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Статті в журналах з теми "DSC Measurement"

Автор: Grafiati

Опубліковано: 3 червня 2025

Оновлено: 31 липня 2025

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1

Distler, Johanna, Thomas Wöhrl, Robin Werner, et al. "Miniaturized differential scanning calorimeter with an integrated mass sensing system: first steps." Journal of Sensors and Sensor Systems 12, no. 1 (2023): 9–19. http://dx.doi.org/10.5194/jsss-12-9-2023.

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Abstract. In this paper, the first steps towards integrating a mass sensing system into an existing miniaturized ceramic DSC (differential scanning calorimetry) chip are presented. A vibration setup is developed based on the mass-dependent change in frequency of the DSC chip as an oscillating cantilever. A simulation model reveals that the resolution of the measurement can be improved by reducing the chip thickness. In this study, different measurement methods (acoustic, optical, and piezoresistive) are investigated. Three complete measurement systems are set up and evaluated with regard to th

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2

Behrends, Gert, Dirk Stöbener, and Andreas Fischer. "Integrated, Speckle-Based Displacement Measurement for Lateral Scanning White Light Interferometry." Sensors 21, no. 7 (2021): 2486. http://dx.doi.org/10.3390/s21072486.

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Lateral scanning white light interferometry (LSWLI) is a promising technique for high-resolution topography measurements on moving surfaces. To achieve resolutions typically associated with white light interferometry, accurate information on the lateral displacement of the measured surface is essential. Since the uncertainty requirement for a respective displacement measurement is currently not known, Monte Carlo simulations of LSWLI measurements are carried out at first to assess the impact of the displacement uncertainty on the topography measurement. The simulation shows that the uncertaint

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3

Danley, Robert L. "New modulated DSC measurement technique." Thermochimica Acta 402, no. 1-2 (2003): 91–98. http://dx.doi.org/10.1016/s0040-6031(02)00541-5.

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4

Danley, Robert L. "New heat flux DSC measurement technique." Thermochimica Acta 395, no. 1-2 (2002): 201–8. http://dx.doi.org/10.1016/s0040-6031(02)00212-5.

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5

Peret, Anthony, Kelly W. Capel, Mu-Lan Jen, et al. "Perfusion MRI Techniques: Beyond DSC." Neurographics 13, no. 3 (2023): 210–29. http://dx.doi.org/10.3174/ng.2100041.

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The use of brain hemodynamics is important in the assessment of numerous pathophysiologic conditions. The measurement of perfusion or delivery of blood to tissues by MR imaging is essential for neuroradiologists to understand and appropriately apply to clinical practice. Several different approaches are used. DSC and dynamic contrast-enhanced MR imaging study the signal change (according to T2* and T1, respectively) induced by an exogenous contrast agent, allowing the measurement of CBF, CBV, and time-related parameters. Blood oxygen level‐dependent (BOLD) MR imaging measures the T2* signal ch

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6

Gao, Maotiao, Shiqi Zhao, Hongjun Yang, Xuehong Wu, and Yingjie Xiao. "An Analysis of the Influence of DSC Parameters on the Measurement of the Thermal Properties of Phase-Change Material." Materials 17, no. 23 (2024): 5689. http://dx.doi.org/10.3390/ma17235689.

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A differential scanning calorimeter (DSC) is widely used for measuring the thermal properties of phase-change materials (PCMs). Optimizing test conditions based on material characteristics is essential for accurate results. This study investigates the effects of experimental parameters, including sample mass, heating rate, measurement modes, and atmosphere flow rate, on the phase-change enthalpy and phase-change temperature results. The findings indicate that variations in sample mass and heating rate lead to significant changes in phase-change temperatures, while an increase in purge gas flow

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7

MIYATI, TOSHIAKI. "Measurement of cerebral hemodynamics using DSC-MRI." Japanese Journal of Radiological Technology 58, no. 1 (2002): 58–66. http://dx.doi.org/10.6009/jjrt.kj00003111345.

