Дисертації з теми "Surface-Enhanced Spectroscopy"
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Zagdoun, Alexandre. "Dynamic Nuclear Polarisation Surface Enhanced NMR Spectroscopy." Phd thesis, Ecole normale supérieure de lyon - ENS LYON, 2014. http://tel.archives-ouvertes.fr/tel-01065554.
Scherzer, Ryan D. "Degradation Resistant Surface Enhanced Raman Spectroscopy Substrates." UNF Digital Commons, 2017. http://digitalcommons.unf.edu/etd/760.
Xie, Yu-Tao. "Surface-enhanced hyper raman and surface-enhanced raman scattering : novel substrates, surface probing molecules and chemical applications /." View abstract or full-text, 2007. http://library.ust.hk/cgi/db/thesis.pl?CHEM%202007%20XIE.
Gant, Virgil Alexander. "Detection of integrins using surface enhanced raman spectroscopy." Thesis, Texas A&M University, 2003. http://hdl.handle.net/1969.1/2304.
Cunningham, Dale. "Fundamental studies of surface enhanced resonance Raman spectroscopy." Thesis, University of Strathclyde, 2007. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.438120.
Sockalingum, Dhruvananda. "Surface enhanced Raman spectroscopy in the near-infrared." Thesis, University of Southampton, 1992. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.315640.
Sharma, Narayan. "Solution Processable Surface Enhanced Raman Spectroscopy (SERS) Substrate." Bowling Green State University / OhioLINK, 2015. http://rave.ohiolink.edu/etdc/view?acc_num=bgsu1434375587.
Tsoutsi, Dionysia. "Inorganic Ions Sensing by surface-enhanced Raman scattering spectroscopy." Doctoral thesis, Universitat Rovira i Virgili, 2015. http://hdl.handle.net/10803/288213.
En este proyecto de tesis se ha conseguido desarrollar un sistema de detección, identificación y cuantificación independiente de iones inorgánicos. La detección de los iones se basa en su diferente afinidad hacia diferentes ligandos orgánicos a través de la espectroscopia de dispersión Raman aumentada por superficies (surface-enhanced Raman scattering, SERS). En resumen, como sustrato se utilizarán nanopartículas de plata o microesferas nanoestructuradas que se prepararán mediante la adsorción de nanopartículas de oro sobre la superficie de microesferas de sílice mediante el protocolo de capa por capa y su posterior crecimiento epitaxial con plata. Este último paso se realizará mediante protocolos desarrollados en nuestro laboratorio y tiene como objetivo la obtención de superficies plasmónicas discretas altamente eficientes en SERS. Los sustratos se funcionalizarán posteriormente con ligandos orgánicos tiolados con alta afinidad por iones inorgánicos (el fluoróforo orgánico, amino-MQAE y la terpiridina, pztpy-DTC). Como paso siguiente, se realizará la detección y cuantificación simultánea de los iones combinando para su detección espectroscopia SERS. Los cambios espectrales SERS en el modo de vibración de los ligandos orgánicos están correlacionados como función de la concentración de cada ion con límites de detección comparables a los de varios métodos analíticos convencionales.
In this research project we successfully developed a novel sensing system for the identification and quantification of inorganic ions independently by means of surface-enhanced Raman scattering (SERS) spectroscopy. The detection of the ions is based on their different affinity toward various organic ligands. In summary, we use as SERS-active substrates, either silver nanoparticles or composite nanostructured particles prepared by adsorption of gold nanoparticles on the surface of silica microbeads, using layer-by-layer assembly protocol and the subsequent epitaxial overgrowth of silver. This last step is performed using protocols developed in our laboratory and aims to the fabrication of highly plasmonic surfaces for SERS experiments. Next, the substrates are functionalized with thiolated organic ligands with high affinity toward inorganic ions (amino-MQAE, an organic fluorophore, and pztpy-DTC, a terpyridine). As a further step, the simultaneous identification and quantification of the ions, using SERS spectroscopy, is performed. Vibrational changes in the SERS spectra of the organic ligands are correlated as a function of the concentration of each ion with limits of detection comparable to those of several conventional analytical methods.
