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Добірка наукової літератури з теми "Nmr hrmas"

Автор: Grafiati

Опубліковано: 4 вересня 2022

Оновлено: 31 липня 2025

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Статті в журналах з теми "Nmr hrmas"

Liguori, Domenico, and Pierluigi Mazzei. "HRMAS NMR Spectroscopy to Identify the Primary Metabolome of Bracigliano PGI Sweet Cherries and Correlate It with Nutraceutical and Quality Parameters." Foods 14, no. 12 (2025): 2120. https://doi.org/10.3390/foods14122120.

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In 2023, the Italian Bracigliano sweet cherries were awarded the important European label PGI. However, reliable information on the compositional and nutraceutical quality of this product is still relatively undefined and fragmented. Therefore, we investigated fresh Bracigliano PGI cherries (Pallaccia, Spernocchia, and Principe varieties) via HRMAS NMR spectroscopy in the semi-solid state, even though it represents an innovative and powerful technique that is still drastically unexplored. We demonstrated the HRMAS NMR suitability for this fruit type as well as identified the primary metabolome

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Castejón, David, José Segura, Karen Paola Cruz-Díaz, et al. "A Metabolomics Study by 1H HRMAS NMR: From Sheep Milk to a Pressed-Curd Cheese: A Proof of Concept." Analytica 5, no. 2 (2024): 170–86. http://dx.doi.org/10.3390/analytica5020011.

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For the first time, High-Resolution Magic Angle Nuclear Magnetic Resonance spectroscopy (NMR-HRMAS) was applied to directly identify specific metabolites from a Spanish raw ewe’s milk and enzymatic coagulation pressed-curd cheese (Protected Geographical Indication: Castellano) manufactured by two procedures (traditional/artisanal vs. industrial) and including the ewe’s raw milk. The NMR parameters were optimized to study the complex matrixes of this type of cheese. In addition, conventional overcrowded 1H-NMR-HRMAS spectra were selectively simplified by a Carr–Purcell–Meiboom–Gill (CPMG) seque

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Martínez-Bisbal, M. Carmen, Vicent Esteve, Beatriz Martínez-Granados, and Bernardo Celda. "Magnetic Resonance Microscopy Contribution to Interpret High-Resolution Magic Angle Spinning Metabolomic Data of Human Tumor Tissue." Journal of Biomedicine and Biotechnology 2011 (2011): 1–8. http://dx.doi.org/10.1155/2011/763684.

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HRMAS NMR is considered a valuable technique to obtain detailed metabolic profile of unprocessed tissues. To properly interpret the HRMAS metabolomic results, detailed information of the actual state of the sample inside the rotor is needed. MRM (Magnetic Resonance Microscopy) was applied for obtaining structural and spatially localized metabolic information of the samples inside the HRMAS rotors. The tissue was observed stuck to the rotor wall under the effect of HRMAS spinning. MRM spectroscopy showed a transference of metabolites from the tissue to the medium. The sample shape and the metab

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Valentini, Massimiliano, Mena Ritota, Caterina Cafiero, Sara Cozzolino, Liviana Leita, and Paolo Sequi. "The HRMAS-NMR tool in foodstuff characterisation." Magnetic Resonance in Chemistry 49 (December 2011): S121—S125. http://dx.doi.org/10.1002/mrc.2826.

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Lippens, Guy, Maryse Bourdonneau, Christophe Dhalluin, et al. "Study of Compounds Attached to Solid Supports Using High Resolution Magic Angle Spinning NMR." Current Organic Chemistry 3, no. 2 (1999): 147–69. http://dx.doi.org/10.2174/1385272803666220131194702.

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This article presents an overview of high resolution magic angle spinning (HRMAS) NMR applied to solid phase synthesis. The different interactions existing in such samples are described and analyzed with respect to their effect on the linewidth of the sample. The critical element leading to the relatively narrow linewidth observed in such compounds using HRMAS is shown to be the averaging of the magnetic susceptibility differences at the resin bead I solvent interface. The hardware required to record such spectra is described with an emphasis on probe technology. Applications of HRMAS to a tet

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Ben Sellem, D., K. Elbayed, A. Neuville, et al. "Metabolomic Characterization of Ovarian Epithelial Carcinomas by HRMAS-NMR Spectroscopy." Journal of Oncology 2011 (2011): 1–9. http://dx.doi.org/10.1155/2011/174019.

