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Дисертації з теми "Metal carbonyl compounds"

Автор: Grafiati

Опубліковано: 25 липня 2024

Оновлено: 31 липня 2025

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1

Taylor, Paul H. "Metal free-oxygenation of carbonyl compounds." Thesis, Cardiff University, 2010. http://orca.cf.ac.uk/54244/.

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The findings to date have contributed to the development of a novel and useful class of synthetic protocol and have resulted in a greatly enhanced understanding of the fundamental workings of the &agr;-oxygenation.

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2

Bojczuk, M. "Carbonyl exhange mechanisms in transition metal compounds." Thesis, University of Kent, 1986. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.372765.

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3

Lorusso, Patrizia. "Metal catalysed alkylation of carbonyl compounds with formaldehyde." Thesis, University of St Andrews, 2015. http://hdl.handle.net/10023/7823.

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Formaldehyde is a chemical used widely in the manufacture of building materials. A remarkable example is represented by the Lucite two-step Alpha technology for the large scale production of methyl methacrylate (MMA), the essential building block of all acrylic-based products. Esters and ketones are important intermediates in the manufacture of acrylate esters therefore α-hydroxymethylenation of carbonyl compounds using formaldehyde as a one carbon alkylating agent and subsequent dehydration to the corresponding methylenated derivatives has been explored in the current work. We report a novel

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4

Llewellyn, Simon. "Acyl carbonyl transition metal compounds : their homologation and hydrogenation." Thesis, University of Oxford, 2005. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.433556.

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5

洪若華 and Yeuk-wah Hung. "The chemistry of Osmium-Rhodium mixed-metal carbonyl clusters." Thesis, The University of Hong Kong (Pokfulam, Hong Kong), 1998. http://hub.hku.hk/bib/B3121535X.

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6

Hung, Yeuk-wah. "The chemistry of Osmium-Rhodium mixed-metal carbonyl clusters /." Hong Kong : University of Hong Kong, 1998. http://sunzi.lib.hku.hk/hkuto/record.jsp?B19904988.

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7

Ladogana, Santino. "Kinetics and Mechanisms of Metal Carbonyls." Thesis, University of North Texas, 1998. https://digital.library.unt.edu/ark:/67531/metadc278709/.

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Pulsed laser flash photolysis with both visible and infrared detection has been applied to the study of the displacement of weakly coordinating ligands (Lw) by strongly "trapping" nucleophiles (Ls) containing either an olefinic functionality (Ls = 1-hexene, 1-decene, 1-tetradecene) or nitrogen (Ls = acetonitrile, hydrocinnamonitrile) from the photogenerated 16 electron pentacarbonylchromium (0) intermediate. 5-Chloropent-l-ene (Cl-ol), a potentially bidentate ligand, has been shown to form (ol-Cl) pentacarbonylchromium (0), in which Cl-ol is bonded to Cr via a lone pair on the chlorine, and is

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8

Mansour, Saber E. (Saber El-Sayed). "The Nature of Intermediates Produced Through Ligand-Substitution Reactions of Octahedral Metal Carbonyls." Thesis, North Texas State University, 1986. https://digital.library.unt.edu/ark:/67531/metadc331634/.

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Pulsed laser time-resolved ligand-substitution photochemistry for (DTO)W(CO)4, (DTN)W(CO)4, and (NP)Mo(CO)4 (DTO = 2,2,7,7-tetramethyl-3,6-diathiaoctane; DTN = 2,2,8,8- tetramethyl-3,7-diathianonane; NP = l-diethylamino-2- diphenylphosphinoethane) proceeds via initial fission of the W-S and Mo-P bonds, affording Cs and C4v five-coordinate intermediates for DTN and NP but largely Cs for DTO. The rates of reaction of these intermediates, via chelate ring closure and competitive bimolecular interaction with Lewis bases (= L, alkylphosphines and alkyl phosphites) for the Cs intermediates and via b

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9

王淑儀 and Shuk-yee Janet Wong. "The chemistry of osmium carbonyl clusters containing oxime and oxo ligands." Thesis, The University of Hong Kong (Pokfulam, Hong Kong), 2003. http://hub.hku.hk/bib/B31244932.

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10

Ismail, Ashraf A. "Chalcocarbonyl chemistry : application in hormonal receptor determination, metalloporphyrins and metal-arene bond activation." Thesis, McGill University, 1985. http://digitool.Library.McGill.CA:80/R/?func=dbin-jump-full&object_id=72063.

