S. Hotsulia. "In silico study of properties in the series of 1-alkyl-4-(((5-nitrofuran-2-yl)methylene)amino)- 1,2,4-triazole halides." Current issues in pharmacy and medicine: science and practice 17, no. 1 (2024): 10–16. http://dx.doi.org/10.14739/2409-2932.2024.1.297734.

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1,2,4-Triazole derivatives open up wide horizons for modern medicinal chemists to develop innovative drugs. The use of 1,2,4-triazole derivatives in pharmacological research is based on their ability to produce an effective effect on biological systems and interact with molecular targets. These azoles can be used to regulate various physiological processes, which opens up the possibility of their effective use in the treatment of various diseases. Targeted modification of the structure of 1,2,4-triazole derivatives opens up wide opportunities for the creation of biologically active compounds w

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21

Miao, Li, Xu, Deng, and Ji. "A Three-Dimensional Cadmium(II) Coordination Network Based on 1,3-Di-(1,2,4-triazole-4-yl)benzene: Synthesis, Structure, and Luminescence Properties." Crystals 9, no. 11 (2019): 592. http://dx.doi.org/10.3390/cryst9110592.

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1,2,4-Triazole and its derivatives have been investigated extensively in the construction of coordination polymers. Using a 1,2,4-triazole ligand 1,3-di-(1,2,4-triazole-4-yl)benzene (dtb), a new three-dimensional coordination polymer, {[Cd2(dtb)2(SO4)(H2O)]·(1,2-H2bdc)·SO4}n (1) (1,2-H2bdc = 1,2-benzenedicarboxylic acid), was synthesized under solvothermal conditions. Single-crystal X-ray diffraction analysis revealed that there are two crystallographically different Cd(II) ions in 1 with distorted pentagonal bipyramidal [CdN4O3] geometry and distorted octahedral [CdN4O2] geometry, respectivel

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22

Kravchenko, T. V., O. I. Panasenko, and Ye G. Knysh. "Synthesis and physicochemical properties 4-((R))amino)-5-methyl-4H-1,2,4-triazole-3-thiols." Farmatsevtychnyi zhurnal, no. 6 (August 14, 2018): 55–59. http://dx.doi.org/10.32352/0367-3057.6.16.02.

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Purposeful synthesis of derivatives of 1,2,4-triazole is one of the most important branches of modern pharmaceutical science Modern pharmaceutical market of domestic medicines requires constant updates of existing range. It makes possible the synthesis of new compounds with a predicted biological activity. The main advantage of derivatives of 1,2,4-triazole is high efficiency and low toxic. That is promising factor for creation of new chemical compounds. Analysis of literary data of past few years has showed that there is not enough information about synthesis, physical, chem

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23

Gotsulya, A. S., D. P. Verba, O. I. Panasenko, and Ye G. Knysh. "Synthesis and study of the properties of derivatives 4-phenyl-5-(1H-pyrrol-2-yl)-4H-1,2,4-triazole-3-thiols." Farmatsevtychnyi zhurnal, no. 1 (August 14, 2018): 59–66. http://dx.doi.org/10.32352/0367-3057.1.17.08.

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The successful use of drugs, derivatives of 1,2,4-triazole, creates the conditionsfor the production and investigation of properties of new derivatives of this heterocyclic system. The aim of this work was synthesis and study of physical and chemical properties of new derivatives of 1,2,4-triazole-3-thiol containing synthon of pyrrole. The object of the study was a 4-phenyl-5-(pyrrol-2-yl)-1,2,4-triazole-3-ylthio-R-carbothioamides. To achieve this goal it was necessary to solve following tasks: to conduct the selection of the optimum base structure to determine the most effic

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Frolova, Yu S., A. H. Kaplaushenko, T. V. Ihnatova, and T. M. Kaplaushenko. "Synthesis methods of 1,2,4-triazole-3-thiones: review." Current issues in pharmacy and medicine: science and practice 17, no. 2 (2024): 187–96. http://dx.doi.org/10.14739/2409-2932.2024.2.302616.

