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Artykuły w czasopismach na temat "Solvent-free multi-component reactions"

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Crawford, Deborah E., Clodagh K. Miskimmin, John Cahir, and S. L. James. "Continuous multi-step synthesis by extrusion – telescoping solvent-free reactions for greater efficiency." Chemical Communications 53, no. 97 (2017): 13067–70. http://dx.doi.org/10.1039/c7cc06010f.

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Herein, we demonstrate that several reactions can be telescoped into a single continuous process and/or be carried out as a continuous multi-component reaction (MCR), by twin screw extrusion (TSE), in the complete absence of solvent.
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Gadhave, Anil G., Sanket B. Shirsath, Amol R. Parhad, Bhagwat K. Uphade, and Dilip S. Aute. "Green and efficient synthesis of 2H-indazolo[2,1-b]phthalazine-triones using PPA-polyborate under solvent-free conditions." INDIAN JOURNAL OF HETEROCYCLIC CHEMISTRY 35, no. 02 (2025): 501. https://doi.org/10.59467/ijhc.2025.35.501.

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Polyphosphoric acid (PPA)-polyborate as a solid acid new catalyst was prepared by the reaction between PPA and polyborate. 2H-Indazolo[2,1-b]phthalazine-1,6,11(13H)-triones were synthesized under solvent-free conditions through one-pot tri-component reaction involving substituted aryl aldehydes, phthalhydrazide, and dimedone in the presence of PPA-polyborate catalyst. The main advantages of this study are good to excellent yields, use of less hazardous chemical, shorter reaction times, gentler reaction conditions, reduced chemical waste, increased energy efficiency, environmentally friendly pa
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Hossein Nia, Roghayeh, Manouchehr Mamaghani, and Fatame Tavakoli. "Isatin: A key player in multi-component reactions for heterocycle synthesis." Current Chemistry Letters 14, no. 3 (2025): 441–48. https://doi.org/10.5267/j.ccl.2025.3.007.

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Considering the very important medicinal and biological properties of heterocycles including isatin skeleton, synthesis of isatin-containing compounds has attracted the attention of medicinal and organic chemists, especially researchers involved in the synthesis of heterocycles. The present review focuses on the recent investigation in the synthesis of heterocycles with isatin moiety using isatin derivatives as reaction reactants via multi-component for the period of 2014–2024. The reports were classified according to the conditions of the reactions, which distinguishes this review from simila
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Kong, Lingbin, Rong Huang, Haodan He, Yunxiang Fan, Jun Lin, and Shengjiao Yan. "Multi-component solvent-free cascade reaction of 2-cyanoacetamides: regioselective synthesis of pyridin-2-ones bearing quaternary centers." Green Chemistry 22, no. 1 (2020): 256–64. http://dx.doi.org/10.1039/c9gc03692j.

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Karimi, Hirbod. "Copper Zirconium Phosphate as an Efficient Catalyst for Multi-component Reactions in Solvent-Free Conditions." Iranian Journal of Science and Technology, Transactions A: Science 42, no. 1 (2018): 219–35. http://dx.doi.org/10.1007/s40995-018-0495-y.

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Sadeghpour, Mahdieh, and Fatemeh Bagheri. "Novel Synthetic Approach for the Access of Functionalised 4H-Chromenes." Journal of Chemical Research 40, no. 12 (2016): 740–43. http://dx.doi.org/10.3184/174751916x14792153319761.

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A simple, efficient and high-yielding one-pot protocol for the synthesis of novel functionalised 4H-chromenes and chromene carboxylic acids has been developed using multi-component domino coupling reactions of anil-like compounds with 1,3-diketones and indole in the presence of formic acid catalyst under solvent-free conditions. The protocol avoids the use of expensive catalysts, toxic solvents and chromatographic separation.
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Mahmoud, Naglaa F. H., and Ahmed M. El‐Saghier. "Multi‐component Reactions, Solvent‐free Synthesis of Substituted Pyrano‐pyridopyrimidine under Different Conditions Using ZnO Nanoparticles." Journal of Heterocyclic Chemistry 56, no. 6 (2019): 1820–24. http://dx.doi.org/10.1002/jhet.3556.

