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1

Ahmed, Amena Alyas, Natiq Ghanim Ahmed, and Ahmad Khuder Ahmad. "Synthesis of New Substituted Tetrazole and 4-Thiazolidinone from Schiff's Bases." Pakistan Journal of Scientific & Industrial Research Series A: Physical Sciences 63, no. 1 (2020): 1–11. http://dx.doi.org/10.52763/pjsir.phys.sci.63.1.2020.1.11.

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 The present work involved the synthesis of compound (1) (1-amino-4-methyl-6-phenyl pyrimidine- 2-(1H)-thione). This compound reacts with different aromatic aldehyde using glacial acetic acid as catalytic on absolute ethanol to give a new series of Schiff's bases (2-7). New thiazolidine-4-one were prepared from reactions of Schiff's bases (2,3,4,7) with thioglycolic acid in absolute ethanol giving compounds (8-11). Finally the preparation of new tetrazole derivatives (12-15) by reaction of Schiff's bases (2,3,4,7) with sodium azide in THF. The structure of the synthesized compounds are c
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2

Veerabhadraiah, Udarapu, Vedeela Rajeswar Rao, and Tadepalcy Venkata Padmanabha Rao. "Reaction of mercaptoacetic acid and chloroacetyl chloride with benzalamino thiazolyl coumarins." Collection of Czechoslovak Chemical Communications 55, no. 2 (1990): 535–39. http://dx.doi.org/10.1135/cccc19900535.

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2-Aryl-3-[4-(2-oxo-2H-1-benzopyran-3-yl)-2-thiazolyl]-4-thiazolidinones (III), have been synthesized by the reaction of Schiff's bases (II) derived from 3-(2-amino-4-thiazolyl)-2H-1-benzopyran-2-ones (I) with mercaptoacetic acid. The Schiff's bases on reaction with chloroacetyl chloride in the presence of triethylamine in dioxane gave chloroacetamido derivative (IV) instead of expected compound V.
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3

Alalam, Nuha, and Salwa Bashir. "Utilizing Schiff's bases for Accurate Determination of Pb(II)and Hg(II) Concentrations in Aqueous Solutions." Oriental Journal Of Chemistry 40, no. 3 (2024): 753–57. http://dx.doi.org/10.13005/ojc/400316.

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In this study, the effectiveness of the synthesized Schiff's base, N,N-bis(acetonylacetone)-p-aminoacetophenone-o-phenylene diamine, in detecting environmental pollutants, including mercury (Hg(II)) and lead (Pb(II)), using UV/VIS spectrophotometry, was evaluated. Acetonitrile was chosen as the optimal solvent. Emphasis was placed on reaction conditions, including micelle effects, to enhance results. The study underscores the importance of Schiff's base compounds for environmental monitoring, particularly in detecting mercury and lead pollution.
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4

Hietala, E. L., L. Tjaderhane, and M. Larmas. "Dentin Caries Recording with Schiff's Reagent, Fluorescence, and Back-scattered Electron Image." Journal of Dental Research 72, no. 12 (1993): 1588–92. http://dx.doi.org/10.1177/00220345930720121001.

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After being weaned, the Wistar rats (12) were fed on a sucrose diet for five weeks to induce dental caries. Tetracycline was injected intraperitoneally into 7 of them to label the mineralizing dentin front. Five rats without tetracycline injection were used to verify spontaneous fluorescence. The evidently carious area under one prominent fissure from each mandibular molar hemisected sagittally in the midline was photographed under ultraviolet light so that autofluorescence would be revealed. The jaws were then stained with Schiff's reagent and photographed under normal light and again under u
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5

Rosenquist, T. H., and J. R. McCoy. "A new interpretation of the direct Schiff reaction of elastic connective tissue." Journal of Histochemistry & Cytochemistry 35, no. 11 (1987): 1205–15. http://dx.doi.org/10.1177/35.11.2443556.

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A direct Schiff reaction of elastic tissues has been known for many years, but the nature of the native aldehyde-rich components has not been clear. In this study, chicken, quail, and rat embryos and adult rat lung, aorta, and kidney were fixed in methacarn or in a formalin solution, embedded in paraffin, and sections of 8-10 micron obtained. Rehydrated sections were incubated for various periods in solutions of the enzymes chondroitinase ABC, clostripain, collagenase, elastase, heparatinase, hyaluronidase, subtilisin Carlsberg ("protease"), or trypsin, and in solutions of phosphomolybdic acid
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6

Jassim, Ibtisam, and Omar AbdulMohsin. "Synthesis, Characterization and Study of Biological Activity of Some New Schiff Bases." Academic Science Journal 3, no. 2 (2025): 166–83. https://doi.org/10.24237/asj.03.02.849b.