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Objectives. The objectives of the present study are to determine if a metabolomic study by HRMAS-NMR can (i) discriminate between different histological types of epithelial ovarian carcinomas and healthy ovarian tissue, (ii) generate statistical models capable of classifying borderline tumors and (iii) establish a potential relationship with patient's survival or response to chemotherapy.Methods. 36 human epithelial ovarian tumor biopsies and 3 healthy ovarian tissues were studied using1H HRMAS NMR spectroscopy and multivariate statistical analysis.Results. The results presented in this study

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Ritota, Mena, Lorena Casciani, Sebastiana Failla, and Massimiliano Valentini. "HRMAS-NMR spectroscopy and multivariate analysis meat characterisation." Meat Science 92, no. 4 (2012): 754–61. http://dx.doi.org/10.1016/j.meatsci.2012.06.034.

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Metelo, Ana M., Nuria Arias-Ramos, Pilar Lopez-Larrubia, and M. Margarida C. A. Castro. "Metabolic effects of VO(dmpp)2 – an ex vivo1H-HRMAS NMR study to unveil its pharmacological properties." New Journal of Chemistry 43, no. 45 (2019): 17841–49. http://dx.doi.org/10.1039/c9nj02491c.

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Weng, JianXiang, Isabella H. Muti, Anya B. Zhong, et al. "A Nuclear Magnetic Resonance Spectroscopy Method in Characterization of Blood Metabolomics for Alzheimer’s Disease." Metabolites 12, no. 2 (2022): 181. http://dx.doi.org/10.3390/metabo12020181.

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There is currently a crucial need for improved diagnostic techniques and targeted treatment methods for Alzheimer’s disease (AD), a disease which impacts millions of elderly individuals each year. Metabolomic analysis has been proposed as a potential methodology to better investigate and understand the progression of this disease. In this report, we present our AD metabolomics results measured with high resolution magic angle spinning (HRMAS) nuclear magnetic resonance (NMR) on human blood plasma samples obtained from AD and non-AD subjects. Our study centers on developments of AD and non-AD m

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Castejón, David, José Segura, Karen P. Cruz-Díaz, et al. "1H HRMAS NMR Metabolomics for the Characterization and Monitoring of Ripening in Pressed-Curd Ewe’s Milk Cheeses Produced Through Enzymatic Coagulation." Foods 14, no. 13 (2025): 2355. https://doi.org/10.3390/foods14132355.

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A comprehensive characterization of two pressed-curd cheeses produced from ewe’s milk using enzymatic coagulation—Manchego cheese (with Protected Designation of Origin, PDO) and Castellano cheese (with Protected Geographical Indication, PGI)—was performed throughout the manufacturing process (industrial or traditional) and ripening stages (2, 9, 30, 90, and 180 days). Proton high-resolution magic angle spinning nuclear magnetic resonance (1H HRMAS NMR) spectroscopy, combined with Principal Component Analysis (PCA) and cluster analysis, was applied to intact cheese samples. The combination of t

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Дисертації з теми "Nmr hrmas"

Stenman, Katarina. "Prostate Cancer Diagnosis : experimental and Clinical Studies With HRMAS NMR Spectroscopy." Doctoral thesis, Umeå universitet, Institutionen för strålningsvetenskaper, 2011. http://urn.kb.se/resolve?urn=urn:nbn:se:umu:diva-43651.

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A few abnormal cells found in a small piece of prostate tissue are most consequential for a man’s future. The prevalence of prostate cancer (PCa) is increasing globally. The main instigating factor for this cancer is not yet known, but it appears to be the consequence of many variables such as an increasingly older population, more frequent PSA-testing, and factors involving lifestyle. Prostate cancer screening, as an equivalent for breast cancer screening, has been suggested but unfortunately there are no accurate diagnostic tools available for this type of screening. The reason for this is

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Ben, Sellem Dorra. "Métabolomique RMN HRMAS dans les cancers gynécologiques." Thesis, Strasbourg, 2013. http://www.theses.fr/2013STRAD027.

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Le cancer est la première cause de morbi-mortalité dans le monde. La recherche de biomarqueurs diagnostiques, pronostiques et prédictives de la réponse aux traitements est capitale dans l’amélioration de la prise en charge de ce fléau mondial. Nous avons choisi une technique récente qui est la spectroscopie RMN HRMAS et des méthodes d’analyse statistique robustes (PCA et PLS-DA), afin d’établir les profils métaboliques des cancers épithéliaux de l’ovaire et des cancers mammaires. Nous avons établi, après un rappel théorique de la spectroscopie RMN HRMAS, un état d’art des applications médicale

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Löbel, Franziska. "Identification of Prostate Cancer Metabolomic Markers by 1H HRMAS NMR Spectroscopy and Quantitative Immunohistochemistry." Doctoral thesis, Universitätsbibliothek Leipzig, 2015. http://nbn-resolving.de/urn:nbn:de:bsz:15-qucosa-178285.