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8

Isayev, A. I., and J. S. Deng. "Nonisothermal Vulcanization of Rubber Compounds." Rubber Chemistry and Technology 61, no. 2 (1988): 340–61. http://dx.doi.org/10.5254/1.3536192.

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Abstract In the present paper, progress has been made in developing a model for nonisothermal vulcanization of rubber compounds. The model is presently based on differential scanning calorimetry (DSC) measurements of heat evolved during vulcanization. The model parameters are determined from several isothermal DSC scans including measurements of induction time and rate of vulcanization. This model has conveniently been employed for a calculation of the temperature distribution during vulcanization of a rubber slab based on a one-dimensional heat-conduction equation with a heat-generation term.

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9

Hinz, Hans-Jürgen, and Frederick P. Schwarz. "Measurement and analysis of results obtained on biological substances with differential scanning calorimetry (IUPAC Technical Report)." Pure and Applied Chemistry 73, no. 4 (2001): 745–59. http://dx.doi.org/10.1351/pac200173040745.

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Differential scanning calorimeters (DSCs) have been widely used to determine the thermodynamics of phase transitions and conformational changes in biological systems including proteins, nucleic acid sequences, and lipid assemblies. DSCs monitor the temperature difference between two vessels, one containing the biological solution and the other containing a reference solution, as a function of temperature at a given scan rate. Recommendations for DSC measurement procedures, calibration procedures, and procedures for testing the performance of the DSC are described. Analysis of the measurements

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10

Warnert, E. A. H., F. Incekara, A. J. P. E. Vincent, et al. "P04.11 Voxelwise correlation between vascular MRI parameters obtained with ASL and DSC is decreased in IDH-wt non-enhancing glioma." Neuro-Oncology 21, Supplement_3 (2019): iii31. http://dx.doi.org/10.1093/neuonc/noz126.106.

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Abstract BACKGROUND Comparative studies of dynamic susceptibility contrast (DSC) based measurement of cerebral blood volume (CBV) or cerebral blood flow (CBF) and arterial spin labelling (ASL) based measurement of CBF have previously shown good correlation of these parameters in human glioma. However, these studies were mostly done before inclusion of the mutation status of the isocitrate dehydrogenase (IDH) encoding gene in brain tumour classification. In light of the call for gadolinium-free imaging, here we investigate the effect of IDH-mutation status on the correlation between ASL and DSC

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11

Liu, Yifan, Jinlin Sun, Zhiqiang Pu, Jianqiang Yi, and Shiliang Pu. "Robust fuzzy tracking control for flexible air-breathing hypersonic vehicles with measurement noises." Transactions of the Institute of Measurement and Control 41, no. 13 (2019): 3818–35. http://dx.doi.org/10.1177/0142331219837590.

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Measurement noise is an obstacle to the performance improvement of a flexible air-breathing hypersonic vehicle. This paper explores a robust fuzzy tracking control scheme for the longitudinal dynamics of the hypersonic vehicle, which is constructed by utilizing type-2 fuzzy adaptive technique and dynamic surface control (DSC) approach. The control scheme is comprised of two parts: the state estimators and tracking controllers of velocity and altitude. The state estimators are designed by using the type-2 fuzzy logic system-based approximators, which guarantees the estimation of real states fro

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12

Fejes, Gergő Richárd, Viktor Gonda, and Károly Széll. "Analysis of Recrystallization Peak Occuring During DSC Measurement." Acta Materialia Transilvanica 1, no. 2 (2018): 73–76. http://dx.doi.org/10.2478/amt-2018-0024.