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In the present study, ( Schiff's bases 6a - 6e) and (new amids derivatives 6f - 6j) have been synthesized . The glutaroyl chloride(2) has been prepared by the reacting of glutaric acid and thionyl chloride in presence of (DMF) . The new compound bis(4-formylphenyl) glutarate (3) has been Synthesized from reaction of one mole of glutaroyl chloride and two moles of 4-hydroxybenzaldehyde . Compound 4,4'-(glutaroylbis(oxy))dibenzoic acid (4) was Synthesized from one mole of glutaroyl chloride and two moles of 4-hydroxybenzoic acid, while compound bis(4-(chlorocarbonyl)phenyl) glutarate (5) was pre
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7

Galvez, Enrique, Isabel Iriepa, Antonio Lorente, Jose Miguel Mohedano, Feliciana Florencio, and Severino Garcia-Blanco. "Synthesis and structural study of aminals derived from 8-aminoquinoline and 1-aminonaphtalene." Canadian Journal of Chemistry 65, no. 4 (1987): 687–92. http://dx.doi.org/10.1139/v87-117.

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Reaction of 8-aminoquinoline with pyridine-2-carboxaldehyde (2), pyridine-3-carboxaldehyde (3), pyridine-4-carboxaldehyde (4), and benzaldehyde (5) yields the corresponding aminals or Schiff's bases according to reaction conditions; analogous results are obtained from the reaction of 1-amino-naphtalene with pyridine-2-carboxaldehyde (6). On the other hand, reaction of 8-aminoquinoline with thiophene-2-carboxaldehyde or pyrrole-2-carboxaldehyde yields neither the aminal nor the Schiff's base. Crystals of 4 (C24H19N5) belong to the triclinic space group [Formula: see text]. Cell dimensions are a
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8

Khudheyer Jawad Kadem. "Synthesis of Heterocyclic Compounds Containing Sulphur From Ethylene Diamine Tetra Acetic acid Derivatives." International Journal of Research in Pharmaceutical Sciences 11, SPL4 (2020): 1006–11. http://dx.doi.org/10.26452/ijrps.v11ispl4.4236.

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In this work, three novel Schiff's bases subsidiaries were set up from Ethylene Diamine Tetra Acetic corrosive Derivatives(K1, K2 and K3); (K1) which was blend from response of EDTA with 4-hydroxybenzaldehyde and 2,4-dintrophenyl hydrazine. (K2) which was union from response of EDTA with vinilline and 2,4-dintrophenyl hydrazine. (K3) which was amalgamation from response of EDTA with 4-aminoacetophenone and 2,4-dintrophenyl hydrazine after that combination three novel hetrocyclic compound Containing Sulfur molecule; Derivative with compounds containing carbonyl group (aldehyde or ketone) the ca
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9

Liu, Ying, Di Zhao, and Jiang Tao Wang. "Preparation of O-Carboxymethyl Chitosan by Schiff Base and Antibacterial Activity." Advanced Materials Research 647 (January 2013): 794–97. http://dx.doi.org/10.4028/www.scientific.net/amr.647.794.

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A novel method of preparation O-Carboxymethyl chitosan (OCMC) was studied that the product was prepared by reaction of Schiff's base of chitosan. Schiff base of chitosan (BCTS) was synthesized by the reaction of chitosan with aromatic aldehyde, then BCTS reacted with chloroacetic acid and removed the group of amino protection to get the target product. The chitosan derivative was characterized by FT-IR spectroscopy, 1HNMR and elemental analysis. Elemental analysis results confirmed that the degree of substitution(DS) of OCMC was 0.83. Solubility of OCMC in water and organic solvents was demons
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10

Journal, Baghdad Science. "Synthesis of some Schiff's bases derivatives from aminoazo compounds." Baghdad Science Journal 4, no. 3 (2007): 416–19. http://dx.doi.org/10.21123/bsj.4.3.416-419.

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Reaction of,2- [( 4- amio phenyl ) diazenyl] 1,3,4- thiadiazole -5- thiol (S1) with p- chlorobenzeldehyde,3,4 – dimethoxy benzaldehyde and pyrrol-2- carbonxaldehyde gave -5- [{4-(4-chlorobenzylidene amino) phenyl} diezenyl]-1,3,4- thiadiazole-2- thiol (S2),5-[{ 4-[(3,4- dimethoxybenzyldene )amino phenyl ] diazenyl)-1,3,4- thiadiazole-2-thiol,(S3) and -5- [4-(1,H – pyrrol -2- yl- methylene)amino phenyl] diazenyl)-1,3,4- thiadiazole-2- thiol (S4) respectively as schiff's bases compounds. On the same route-2-[(4-amino-1- naphthyl ) diazenyl] -1,3,4- thiadiazole -5- thiol (S5) reacts with –p- chlo
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11

MOHAMMAD, Hawraa Jabbar, Ali Khalaf ALI, and Zainab Abdul Jabbar Ridha AL ALI. "COMPARATIVE HISTOCHEMICAL AND HISTOMORPHOMETRICAL STUDY OF ESOPHAGUS STRUCTURES IN SHEEP (Ovis aries) AND RABBITS (Oryctolagus Cuniculus)." Periódico Tchê Química 17, no. 36 (2020): 457–75. http://dx.doi.org/10.52571/ptq.v17.n36.2020.472_periodico36_pgs_457_475.pdf.