Yang, Mingwei. "In Situ Arsenic Speciation using Surface-enhanced Raman Spectroscopy." FIU Digital Commons, 2017. http://digitalcommons.fiu.edu/etd/3387.
Grytsyk, Natalia. "Development of the surface-enhanced infrared spectroscopic approach and surface-enhanced Raman spectroscopy coupled with electrochemistry to study reaction mechanism of membrane proteins." Thesis, Strasbourg, 2017. http://www.theses.fr/2017STRAF057/document.
This thesis concerns the development of surface-enhanced infrared and Raman spectroscopic approaches: surface-enhanced infrared absorption spectroscopy (SEIRAS) combined with perfusion cell and surface-enhanced Raman spectroscopy (SERS) combined with electrochemistry. Within the first project different proteins were studied: Lactose Permease (LacY), complex I and IM30.The pKa of Glu325 in LacY WT and in different mutants carrying mutations in the proton translocation active center was determined. WT complex I was oxidized with different oxidizing agents and reduced with NADH. Corresponding redox-induced conformational changes were studied. The evidence was given that Mg2+ ions induce conformational changes in the protein IM30.Within the second project the spectroelectrochemical cell containing gold grid electrode was adopted for the studies of redox active proteins. This gold grid serves both as working electrode and as SERS active substrate. First Cyt c, Hb and Mb were used to validate the setup and then the approach was extended to study a membrane protein
Huang, Qunjian. "Surface-enhanced raman scattering and surface-enhanced hyper raman scattering : a systematic study of various probing molecules on novel substrates /." View Abstract or Full-Text, 2003. http://library.ust.hk/cgi/db/thesis.pl?CHEM%202003%20HUANG.
Kier, Ruth. "Flow systems for use in surface enhanced resonance raman spectroscopy." Thesis, University of Strathclyde, 2002. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.249054.
He, Lili Lin Mengshi. "Application of surface enhanced Raman spectroscopy to food safety issues." Diss., Columbia, Mo. : University of Missouri--Columbia, 2009. http://hdl.handle.net/10355/6859.
Marshall, Addison Robert Lee. "Surface enhanced Raman spectroscopy for single molecule detection and biosensing." Thesis, University of Hull, 2017. http://hydra.hull.ac.uk/resources/hull:16553.
Nicolson, Fay. "Through barrier detection using surface enhanced spatially offset Raman spectroscopy." Thesis, University of Strathclyde, 2018. http://digitool.lib.strath.ac.uk:80/R/?func=dbin-jump-full&object_id=30290.
Panagoulia, Danai. "Surface enhanced Raman spectroscopy of the ionic liquid-metal interface." Thesis, University of Southampton, 2018. https://eprints.soton.ac.uk/422133/.
Hansson, Freja. "Detection of Contaminants in Water Using Surface Enhanced Raman Spectroscopy." Thesis, Luleå tekniska universitet, Institutionen för teknikvetenskap och matematik, 2021. http://urn.kb.se/resolve?urn=urn:nbn:se:ltu:diva-85943.
Wei, Haoran. "Surface-Enhanced Raman Spectroscopy for Environmental Analysis: Optimization and Quantitation." Diss., Virginia Tech, 2018. http://hdl.handle.net/10919/93204.
PHD
Tian, Hong. "Investigation of Thin Molecular Films by Surface Enhanced Vibrational Spectroscopy." The Ohio State University, 2008. http://rave.ohiolink.edu/etdc/view?acc_num=osu1227038646.
Chowdhury, Mustafa Habib. "The use of Surface Enhanced Raman Spectroscopy (SERS) for biomedical applications." Texas A&M University, 2005. http://hdl.handle.net/1969.1/4816.
Syed, Azfar A. "Surface enhanced Raman spectroscopy for ultra-sensitive detection of energetic materials." Thesis, Cranfield University, 2010. http://dspace.lib.cranfield.ac.uk/handle/1826/4644.