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Kamali, Fatemeh, and Farhad Shirini. "Introduction of Fe3O4@SiO2–ZrCl2-MNPs for the efficient promotion of some multi-component reactions under solvent-free conditions." New Journal of Chemistry 41, no. 20 (2017): 11778–91. http://dx.doi.org/10.1039/c7nj01863k.

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In the work, the preparation, characterization and use of Fe<sub>3</sub>O<sub>4</sub>@SiO<sub>2</sub>–ZrCl<sub>2</sub>-MNPs as nano magnetic reagents in the promotion of some multi-component reactions is reported.
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Kishore, Ram, Monika Kamboj, and Manisha Shukla. "Triton-B Mediated One-Pot Multicomponent Synthesis of 3,5 Substituted Tetrahydro-2H-1,3,5-Thidiazine-2-Thiones." Oriental Journal of Chemistry 34, no. 6 (2018): 2878–83. http://dx.doi.org/10.13005/ojc/340627.

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A new-fangled, proficient, one-pot multi component, intramolecular C-S bond formation reaction, mediated by phase transfer catalyst, Triton-B, is described in this paper. The reaction of alkyl/ phenyl amines, CS2 and formaldehyde catalyzed via Triton-B resulted in formation of 3-(Alkyl or aryl methyl),5-(Alkyl or aryl methyl) substituted tetrahydro-2H-1,3,5-thiadiazine-2-thiones compounds(1a-15a). These compounds (1a-15a) were characterized with the help of elemental analysis, IR, NMR and mass spectroscopic methods. The PTC mediated reactions require mild reaction condition and reduced time pe
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Rehman, Nuzhat, Ayaz Mahmood Dar, Raja Feroz Ahmad Haji, et al. "Green and Efficient Synthesis of Dihydropyrimidinone Analogues via Hpa-Clay Catalyzed Biginelli Reaction." Chemistry Journal of Moldova 19, no. 1 (2024): 76–83. http://dx.doi.org/10.19261/cjm.2024.1135.

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This study introduces an environmentally sustainable approach for the synthesis of 3,4-dihydropyrimidin-2(1H)-ones (DHPMs), via the Biginelli reaction. A heterogeneous catalyst, Heteropolyacid-Clay (HPA-Clay), is developed by immobilizing H5PV2W10O40 on Montmorillonite KSF clay. The catalyst exhibits enhanced stability and catalytic efficiency, confirmed through X-ray powder diffraction and scanning electron microscopy. Utilizing a one-pot multi-component strategy under solvent-free conditions, various aldehydes, urea or thiourea, and ethylacetoacetate generate DHPMs with excellent yields and
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Streszczenia konferencji na temat "Solvent-free multi-component reactions"

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Bilgili, Hatice Kubra, Gozde Ozaydin Ince, Melis Emanet, and Gullu Kiziltas Sendur. "Fabrication of 3D Bone Scaffolds Functionalized With Spatiotemporal Release of BMP-2 Growth Factor via iCVD to Enhance Osteoregeneration." In ASME 2020 International Mechanical Engineering Congress and Exposition. American Society of Mechanical Engineers, 2020. http://dx.doi.org/10.1115/imece2020-24072.

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Abstract 3D scaffolds are known to be used in bone tissue engineering applications due to their great potential of providing multi-functionalized environment for cells. Different production techniques have been used focusing on changing geometrical features or adding biological/chemical compounds to improve the functionality of current 2D/3D scaffolds. A critical component to this functionalization relates to the effect of endogenous and exogeneous growth factors (GF) in the bone regeneration process that could be incorporated to the scaffolds via Initiated Chemical Vapor Deposition (iCVD) whi
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