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Background Prostate cancer (PCa) is the most frequently diagnosed malignant disease among adult males in the USA and the second leading cause of cancer deaths in men. Due to the lack of diagnostic tools that are able to differentiate highly malignant and aggressive cases from indolent tumors, overtreatment has become very common in the era of prostate specific antigen (PSA) screening. New diagnostic methods to determine biological status, malignancy, aggressiveness and extent of PCa are urgently needed. 1H High Resolution Magic Angle Spinning Nuclear Magnetic Resonance Spectroscopy (1H HRMAS M

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Moussallieh, François-Marie. "La métabolomique par spectroscopie RMN HRMAS appliquée en cancerologie." Thesis, Strasbourg, 2012. http://www.theses.fr/2012STRAF058.

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Le Cancer, l’une des pathologies les plus fréquentes au sein de la population, possède encore actuellement un taux de morbi-mortalité important tous sexes confondus, et ce malgré les importants progrès diagnostiques et thérapeutiques réalisés. D’un point de vue diagnostique, dans une approche dite de « Biologie de systèmes », en complément de l’étude anatomo- pathologique qui reste la référence, de nouvelles techniques ont été développées pour la caractérisation de profils métaboliques (Métabolomique) d’échantillons tissulaires pathologiques ou non, parmi lesquelles la Spectroscopie RMN HRMAS.

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Lazariev, Andrii. "A quantum mechanics-based approach for optimization of metabolite basis-sets : application to quantitation of HRMAS-NMR signals." Phd thesis, Université Claude Bernard - Lyon I, 2011. http://tel.archives-ouvertes.fr/tel-00843311.

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From day to day, the role of HRMAS (High-Resolution Magic Angle Sinning) Nuclear Magnetic Resonance Spectroscopy (NMRS) in medical diagnosis is increasing. This technique enables setting up metabolite profiles of ex vivo pathological and healthy tissue. Automatic spectrum quantitation enables monitoring of diseases. However for several metabolites, the values of chemical shifts of proton groups may slightly differ according to the micro-environment in the tissue or cells, in particular to its pH. This hampers accurate estimation of the metabolite concentrations mainly when using quantitation a

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Battini, Stéphanie. "Métabolomique par spectroscopie RMN HRMAS appliquée à l’hyperparathyroïdie et aux tumeurs pancréatiques." Thesis, Strasbourg, 2017. http://www.theses.fr/2017STRAJ005/document.

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La spectroscopie RMN Haute Résolution en Rotation à l’Angle Magique (HRMAS) permet la caractérisation métabolomique tissulaire. Nous avons caractérisé par RMN HRMAS le profil métabolomique des glandes parathyroïdiennes hypersécrétantes. Celui de l’hyperparathyroïdie primaire (HPT1) a été comparé à celui des HPT rénales. Au sein des HPT1, la distinction a pu être faite entre pathologie uni- et multi-glandulaire. Le profil métabolomique du tissu pancréatique sain a été comparé à celui du tissu tumoral. Aussi, les patients longs/courts-survivants ont pu être distingués. La relation entre le phéno

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Benahmed, Malika Amel. "La métabolomique par la spectroscopie RMN HRMAS dans le cadre de l'évaluation de la qualité du greffon pour la transplantation pulmonaire." Thesis, Strasbourg, 2012. http://www.theses.fr/2012STRAF033.

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La transplantation pulmonaire est une alternative thérapeutique ultime dans de nombreuses maladies pulmonaires sévères, en particulier chez des patients atteints de mucoviscidose (Cystic Fibrosis) , de fibrose pulmonaire idiopathique (IPF idiopathie pulmonary fibrosis), delymphangioléiomyomatose (LAM) ou d'hypertension pulmonaire. Cependant, les besoins en greffe dépassent largement le nombre de transplantations pratiquées en France. Les causes de ce déséquilibre incluent un trop faible nombre de donneurs potentiels en raison de critères actuels pour l'acceptation du greffon qui sont restreint

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Nambiath, chandran Jima. "Development of NMR methodology for the analysis and simplification of complex mixtures." Thesis, Aix-Marseille, 2013. http://www.theses.fr/2013AIXM4306.