Israelsen, Nathan. "Surface-Enhanced Raman Spectroscopy-Based Biomarker Detection for B-Cell Malignancies." DigitalCommons@USU, 2015. https://digitalcommons.usu.edu/etd/4605.
Wigginton, Krista Rule. "Surface Enhanced Raman Spectroscopy as a Tool for Waterborne Pathogen Testing." Diss., Virginia Tech, 2008. http://hdl.handle.net/10919/29330.
Ph. D.
Jain, Ishan. "Paper-Based Sensors for Contaminant Detection Using Surface Enhanced Raman Spectroscopy." Thesis, Virginia Tech, 2015. http://hdl.handle.net/10919/53946.
Master of Science
Shadi, Iqbal Tahear. "Surface enhanced resonance Raman spectroscopy of dyes : semi-quantitative trace analysis." Thesis, University of Greenwich, 2005. http://gala.gre.ac.uk/6296/.
Syed, A. A. "Surface enhanced raman spectroscopy for ultra-sensitive detection of energetic materials." Thesis, Department of Materials and Applied Science, 2010. http://dspace.lib.cranfield.ac.uk/handle/1826/4644.
Berruyer, Pierrick. "Three-Dimensional Structure Determination of Surface Sites with Dynamic Nuclear Polarization Surface Enhanced NMR Spectroscopy." Thesis, Lyon, 2017. http://www.theses.fr/2017LYSEN042/document.
The ability to understand the properties of chemical systems relies on their detailed description at the molecular level. Over the last century, several methods based on X-ray diffraction have allowed a structure-based understanding of many materials. However, several key questions often remain unanswered. In particular when the system under investigation is located on a surface. Although an extensive range of surface-sensitive methods are available for surface science and give valuable information, they only lead to a partial understanding of surfaces at the molecular level. Moreover, these methods are not compatible with all kinds of materials and usually require the use of a model and pristine surface. Solid-State NMR would be a method of choice to characterize surfaces. However, the approach suffers from its intrinsically low sensitivity and this is strongly emphasize in the case of surfaces where the atoms of interest are diluted in the matrix. Dynamic Nuclear Polarization (DNP) applied to surfaces (SENS) recently emerged as a very promising method to characterize surface sites. It offers a dramatic enhancement of NMR sensitivity and DNP applied to materials has led to many examples in the last ten years. In the present thesis, I have shown that DNP SENS, in combination with EXAFS, allowed the detailed 3D structure determination of the silica-supported organometallic complex determined with a precision of 0.7 angstroms. In parallel, some experimental aspect of DNP SENS have been explored. A spin diffusion has been developed to understand diffusion of hyperpolarization in porous media. A new aqueous DNP matrix, coined DNP Jelly, has been developed to characterize nanoparticles and thus expanding experimental range of DNP SENS. Finally, the first experiment of DNP NMR at fast magic angle spinning (up to 40 kHz) and high field are reported
Boddu, Naresh Kumar. "Trace analysis of biological compounds by surface enhanced Raman scattering (SERS) spectroscopy /." Connect to resource online, 2008. http://rave.ohiolink.edu/etdc/view?acc_num=ysu1229542206.
Touzalin, Thomas. "Tip-enhanced Raman spectroscopy on electrochemical systems." Thesis, Sorbonne université, 2018. http://www.theses.fr/2018SORUS364.