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Abstract Severe plastic deformation (SPD) is a well-established methodology for the processing of bulk ultrafine grained materials. Among various methods, equal channel angular pressing (ECAP) is the most popular way of creating ultrafine grained materials. The stored energy after ECAP in these substances highly influences the microstructural processes: recovery and recrystallization of the processed materials. We analyzed the recrystallization kinetics of room and elevated temperature ECAP processed copper samples using differential scanning calorimetry (DSC). For the processing of the measur

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13

KUMAGAI, Hitoshi, Kozo NAKAMURA, and Junichi FUJIWHARA. "DSC measurement of frozen water in liquid foods." Agricultural and Biological Chemistry 49, no. 11 (1985): 3097–101. http://dx.doi.org/10.1271/bbb1961.49.3097.

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14

Hakvoort, G. "Measurement of heterogeneously catalyzed gas reactions by DSC." Journal of Thermal Analysis 47, no. 2 (1996): 445–52. http://dx.doi.org/10.1007/bf01983986.

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15

Kumagai, Hitoshi, Kozo Nakamura, and Junichi Fujiwhara. "DSC Measurement of Frozen Water in Liquid Foods." Agricultural and Biological Chemistry 49, no. 11 (1985): 3097–101. http://dx.doi.org/10.1080/00021369.1985.10867241.

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16

Thomsen, H., E. Steffensen, and E.-M. Larsson. "Perfusion MRI (dynamic susceptibility contrast imaging) with different measurement approaches for the evaluation of blood flow and blood volume in human gliomas." Acta Radiologica 53, no. 1 (2012): 95–101. http://dx.doi.org/10.1258/ar.2011.110242.

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Background Perfusion magnetic resonance imaging (MRI) is increasingly used in the evaluation of brain tumors. Relative cerebral blood volume (rCBV) is usually obtained by dynamic susceptibility contrast (DSC) MRI using normal appearing white matter as reference region. The emerging perfusion technique arterial spin labelling (ASL) presently provides measurement only of cerebral blood flow (CBF), which has not been widely used in human brain tumor studies. Purpose To assess if measurement of blood flow is comparable with measurement of blood volume in human biopsy-proven gliomas obtained by DSC

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17

Atef, Eman, Harsh Chauhan, Dev Prasad, Dunesh Kumari, and Charles Pidgeon. "Quantifying Solid-State Mixtures of Crystalline Indomethacin by Raman Spectroscopy Comparison with Thermal Analysis." ISRN Chromatography 2012 (February 6, 2012): 1–6. http://dx.doi.org/10.5402/2012/892806.

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This paper investigates Raman spectroscopy as a quick and reliable method to quantify the alpha (α) and gamma (γ) polymorphic forms of indomethacin compared to differential scanning calorimetry (DSC). Binary mixtures with different ratios of α and γ indomethacin were prepared and analyzed by Raman and DSC. The Raman method was found to be more reliable and superior compared to DSC. The partial conversion of the alpha to gamma polymorphic form during the DSC measurement was the major limitation for the use of full DSC as a quantitative method and resulted in difference between the calculated an

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18

Wudy, Katrin, Maximilian Drexler, Lydia Lanzl, and Dietmar Drummer. "Analysis of time dependent thermal properties for high rates in selective laser sintering." Rapid Prototyping Journal 24, no. 5 (2018): 894–900. http://dx.doi.org/10.1108/rpj-01-2017-0013.

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Purpose The thermal history during laser exposure determines part properties in selective laser sintering (SLS). The purpose of this study is to introduce a new measurement technique based on a CO2 laser unit combined with a high-speed DCS. A first comparison of the thermal history during laser exposure measured with Laser-high-speed-(HS)-differential scanning calorimetry-(DSC) and in SLS process is shown. Design/methodology/approach This Laser-HS-DSC allows an imitation of the SLS-process in a very small scale, as the sample is directly heated by a CO2 laser. For this study, the laser power a

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19

Varallyay, Csanad G., Eric Nesbit, Rongwei Fu, et al. "High-Resolution Steady-State Cerebral Blood Volume Maps in Patients with Central Nervous System Neoplasms Using Ferumoxytol, a Superparamagnetic Iron Oxide Nanoparticle." Journal of Cerebral Blood Flow & Metabolism 33, no. 5 (2013): 780–86. http://dx.doi.org/10.1038/jcbfm.2013.36.