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1,2,4-Triazole-containing compounds are unique heterocyclic compounds present in an array of pharmaceuticals and biologically important compounds used in drug-discovery studies against cancer cells, microbes, and various types of diseases in the human body. The aim of the study was to analyze in detail and combine the available literature materials to study the reactions associated with the formation of different classes of derivatives of 1,2,4-triazole-3-thione and to study their physical-chemical properties. Various innovative methods have been proposed and explored for synthesizing differen

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Ihmood Kh. Juber. "Synthesis and Characterization of 1,2,3- Triazole Derivatives from D-Mannitol." Tikrit Journal of Pure Science 22, no. 9 (2023): 58–68. http://dx.doi.org/10.25130/tjps.v22i9.876.

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This research included the use of azido D-Mannitol (3) to synthesize 1,2,3 triazole derivatives. Azido D – Mannitol (3) itself used as an intermediate which was prepared from reaction of 1, 2:5, 6-Di-o-isopropylidene-3,4-di-p-tosyl-D-Mannitol (2) with sodium azide. The prepared compound (3) was allowed to react with alkenes for the formation of corresponding 1,2,3 triazole (4a-e ). The structures of some prepared compounds were confirmed by physical properties and spectroscopic methods FT-IR , 1H-NMR , 13C-NMR and Mass spectra in addition to use TLC.

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Shaltout, Assem D., Ahmed T. Salem, and Ahmed S. Kilany. "Effect of Pre-bloom Sprays and Soil Drenches of Paclobutrazol on Growth, Yield, and Fruit Composition of ‘Roumi Red’ Grapes." Journal of the American Society for Horticultural Science 113, no. 1 (1988): 13–17. http://dx.doi.org/10.21273/jashs.113.1.13.

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Abstract Trials were conducted using paclobutrazol (PP333) either as a foliar application or a soil drench to improve berry set and yield of ‘Roumi Red’ grapes (Vitis vinifera L.). Concentrations of 100 and 250 ppm (foliar applications) and 2 ml/vine as a ground application had no effect on either chlorophyll and carotenoid leaf content or physical and chemical properties of berries, other than cluster weight and number of berries/cluster, which increased significantly. Concentrations of 1000, 1500, and 2000 ppm and 4 ml/vine reduced shoot and internode length as well as °Brix, whereas physica

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Kucherenko, L. I., T. S. Brytanova, and A. S. Hotsulia. "Synthesis, molecular docking, and ADME analysis of a series of 4-amino-3,5-dimethyl-1,2,4-triazole derivatives." Current issues in pharmacy and medicine: science and practice 16, no. 2 (2023): 147–53. http://dx.doi.org/10.14739/2409-2932.2023.2.281039.

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The heterocyclic system of 1,2,4-triazole enables the successful creation of promising biologically active compounds. By creating a range of derivatives based on 4-amino-3,5-dimethyl-1,2,4-triazole, the spectrum of potential biologically active compounds can be expanded. The aim of the work was the synthesis and in silico justification of the prospects for the search for biologically active compounds among 4-amino-3,5-dimethyl-1,2,4-triazole derivatives. Materials and methods. The work uses modern methods for synthesizing organic compounds, followed by confirmation of their individuality and s

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Abd Alrazzak, Nour. "Synthesis of new azo compounds based on 4-aminosalicylic acid and study anti-corrosive activity." Bulletin of the Chemical Society of Ethiopia 38, no. 2 (2024): 473–79. http://dx.doi.org/10.4314/bcse.v38i2.14.

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New azo dyes were prepared from 4-amino-2-hydroxy-benzoic acid in two steps; the first step includes preparation the diazonium salt. Then, diazonium compound coupled with different aromatic compounds containing donating groups (orcinol, 2,6-dimethylphenol, hydroquinone, catechol, 1,2,4-triazole, 2-methyl-naphthol and 4-toluidine, respectively). The physical properties of synthesized compounds were studied like melting point and solubility. The target molecules were characterized using FTIR, NMR and CHNS techniques. The activity of the compounds 1, 3 and 5 as anticorrosion on carbon steel in 0.