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The reaction of ((eta)-Arene)Cr(CO)(,2)(CX) (X = S, Se) complexes with excess (RO)(,3)P (R = Me, Et, n-Bu, Ph) yields Cr(CO)(,2)(CX) (RO)(,3)P (,3), predominantly as the mer I isomer, in which a phosphite ligand is trans to CX. Arene displacement from ((eta)-C(,6)H(,6))Cr(CO)(,2)(CX) by tridentate phosphine ligands L-L-L L-L-L = (Me)C(CH(,2)P(Ph)(,2))(,3), (Ph(,2)PCH(,2)CH(,2))(,2)PhP gives fac-(L-L-L)Cr(CO)(,2)(CX) products. The molecular structures of Cr(CO)(,2)(CX) (MeO)(,3)P (,3) have been determined by single crystal X-ray diffraction. Intramolecular isomerization of these complexes as we

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11

Keiller, B. T. "The vibrational spectra of metal cluster compounds containing organic ligands." Thesis, University of East Anglia, 1988. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.383722.

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12

何毅雯 and Ngai-man Emmie Ho. "The chemistry of ruthenium carbonyl clusters containing nitrene and nitrido ligands." Thesis, The University of Hong Kong (Pokfulam, Hong Kong), 2000. http://hub.hku.hk/bib/B3124029X.

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13

Ho, Ngai-man Emmie. "The chemistry of ruthenium carbonyl clusters containing nitrene and nitrido ligands /." Hong Kong : University of Hong Kong, 2000. http://sunzi.lib.hku.hk/hkuto/record.jsp?B21982351.

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14

Li, Yat. "Syntheses, structural characterization and electrochemistry of tetraosmium carbonyl clusters and catalytic properties of tetraosmium-gold mixed-metal clusters /." Hong Kong : University of Hong Kong, 2002. http://sunzi.lib.hku.hk/hkuto/record.jsp?B25155064.

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15

Curtis, H. "Synthesis, characterisation and reactivity of transition metal carbido-carbonyl cluster and other organometallic compounds." Thesis, University of Cambridge, 1986. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.377825.

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16

Wasmund, Eric Bain Coley Ken. "A study of powder making by the decomposition of nickel carbonyl in an aerosol tube reactor." *McMaster only, 2005.

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17

Potratz, Christopher M. "The Synthesis, Structure and Characterization of Extended Cobalt Ruthenium Carbonyl Compounds." The Ohio State University, 2010. http://rave.ohiolink.edu/etdc/view?acc_num=osu1275413923.

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18

Ting, Fai Lung. "The chemistry of osmium and ruthenium carbonyl clusters with functionalized alkyne and phosphine ligands." HKBU Institutional Repository, 2001. http://repository.hkbu.edu.hk/etd_ra/296.

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19

李軼 and Yat Li. "Syntheses, structural characterization and electrochemistry of tetraosmium carbonyl clusters and catalytic properties of tetraosmium-gold mixed-metal clusters." Thesis, The University of Hong Kong (Pokfulam, Hong Kong), 2002. http://hub.hku.hk/bib/B31243356.

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20

Middleton, Mark D. "Synthesis of novel amino acids and peptides by rearrangement of ammonium ylides generated from metal carbenoids." Thesis, University of Nottingham, 2003. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.289457.

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21

Bhattacharyya, Nripendra Kumar. "Preparation and characterization of binuclear carbonylates of the iron triad and tetranuclear carbonylates of iridium : the condensation of mononuclear hydrido carbonylates to trinuclear hybrido carbonylates of the iron triad /." The Ohio State University, 1985. http://rave.ohiolink.edu/etdc/view?acc_num=osu1487260135356797.

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22

Buitrago, Elina. "Transition metal-catalyzed reduction of carbonyl compounds : Fe, Ru and Rh complexes as powerful hydride mediators." Doctoral thesis, Stockholms universitet, Institutionen för organisk kemi, 2012. http://urn.kb.se/resolve?urn=urn:nbn:se:su:diva-75795.

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Анотація:

A detailed mechanistic investigation of the previously reported ruthenium pseudo-dipeptide-catalyzed asymmetric transfer hydrogenation (ATH) of aromatic ketones was performed. It was found that the addition of alkali metals has a large influence on both the reaction rate and the selectivity, and that the rate of the reaction was substantially increased when THF was used as a co-solvent. A novel bimetallic mechanism for the ruthenium pseudo-dipeptide-catalyzed asymmetric reduction of prochiral ketones was proposed. There is a demand for a larger substrate scope in the ATH reaction, and heteroar

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23

Zhang, Shulin. "Studies of Solvent Displacement from Solvated Metal Carbonyl Complexes of Chromium, Molybdenum, and Tungsten." Thesis, University of North Texas, 1990. https://digital.library.unt.edu/ark:/67531/metadc331992/.

