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1

Nelwamondo, Aubrey Ndifelani. "Solid state thermal decomposition of amide complexes of nickel(II) chloride." Thesis, Rhodes University, 1997. http://hdl.handle.net/10962/d1005008.

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The thermal decompositions of a series of amide complexes of nickel(II) chloride have been studied. Thermochemical, kinetic, structure and solid-state stability correlations have been investigated. Complexes containing homologous amide ligands (L) of the form NiLCℓ₂, Ni₃L₂Cℓ₆, Ni₃LCℓ₆, NiL₂Cℓ₂(2H₂0) and ML₂Cℓ₂ (where M = Ni(II), Co(II) or Cu(II)) have been prepared. Chemical analysis, spectral and thermogravimetric measurements were used to characterize the complexes and their decomposition stoichiometries. Three sets of reactions were identified as yielding stable products in a single step: (
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2

Sobocinski, Raymond Louis 1962. "LASER-INDUCED THERMAL DECAY OF PYRIDINE AND CHLORIDE SURFACE-ENHANCED RAMAN SCATTERING AS A PROBE OF SILVER SURFACE-ACTIVE SITES." Thesis, The University of Arizona, 1987. http://hdl.handle.net/10150/276553.

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The activation parameters for the temperature dependent irreversible loss of surface-enhanced Raman scattered (SERS) intensity from pyridine and chloride adsorbed at silver surfaces in an electrochemical environment have been determined. Laser-induced heating is introduced as a probe of the chemical nature of SERS-active sites. Surface temperatures are calculated from spectroscopic data. The activation energies associated with the destruction of SERS-active sites at a surface roughened by an illuminated oxidation-reduction cycle (ORC) are 12.8 ± 3.2 kcal/mole and 27.7 ± 3.1 kcal/mole for pyrid
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3

Ramacieri, Patricia. "Microstructure and kinetics of thermal degradation of alkene copolymers of vinyl chloride." Thesis, McGill University, 1986. http://digitool.Library.McGill.CA:80/R/?func=dbin-jump-full&object_id=72819.

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Uysal, Idil. "The Synthesis Of Zinc, Chloride And Fluoride Doped Nano Hydroxylapatites By Precipitation Method And Investigation Of Their Mechanical, Structural And Biological Properties." Master's thesis, METU, 2011. http://etd.lib.metu.edu.tr/upload/12613481/index.pdf.

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This study aimed synthesizing hydroxylapatite (HA) and Zn2+, F- and Cl- doped HA by solution precipitation method. The synthesized compounds were sintered at 1100&deg<br>C for 1h. For structural characterization, density of the samples were measured by Archimedes&rsquo<br>method. It was observed that Zn2+ addition increased the density significantly whereas F- caused a decrease and Cl- increased the density with a little amount. XRD was applied to the samples and it was found that co-doping of Zn2+ and F- ions decreased the unit cell volume of HA with F- addition. Other compositions gave fluct
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Kulkarni, Ambarish J. "Atomistic Characterization and Continuum Modeling of Novel Thermomechanical Behaviors of Zinc Oxide Nanostructures." Diss., Georgia Institute of Technology, 2007. http://hdl.handle.net/1853/19761.

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ZnO nanowires and nanorods are a new class of one-dimensional nanomaterials with a wide range of applications in NEMS. The motivation for this work stems from the lack of understanding and characterization of their thermomechanical behaviors essential for their incorporation in nanosystems. The overall goal of this work is to develop a fundamental understanding of the mechanisms controlling the responses of these nanostructures with focus on: (1) development of a molecular dynamics based framework for analyzing thermomechanical behaviors, (2) characterization of the thermal and mechanical beha
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Nethavhanani, Takalani. "Synthesis of zinc oxide nanoparticles by a green process and the investigation of their physical properties." University of the Western Cape, 2017. http://hdl.handle.net/11394/6295.