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Cerebral blood volume (CBV) measurement complements conventional magnetic resonance imaging (MRI) to indicate pathologies in the central nervous system (CNS). Dynamic susceptibility contrast (DSC) perfusion imaging is limited by low resolution and distortion. Steady-state (SS) imaging may provide higher resolution CBV maps but was not previously possible in patients. We tested the feasibility of clinical SS-CBV measurement using ferumoxytol, a nanoparticle blood pool contrast agent. SS-CBV measurement was analyzed at various ferumoxytol doses and compared with DSC-CBV using gadoteridol. Ninety

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20

Koenig, Andreas, Leonie Schmohl, Johannes Scheffler, et al. "Is Micro X-ray Computer Tomography a Suitable Non-Destructive Method for the Characterisation of Dental Materials?" Polymers 13, no. 8 (2021): 1271. http://dx.doi.org/10.3390/polym13081271.

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The aim of the study was to investigate the effect of X-rays used in micro X-ray computer tomography (µXCT) on the mechanical performance and microstructure of a variety of dental materials. Standardised bending beams (2 × 2 × 25 mm3) were forwarded to irradiation with an industrial tomograph. Using three-dimensional datasets, the porosity of the materials was quantified and flexural strength was investigated prior to and after irradiation. The thermal properties of irradiated and unirradiated materials were analysed and compared by means of differential scanning calorimetry (DSC). Single µXCT

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21

Danes, Florin, and Bertrand Garnier. "Improved Differential Scanning Calorimetric Measurement Method for the Small Reaction Heat Capacities." Rubber Chemistry and Technology 78, no. 1 (2005): 114–29. http://dx.doi.org/10.5254/1.3547865.

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Abstract Heat capacities of the different rubber states are important features for the engineering calculation of rubber manufacturing. The heat capacity change Δcp due to the vulcanization process has been measured with a differential scanning calorimeter (DSC) only after reducing the standard error of a Δcp measurement under 5 J kg−1 K−1. For this purpose, we used sealed (up to 150 bar) DSC sample pans which avoid mass losses. Heat capacities before and after vulcanization were measured on the same samples using special DSC procedure and reversible thermal effects due to rubber components we

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22

李, 碧桃. "A Time-Dependent Based Automatic Measurement and Control System for Oil Viscosity." Dynamical Systems and Control 07, no. 02 (2018): 85–91. http://dx.doi.org/10.12677/dsc.2018.72009.

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23

Kong, Y., and J. N. Hay. "The measurement of the crystallinity of polymers by DSC." Polymer 43, no. 14 (2002): 3873–78. http://dx.doi.org/10.1016/s0032-3861(02)00235-5.

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24

Boller, A., Y. Jin, and B. Wunderlich. "Heat capacity measurement by modulated DSC at constant temperature." Journal of Thermal Analysis 42, no. 2-3 (1994): 307–30. http://dx.doi.org/10.1007/bf02548519.

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25

Sillinger, T., P. Than, B. Kocsis, and D. Lőrinczy. "DSC measurement of cartilage destruction caused by septic arthritis." Journal of Thermal Analysis and Calorimetry 82, no. 1 (2005): 221–23. http://dx.doi.org/10.1007/s10973-005-0870-8.

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26

Arita, Y., T. Ogawa, B. Tsuchiya, and T. Matsui. "Heat capacity measurement and DSC study of hafnium hydrides." Journal of Thermal Analysis and Calorimetry 92, no. 2 (2008): 403–6. http://dx.doi.org/10.1007/s10973-007-8960-4.

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27

Demensky, G. K., and O. A. Teplov. "Measurement of the thermal capacity of solids by DSC." Journal of Thermal Analysis 32, no. 2 (1987): 451–61. http://dx.doi.org/10.1007/bf01912697.