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Lu, Zhiqiang, Yanzhi Li, Yi Ru, et al. "The Structure and Property of Two Different Metal-Organic Frameworks Based on N/O-Donor Mixed Ligands." Crystals 11, no. 9 (2021): 1129. http://dx.doi.org/10.3390/cryst11091129.

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Two different metal-organic frameworks (MOFs) [Cd2(AZN)(HAZN)(btc)(Hbtc)·4H2O]·2H2O (1), and [Zn3(AZN)2(btc)2·4H2O] (2) were synthesized by the reactions of different metal salts with mixed ligands of 1-(4-(1H-imidazol-5-yl)phenyl)-1H-1,2,4-triazole (AZN) and trimesic acid (H3btc). The different metal centers in the reaction condition have important impact on the resulting structures of MOFs 1 and 2. Compound 1 is a one-dimensional (1D) chain structure, while 2 features a three-dimensional (3D) framework with 3-fold interpenetration topology of Point (Schläfli) symbol of (6·82)4(62·82·102). Fu

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Mele, Andrea, Federica Arrigoni, Catherine Elleouet, François Y. Pétillon, Philippe Schollhammer, and Giuseppe Zampella. "Insights into Triazolylidene Ligands Behaviour at a Di-Iron Site Related to [FeFe]-Hydrogenases." Molecules 27, no. 15 (2022): 4700. http://dx.doi.org/10.3390/molecules27154700.

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The behaviour of triazolylidene ligands coordinated at a {Fe2(CO)5(µ-dithiolate)} core related to the active site of [FeFe]-hydrogenases have been considered to determine whether such carbenes may act as redox electron-reservoirs, with innocent or non-innocent properties. A novel complex featuring a mesoionic carbene (MIC) [Fe2(CO)5(Pmpt)(µ-pdt)] (1; Pmpt = 1-phenyl-3-methyl-4-phenyl-1,2,3-triazol-5-ylidene; pdt = propanedithiolate) was synthesized and characterized by IR, 1H, 13C{1H} NMR spectroscopies, elemental analyses, X-ray diffraction ,and cyclic voltammetry. Comparison with the spectro

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Bailey, Nicholas, Alaina Atanes, and Bradley O. Ashburn. "(E)-3-(4-Chlorophenyl)-1-(2-fluoro-4-methoxyphenyl)-2-propen-1-one." Molbank 2021, no. 1 (2021): M1184. http://dx.doi.org/10.3390/m1184.

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Natural products known as chalcones show promise as chemotherapeutic agents for the neglected tropical disease known as leishmaniasis. Our objective is to synthesize new targets of opportunity that may lead to better treatments of this debilitating disease. Claisen-Schmidt condensation of 4-chlorobenzaldehyde with 2′-fluoro-4′-methoxyacetophenone using aqueous sodium hydroxide in ethanol yielded the novel compound (E)-3-(4-chlorophenyl)-1-(2-fluoro-4-methoxyphenyl)-2-propen-1-one. The product was obtained in good yield and purity after recrystallization from ethyl acetate/hexane. With the know

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Kholodniak, О. V., Yu V. Shubina, and S. I. Kovalenko. "Heterocyclizations based on N-(R-hydrazine-1-carbonothioyl)cycloalkancarboxamides: functionalized azoles and their antimicrobial activity." Current issues in pharmacy and medicine: science and practice 15, no. 1 (2022): 5–12. http://dx.doi.org/10.14739/2409-2932.2022.1.252037.