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Magister Scientiae - MSc (Physics)<br>Zinc oxide (ZnO) is a wide and direct semiconductor with a wurtzite crystal structure. Its multifunctionality as the ideal candidate in applications such as blue-UV light emitting diodes, transparent conducting oxide, selective gas sensor and efficient catalyst support among others, has attracted a significant interest worldwide. Nano-scaled ZnO has been synthesized in a plethora of shapes. A rich variety of physical and chemical methodologies have been used in the synthesis of undoped or doped ZnO. However, such methods either necessitate relatively
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7

Tarkin, Eylem. "Characterization And Study Of Solution Properties Of Poly(propylene Oxide) Synthesized By Metal Xanthate Catalysts." Master's thesis, METU, 2003. http://etd.lib.metu.edu.tr/upload/1086099/index.pdf.

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Zinc xanthates polymerize propylene oxide into high polymer (PPO) with coordination mechanism. In order to identify structure and stereoisomerisms of this polymer, PPO was subjected to thermal and column fractionation. Obtained fractions were characterized by end-group analysis, cryoscopy, viscometry, IR and 13C-NMR spectroscopy, melting temperature. PPO is composed of a high molecular weight, stereoregular, crystallizable polymer (K-polymer) with low molecular weight (=500 g/mol) D-polymer. Presence of double bonds and hydroxyl terminals was interpreted as the product of an anionic mechanism.
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Granowski, Gregory A. "Recycling of PVC and XLPE for High Impact Resistance in Spool Development." Thesis, University of North Texas, 2018. https://digital.library.unt.edu/ark:/67531/metadc1157640/.

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My work focuses on taking waste wire-grade PVC = poly(vinyl chloride) and waste XLPE = cross-linked polyethylene and recycle them into small wire/cable spool technology in order to reduce waste cost and reduce cost of spool production. The PVC and XLPE were provided by Encore Wire Corp. of McKinney, TX; they have also defined the standard to which I am comparing my results. The end goal is to incorporate as much PVC and XLPE into the spools while maintaining material toughness, impact resistance, as well as cost-effectiveness in the implementation of the waste materials. The work has been divi
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9

Rajko, Radovanović. "Uticaj sastava polivinilhloridnih smeša i tehnoloških uslova proizvodnje na svojstva penastih podnih obloga." Phd thesis, Univerzitet u Novom Sadu, Tehnološki fakultet Novi Sad, 2016. http://www.cris.uns.ac.rs/record.jsf?recordId=101048&source=NDLTD&language=en.

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Mogućnost primene polivinilhloridnih (PVC) podnih obloga je određena krajnjim svojstvima koja zavise od sastava obloge i načina proizvodnje. Zbog složenog sastava i različitih načina pripreme PVC podnih obloga, veoma je te&scaron;ko tačno proceniti uticaj pojedinačnog procesnog parametara na svojstva dobijenog proizvoda. U ovom radu, da bi se ispitao uticaj sastava polivinilhloridnih sme&scaron;a na svojstva PVC podnih obloga pripremljeno je 27 receptura u kojima su varirane: koncentracije kalcijumkarbonata (40, 70 i 100 phr), koncentracije sredstva za ekspanziju, azodikarbonamida ADC (0,8, 1,
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10

Wang, Yen-Ching, and 王衍晴. "Processes and properties of the thermal sprayed zinc doped hydroxyapatite coating." Thesis, 2014. http://ndltd.ncl.edu.tw/handle/2j5dkf.

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碩士<br>國立臺北科技大學<br>材料科學與工程研究所<br>102<br>In this study, we prepared zinc-doped hydroxyapatite by the co-precipitation method, the purpose is to make artificial bone material has ability of antibacterial. The co-precipitation method prepared hydroxyapatite with add different concentrations of zinc chloride. Detected the weight loss by TGA to determine the sintering temperature of the pyrolysis temperature.Detected by XRD, the experimental results show that after sintering, it has some new phases generated of ZnO and CaZn2 (PO4)2, and the strength of new phases will high over than hydroxyapatite p
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"Studies on thermal stabilities of transparent dielectrics/ZnO heterostructures." 2007. http://library.cuhk.edu.hk/record=b5893211.