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Flash photolysis techniques were applied to studies of solvent displacement by Lewis bases (L) from solvated metal carbonyl complexes of Cr, Mo, and W. On the basis of extensive studies of the reaction rate laws, activation parameters , and linear-free-energy-relationships, it was concluded that the mechanisms of solvent displacement reactions depend on the electronic and steric properties of the solvents and L, as well as the identities of the metal atoms. The strengths of solvent-metal bonding interactions, varying from ca. 7 to 16 kcal/mol, and the bonding "modes" of solvents to metals are

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24

Awad, Hani H. (Hani Hanna). "Thermal and Flash Photolysis Studies of Ligand-Exchange Reactions of Substituted Metal Carbonyl Complexes of Cr and Mo." Thesis, University of North Texas, 1989. https://digital.library.unt.edu/ark:/67531/metadc332097/.

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Thermal and flash photolysis studies of ligand-substitution reactions of cis-(pip)(L)M(CO)_4 by L' (pip = piperidine; L, L' = CO, phosphines, phosphites; M = Cr, Mo) implicate square-pyramidal [(L)M(CO)_4], in which L occupies a coordination site in the equatorial plane, as the reactive species. In chlorobenzene (= CB) solvent, the predominant species formed after flash photolysis and a steady-state intermediate for the thermal reaction is cis—[(CB)(L)M(CO)_4], for which rates of CB-dissociation increase with increasing steric demands of coordinated L. Rates of CB-dissociation from trans-[(CB)

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25

Siriwardane, Upali. "Systematic syntheses of iron-triad (Fe,Ru,Os) tetranuclear clusters by redox condensation reactions of [Ru(3);CO(11)) and [Os(3);CO(11)] trinuclear carbonylates; co-crystallization of ruthenium-osmium clusters /." The Ohio State University, 1985. http://rave.ohiolink.edu/etdc/view?acc_num=osu1487264603216477.

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26

Daghetta, M. A. A. "USE OF POLIPHOSPHANES IN THE ASSEMBLY OF DISCRETE OR POLYMERIC COORDINATION COMPOUNDS." Doctoral thesis, Università degli Studi di Milano, 2010. http://hdl.handle.net/2434/155259.

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Although phosphanes show useful features for the coordination chemistry, their use as pure structural building blocks, to join metal centres in larger aggregates, has not been yet well explored. In this work, synthesis and characterization of discrete and polymeric coordination compounds are presented. As metal centres both monometallic and cluster compounds have been used, whereas as ligands we have used poliphosphanes both commercially available and synthesised in our laboratories. For simplicity we can classify them in: rigid diphosphanes, flexible diphosphanes and rigid poliphosphanes.

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27

Zheng, Jianxia. "Earth-abundant metal complexes for catalyzed hydroelementation." Thesis, Rennes 1, 2014. http://www.theses.fr/2014REN1S148/document.

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Ce travail de recherche est consacré au développement de catalyseurs à base de métaux de transition abondants de la première rangée du tableau périodique, tels que Mn, Fe, et Ni, pour les réactions d'hydro-élémentation. Tout d'abord, l'hydrosilylation de cétones et d'aldéhydes a été accomplie en utilisant un système catalytique simple Ni(OAc)₂ 4H2O/PCy₃ avec le PMHS, silane peu coûteux et stable en tant que source d'hydrure. L'amination réductrice d'aldéhydes avec des amines a également été réalisée avec le même système catalytique et le TMDS, comme silane. Deuxièmement, l’efficacité des compl

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28

Naeemi, Qaseem [Verfasser]. "Studies in Enantioselective Transition Metal Catalysis Using Modular Phosphine-Phosphite Ligands Copper-catalyzed 1,4-Addition of Grignard Reagents to alpha,beta-Unsaturated Carbonyl Compounds / Qaseem Naeemi." München : Verlag Dr. Hut, 2012. http://d-nb.info/1020299428/34.

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29

Abdali, Abdelkrim. "Fonctionnalisation de complexes polyeniques de fer-tricarbonyle : nouvelles voies d'acces aux dienones silylees aux trienes gem-difonctionnels et aux epoxydienes." Université Louis Pasteur (Strasbourg) (1971-2008), 1988. http://www.theses.fr/1988STR13103.

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30

SEMRA, ASSIA. "Substitutions nucleophiles en serie arenetricarbonylchrome." Paris 6, 1987. http://www.theses.fr/1987PA066622.