The in situ investigation of electrochemical interfaces structures at the nanoscale is a key element in the understanding of charge and electron transfer mechanisms e.g. in the fields of energy storage or electrocatalysis. This thesis introduces the implementation of tip-enhanced Raman spectroscopy (TERS) in liquid and in electrochemical conditions enabling the nanoscale analysis of electrified solid/liquid interfaces through the strong and local electric field enhancement at gold or silver scanning tunneling microscopy (STM) probes. The ability of TERS to image inhomogeneities in the coverage density of a self-assembled monolayer (SAM) through a layer of organic solvent on gold was demonstrated. A TERS-inspired analytical tool was also developed, based on a TERS tip used simultaneously as a single-hot spot surface-enhanced Raman spectroscopy (SERS) platform and as a microelectrode (EC tip SERS). The reduction of an electroactive SAM could then be monitored by electrochemical and in situ SERS measurements. In situ electrochemical STM-TERS was also evidenced through the imaging of local variations of the electric field enhancement on peculiar sites of a gold electrode with a lateral resolution lower than 8 nm. Finally TERS also demonstrated to be efficient in investigating the structure of organic layers grafted either by electrochemical reduction or spontaneously. This work is therefore a major advance for the analysis of functionalized surfaces
Sheremet, E., A. G. Milekhin, R. D. Rodriguez, T. Weiss, M. Nesterov, E. E. Rodyakina, O. D. Gordan, et al. "Surface- and tip-enhanced resonant Raman scattering from CdSe nanocrystals." Universitätsbibliothek Chemnitz, 2015. http://nbn-resolving.de/urn:nbn:de:bsz:ch1-qucosa-161500.
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Willner, Marjorie Rose. "Environmental Analysis at the Nanoscale: From Sensor Development to Full Scale Data Processing." Diss., Virginia Tech, 2018. http://hdl.handle.net/10919/94644.
Ph. D.
Coyle, Candace Mikki. "Surface-enhanced Raman spectroscopic studies of organonitriles on copper colloids." Morgantown, W. Va. : [West Virginia University Libraries], 1999. http://etd.wvu.edu/templates/showETD.cfm?recnum=919.
Title from document title page. Document formatted into pages; contains xvii, 169 p. : ill. Vita. Includes abstract. Includes bibliographical references.
Liu, Jing. "Systematic studies of protein immobilization by surface plasmon field-enhanced fluorescence spectroscopy." [S.l.] : [s.n.], 2005. http://deposit.ddb.de/cgi-bin/dokserv?idn=975928848.
Doherty, Matthew David. "Plasmonic nano-antenna arrays for surface enhanced Raman spectroscopy and other applications." Thesis, Queen's University Belfast, 2013. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.601361.
Sirimuthu, Narayana M. S. "Increasing the range and reproducibility of quantitative surface-enhanced Raman spectroscopy (SERS)." Thesis, Queen's University Belfast, 2006. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.431477.
Mallinder, Benjamin. "Detection of deoxyribonucleic acid by surface enhanced resonance Raman scattering spectroscopy (SERRS)." Thesis, University of Strathclyde, 2002. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.248771.
Frano, Kristen A. "Surface-Enhanced Raman and Single-Molecule Spectroscopy Studies of Fugitive Artists' Pigments." W&M ScholarWorks, 2015. https://scholarworks.wm.edu/etd/1539791830.
Carneiro, Leandro de Bispo. "Detecção do peptídeo p17 (HIV) baseado em SERS (Surface-enhanced Raman Spectroscopy) /." Araraquara, 2015. http://hdl.handle.net/11449/138424.