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28

Isayec, A. I., and M. Wan. "Injection Molding of Rubber Compound with Rheology Affected by Vulcanization: Part I. Material Characterization." Rubber Chemistry and Technology 69, no. 2 (1996): 277–93. http://dx.doi.org/10.5254/1.3538373.

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Abstract Rheological behavior of rubber is highly sensitive to the thermal history and cure kinetics. Rheological characterization for SBR compound is carried out using a capillary rheometer and modified Mooney viscometer. The viscosity function, which is not only temperature and shear-rate dependent but also cure-level dependent, is constructed. A modification of Cross model is proposed and verified to predict the rheological and chemorheological behaviors of SBR compounds. This rheological characterization is combined with vulcanization kinetic characterization. The parameters of vulcanizati

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29

Fang, Wen Bo, and Chong Jie Wang. "Heat Transfer Enhancement Analysis of Microencapsulated Phase Change Suspension." Applied Mechanics and Materials 361-363 (August 2013): 239–43. http://dx.doi.org/10.4028/www.scientific.net/amm.361-363.239.

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This paper investigates heat transfer enhancement of the microencapsulated phase change material (MPCM) suspension. The specific heat of tested sample is measured by A Differential Scan Calorimeter (DSC) analysis. The corrected factor of sample is obtained by theoretical analysis and DSC measurement. The thermal conductivity is obtained by theoretical analysis and verified by previous works.

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30

Krishnamohan, S., S. Ramanathan, and V. Ramakrishnan. "Specific Heat Measurements of Ti6Al4V/Nano SiCp Composite." Journal of Computational and Theoretical Nanoscience 14, no. 1 (2017): 742–46. http://dx.doi.org/10.1166/jctn.2017.6267.

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The elevated strength, low weight ratio and excellent corrosion resistance intrinsic to titanium and its alloys has led to a wide range of successful applications which ensures high levels of unswerving performance in aerospace. The performance of the Thermal Control System extremely depends on the thermal behavior of the materials used in its elements. The measurements of the thermal properties of materials are necessary for better understanding of the thermal design. Differential scanning calorimetry (DSC) is the most extensively used thermal method for finding wealth of information about a

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31

Dhar, Rajat, Guido J. Falcone, Yasheng Chen, et al. "Deep Learning for Automated Measurement of Hemorrhage and Perihematomal Edema in Supratentorial Intracerebral Hemorrhage." Stroke 51, no. 2 (2020): 648–51. http://dx.doi.org/10.1161/strokeaha.119.027657.

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Background and Purpose— Volumes of hemorrhage and perihematomal edema (PHE) are well-established biomarkers of primary and secondary injury, respectively, in spontaneous intracerebral hemorrhage. An automated imaging pipeline capable of accurately and rapidly quantifying these biomarkers would facilitate large cohort studies evaluating underlying mechanisms of injury. Methods— Regions of hemorrhage and PHE were manually delineated on computed tomography scans of patients enrolled in 2 intracerebral hemorrhage studies. Manual ground-truth masks from the first cohort were used to train a fully c

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32

Hisada, Shota, Mitsuhiro Matsuda, Minoru Nishida, Carlo Biffi, and Ausonio Tuissi. "Microstructure and Martensitic Transformation Behavior in Thermal Cycled Equiatomic CuZr Shape Memory Alloy." Metals 9, no. 5 (2019): 580. http://dx.doi.org/10.3390/met9050580.

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Equiatomic CuZr alloy undergoes a martensitic transformation from the B2 parent phase to martensitic phases (P21/m and Cm) below 150 °C. We clarified the effect of the thermal cycling on the morphology and crystallography of martensite in equiatomic CuZr alloy using a transmission electron microscopy. The 10th cycled specimens consisted of different multiple structures at the maximum temperature of differential scanning calorimetry (DSC) measurement −400 °C and 500 °C, respectively. At the maximum temperature 400 °C of DSC measurement, it is composed of the fine plate-like variants, and a lame

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33

Chaloupka, Alexander, André Wedel, Iman Taha, Natalie Rudolph, and Klaus Drechsler. "Phase Change Detection in Neat and Fiber Reinforced Polyamide 6 Using Dielectric Analysis." Materials Science Forum 825-826 (July 2015): 944–51. http://dx.doi.org/10.4028/www.scientific.net/msf.825-826.944.