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Evolution between animals causes many changes so that it can adapt to its environments. Each species has unique features that help them survive and can consume different types of food. Sheep and rabbits are economically important animals and used in many aspects of veterinary medicine.This study aimed to compare the histomorphometric and histochemical features of the esophagus of twenty sheep (n = 10) and rabbit (n = 10) adult males. The samples were collected from slaughterhouse and market Misan and were used for histological studies of two types of stains, hematoxylin and eosin, and special
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12

Hussein, Kawther Adeeb, Naser Shaalan, Aliaa Khauon Lafta, and Janan Majeed Al Akeedi. "Preparation, Characterization, and Biological Activity of La(III), Nd(III), Er(III), Gd(III), and Dy(III) Complexes with Schiff Base Resulted from Reaction of 4-Antipyrinecarboxaldehyde and 2-Aminobenzothiazole." Indonesian Journal of Chemistry 24, no. 2 (2024): 358. http://dx.doi.org/10.22146/ijc.87262.

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The research includes the preparation of several complexes of the internal transition elements lanthanide (Ln = La, Nd, Er, Gd, and Dy) containing the 4f shell, with Schiff bases resulting from condensation reactions between 4-antipyrinecarboxaldehyde and 2-aminobenzothiazoles. Schiff's base was identified using FTIR spectra, UV-vis spectroscopy, elemental microanalysis CHNSO, nuclear magnetic resonance, mass spectrometry, and TGA thermal analysis. The complexes were studied and identified with elemental microanalysis CHNSO, FTIR spectroscopy, UV-vis spectroscopy, TGA thermal analysis, conduct
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13

Muntaha .Y. Hayal and Mahmood Shakir Magtoof. "Synthesis, Characterization of some New 4-Thiazolidinone of Acenaphthoquinone." University of Thi-Qar Journal of Science 8, no. 2 (2022): 76–79. http://dx.doi.org/10.32792/utq/utjsci.v8i2.816.

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This work summarized with Synthesis of schiff's bases 1(a-c) from reaction of parent compound acenaphthoquinon with primary amines . Treating of imines compounds with thioglycolic acid was produced thiazolidinone derivatives 2 (a-c) .The structures of synthesized compounds were confirmed by using some spectroscopic analysis such as FT.IR , 1H-NMR and 13C-NMR spectral
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14

H. Abed Elwahab Al-Somaidai, Gazwan. "Synthesis and study the biological activity of some new derivatives of 1,2,4-triazole compounds." Tikrit Journal of Pharmaceutical Sciences 1, no. 1 (2023): 64–70. http://dx.doi.org/10.25130/tjphs.2005.1.8.64.70.

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Some derivatives of triazoles have been synthesized . These derivatives (Schiff's bases) were resulted from the reaction of (3-( 4-methoxy phenyl)-4-amino-5 mercapto-1,2,4-triazole and the corresponding substituted benzaldehydes in presence of glacial acetic acid . The chemical structures of the products were characterized by IR and UV spectra, elemental analysis C.H.N and the biological activity were studied against different kinds of bacteria.
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15

Flores-Morales, Patricio, Soledad Gutiérrez-Oliva, Eduardo Silva, and Alejandro Toro-Labbé. "Insights into the Maillard reaction. The mechanism of Schiff's base formation from the reaction force perspective." Molecular Physics 107, no. 15 (2009): 1587–96. http://dx.doi.org/10.1080/00268970902980060.

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16

Mahdi, Omar, Hanaa Salih, and Abdullah Kshash. "Design, Synthesis of a Novel Banana-Shaped Compounds via Esterification." Diyala Journal For Pure Science 17, no. 4 (2021): 81–92. http://dx.doi.org/10.24237/djps.17.04.568c.

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Schiff's Bases were synthesized from the reaction of p-amino benzoic acid and alkoxybenzaldehyde in absolute ethanol and reacted with (E)-3-((4-hydroxybenzylidene) amino) phenol used DCC (N,N'-Dicyclocarbodiimide) and DAMP (4-(Dimethylamino) pyridine ) to 3-(((E)-4-((4-(((E)-4 alkoxy benzylidene) amino) benzoyl) oxy) benzylidene) amino) phenyl4- (E)- 4-alkoxy benzyli dene ) amino) benzoate. The structures of the products were confirmed by their melting points, FT-IR, 1HNMR spectra.
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17

Journal, Baghdad Science. "Synthesis of New Heterocyclic Derivatives from 4-(3, 5-Dimethyl-1-phenyl-1H-pyrazol-4-ylazo)- benzoic acid." Baghdad Science Journal 7, no. 1 (2010): 727–36. http://dx.doi.org/10.21123/bsj.7.1.727-736.

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In this work pyrazolin derivatives were prepared from the diazonium chloride salt of 4-aminobenzoic acid. Azo compounds were prepared from the reaction of an ethanolic solution of sodium acetate and calculated amount of active methylene compound namely, acetyl acetone to obtain the corresponding hydrazono derivative (1). Cyclocondensation reaction of compounds (1) with hydrazine hydrate and phenyl hydrazine in boiling ethanol affording the corresponding pyrazoline-5-one derivatives of 4-aminobenzoic acid (2,3). Then compound (3) was reacted with thionyl chloride to give the corresponding acid
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18

Elwakeel, Khalid Z., Ahmed M. Elgarahy, and Samya H. Mohammad. "Magnetic Schiff's base sorbent based on shrimp peels wastes for consummate sorption of chromate." Water Science and Technology 76, no. 1 (2017): 35–48. http://dx.doi.org/10.2166/wst.2017.184.