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31

Nuel, Didier. "Etude de la reactivite de fragments alkylidynes dans des clusters trinucleaires du fer." Toulouse 3, 1986. http://www.theses.fr/1986TOU30206.

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Анотація:

Reactivite des complexes fe::(3)(co)::(9)(cch::(3))(coc::(2)h::(5)) ou fe::(3)(co)::(10)(cch::(3))(h). Les reactions de couplage des groupes alkylidynes avec les algues sont faciles. L'action de co a mis en evidence le couplage reversible dans des conditions douces de 2 fragments alkylidynes. En general, la presence du coordinat hydruro rend les reactions plus complexes

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32

Rouida, Bouchaïb. "Syntheses diastereoselectivites de complexes chiraux du molybdene et du fer carbonyle par action de derives asymetriques du phosphore." Paris 6, 1988. http://www.theses.fr/1988PA066515.

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La reaction photochimique de plusieurs phosphines asymetriques avec des complexes carbonyles du fer et du molybdene cyclopentadienyls fournit des complexes chiraux. Ceux-ci se forment par couples de diastereoisomeres en proportions variables. L'effet sterique de ces phosphines sur le mecanisme de reaction est etudie. D'autre part, lorsque le complexe cyclopentadienyl carbonyle du fer comporte une liaison fer-silicium, fer-germanium ou fer-etain il se produit des interactions conduisant a des inductions diastereotopiques importantes

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33

Jund, Rodolphe. "Electrochimie de clusters mixtes tetrametalliques." Université Louis Pasteur (Strasbourg) (1971-2008), 1987. http://www.theses.fr/1987STR13175.

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34

Neff, Denis. "Complexes alleniques de cyclopentadienyle manganese dicarbonyle : acces aux allenes optiquement actifs, etude de photodecomplexations et syntheses de complexes difonctionnels." Université Louis Pasteur (Strasbourg) (1971-2008), 1988. http://www.theses.fr/1988STR13122.

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35

GOMES, DE LIMA LUIS CARLOS. "Reactions d'alcynes cyanes (monocyanoacethylene et dicyanoacethylene), vis-a-vis de complexes organometalliques du fer, du cobalt, du molybdene et du tungstene." Brest, 1986. http://www.theses.fr/1986BRES2009.

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Анотація:

Etude de la reactivite de complexes thiolates du fer et du tungstene (cp(co)::(n) m(sch::(3))) vis a vis du mono et du dicyanoacetylene. Aptitude des complexes de co(i) a intervenir dans la formation de molecules organiques. Nature des liaisons m-pb(m=mo ou w) dans les complexes cp(co)::(3)m-pbr::(3) et (cp(co)::(3)m)::(2) pbr::(2). Donnes de rmn de **(95)mo et **(207)pb

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36

Greene, Timothy Michael. "Spectroscopic and structural studies of some reactive hydride and organometallic compounds." Thesis, University of Oxford, 1995. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.282165.

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37

Caminade, Anne-Marie. "Stabilisation par complexation d'entites phosphorees de basse coordinence." Toulouse 3, 1988. http://www.theses.fr/1988TOU30073.

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Анотація:

On obtient selon le substituant organique du phosphore, des complexes de phosphines, diphosphanes halogenes et de derives phosphores a base coordinence (phosphine, phosphalcine, diphosphine, phosphacumulene

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38

Wu, Guanmin Richmond Michael G. "Synthesis characterization, and kinetics of isomerization, C-H and P-C bond activation for unsaturated diphosphine-coordinated triosmium carbonyl clusters." [Denton, Tex.] : University of North Texas, 2008. http://digital.library.unt.edu/permalink/meta-dc-6037.

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39

Gomes, de Lima Bernardes Miriam. "Réactivité de complexes organométalliques mono- et dinucléaires : synthèse de thiolato-composés du molybdène, du tungstène et du cobalt : étude de la formation de liaisons c-c dans la sphère de coordination du métal." Brest, 1986. http://www.theses.fr/1986BRES2008.

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Caracterisation des complexes ((c::(5)h::(5))(co)::(2) lwc(cf::(3)) = c(cf::(3))h) et (c::(5)h::(5))(co) lwc(o)c(cf::(3)) = c(cf::(3))h) (l=co,pr::(3),p(or)::(3)) synthese de complexes dinucleaires de mo et w. L'addition oxydante de dialkylsulfure a des derives biportes de mo(ii) et w(ii) a donne lieu a la formation de complexes thiolato triportes ((c::(5)h::(5))(co)m(mu -sr)::(3)m(co)(c::(5)h::(5)))tx**(-)

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40

Foulet-Fonseca, Gloria. "Etude par spectroscopie vibrationnelle des complexes méthylcarbyniques et méthylcarbéniques de chrome." Paris 13, 1987. http://www.theses.fr/1987PA132028.

