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Статті в журналах з теми "Synthesis processes"

Автор: Grafiati

Опубліковано: 28 травня 2022

Оновлено: 31 липня 2025

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1

Tarabanko, V. E., M. A. Smirnova та E. G. Zhizhina. "Processes for the synthesis of γ-acetopropyl alcohol". Kataliz v promyshlennosti 22, № 2 (2022): 5–17. http://dx.doi.org/10.18412/1816-0387-2022-2-5-17.

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Анотація:

The literature on the existing processes for the synthesis of γ-acetopropyl alcohol (acetopropanol, 5-hydroxypentan-2-one, APA) is reviewed. This substance is used to produce vitamin B1, antimalarial drugs and polymers. The promising methods for APA production are the hydrogenation-hydration of sylvan (2-methylfuran), hydrogenation of furfural, and syntheses based on allyl acetate, sodium acetoacetic ether, and γ-butyrolactone.

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2

Padwa, A. "Application of cascade processes toward heterocyclic synthesis." Pure and Applied Chemistry 75, no. 1 (2003): 47–62. http://dx.doi.org/10.1351/pac200375010047.

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The reactions of N-acyliminium ions with tethered π-bonds are among the most important methods for preparing complex nitrogen-containing heterocycles. Pummerer-based cyclizations are also finding widespread application in both carbo- and heterocyclic syntheses. As part of a program concerned with new methods for alkaloid synthesis, we became interested in using a linked Pummerer/N-acyliminium ion cyclization sequence since we felt that this combination offers unique opportunities for the assemblage of complex target molecules. A synthetic method that combines transformations of different react

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3

Alomair, Abdulaziz A., Sama M. Al-Jubouri, and Stuart M. Holmes. "A novel approach to fabricate zeolite membranes for pervaporation processes." Journal of Materials Chemistry A 3, no. 18 (2015): 9799–806. http://dx.doi.org/10.1039/c5ta00124b.

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4

Gogin, L. L., E. G. Zhizhina, and Z. P. Pai. "Processes for synthesis of altax." Kataliz v promyshlennosti 19, no. 3 (2019): 170–77. http://dx.doi.org/10.18412/1816-0387-2019-3-170-177.

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Literature analysis was focused on the existing processes for synthesis of altax (2,2’-dibenzothiazolyldisulfide) as an important rubber vulcanization accelerator. Oxidation of mercaptobenzothiazole (captax) with various oxidants such as oxygen in the presence of catalysts, hydrogen peroxide etc., as well as electrochemical oxidation was shown to be the primary way to altax. The data from literature were the basis to develop a low-tonnage technology for synthesis of altax; the technology was developed at the Boreskov Institute of Catalysis and tested using a pilot setup at the Volgograd Depart

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5

Jarkin, Vladimir N., Oleg A. Kisarin, and Tatyana V. Kritskaya. "Methods of trichlorosilane synthesis for polycrystalline silicon production. Part 1: Direct synthesis." Modern Electronic Materials 7, no. (1) (2021): 1–10. https://doi.org/10.3897/j.moem.7.1.64953.

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Анотація:

Novel technical solutions and ideas for increasing the yield of solar and semiconductor grade polycrystalline silicon processes have been analyzed. The predominant polycrystalline silicon technology is currently still the Siemens process including the conversion of technical grade silicon (synthesized by carbon-thermal reduction of quartzites) to trichlorosilane followed by rectification and hydrogen reduction. The cost of product silicon can be cut down by reducing the trichlorosilane synthesis costs through process and equipment improvement. Advantages, drawbacks and production cost reductio

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6

Schmidlin, D. J. "The synthesis of transient processes." IEEE Transactions on Circuits and Systems II: Analog and Digital Signal Processing 42, no. 11 (1995): 729–32. http://dx.doi.org/10.1109/82.475252.

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7

Coffman, Edward G. "Synthesis of local-rule processes." ACM SIGMETRICS Performance Evaluation Review 39, no. 4 (2012): 24. http://dx.doi.org/10.1145/2185395.2185400.

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8

Harjo, Benny, Ka Ming Ng, and Christianto Wibowo. "Synthesis of Supercritical Crystallization Processes." Industrial & Engineering Chemistry Research 44, no. 22 (2005): 8248–59. http://dx.doi.org/10.1021/ie050791j.

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9

Mallick, S. K. "Synthesis of stagewise separation processes." Computers & Chemical Engineering 15, no. 6 (1991): 427–36. http://dx.doi.org/10.1016/0098-1354(91)87020-a.

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10

Berry, David A., and Ka M. Ng. "Synthesis of reactive crystallization processes." AIChE Journal 43, no. 7 (1997): 1737–50. http://dx.doi.org/10.1002/aic.690430711.

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11

Samant, Ketan D., and Ka M. Ng. "Synthesis of extractive reaction processes." AIChE Journal 44, no. 6 (1998): 1363–81. http://dx.doi.org/10.1002/aic.690440615.

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12

Schroer, Joseph W., Christianto Wibowo, and Ka M. Ng. "Synthesis of chiral crystallization processes." AIChE Journal 47, no. 2 (2001): 369–87. http://dx.doi.org/10.1002/aic.690470214.