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Magnetic Schiff's base chitosan composite has been prepared starting from shrimp peels as a raw material. Chitosan extraction involved three main stages as preconditioning, demineralization deproteinization and deacetylation. Chitosan modification process took place through the reaction between chitosan and polymeric Schiff's base of thiourea/glutaraldehyde in the presence of magnetite. The synthetic hybrid composite was characterized by Fourier transform infrared spectroscopy and scanning electron microscopy-energy dispersive X-ray analyses and tested as sorbent for Cr(VI) recovery from aqueo
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19

Yaramapa, Hari Babu, Cirandur Suresh Reddy, Venugopal Maralla, and Pedaiahgari Vasugovardhana Reddy. "New 2-aryloxy Macroheterocyclic Phosphates." Journal of Chemical Research 2005, no. 9 (2005): 587–89. http://dx.doi.org/10.3184/030823405774308880.

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A new class of phosphorus macroheterocycles (4a–j) has been synthesised in two steps. The reaction of 1 mole of 3,4-diamino-1,2,5-oxadiazole (1) with 2 moles of aqueous formaldehyde gave a Schiff's base which subsequently underwent addition with 2 moles of 4-t-butylphenol in 1,4-dioxane, afforded N,N-bis-(5-t-butyl-2-hydroxybenzyl)furazan-3,4-diamine (2). Cyclisation of 2 in situ with various substituted aryl phosphorodichloridates (3a–j) in the presence of Et3N in THF afforded 13-membered macroheterocycles (4a–j) containing P, N, O and C in good yields.
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20

Almehmadi, Mazen, Mamdouh Allahyani, Ayman Al-hazmi, and Mohammad Asif. "Synthesis and in vitro anti-bacterial evaluation of some 3-((4-(4-(arylideneamino)-5-mercapto-4H-1,2,4- triazol-3-yl)phenyl)imino)isoindolin-1-one derivatives." INDIAN JOURNAL OF HETEROCYCLIC CHEMISTRY 35, no. 01 (2025): 135. https://doi.org/10.59467/ijhc.2025.35.135.

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Some 3-((4-(4-(arylideneamino)-5-mercapto-4H-1,2,4-triazol-3-yl)phenyl)imino)isoindolin-1-one derivatives (3a-e) were synthesized by the reaction of 3-((4-(4-amino-5-mercapto-4H-1,2,4-triazol-3-yl)phenyl)imino)indolin-2-one (2) with aryl aldehydes. The in vitro anti-bacterial activity of the synthesized compounds was tested against Gram-negative (Escherichia coli) and Gram-positive (Staphylococcus aureus) bacteria. Some compounds (3a-c) exhibited satisfactory antibacterial efficacy against tested bacteria. The most effective compound against tested bacteria was compound 3a.. KEYWORDS :Indoledi
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21

Shanthi, Krishnamoorthy, and Natesan Balasubramanian. "A Simple Spectrophotometric Method for the Determination of Hydrogen Sulfide Based on Schiff's Reaction." Microchemical Journal 53, no. 2 (1996): 168–74. http://dx.doi.org/10.1006/mchj.1996.0024.

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22

Merrett, M., D. K. Stammers, R. D. White, R. Wootton, and G. Kneen. "Characterization of the binding of the anti-sickling compound, BW12C, to haemoglobin." Biochemical Journal 239, no. 2 (1986): 387–92. http://dx.doi.org/10.1042/bj2390387.

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The anti-sickling agent BW12C [Beddell, Goodford, Kneen, White, Wilkinson & Wootton (1984) Br. J. Pharmacol. 82, 397-407] was designed to left-shift the oxygen saturation curve of haemoglobin (HbA) by preferential binding to the oxy conformation at a single site between the terminal amino groups of the alpha-chains through Schiff's base formation, ionic and hydrophobic interactions. In the present work, Schiff's base linkages formed with [14C]BW12C were reduced with NaBH4 and the alpha- and beta-globin chains separated. Under oxy conditions at a molar ratio of 2:1, the covalently bound BW1
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23

THORNALLEY, Paul J., Annika LANGBORG, and Harjit S. MINHAS. "Formation of glyoxal, methylglyoxal and 3-deoxyglucosone in the glycation of proteins by glucose." Biochemical Journal 344, no. 1 (1999): 109–16. http://dx.doi.org/10.1042/bj3440109.

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The glycation of proteins by glucose has been linked to the development of diabetic complications and other diseases. Early glycation is thought to involve the reaction of glucose with N-terminal and lysyl side chain amino groups to form Schiff's base and fructosamine adducts. The formation of the α-oxoaldehydes, glyoxal, methylglyoxal and 3-deoxyglucosone, in early glycation was investigated. Glucose (50 mM) degraded slowly at pH 7.4 and 37 °C to form glyoxal, methylglyoxal and 3-deoxyglucosone throughout a 3-week incubation period. Addition of t-BOC-lysine and human serum albumin increased t
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24

Devi, Kalpana, and Monica Kachroo. "Synthesis and Docking Studies of Oxazine Derivatives as Anti-inflammatory and Antioxidant Agents." DER PHARMA CHEMICA 13, no. 3 (2021): 9. https://doi.org/10.5281/zenodo.11070994.