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Synthesis and structural modification of azoles remains an important area of medical chemistry and allows to obtain new compounds with a wide range of biological activity. Among the significant number of azoles, 1,3,4-thiadiazoles and 1,2,4-triazoles attract special attention, among which are known drugs, larvicides, insecticides, growth regulators, etc. Even though heterocyclizations of functionally substituted hydrazines for their synthesis are well studied, N-(R-hydrazine-1-carbonothioyl)cycloalkanecarboxamides, and nowadays, remain reagents with undiscovered potential. Moreover, the introd

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Kuan, Houin, Yuhan Xie, Yuzhu Guo, Alessandra Gianoncelli, Giovanni Ribaudo, and Paolo Coghi. "(2R, 4S, 5S) 1-(4-(4-(((7-Chloroquinolin-4-yl)amino)methyl)-1H-1,2,3-triazol-1-yl)-5-(hydroxymethyl)tetrahydrofuran-2-yl)-5-methylpyrimidine-2,4(1H,3H)-dione." Molbank 2023, no. 3 (2023): M1681. http://dx.doi.org/10.3390/m1681.

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1,2,3-triazole pharmacophore is a widely recognized motif used for a variety of applications, including drug discovery, chemical biology, and materials science. We herein report the synthesis of a derivative of azidothymidine (AZT), which was combined with the 7-chloro quinoline scaffold through a 1,4-disubstituted 1,2,3-triazole. The chemical structure of the new molecule was fully characterized by Fourier transform infrared (FTIR) spectroscopy, proton nuclear magnetic resonance (1H-NMR), carbon-13 nuclear magnetic resonance (13C-NMR), heteronuclear single quantum coherence (HSQC), heteronucl

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Fedotov, S. O., A. S. Hotsulia, and Yu V. Karpenko. "Synthesis and analgesic activity of new pyrazole-containing derivatives of 1,2,4-triazole-3-thiol." Current issues in pharmacy and medicine: science and practice 16, no. 3 (2023): 205–12. http://dx.doi.org/10.14739/2409-2932.2023.3.288364.

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Pain represents a primary symptom of numerous diseases and conditions, affecting millions of people worldwide. Effective analgesic medications can alleviate or eliminate pain, thereby enhancing patients’ quality of life and assisting them in resuming normal physical and social activities. However, several existing analgesics may carry unwanted side effects, such as ulcers, blood clotting issues, drowsiness, and more. The development of new analgesics is focused on creating drugs that are both effective and associated with fewer adverse effects. Considering the continuous rise in the number of

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35

Gökce, Halil, Fatih Şen, Yusuf Sert, Bakr F. Abdel-Wahab, Benson M. Kariuki, and Gamal A. El-Hiti. "Quantum Computational Investigation of (E)-1-(4-methoxyphenyl)-5-methyl-N′-(3-phenoxybenzylidene)-1H-1,2,3-triazole-4-carbohydrazide." Molecules 27, no. 7 (2022): 2193. http://dx.doi.org/10.3390/molecules27072193.

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The title compound was synthesized and structurally characterized. Theoretical IR, NMR (with the GIAO technique), UV, and nonlinear optical properties (NLO) in four different solvents were calculated for the compound. The calculated HOMO–LUMO energies using time-dependent (TD) DFT revealed that charge transfer occurs within the molecule, and probable transitions in the four solvents were identified. The in silico absorption, distribution, metabolism, and excretion (ADME) analysis was performed in order to determine some physicochemical, lipophilicity, water solubility, pharmacokinetics, drug-l

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Malook, M. V., O. S. Matrosov, S. M. Kramarev, and O. V. Shtemenko. "New nitrification inhibitors based on copper(II) complex compounds." Voprosy Khimii i Khimicheskoi Tekhnologii, no. 3 (June 2023): 94–102. http://dx.doi.org/10.32434/0321-4095-2023-148-3-94-102.

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The work presents the results of research aimed at the synthesis of new nitrification inhibitors based on complex compounds of Cu2+ with 4-amino-1,2,4-triazole (ATC) and dicyandiamide (DCD). The purpose of the conducted work is the synthesis of new nitrification inhibitors based on complex copper compounds followed with subsequent studies of their structure, properties and biological activity. Four compounds of different compositions were obtained. A number of physical and chemical properties of substances were established: thermal behavior, and solubility in the KAS-28 system (a saturated sol

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Fedotov, S. O., A. S. Hotsulia, and O. I. Panasenko. "Synthesis and properties of some 3-(5-(4-methoxyphenyl)pyrazol-3-yl)-6-R-[1,2,4]triazolo[3,4-b][1,3,4]thiadiazoles." Current issues in pharmacy and medicine: science and practice 15, no. 2 (2022): 117–22. http://dx.doi.org/10.14739/2409-2932.2022.2.259227.