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In this study online-capable dielectric analysis techniques were investigated to show its potential on the example of detecting phase transitions of polyamide 6 (PA6) and its composites. The differential scanning calorimetry (DSC), a standard testing method commonly applied in thermophysical analysis, is used as a reference method throughout this work. Dielectric measurement techniques are introduced as a means for providing an online measuring concept that is able to monitor phasechanges in both neat, as well as glass and carbon reinforced PA6. Whereas a simple sensor setup has proven to be a

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34

Chen, Zhe, Wei Huang, Peng Fei Fang, Wen Yu та Shao Jie Wang. "Positron Lifetimes and Crystallinity of γ-Irradiated Polypropylenes". Materials Science Forum 733 (листопад 2012): 163–66. http://dx.doi.org/10.4028/www.scientific.net/msf.733.163.

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The microstructure of the polypropylenes (PP) irradiated by gamma ray was studied by positron lifetime technique and differential scanning calorimetry (DSC). Lifetime measurement shows o-Ps intensity decreases with increasing γ irradiation dose. The crystallinity of irradiated samples was detected by DSC method. The correlation between o-Ps intensity and crystallinity indicates γ-ray can induce higher crystallinity in the polypropylene at low irradiation dose.

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35

Tosolin, A., Soucek P., Beneš O., Vigier J.-F., Luzzi L., and Konings R.J.M. "Synthesis of plutonium trifluoride by hydro-fluorination and novel thermodynamic data for the PuF2-LiF system." Journal of Nuclear Materials 503, no. 2018 (2019): 171–77. https://doi.org/10.1016/j.jnucmat.2018.02.037.

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PuF3 was synthetized by hydro-fluorination of PuO2 and subsequent reduction of the product by hydrogenation. The obtained PuF3 was analysed by X-Ray Diffraction (XRD) and found phase-pure. High purity was also confirmed by the melting point analysis using Differential Scanning Calorimetry (DSC). PuF3 was then used for thermodynamic assessment of the PuF3-LiF system. Phase equilibrium points and enthalpy of fusion of the eutectic composition were measured by DSC. XRD analyses of selected samples after DSC measurement confirm that after solidification from the liquid, the system returns to a mix

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36

Ishiyama, Taishi, Kazukui Kobayashi, Yoshihiko Yokoyama, Toyohiko J. Konno, Akihiro Iwase, and Fuminobu Hori. "Structural Relaxation of Open Volume in Hyper-Eutectic Zr-Cu-Al Bulk Amorphous Alloys Measured by Positron Annihilation." Defect and Diffusion Forum 373 (March 2017): 130–33. http://dx.doi.org/10.4028/www.scientific.net/ddf.373.130.

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The Zr-Cu-Al bulk amorphous (BA) alloys, which have no long-range ordered structure, possess various properties such as high strength and toughness with compositional dependence. In the present study, in order to estimate the natures of local structure change and relaxation behavior of hyper-eutectic BA alloys during annealing, positron annihilation measurements and density measurement have been performed for hyper-eutectic Zr-Cu-Al BA alloys with annealing. The enthalpy relaxation and structural relaxation was also measured by differential scanning calorimetry (DSC) measurement. These results

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37

Trawiński, Bartosz, Marcin Łapiński, and Bogusław Kusz. "The unstable thermoelectric effect in non-stoichiometric Cu2Se during the non-equilibrium phase transition." Journal of Materials Science 56, no. 24 (2021): 13705–14. http://dx.doi.org/10.1007/s10853-021-06170-z.