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A new series of N-(4-{4-(substituted phenyl)-2-[(4-fluro-benzylidene)-amino]-6H-[1,3] oxazine-6-yl}-phenyl)-isonicotiamide were synthesized by reaction of p-amino acetophenone with isonicotinyl chloride to obtain the secondary amides. ClaisenSchmidth condensation reaction with substituted aldehydes led to the formation of corresponding chalcones. These chalcones were cyclized with urea to form oxazine which further reacted with p-fluorobenzaldehyde to form the corresponding Schiff’s bases. All the synthesized compounds were characterized by IR and 1HNMR spectral data, mass spectra and el
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25

Devi, Kalpana, and Monica Kachroo. "Synthesis and Docking Studies of Oxazine Derivatives as Anti-inflammatory and Antioxidant Agents." Der Pharma Chemica 13, no. 3 (2021): 9. https://doi.org/10.5281/zenodo.14722735.

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A new series of N-(4-{4-(substituted phenyl)-2-[(4-fluro-benzylidene)-amino]-6H-[1,3] oxazine-6-yl}-phenyl)-isonicotiamide were synthesized by reaction of p-amino acetophenone with isonicotinyl chloride to obtain the secondary amides. ClaisenSchmidth condensation reaction with substituted aldehydes led to the formation of corresponding chalcones. These chalcones were cyclized with urea to form oxazine which further reacted with p-fluorobenzaldehyde to form the corresponding Schiff’s bases. All the synthesized compounds were characterized by IR and 1HNMR spectral data, mass spectra and el
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26

Biswa, Mohan Sahoo, Nagamounika K., and Krishna Banik Bimal. "Microwave-assisted synthesis of Schiff's bases of 1,2,4-triazole derivatives and their anthelmintic activity." Journal of Indian Chemical Society Vol. 95, Nov 2018 (2018): 1289–94. https://doi.org/10.5281/zenodo.5652476.

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Department of Pharmacy, Vikas Group of Institutions, Nunna, Krishna District, Vijayawada-521 229, Andhra Pradesh, India E-mail: drbiswamohansahoo@gmail.com Community Health System of South Texas, Edinburg, Texas 78539, USA E-mail: bimalbanik10@gmail.com <em>Manuscript received on line 26 September 2018, accepted 01 November 2018</em> Schiff&rsquo;s bases of 1,2,4-triazole-3-thiol are synthesized by multistep reactions. Schiff bases are the condensation products of primary amines with carbonyl compounds. These compounds possess imine or azomethine (-C=N-) functional group in their structure and
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27

H. Abid, Obaid, and Omar G. Mahdy. "Formation of 1,5-Disubstituted 2-hydroxypyrroles via Reaction of 2-(Triphenylphosphoranylidene) succinic Anhydride with Schiff's Bases." Journal of University of Anbar for Pure Science 11, no. 2 (2017): 34–40. http://dx.doi.org/10.37652/juaps.2017.141587.

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28

Jaffe, E. K., and D. Hanes. "Dissection of the early steps in the porphobilinogen synthase catalyzed reaction. Requirements for Schiff's base formation." Journal of Biological Chemistry 261, no. 20 (1986): 9348–53. http://dx.doi.org/10.1016/s0021-9258(18)67661-6.

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Михайлов, Степан Петрович, Михаил Геннадьевич Сульман, Валентин Юрьевич Долуда, and Валентина Геннадьевна Матвеева. "COMPARISON OF THEORETICAL FOUNDATIONS AND EXPERIMENTAL DATA OF THE REACTION FOR OBTAINING N-METHYL-D-GLUCOSIMINE." Вестник Тверского государственного университета. Серия: Химия, no. 4(42) (December 21, 2020): 16–26. http://dx.doi.org/10.26456/vtchem2020.4.2.

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Представленная статья посвящена сравнительному анализу теоретических основ синтеза N-метилглюкамина (основание Шиффа) и экспериментальных данных. N-метил-D-глюкозимин, это промежуточный продукт получения N-метил-D-глюкозамина, широко используемого в фармацевтике, в качестве балластного вещества или противоиона, улучшающего биодоступность основного лекарственного средства. Проведена оценка кинетических параметров синтеза, рассчитан максимальный достигаемый выход. Применение термодинамических расчетов позволяет оценить влияния условий проведения химических процессов на выход целевых продуктов, а
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30

Jamin, D., J. Demers, I. Shulman, HT Lam, and R. Momparler. "An explanation for nonimmunologic adsorption of proteins onto red blood cells: Schiff's base reactions." Blood 67, no. 4 (1986): 993–96. http://dx.doi.org/10.1182/blood.v67.4.993.993.