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Pyrazole and 1,2,4-triazole derivatives play an important strategic role in modern medicine and pharmacy. This fact is due to the significant possibilities of chemical modification and significant pharmacological potential among the derivatives of these heterocycles. The introduction of 1,2,4-triazole and pyrazole fragments into the structure of new substances allows to influence the formation of a certain type of activity. The structural combination of these heterocycles in one molecule increases the likelihood of interaction with various biological targets. At the same time, the creation of

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Zych, Dawid, and Aneta Slodek. "The Impact of a 1,2,3-Triazole Motif on the Photophysical Behavior of Non-K Tetrasubstituted Pyrene with a Substitution Pattern Providing the Long Axial Symmetry." Molecules 27, no. 13 (2022): 4314. http://dx.doi.org/10.3390/molecules27134314.

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1,3,6,8-Tetrasubstituted pyrene derivatives with two types of substituents (4-(2,2-dimethylpropyloxy)pyridine, 1-decyl-1,2,3-triazole, 1-benzyl-1,2,3-triazole, and pyrazole), substituted in such a way that provides the long axial symmetry, are prepared and characterized in the present study. To the best of our knowledge, the pyrene derivative containing the same heteroaryl motif (triazole) but substituted by two various alkyls, straight decyl and benzyl-based side chains (C), is reported for the first time. For comparison, compounds with one kind of triazole motif and substituted pyridine or p

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Bahsis, Lahoucine, Meryem Hrimla, Hicham Ben El Ayouchia, Hafid Anane, Miguel Julve, and Salah-Eddine Stiriba. "2-Aminobenzothiazole-Containing Copper(II) Complex as Catalyst in Click Chemistry: An Experimental and Theoretical Study." Catalysts 10, no. 7 (2020): 776. http://dx.doi.org/10.3390/catal10070776.

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The reaction of copper(II) acetate with the 2-aminobenzothiazole (abt) heterocycle affords the new copper(II) complex of formula [Cu(abt)2(OOCCH3)2] (1) in a straightforward manner. Compound 1 served as a precatalyst for azide/alkyne cycloaddition reactions (CuAAC) in water, leading to 1,4-disubstituted-1,2,3-triazole derivatives in a regioselective manner and with excellent yields at room temperature. The main advantages of the coordination of such a heterocyclic ligand in 1 are its strong σ-donating ability (N-Cu), nontoxicity and biological properties. In addition, the click chemistry react

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Al-Smaisim, Rafah F., Redha E. Al-Bayati, and Abdul Hussain K. Sharba. "Synthesis of New Heterocyclic compounds derived from Pyrazoline-5-one compound." Al Mustansiriyah Journal of Pharmaceutical Sciences 9, no. 1 (2011): 123–31. http://dx.doi.org/10.32947/ajps.v9i1.278.

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In this work new heterocyclic pyrazolin derivatives have been synthesized from diazonium chloride salt of 4-aminobenzoic acid: firstly, Azo compounds were prepared from the reaction of an ethanolic solution of sodium acetate and calculated amount of active methylene compound namely, (ethyl acetoacetate)obtain the corresponding hydrazono derivative (1). Secondly, Cyclocondensation reaction of compound (1) with hydrazine hydrate (2) in boiling ethanol affording the corresponding pyrazoline-5-one. Then compound (2) reacted with thionyl chloride to give the corresponding acid chloride derivative(3

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Dovbnia, D. V., A. H. Kaplaushenko, and Yu S. Frolova. "Synthesis and transformation in the series of 2-((5-(2,4- and 3,4-dimethoxyphenyl)-3H-1,2,4-triazole-3-yl)thio)acetic acids." Current issues in pharmacy and medicine: science and practice 14, no. 1 (2021): 12–16. http://dx.doi.org/10.14739/2409-2932.2021.1.226741.