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Ces travaux de thèse portent sur l'analyse des mélanges réels et synthétiques complexes composés de petites molécules à l'aide de la RMN HRMAS. Dans une première partie, une approche RMN HRMAS basée sur l'analyse métabolomique en combinaison avec des techniques de reconnaissance des formes (PCA et O-PLS-DA) a été appliquée pour le diagnostic des lésions thyroïdiennes indéterminées et étudier également les effets biologiques négatifs des nanoparticules d'aluminium sur pseudomonas brassicacearum. Dans une seconde partie, nous avons étudié la RMN chromatographique en utilisant la silice comme mat

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Nambiath, chandran Jima. "Development of NMR methodology for the analysis and simplification of complex mixtures." Electronic Thesis or Diss., Aix-Marseille, 2013. http://www.theses.fr/2013AIXM4306.

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Ruhl, Isaiah Daniel. "High Resolution Magic Angle Spinning NMR Studies of Botryococcus Braunii." Columbus, Ohio : Ohio State University, 2009. http://rave.ohiolink.edu/etdc/view?acc%5Fnum=osu1244008200.

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Частини книг з теми "Nmr hrmas"

Tilgner, Marlon, Tim S. Vater, Piet Habbel, and Leo L. Cheng. "High-Resolution Magic Angle Spinning (HRMAS) NMR Methods in Metabolomics." In NMR-Based Metabolomics. Springer New York, 2019. http://dx.doi.org/10.1007/978-1-4939-9690-2_4.

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Mazzei, P., A. Piccolo, and M. Valentini. "Intact Food Analysis by Means of HRMAS-NMR Spectroscopy." In Modern Magnetic Resonance. Springer International Publishing, 2017. http://dx.doi.org/10.1007/978-3-319-28275-6_16-1.

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Mazzei, P., A. Piccolo, and M. Valentini. "Intact Food Analysis by Means of HRMAS-NMR Spectroscopy." In Modern Magnetic Resonance. Springer International Publishing, 2018. http://dx.doi.org/10.1007/978-3-319-28388-3_16.

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Alam, Todd M. "Chapter 4. High Resolution Magic Angle Spinning (HRMAS) Pulse Field Gradient (PFG) NMR Diffusometry Studies of Swollen Polymers." In NMR Methods for Characterization of Synthetic and Natural Polymers. Royal Society of Chemistry, 2019. http://dx.doi.org/10.1039/9781788016483-00063.

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Simon, Gaëlle, Nelly Kervarec, and Stéphane Cérantola. "HRMAS NMR Analysis of Algae and Identification of Molecules of Interest via Conventional 1D and 2D NMR: Sample Preparation and Optimization of Experimental Conditions." In Methods in Molecular Biology. Springer New York, 2015. http://dx.doi.org/10.1007/978-1-4939-2684-8_12.

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SRIVASTAVA, Dr SHATAKSHI. "ACQUISITION PARAMETERS FOR HRMAS NMR OF DISEASED AND NORMAL TISSUES." In INTERDISCIPLINARY APPROACH OF SCIENCES IN NANOTECHNOLOGY AND METABOLOMICS. GRF BOOKS, 2022. http://dx.doi.org/10.52458/9789391842741.2022.eb.grf.asu.ch-07.

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SRIVASTAVA, Dr SHATAKSHI. "HRMAS (HIGH RESOLUTION MAGIC ANGLE SPINNING) NMR (NUCLEAR MAGNETIC RESONANCE) SPECTROSCOPY AND EFFECT OF PHYSICAL VARIABLES." In INTERDISCIPLINARY APPROACH OF SCIENCES IN NANOTECHNOLOGY AND METABOLOMICS. GRF BOOKS, 2022. http://dx.doi.org/10.52458/9789391842741.2022.eb.grf.asu.ch-06.

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Тези доповідей конференцій з теми "Nmr hrmas"

Yang, Zhen, Yefei Wang, Fengtao Zhan, et al. "Investigation of High-efficient Acidizing Inhibitors: Structure and Anti-corrosion Performance of Novel Indolizine Derivatives." In CORROSION 2019. NACE International, 2019. https://doi.org/10.5006/c2019-12744.

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Abstract The novel indolizine derivative inhibitor for acidizing shows an effective corrosion inhibition without the synergism of propargyl alcohol. The inhibitive indolizine derivatives were generated from BQC (Benzyl Quinolinium Chloride, a commonly used key compound in acidizing inhibitor) via a moderate 1,3-dipolar cycloaddition mechanism. High Resolution Mass Spectrometry (HRMS) and NMR were used to confirm the detailed chemical structure. The inhibition of two indolizine derivatives in 15 wt.% HCl for N80 steel were studied by weight loss measurement and electrochemical analysis. Without

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Ekici, Selin, Ren Geryak, Stewart G. Neill, Hui-Kuo Shu, and Candace C. Fleischer. "Abstract 3721: Improved fitting of HRMAS NMR spectra forex vivometabolomic analysis of glioma tissue." In Proceedings: AACR Annual Meeting 2019; March 29-April 3, 2019; Atlanta, GA. American Association for Cancer Research, 2019. http://dx.doi.org/10.1158/1538-7445.am2019-3721.