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Abstract During a phase I evaluation of diglycoaldehyde (INOX), an intravenous chemotherapeutic agent used to treat children with malignancies, all of eight patients tested developed a positive direct antiglobulin test (DAT) in vivo. The DAT became positive within one to seven days after the first administration of the drug and remained positive for up to 12 days following the last dose. The indirect antiglobulin tests were negative. None of the patients showed clinical or laboratory evidence of hemolysis at the time the DAT became positive or during follow-up. Eluates made from the red cells
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Jamin, D., J. Demers, I. Shulman, HT Lam, and R. Momparler. "An explanation for nonimmunologic adsorption of proteins onto red blood cells: Schiff's base reactions." Blood 67, no. 4 (1986): 993–96. http://dx.doi.org/10.1182/blood.v67.4.993.bloodjournal674993.

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During a phase I evaluation of diglycoaldehyde (INOX), an intravenous chemotherapeutic agent used to treat children with malignancies, all of eight patients tested developed a positive direct antiglobulin test (DAT) in vivo. The DAT became positive within one to seven days after the first administration of the drug and remained positive for up to 12 days following the last dose. The indirect antiglobulin tests were negative. None of the patients showed clinical or laboratory evidence of hemolysis at the time the DAT became positive or during follow-up. Eluates made from the red cells of two of
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32

Wang, Yunbing, Qiangguo Du, and Junlian Huang. "Grafting of poly(ethylene oxide) with Schiff's base end group onto chloromethylated polystyrene via Decker-Forster reaction." Macromolecular Rapid Communications 19, no. 5 (1998): 247–50. http://dx.doi.org/10.1002/(sici)1521-3927(19980501)19:5<247::aid-marc247>3.0.co;2-g.

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F. Mousa1, Enaam. "SYNTHESIS, CHARACTERIZATION, AND STUDY THE BIOLOGICAL ACTIVITY OF SOME SCHIFF'S BASES, AND 1,3 - OXAZEPINE COMPOUNDS DERIVED FROM SULFAMETHOXAZOLE DRUG." iraq journal of market research and consumer protection 13, no. 1 (2021): 43–54. http://dx.doi.org/10.28936/jmracpc13.1.2021.(5).

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This study including synthesis of some new Schiff bases compounds [1‐6] from the reaction of Sulfamethoxazole drug with some aromatic aldehydes in classical Schiff base method then treatment Schiff bases with succinic anhydride to get oxazepines rings [7-11]These derivatives were characterized by melting point, FT‐IR, 1H NMR and mass spectra. Some of synthesized compounds were evaluated in vitro for their antibacterial activities against three kinds of pathogenic strains Staphylococcus aureus, Escherichia coli and Pseudomonas aeruginosa by agar diffusion disk method, and against the fungal spe
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Sukhawipat, Nathapong, Laksana Saengdee, Narongrit Sosa, Pongtanawat Khemthong, Jatuporn Wittayakun, and Pamela Pasetto. "Preparation and Characterization of a Novel Additive for Elastomeric Polymer from Oligoisoprene Modified Mesoporous Silica." Materials Science Forum 1100 (October 19, 2023): 103–8. http://dx.doi.org/10.4028/p-co700w.

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This manuscript presents a novel instant additive for elastomeric polymers, specifically focusing on the modification of synthesized mesoporous silica using carbonyl telechelic natural rubber (CTNR). The surface of mesoporous silica particles was modified using a two-step approach. In the first step, a strategy involving the grafting of 3-aminopropyltriethoxysilane (APTES) onto the silica particles was employed. Subsequently, in the second step, a Schiff's base reaction was carried out between the aldehyde functional group of CTNR and the amines on the modified silica surface. The grafting per
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35

K., Krishnankutty, and Basheer Ummathu Muhammed. "Metal complexes of 1-phenylamino-7 -phenyl-4,6-heptadiene-1,3-dione and its Schiff's base." Journal of Indian Chemical Society Vol. 83, Jul 2006 (2006): 663–67. https://doi.org/10.5281/zenodo.5820951.

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Department of Chemistry, University of Calicut, Calicut-673 635, Kerala, India Department of Chemistry, Unity Women&#39;s College, Manjeri-676 122, Kerala, India E-mail : mbummathur@rediffmail.com <em>Manuscript received 17 February 2006, accepted 24 April 2006</em> A new type of conjugated &beta;-ketoanilide and its Schiff&#39;s base with the keto group attached to olefinic linkage has been synthesized by the reaction of acetoacetanilide and cinnamaldehyde under specified conditions. The existence of these compounds predominantly in the intramolecularly hydrogen bonded enol form has been well
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Panda, Krishna Chandra, B. V. V. Ravi Kumar, and Biswa Mohan Sahoo. "Synthesis of Schiff’s Bases of 1,2,4-Triazole Derivatives under Microwave Irradiation Technique and Evaluation of their Anti-diabetic Activity." Current Microwave Chemistry 8, no. 3 (2021): 215–24. http://dx.doi.org/10.2174/2213335608666210930201144.