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The aim of the work is to develop preparative methods for the synthesis of 2-((5-(2,4- and 3,4-dimethoxyphenyl)-3H-1,2,4-triazole-3-yl)thio)acetic acids, to study the esterification reaction in this regard, to study physical and chemical properties of the obtained substances, and to predict their toxicity. Materials and methods. Compounds were synthesized using reagents and solvents qualified as “ch.p.”. The IUPAC nomenclature as supplemented was used during the preparation. The melting temperature was determined with the capillary method according to HFC (2.2.14) on the device PTP (M).

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Krstulović, Luka, Katarina Mišković Špoljarić, Vesna Rastija, Nikolina Filipović, Miroslav Bajić, and Ljubica Glavaš-Obrovac. "Novel 1,2,3-Triazole-Containing Quinoline–Benzimidazole Hybrids: Synthesis, Antiproliferative Activity, In Silico ADME Predictions, and Docking." Molecules 28, no. 19 (2023): 6950. http://dx.doi.org/10.3390/molecules28196950.

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The newly synthesized quinoline–benzimidazole hybrids containing two types of triazole-methyl-phenoxy linkers were characterized via NMR and elemental analysis. Additional derivatization was achieved by introducing bromine at the C-2 position of the phenoxy core. These novel hybrids were tested for their effects on the growth of the non-tumor cell line MRC-5 (human fetal lung fibroblasts), leukemia and lymphoma cell lines: Hut78, THP-1 and HL-60, and carcinoma cell lines: HeLa and CaCo-2. The results obtained, presented as the concentration that achieves 50% inhibition of cell growth (IC50 val

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BAI, FU-QUAN, TAO LIU, XIN ZHOU, JIAN-PO ZHANG, and HONG-XING ZHANG. "THEORETICAL COMPUTATIONAL STUDIES ON ELECTRONIC STRUCTURES, SPECTROSCOPIC PROPERTIES AND NITROGEN HETEROATOM EFFECT OF A SPECIES OF ASYMMETRICAL DIIMINE LIGAND PLATINUM(II) COMPLEXES." Journal of Theoretical and Computational Chemistry 08, no. 04 (2009): 603–13. http://dx.doi.org/10.1142/s0219633609004952.

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Electronic structures and spectroscopic properties of a series of platinum(II) complexes based on the C-linked asymmetrical diimine ligand (2-pyridyl-pyrazole (1), 2-pyridyl-1,2,4-triazole (2), 2-pyridyl-tetrazole (3), 2-pyrazine-pyrazole (4) have been studied by the time-dependent density functional theory calculations with polarizable continuum model. The ground- and excited-state structures were optimized by the density functional theory and single-excitation configuration interaction methods, respectively. The calculated structures and spectroscopic properties are in agreement with the cor

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Yang, Xinbo, Nan Li, Yuchuan Li, and Siping Pang. "Insensitive High-Energy Density Materials Based on Azazole-Rich Rings: 1,2,4-Triazole N-Oxide Derivatives Containing Isomerized Nitro and Amino Groups." International Journal of Molecular Sciences 24, no. 4 (2023): 3918. http://dx.doi.org/10.3390/ijms24043918.

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It is an arduous and meaningful challenge to design and develop new energetic materials with lower sensitivity and higher energy. How to skillfully combine the characteristics of low sensitivity and high energy is the key problem in designing new insensitive high-energy materials. Taking a triazole ring as a framework, a strategy of N-oxide derivatives containing isomerized nitro and amino groups was proposed to answer this question. Based on this strategy, some 1,2,4-triazole N-oxide derivatives (NATNOs) were designed and explored. The electronic structure calculation showed that the stable e

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Fluck, Ekkehard, Manfred Spahn та Gernot Heckmann. "Neue 1-Aza-2 λ5, 4 λ5-diphosphirine (2 λ5, 4 λ5-Diphosphapyridine) / New 1 -Aza-2λ5, 4λ5-diphosphirines (2λ5, 4λ5-Diphosphapyridines)". Zeitschrift für Naturforschung B 46, № 6 (1991): 762–66. http://dx.doi.org/10.1515/znb-1991-0610.