Banca: Marcelo Nalin
Banca: Antonio Aparecido Pupim Ferreira
Banca: Gustavo Fernandes Souza Andrade
Banca: Airton Abrahan Martin
Resumo: A espectroscopia de Raman intensificada por superfície (SERS, termo em inglês Surfaceenhanced Raman Spectroscopy) é uma técnica promissora que mostra a sensibilidade para a detecção da interação de biomoléculas que são importantes para detecção precoce de doenças. O vírus da imunodeficiência humana (HIV) têm sido um grande problema por várias décadas. Existem vários métodos de deteção baseados na interação específica de anticorpos, tais como, o ELISA e os testes rápidos (TR's). No entanto, novas estratégias têm sido desenvolvidas para rápido diagnóstico do vírus HIV, e uma prova de conceito de detecção do peptídeo p17-1 foi descrito neste trabalho. A proteina matriz p17 é uma essencial proteína no ciclo de replicação do vírus HIV. As fases iniciais da replicação do vírus envolve a pré integração do complexo do DNA no núcleo do p17 desempenhando um papel na ligação de RNA viral e transporte para a membrana. Neste trabalho foram descritos duas plataformas SERS para a detecção do vírus HIV baseado no peptide p17 -1 (sequência LSGGELDRWEKIRLPGG). O anticorpo foi imobilizado em um substrato de ouro usando duas diferentes camadas automontadas (SAM). A primeira SAM, os substratos de ouro foram imersos em uma solução aquosa de 11 mercaptoundecanóico (MUA). Na segunda SAM, os substratos foram imersos em uma mistura aquosa de politietileno glicol (SHPEG- COOH e SH-PEG-CH3). Aqui serão chamados de SAM-MUA e SAM-PEG, respectivamente. Ambas as SAM's foram imersas emu ma solução de anticorpo (anti-p17) e foram descritas como plataforma d captura MUA e PEG. Ambas plataformas foram funcionalizadas com o peptídeo p17-1. Sondas SERS foram preparadas com nanopartículas de ouro e revestidas com uma molécula Raman reporter (azul de Nilo A) e funcionalizadas com um anticorpo anti-p17. Estas estruturas (sonda SERS e plataformas de captura) formam um ensaio sanduíche...
Abstract: Surface-enhanced Raman Scattering (SERS) technique offers great promises for simplified and sensitive detection of biomolecular interactions that are relevant for early disease diagnostics. Human immunodeficiency virus (HIV) has been a problem for decades. There are several methods of diagnostics based on antibodies specific reactions, such as enzyme-linked immunosorbent assays (ELISAs) and rapid test (RT). However, new strategies have been developed for rapid HIV diagnostics and, as a proof-of-concept, peptide p17-1 was considered here. The matrix protein p17 is a structural protein that is essential in the life cycle of the retrovirus The early stages of the virus replication involve the pre integration of the DNA complex into the nucleus P17 plays a role in RNA viral binding and transport to the membrane. Here were describe two new SERS platform for HIV detection based on peptide p17-1 (sequence LSGGELDRWEKIRLPGG). The antibody anti-p17 was immobilized in a planar gold surface using two differents self-assembled (SAM) techniques. First SAM, were obtained by immersion of the surface into ethanolic solution of 11-Mercaptoundecanoic acid (MUA). Second SAM were obtained by immersion in aqueous solution aquous mixtures of (SH-PEG-COOH/SH-PEG-CH3) and polyethylene glycol (PEG,). Here were describe the two platforms as SAM-MUA and SAMPEG, respectively. Both SAM's were immersed in a solution containing the anti-p17. Samples at this step were called capture platform-MUA and capture platform-PEG. Both capture platforms were funcionalizated with the peptide p17-1. SERS probes were prepared with gold nanoparticles coated with a Raman reporter molecule (Nile Blue A) and, functionalized with an anti-p17. These structures (SERS probe and capture platforms) allow for a sandwich assay, a strategy regularly used for high-sensitivity detection. The light blue color in the SERS mapping represents peptide strong...
Doutor
Ohlhaver, Christopher M. "Use of Surface Enhanced Raman Spectroscopy for the Detection of Bioactive Lipids." VCU Scholars Compass, 2018. https://scholarscompass.vcu.edu/etd/5551.
Boddu, Naresh K. "Trace Analysis of Biological Compounds by Surface Enhanced Raman Scattering (SERS) Spectroscopy." Youngstown State University / OhioLINK, 2008. http://rave.ohiolink.edu/etdc/view?acc_num=ysu1229542206.
De, Jesus Jenny Padua. "HEAVY METAL DETECTION IN AQUEOUS ENVIRONMENTS USING SURFACE ENHANCED RAMAN SPECTROSCOPY (SERS)." Miami University / OhioLINK, 2017. http://rave.ohiolink.edu/etdc/view?acc_num=miami1513185193940902.
Papadopoulou, Evanthia. "Detection of DNA components and DNA sequences by surface-enhanced Raman spectroscopy." Thesis, Queen's University Belfast, 2011. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.546409.