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Background: Schiff bases play a key role in the generation of a large number of biologically active compounds via cycloaddition, replacement, and ring closure reactions. Objective: The objective of this study is to optimize the purity and yield of the product, improve the reaction time, and make the reaction more eco-friendly with the help of microwave-assisted organic synthesis. Methods: New series of Schiff’s bases of triazole derivatives were achieved via multicomponent reactions. The starting material benzohydrazide 1 was obtained by esterification of benzoyl chloride with methanol in the
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Neetu, Agrawal, K. Upadhyay Prabhat, Shah Kamal, and Mishra Pradeep. "Antidiabetic activity of some synthesized 2-(substituted phenyl)-3-(naphthalen1-yl)thiazolidin-4-ones." Journal of Indian Chemical Society Vol. 94, Aug 2017 (2017): 913–19. https://doi.org/10.5281/zenodo.5597261.

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Institute of Pharmaceutical Research, GLA University, 17 Km Stone, NH-2, Mathura-Delhi Road, P.O. Chaumuhan, Mathura-281 406, Uttar Pradesh, India <em>E-mail</em> : kumkumagr.1990@gmail.com, neetu.agrawal@gla.ac.in, prabhat.upadhyaya@gla.ac.in, kamal0603@gmail.com, directoripr@gla.ac.in <em>Manuscript received 08 February 2017, revised 02 June 2017, accepted 15 June 2017</em> The title compounds (Tz<sub>1-10</sub>) were synthesized by the reaction of thioglycollic acid on Schiff&rsquo;s bases (L<sub>1-10</sub>) formed with 1-naphthylamine and substituted benzaldehydes. These were characterized
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Rao, V. Koteswara, S. Subba Reddy, B. Satheesh Krishna, K. Reddi Mohan Naidu, C. Naga Raju, and S. K. Ghosh. "Synthesis of Schiff's bases in aqueous medium: a green alternative approach with effective mass yield and high reaction rates." Green Chemistry Letters and Reviews 3, no. 3 (2010): 217–23. http://dx.doi.org/10.1080/17518251003716550.

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39

Kiss, R., I. Salmon, I. Camby, S. Gras, and J. L. Pasteels. "Characterization of factors in routine laboratory protocols that significantly influence the Feulgen reaction." Journal of Histochemistry & Cytochemistry 41, no. 6 (1993): 935–45. http://dx.doi.org/10.1177/41.6.8315284.

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We investigated the parameters that could affect the cytophotometric analysis of cell nuclei stained by the Feulgen reaction. These parameters included: the hydrolysis temperature (in the normal "room temperature" range); the composition of the Schiff's reagent; the speed of centrifugation of the cell suspensions; the mode of preservation [air-drying or ethanol-formalin-acetic acid (EFA) fixation]; the fixation time; the pronase digestion time; and the concentration of pronase used to obtain cell suspensions from archival (formalin-fixed, paraffin-embedded) materials. Relatively homogeneous ma
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Taper, Henryk S., Marie Paule Somer, Marc Lans, Jacques de Gerlache, and Marcel Roberfroid. "Histochemical detection of the in vivo produced cellular aldehydes by means of direct Schiff's reaction in CCl4 intoxicated rat liver." Archives of Toxicology 61, no. 5 (1988): 406–10. http://dx.doi.org/10.1007/bf00334622.

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Gulyakevich, O. V., and A. L. Mikhal'chuk. "Cyclocondensation of benzylideneanilines with 2-(thiazolyl-4)cyclohexane-1,3-dione hydrochlorides. A novel reaction in the series of Schiff's bases." Russian Chemical Bulletin 44, no. 10 (1995): 1977–78. http://dx.doi.org/10.1007/bf00707246.

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Ju, Huaqiang, Fengbo Zhu, Hao Xing, Zi Liang Wu, and Feihe Huang. "Ultrastiff Hydrogels Prepared by Schiff's Base Reaction of Bis(p -Formylphenyl) Sebacate and Pillar[5]arene Appended with Multiple Hydrazides." Macromolecular Rapid Communications 38, no. 20 (2017): 1700232. http://dx.doi.org/10.1002/marc.201700232.

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Troitskaya, L. L., S. T. Ovseenko, V. I. Sokolov, and M. Gruselle. "Cyclopalladation of Schiff's bases in the ruthenocene series. The possibility of application of the asymmetric version of the reaction to metalloceneimines." Russian Chemical Bulletin 47, no. 7 (1998): 1382–85. http://dx.doi.org/10.1007/bf02495571.

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44

Aniket Sonawane, Ganesh Sonawane, Kajal Pansare, Chandrashekhar Patil, Sunil Mahajan, and Deepak Sonawane. "Phytochemical analysis and antifungal effect of extracted cinnamaldehyde against some fungal species." World Journal of Biology Pharmacy and Health Sciences 20, no. 3 (2024): 193–202. https://doi.org/10.30574/wjbphs.2024.20.3.1007.