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Анотація:

Etude en particulier de complexes, du type br(co)::(4)crcch::(3), br(co)::(4)crcchd::(2) et d'une série de mélanges isotopiques. Mise en évidence de la non-équivalence des liaisons c-h du groupe methyle. Etablissement d'un champ de forces pour les complexes méthylcarbyniques

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41

Lock, S. J. "Water-tolerant organometallic reactions : nucleophilic additions to carbonyl compounds using allyl metals in aqueous solution." Thesis, Swansea University, 2003. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.637942.

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Against a background of the reactivity of traditional organometallics, this work describes nucleophilic addition reactions that take place <i>via</i> the intervention of metals in the presence of water. The experimental work focuses on allylation of aldehydes in water-containing solvents using nickel, bismuth and aluminium. Chapter 1 outlines the current influence of environmental issues on the practice of chemistry and the value of water as a solvent. Carbon-carbon bond formation is discussed in the context of mechanism and common methods are reviewed, particularly with respect to reaction of

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42

Etienne, Michel. "Réactivité de complexes dinucléaires hydrure et alcénylidène ponte du fer vis-a-vis d'hydrocarbures cyanes insatures (mono et dicyanoacétylène, tétracyanoethylène)." Brest, 1988. http://www.theses.fr/1988BRES2009.

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Анотація:

Preparation de complexes avec des coordinats cyano-4 butadienyldene portants. On obtient egalement des complexes dinucleaires avec le tricyano-3,4,4 butadienylidene-1,3. Mecanisme ses reactions de migration de l'hydrogene allylique

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43

Laurent, Pascale. "Complexes acyl, alcoxycarbonyl et alkyl tetracarbonylfer : intermédiaires dans la carbonylation catalytique d'halogénures d'alkyle." Brest, 1989. http://www.theses.fr/1989BRES2002.

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44

Holmes, Brett. "Mobilization of Metals and Phosphorous from Intact Forest Soil Cores by Dissolved Inorganic Carbon: A Laboratory Column Study." Fogler Library, University of Maine, 2007. http://www.library.umaine.edu/theses/pdf/HolmesB2007.pdf.

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45

Achi, Sabah Samira. "Nouvelle voie d'acces aux acides alpha -amines, par catalyse homogene a l'aide de complexes de metaux de transition, synthese de nouveaux complexes phosphores chiraux du tungstene pentacarbonyle." Paris 6, 1987. http://www.theses.fr/1987PA066227.

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46

Odongo, Onduru Stephen. "Rhenium(I) tricarbonyl complexes synthesis, photophysics, swithing and recognition properties /." Diss., Online access via UMI:, 2005.

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47

Bates, Sarah Anne. "Fourier transform infrared isotopic studies on novel metal-carbon clusters trapped in Ar matrix environments." [Fort Worth, Tex.] : Texas Christian University, 2008. http://etd.tcu.edu/etdfiles/available/etd-04222008-113234/unrestricted/bates.pdf.

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48

Wang, Yi. "Metal-organic and organic photosensitizers for photocatalytic hydrogen generation and carbon dioxide reduction." HKBU Institutional Repository, 2017. https://repository.hkbu.edu.hk/etd_oa/414.

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This thesis is focused on developing metal-organic and organic molecules for photocatalytic water splitting and carbon dioxide reduction. In chapter 1, an overview of hydrogen production, dye-sensitized solar cells and carbon dioxide reduction are provided. The development history and reaction mechanisms of catalytic systems are introduced along with the typical examples in each field. The applications of both metal-organic and organic compounds are covered. In chapter 2, nine molecular organic photosensitizers were designed and synthesized. The nine molecules were employed as the photosensiti

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Ying, Fang. "Au/CeO₂ based catalysts for catalytic oxidation of volatile organic compounds and carbon monoxide." HKBU Institutional Repository, 2010. http://repository.hkbu.edu.hk/etd_ra/1185.

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Yang, Ning. "Synchrotron Diffraction Studies of Spontaneous Magnetostriction in Rare Earth Transition Metal Compounds." Washington, D.C. : Oak Ridge, Tenn. : United States. Dept. of Energy. Office of Science ; distributed by the Office of Scientific and Technical Information, U.S. Dept. of Energy, 2004. http://www.osti.gov/servlets/purl/835381-gxv1Km/webviewable/.

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