White, Daniel Joshua. "Nanostructured optical fibre for use as miniature surface-enhanced raman scattering sensors." Swinburne Research Bank, 2008. http://hdl.handle.net/1959.3/42062.
Thesis submitted in fulfilment for the degree of Doctor of Philosophy, Centre for Atom Optics and Ultrafast Spectroscopy, Faculty of Engineering and Industrial Sciences, Swinburne University of Technology, 2008. Typescript. Bibliography: p. 151-160.
Hu, Yuan [Verfasser]. "Surface-Enhanced Infrared Attenuated Total Reflection Spectroscopy based on Carbon Nanomaterials / Yuan Hu." Ulm : Universität Ulm, 2019. http://d-nb.info/1192373251/34.
Baumann, Axel [Verfasser]. "Studies on membrane protein folding by surface enhanced infrared absorption spectroscopy / Axel Baumann." Berlin : Freie Universität Berlin, 2018. http://d-nb.info/1159900612/34.
Sutton, C. P. "Application of surface enhanced raman spectroscopy to measurements of diffusion through silastic membranes." Thesis, University of Kent, 2000. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.342271.
Lin, Yung-Chun. "Electrochemical surface enhanced Raman spectroscopy of a beacon probe immobilized on Au electrodes." Thesis, University of Southampton, 2018. https://eprints.soton.ac.uk/422134/.
Rodriguez, Raul D., Evgeniya Sheremet, Tanja Deckert-Gaudig, Corinne Chaneac, Michael Hietschold, Volker Deckert, and Dietrich R. T. Zahn. "Surface- and tip-enhanced Raman spectroscopy reveals spin-waves in iron oxide nanoparticles." Universitätsbibliothek Chemnitz, 2015. http://nbn-resolving.de/urn:nbn:de:bsz:ch1-qucosa-168045.
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Gullekson, Corinne. "Surface enhanced Raman spectroscopy of collagen I fibrils." 2011. http://hdl.handle.net/10222/14026.
Liao, Tzu-Yi, and 廖子頤. "Human Blood Diagnostic by Surface Enhanced Raman Spectroscopy." Thesis, 2010. http://ndltd.ncl.edu.tw/handle/73972244522240363517.
國立臺灣海洋大學
光電科學研究所
98
In this thesis, we present the studies of using surface enhanced Raman spectroscopy (SERS) to measure and analyze the glucose concentration in human blood. Our method is based on the following procedures: (1) High-aspect nanochannels of anodic aluminum oxide (AAO) substrates are used to filter blood cells and large biomolecules in whole blood sample. The 200nm-diameter and 200m-long AAO channels can filter the blood and exclude the interference of fluorescence and other complicated Raman signals of large proteins. (2) The filtered blood sample is then covered on the backside of the AAO substrate, which is coated with a nanometer thickness of silver film. The silver coated AAO surface provides metallic nanostructures that can greatly enhance the Raman signals of the filtered blood due to the SERS effect. In this method, only several micro-liters of the blood sample is required. This quantity is suitable for obtaining blood samples from the blood collection needle. With few blood amounts and the AAO-SERS substrate, we got different Raman intensities from different thickness of silver and gold nanostructures by using a 780 nm laser. The optimal condition for SERS on a 200-nm-diameter AAO substrate is silver film with 10 nm thickness. We confirmed that the SERS signals at 1133cm-1 and 494cm-1 can be used to indicate the glucose concentrations. We found positive correlation between the change of SERS signals and the concentration of glucose. The detectable glucose concentration is in the range between 60mg/dl to 360mg/dl, which is suitable for the point-of-care application of the diabetic. From the measurement, we also found that SERS signals were strongly dependent on the preservation of the blood samples. The Raman signal at 725cm-1 which is related to the Adenine was greatly affected by the preservation ways of blood samples. For room-temperature preservation, the 725cm-1 peak significantly increased with time. For 4oC condition, the change of 725cm-1 peak was small. This 725cm-1 SERS peak may be used to indicate the healthy condition of the blood sample.