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This study focused on the extraction of cinnamaldehyde, a key bioactive compound, from cinnamon bark using the Soxhlet extraction method, followed by steam distillation and a three-stage solvent extraction process. The Soxhlet extraction method efficiently extracted various phytochemicals from the cinnamon bark, including aldehydes, alkaloids, steroids, flavonoids, tannins, saponins, resins, and phenols. The isolation of cinnamaldehyde was achieved through steam distillation, a technique known for its ability to selectively extract essential oils. The identification of cinnamaldehyde was confi
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45

JishaMol., V* Binsalma K.S Vivek M. Rubeena V. K. "SYNTHESIS, CHARACTERISATION AND INVITRO ANTIBACTERIAL SCREENING OF NOVEL THIAZOLE ANALOGUES." Indo American Journal of Pharmaceutical Sciences 04, no. 07 (2017): 1944–51. https://doi.org/10.5281/zenodo.831662.

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Thiazole containing N=C-S moiety exhibit broad spectrum of biological activities like fungicidal, antimicrobial, antitubercular activities and thiazole possess biological activities like bactericidal, antifungal, analgesic, antiinflammatory, diuretic, CNS depressant and anticancer activity. Recent literature reports explore the biological importance of thiazole analogues as antibacterial agent. The aim and objective of the present investigation is to develop novel thiazole analogues. In this study 3 novel thiazole analogues were synthesised by Schiff’s reaction of 2-amino-4-phenylthiazole with
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46

Luza, J. G., R. van Gorsel, V. S. Polito, and A. A. Kader. "Chilling Injury in Peaches: A Cytochemical and Ultrastructural Cell Wall Study." Journal of the American Society for Horticultural Science 117, no. 1 (1992): 114–18. http://dx.doi.org/10.21273/jashs.117.1.114.

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Fruits of mid- (`O'Henry'), late (`Airtime'), and extra-late-season (`Autumn Gem') peach [Prunus persica (L.) Batsch] cultivars were examined for changes in cell wall structure and cytochemistry that accompany the onset of mealiness and leatheriness of the mesocarp due to chilling injury. The peaches were stored at 10C for up to 18 days or at SC for up to 29 days. Plastic-embedded sections were stained by the Schiff's-periodic acid reaction, Calcofluor white MR2, and Coriphosphine to demonstrate total insoluble carbohydrates, ß-1,4 glucans, and pectins, respectively. Mealiness was characterize
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Joe, Su Mee, In Seon Lee, Yong Tae Lee, Jun Hyuk Lee, and Byung Tae Choi. "Suppression of Collagen-Induced Arthritis in Rats by Continuous Administration of Dae-Bang-Poong-Tang (Da-Fang-Feng-Tang)." American Journal of Chinese Medicine 29, no. 02 (2001): 355–65. http://dx.doi.org/10.1142/s0192415x0100037x.

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Although Dae-Bang-Poong-Tang (an herbal formula of 15 herbs)-treated rats exhibited a mild inflammation, the significant histological changes including a marked infiltration of inflammatory cells in the synovium and damaged articular cartilages were not observed. The staining abilities of the cartilage such as periodic acid Schiff's reaction in the interterritorial matrix of hyaline cartilage, alcian blue and aldehyde fuchsin staining in the capsule of chondrocytes and in the interterritorial matrix of articular cartilage and Con A, sWGA and BSL-1 affinities of chondrocytes tended to decrease
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Li, Z., L. Gao, Y. T. Wang, W. Zhu, J. L. Ye, and G. H. Li. "Carbohydrate Metabolism Changes in Prunus persica Gummosis Infected with Lasiodiplodia theobromae." Phytopathology® 104, no. 5 (2014): 445–52. http://dx.doi.org/10.1094/phyto-01-13-0025-r.

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Peach gummosis represents a significant global disease of stone fruit trees and a major disease in the south peach production area of the Yangtze River of China. In this study, the carbohydrate composition of peach shoots during infection by Lasiodiplodia theobromae was examined. The expression of genes related to metabolic enzymes was also investigated. Control wounded and noninoculated tissue, lesion tissue, and wounded and inoculated surrounding lesion tissue of peach shoots were analyzed. Soluble sugars, glucose, mannose, arabinose, and xylose significantly increased in inoculated tissues
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Rahman, Aziz-Ur, та M. O. Farooq. "Hofmann rearrangement of diphenylacetamide & ββ-diphenylpropionamide. Schiff's base as a new by-product of the Hofmann reaction. Benzhydryl-amine from diphenylacethydroxamic acid". Recueil des Travaux Chimiques des Pays-Bas 73, № 5 (2010): 423–30. http://dx.doi.org/10.1002/recl.19540730511.

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Tullii, Cristiane F., Emilio C. Miguel, Nathália B. Lima, Kátia V. S. Fernandes, Valdirene M. Gomes, and Maura Da Cunha. "Characterization of stipular colleters of Alseis pickelii." Botany 91, no. 6 (2013): 403–13. http://dx.doi.org/10.1139/cjb-2012-0249.

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Colleters are secretory structures of taxonomic relevance that are characterized by the production of a mucilaginous substance in the shoot apices and the development of organs that act against dehydration, herbivores, and pathogens. However, no studies have investigated the senescence and programmed cell death processes of colleters. The goal of this study was to describe the structure of Alseis pickelii Pilger et Shmale (Cinchonoideae) colleters and to characterize the process of senescence. Colleters in the early development stage have a smooth surface and turgid epidermal cells with dense
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