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Steiner, A., S. Schmidt, C. Fellmann, M. Beer, and L. Cheng. "Kann die ex vivo 1H High Resolution Magic Angle Spinning (HRMAS) NMR Spektroskopie die spätere Entstehung eines Prostatakarzinoms vorhersagen?" In 102. Deutscher Röntgenkongress der Deutschen Röntgengesellschaft e. V. Georg Thieme Verlag KG, 2021. http://dx.doi.org/10.1055/s-0041-1723238.

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Vinci, Giovanni, Pierluigi Mazzei, Alessandro Piccolo, and Maxime Bridoux. "Molecular Insights into the Humeome of Two Contrasting Soils Using HRMS, NMR and GC/TOF MS." In Goldschmidt2020. Geochemical Society, 2020. http://dx.doi.org/10.46427/gold2020.2686.

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Peiwu, L., K. Al-Mefleh, K. van Dijk, et al. "A Novel Hybrid Acid Stimulation/Fracturing Technique Developed for North Kuwait Jurassic Gas, Utilizing Particulate Diverters for Wellbore Diversion." In SPE International Hydraulic Fracturing Technology Conference and Exhibition. SPE, 2023. http://dx.doi.org/10.2118/215664-ms.

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Abstract The North Kuwait Jurassic Gas (NKJG) asset is highly complex. The main target zone is the dolomitic Marrat reservoirs that have been under differential depletion and production for several years. The Marrat are deep carbonates, naturally fractured with low matrix permeability and high conductivity contrasts. Reservoir fluid composition is sour gas condensate and volatile oil mix supported by a weak water primary drive mechanism. The Marrat reservoir is divided into flow units/flow zones with variations in reservoir properties. The variations in properties, conductivity contrasts, and

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Lemus Ringele, GB, E. Axiotis, S. Katsikis, A. Argyropoulou, LA Skaltsounis, and M. Halabalaki. "Investigation of Greek honeys using HR-NMR and LC-HRMS metabolomics, for determination of their geographical, botanical origin and authenticity." In 67th International Congress and Annual Meeting of the Society for Medicinal Plant and Natural Product Research (GA) in cooperation with the French Society of Pharmacognosy AFERP. © Georg Thieme Verlag KG, 2019. http://dx.doi.org/10.1055/s-0039-3399834.

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Diaconu, Dumitrela, Violeta Mangalagiu, Dorina Amariucai-Mantu, Vasilichia Antoci, and Ionel Mangalagiu. "SIX-MEMBERED HETEROCYCLIC SULFONAMIDES: SYNTHESIS, CHARACTERISATION AND ANTIMICROBIAL PROPERTIES." In 23rd SGEM International Multidisciplinary Scientific GeoConference 2023. STEF92 Technology, 2023. http://dx.doi.org/10.5593/sgem2023v/6.2/s25.45.

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Sulfonamides are appropriate ligands for the preparation of coordination compounds with biological activity, as they possess bactericidal, antiviral, antidiabetic, and diuretic properties and some sulfonamide compounds are under clinical evaluation for cancer treatment. Metal complexes provide highly versatile platforms for drug design. Considering the biological potential of the quinoline nucleus, but also of the sulfonamide scaffold (especially antimicrobial), as well as that of the quinoline- sulfonamide combination we have decided to combine the two pharmacophore fragments. And at last, th

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Beteinakis, S., P. Stathopoulos, D. Michailidis, et al. "Comparative quantitative and qualitative studies of extra virgin olive oil using HPTLC, HPLC-DAD, NMR, LC-HRMS & MS/MS methods." In GA 2017 – Book of Abstracts. Georg Thieme Verlag KG, 2017. http://dx.doi.org/10.1055/s-0037-1608520.

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Derbré, S., M. Meunier, D. Bréard, K. Awang, D. Guilet, and A. Schinkovitz. "Matrix free LDI-HRMS combined with MixONat assisted 13C-NMR dereplication: A chemometric approach to identify bioactive natural products from crude extracts." In GA – 70th Annual Meeting 2022. Georg Thieme Verlag KG, 2022. http://dx.doi.org/10.1055/s-0042-1759172.

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