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Abstract The superionic α ↔ β phase transition in Cu1.96Se thermoelectric material is investigated by means of thermal analysis (DSC) and measurements of Seebeck coefficient and electrical conductivity. Results of the DSC measurements with 1–10 K/min heating and cooling rates show that the material is close to the equilibrium phase composition during the transformation. However, the kinetic limitation of the process exists, which is indicated by supercooling. At the beginning of the β → α transition, the most significant kinetic delay was attributed to the nucleation of the α phase. During the

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38

T., B. Sundaresan. "Solid State Mixture Identification of Crystal Indomethacin by Spectroscopy Comparison with Thermal Analysis." International Journal of Trend in Scientific Research and Development 2, no. 6 (2018): 626–30. https://doi.org/10.31142/ijtsrd18583.

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This research investigates Raman spectroscopy as a quick and reliable method to quantify the alpha a and gamma polymorphic forms of indomethacin compared to differential scanning calorimetry DSC . Binary mixtures with different ratios of a and indomethacin were prepared and analyzed by Raman and DSC. The Raman method was found to be more reliable and superior compared to DSC. The partial conversion of the alpha to gamma polymorphic form during the DSC measurement was the major limitation for the use of full DSC as a quantitative method and resulted in difference between the calculated and meas

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39

BAN, Seiji, Masayuki HATTORI, Kiyoharu NARITA, et al. "Glass Transition Temperatures of Dental Porcelains Determined by DSC Measurement." Dental Materials Journal 16, no. 2 (1997): 127–33. http://dx.doi.org/10.4012/dmj.16.127.

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40

Hakvoort, G., L. L. van Reijen, and A. J. Aartsen. "Measurement of the thermal conductivity of solid substances by DSC." Thermochimica Acta 93 (September 1985): 317–20. http://dx.doi.org/10.1016/0040-6031(85)85081-4.

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41

Takahashi, Yoshio. "Latent heat measurement by DSC with sapphire as standard material." Thermochimica Acta 88, no. 1 (1985): 199–204. http://dx.doi.org/10.1016/0040-6031(85)85429-0.

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Qi, Z. N., Z. H. Wan, and Y. P. Chen. "A comparative DSC method for physical aging measurement of polymers." Polymer Testing 12, no. 2 (1993): 185–92. http://dx.doi.org/10.1016/0142-9418(93)90035-n.

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Qiu, Xingdong, Sugata P. Tan, Morteza Dejam, and Hertanto Adidharma. "Novel isochoric measurement of the onset of vapor–liquid phase transition using differential scanning calorimetry." Physical Chemistry Chemical Physics 20, no. 41 (2018): 26241–48. http://dx.doi.org/10.1039/c8cp05613g.

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Ern Kok, Hoi, Kok-Tee Lau, and Nur Hazirah Rosli. "DSC Assessment on Curing Degree of Micron-scaled Adhesive Layer in Lamination-pressed Flexible Printed Circuit Panels." Journal of Mechanical Engineering 18, no. 3 (2021): 131–45. http://dx.doi.org/10.24191/jmeche.v18i3.15418.

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Анотація:

Continuous monitoring and optimisation of the lamination process are critical in negating flexible printed circuit (FPC) delamination risk during operation. The main QC inspection criterion of the lamination adhesive’s curing degree is adhesive thickness. However, this method is prone to measurement error due to poor microscopy image definition and the inspector’s measurement parallax error. The feasibility of using thermal characterisation to measure the difference in curing degrees of micron-scaled adhesive layer of laminated FPC was investigated. Differential scanning calorimetry (DSC) and

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45

Chang, Tung, Kuang-Hua Hsueh, Cheng-Chang Liu, Chen-Rui Cao, and Chi-Min Shu. "A Method to Derive the Characteristic and Kinetic Parameters of 1,1-Bis(tert-butylperoxy)cyclohexane from DSC Measurements." Processes 10, no. 5 (2022): 1026. http://dx.doi.org/10.3390/pr10051026.