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6-(Furan-2-yl)-2,4-tetrakis(dimethylamino)-1-aza-2λ5, 4λ5-diphosphirine (2) and 6-(N-pyrrolidinyl)-2,4-tetrakis(dimethylamino)-1-aza-2λ5, 45-diphosphirine (3) were prepared by reacting 1,1,3,3-tetrakis(dimethylamino)-1 λ5,3 λ5-diphosphete with 2-cyanofuran, and N-cyanopyrrolidine, respectively. 2 and 3 are characterized by their physical properties, NMR, IR, and mass spectra. In 2 two 6J(PH) long range coupling constants could be identified.

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UCHIDA, S. "PHYSICAL PROPERTIES OF HIGH Tc OXIDES." International Journal of Modern Physics B 02, no. 02 (1988): 181–90. http://dx.doi.org/10.1142/s0217979288000147.

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A brief review is given on the current status of experimental research for the high Tc superconductors in Japan. Based upon the recent experimental investigation, the variation of electronic states is discussed for three classes of oxides, BaPb 1−x Bi x O 3, ( La 1−x Sr x)2 CuO 4 and YBa 2 Cu 3 O 7−y with the change of compositions x and the oxygen vacancies y.

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Kucheryavyi, Yu M., A. G. Kaplaushenko, T. V. Panasenko, A. S. Korzhova, and F. Al Zedan. "Synthesis and the study of physical and chemical properties of 2-((5-(phenoxymethyl)-4-R-1,2,4-triazole-3-yl)thio)ethan-1-ols and their derivatives." Journal of Organic and Pharmaceutical Chemistry 13, no. 1(49) (2015): 63–66. http://dx.doi.org/10.24959/ophcj.15.834.

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Bailey, Nicholas, and Bradley O. Ashburn. "(E)-3-[4-(1H-Imidazol-1-yl)phenyl]-1-(4-methylphenyl)prop-2-en-1-one." Molbank 2021, no. 3 (2021): M1269. http://dx.doi.org/10.3390/m1269.

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Imidazole-containing chalcones have been shown to be strongly effective against Aspergillusfumigatus, the causative agent for the disease pulmonary aspergillosis. Claisen–Schmidt condensation of 4-(1H-imidazol-1-yl)benzaldehyde with 4′-methylacetophenone using aqueous sodium hydroxide in methanol yielded the novel compound (E)-3-[4-(1H-imidazol-1-yl)phenyl]-1-(4-methylphenyl)prop-2-en-1-one in good yield and purity after recrystallization from hot methanol. With the known antifungal properties of these combined pharmacophores, this novel compound is suitable for anti-aspergillus activity study

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Erzunov, Dmitry, Vyacheslav Baklagin, Igor Abramov, Vladimir Maizlish, Roman Rumyantsev, and Arthur Vashurin. "4-([1,1′:3′,1′′-terphenyl]-2′-yloxy)-5-chlorophthalonitrile." Molbank 2025, no. 3 (2025): M2028. https://doi.org/10.3390/m2028.

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The study focuses on the synthesis and detailed crystal structure analysis of 4-([1,1′:3′,1′′-terphenyl]-2′-yloxy)-5-chlorophthalonitrile. Using X-ray diffraction methods, the authors achieved the precise refinement of the atomic arrangement, revealing the specific spatial organization of molecules within the crystal lattice. The manuscript thoroughly discusses the key intermolecular interactions—such as hydrogen bonding and π-π stacking—that govern the crystal packing. These interactions play a crucial role in stabilizing the structure and have a direct impact on the material’s physical and c

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Manakov, S. M., and Ye Sagidolda. "Investigation of the physical properties of nanoscale porous silicon films." Physical Sciences and Technology 2, no. 1 (2015): 4–8. http://dx.doi.org/10.26577/2409-6121-2015-2-1-4-8.

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