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Wang, Ranshi = 透明电解质/氧化锌异质结热稳定性的研究 / 王然石.<br>Thesis (M.Phil.)--Chinese University of Hong Kong, 2007.<br>Includes bibliographical references (leaves 130-134).<br>Abstracts in English and Chinese.<br>Wang, Ranshi = Tou ming dian jie zhi/yang hua xin yi zhi jie re wen ding xing de yan jiu / Wang Ranshi.<br>Chapter I. --- Abstract<br>Chapter II. --- Acknowledgement<br>Chapter III. --- Table of contents<br>Chapter IV. --- List of figures<br>Chapter V. --- List of tables<br>Chapter 1 --- Introduction<br>Chapter 1.1 --- Motivations<br>Chapter 1.2 --- Outline of thesis<br>Chapter 2 --- Experimental C
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HSU, YU-WEN, and 徐郁雯. "The Study of Thermal Properties and Rapid Chloride Permeability Testing in Concrete Containing Reclaimed Asphalt Pavement." Thesis, 2019. http://ndltd.ncl.edu.tw/handle/6v4d87.

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碩士<br>國立高雄科技大學<br>土木工程系<br>107<br>The research objective was to assess the mechanical properties, shrinkage, thermal expansion and conductivity, and chloride penetration of concrete containing reclaimed asphalt pavement materials. Rich and lean concrete mixtures were blended by water to cementitious materials (w/c) ratio of 0.5 and the RAP materials were replacing both coarse and fine aggregates by 0, 20, 40, 60, 80, and 100-%. The concrete cylinders and specimens were cast and cured in the water tank for 7, 28, 56, and 90 days. The test results demonstrate as follows: the mixing temperatur
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Coleman, Victoria Anne. "Processing and characterisation of ZnO for device applications." Phd thesis, 2006. http://hdl.handle.net/1885/150587.

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14

Amahiri, Nathan Nwabu. "Synthesis of TPP - linked MWCNTs / PVC composites and study of their mechanical, thermal and fire retardancy properties." Thesis, 2014. http://hdl.handle.net/10210/11329.

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M.Sc. (Chemistry)<br>The fabrication of multiwalled carbon nanotube/polyvinyl chloride (PVC) composites and a study of their thermal, fire retardancy and mechanical properties are reported. Triphenylphosphine linked - multiwalled carbon nanotube (TPP-MWCNT) and pristine MWCNT were used. The MWCNT were embedded in the polymer matrix through melt blending and solvent casting. The phosphorylation of the MWCNT and their dispersion in the PVC matrix was characterized by scanning electron microscopy and Raman spectroscopy. Thermal analysis of the nanocomposites by thermal gravimetric analysis (TGA)
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15

"Synthesis, Structures and Properties of Thermoelectric Materials in the Zn-Sb-In System." Doctoral diss., 2011. http://hdl.handle.net/2286/R.I.9179.

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abstract: The challenging search for clean, reliable and environmentally friendly energy sources has fueled increased research in thermoelectric materials, which are capable of recovering waste heat. Among the state-of-the-art thermoelectric materials &beta;-Zn4Sb3 is outstanding because of its ultra-low glass-like thermal conductivity. Attempts to explore ternary phases in the Zn-Sb-In system resulted in the discovery of the new intermetallic compounds, stable Zn5Sb4In2-&delta; (&delta;=0.15) and metastable Zn9Sb6In2. Millimeter-sized crystals were grown from molten metal fluxes, where indium
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Lin, Wei-Li, and 林煒力. "Investigation on Opto-electrical Properties and Thermal Stability of Zinc Oxide Based Transparent Conductive Oxides Prepared by Atmospheric Pressure Plasma Jet." Thesis, 2010. http://ndltd.ncl.edu.tw/handle/49814308300299820102.

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碩士<br>國立交通大學<br>電子研究所<br>99<br>In this thesis, we use the APPCVD system to deposit the ZnO based transparent conductive oxides (TCO), including IZO, AZO and GZO. The effect of different doping concentration and substrate temperature on the morphological, structural, electrical and optical properties of the thin films has been investigated. Moreover, we investigate the thermal stability of IZO and GZO at different annealing conditions. All films show the preferred (002) orientation perpendicular to the substrate. The minimum resistivity of 1.7E-3 Ωcm was obtained at a substrate temperature of 2
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