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A differential scanning calorimetry (DSC) experiment was carried out to determine the thermal characteristics of harmful substances. Most experimenters only use the results of measurement and rarely conduct in-depth research on the variety of information behind the measurement. This study used Wolfram’s Mathematica as a DSC measurement research tool to plot the peak curve and derive the characteristic parameters graphically for 1,1-Bis(tert-butylperoxy)cyclohexane. The research steps included raw data cleansing, peak curve normalization, characteristic parameter derivation, and total reaction

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Baba, Mohamed, Soney C. George, Jean Luc Gardette, and Jacques Lacoste. "Evaluation of Crosslinking in Elastomers Using Thermoporometry, Densimetry and Diffential Scanning Calorimetry Analysis." Rubber Chemistry and Technology 75, no. 1 (2002): 143–54. http://dx.doi.org/10.5254/1.3547666.

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Abstract The classical methods available for evaluating the degree of crosslinking in elastomers are stress-strain and swelling measurements. In this study, we have adopted a new analytical approach based on thermoporometry, densimetry and DSC for comparing the crosslinking density in elastomers. Crosslinking by chemical reaction or by photo-oxidation has been studied on polymer samples Ethylene-Propylene-Diene rubber (EPDM) and PolyButadiene (PB). Analysis has been done separately for soluble and insoluble fractions. The soluble fraction has been studied by densimetry and the insoluble fracti

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Kishi, A., and H. Toraya. "Simultaneous measurements of X-ray diffraction (XRD) and differential scanning calorimetry (DSC) data under controlled humidity condition: Instrumentation and application to studies on hydration, dehydration, and rehydration processes of pharmaceutical compounds." Powder Diffraction 19, no. 1 (2004): 31–35. http://dx.doi.org/10.1154/1.1649321.

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An instrument for the simultaneous measurement of X-ray powder diffraction (XRD) data and differential scanning calorimetry (DSC) data under a controlled humidity condition has been developed in order to achieve a design concept of reliable and simple in operation. Examples of the application to studies on hydration, dehydration, and rehydration processes of pharmaceutical compounds under various humidity conditions are presented. The usefulness of the present XRD-DSC system will be demonstrated.

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张, 炳瑞. "Based on GNSS and MIMU Fusion of Measurement and Calculation Method of Driving Wheel Slip of Vehicles." Dynamical Systems and Control 08, no. 01 (2019): 1–7. http://dx.doi.org/10.12677/dsc.2019.81001.

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Głowacka, Julia, Łukasz Derpeński, Miłosz Frydrych, Bogna Sztorch, Błażej Bartoszewicz, and Robert E. Przekop. "Robotization of Three-Point Bending Mechanical Tests Using PLA/TPU Blends as an Example in the 0–100% Range." Materials 16, no. 21 (2023): 6927. http://dx.doi.org/10.3390/ma16216927.

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This article presents the development of an automated three-point bending testing system using a robot to increase the efficiency and precision of measurements for PLA/TPU polymer blends as implementation high-throughput measurement methods. The system operates continuously and characterizes the flexural properties of PLA/TPU blends with varying TPU concentrations. This study aimed to determine the effect of TPU concentration on the strength and flexural stiffness, surface properties (WCA), thermal properties (TGA, DSC), and microscopic characterization of the studied blends.

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Yang, Yang, He Liu, and Khalid M. Mosalam. "An Improved Direct Stiffness Calculation Technique for Damage Detection of Bending Structures." Advanced Materials Research 368-373 (October 2011): 2224–28. http://dx.doi.org/10.4028/www.scientific.net/amr.368-373.2224.

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In this paper, a practical application for a continues beam-type bridge, the Truckee river bridge, California, to test the validity of the improved DSC method in the identification of the bridge damage after severe loading such as that caused by an earthquake was discussed. Comparing the calculated stiffness from the improved DSC method with that from design data of the bridge based on the numerical simulation with different damage scenarios in consideration of measurement errors, the location and severity of the damage in the bridge can be accurately and reliably detected. The pushover and se

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