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13

Groschang, T., M. Warter, R. Düssel, and J. Stichlmair. "Synthesis of Batch Distillation Processes." Chemie Ingenieur Technik 73, no. 6 (2001): 625. http://dx.doi.org/10.1002/1522-2640(200106)73:6<625::aid-cite6252222>3.0.co;2-o.

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14

Schmuck, Anne-Kathrin, Thomas Moor, and Rupak Majumdar. "On the relation between reactive synthesis and supervisory control of non-terminating processes." Discrete Event Dynamic Systems 30, no. 1 (2019): 81–124. http://dx.doi.org/10.1007/s10626-019-00299-5.

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AbstractReactive synthesis and supervisory control theory both provide a design methodology for the automatic and algorithmic design of digital systems from declarative specifications. The reactive synthesis approach originates in computer science, and seeks to synthesise a system that interacts with its environment over time and that, doing so, satisfies a prescribed specification. Here, the distinguishing feature when compared to other synthesis problems in computer science is that the interaction is temporal in that it explicitly refers to a sequence of computation cycles. Supervisory contr

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15

Li, Zi Cheng, Zhi Hong Li, Ai Ju Zhang, and Yu Mei Zhu. "Synthesis Processes of Nano Alumina Abrasive." Key Engineering Materials 368-372 (February 2008): 691–93. http://dx.doi.org/10.4028/www.scientific.net/kem.368-372.691.

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Synthesis processes of nano alumina abrasive precursor using precipitation method and sol-gel method were investigated in this study. Using pressureless sintering, the nano alumina abrasive was prepared. Mechanical properties of the samples were measured by using single particle compressive strength tester. The microstructures of them were examined by using field emission scanning electron microscopy (FESEM). The results indicated that the performance and microstructure of the samples are greatly relative to the synthesis processes. Compared with samples prepared by precipitation method, the s

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16

Frontier, Alison J., Shukree Abdul-Rashed, and Connor Holt. "Alkynyl Prins and Alkynyl Aza-Prins Annulations: Scope and Synthetic Applications." Synthesis 52, no. 14 (2020): 1991–2007. http://dx.doi.org/10.1055/s-0039-1690869.

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Анотація:

This review focuses on alkynyl Prins and alkynyl aza-Prins cyclization processes, which involve intramolecular coupling of an alkyne with either an oxocarbenium or iminium electrophile. The oxocarbenium or iminium species can be generated through condensation- or elimination-type processes, to achieve an overall bimolecular annulation that enables the synthesis of both oxygen- and nitrogen-containing saturated heterocycles with different ring sizes and substitution patterns. Also discussed are cascade processes in which alkynyl Prins heterocyclic adducts react to trigger subsequent pericycli

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17

Kalyakulin, Sergey Yu, Vladimir V. Kuzmin, Eduard V. Mitin, Sergey P. Suldin, and Tatiana B. Tyurbeeva. "Synthesis of the Structure of Technological Processes." Engineering Technologies and Systems 30, no. 2 (2020): 287–99. http://dx.doi.org/10.15507/2658-4123.030.202002.287-299.

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Анотація:

Introduction. The purpose of the study is to increase the level of automation of the technical documentation development through solving a problem of synthesis of the structure of technological processes. Materials and Methods. The authors reviewed the current status of the issue of developing the automated structure for technological processes that have shown the complexity of its formalization because of a considerable quantity of factors which must be considered in developing. The algorithm for solving these tasks based on synthesis of technological processes has been developed. Results. Th

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18

Wolfe, Robert R. "Effects of Amino Acid Intake on Anabolic Processes." Canadian Journal of Applied Physiology 26, S1 (2001): S220—S227. http://dx.doi.org/10.1139/h2001-056.

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In the resting state muscle protein breakdown exceeds the rate of muscle protein synthesis, meaning that the balance between synthesis and breakdown is negative. Resistance exercise improves the net balance by stimulating muscle protein synthesis, but nutrient intake is requiredfor synthesis to exceed breakdown (i.e., an anabolic response). Exercise and exogenous amino acids have an additive effect on muscle protein synthesis. There is a timecourse of the response to a steady-state change in amino acid concentration. The signal for stimulation of muscle protein synthesis appears to be the extr

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19

Michels, J. H., P. K. Varshney, and D. D. Weiner. "Synthesis of correlated multichannel random processes." IEEE Transactions on Signal Processing 42, no. 2 (1994): 367–75. http://dx.doi.org/10.1109/78.275609.

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20

Kotov, V. M. "ON INTERACTION PROCESSES IN SYNTHESIS REACTIONS." NNC RK Bulletin, no. 1 (March 30, 2020): 87–92. http://dx.doi.org/10.52676/1729-7885-2020-1-87-92.

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The paper is devoted to the problems of synthesis reaction physics of light elements. In this area, experimental data and models of nuclei interaction processes created on their basis play an important role. Quite accurate experimental data on the interaction cross sections have been accumulated, approximation formulas have been obtained that describe dependences of the cross sections of a number of reactions on nuclear collision energy. However, creation of models that describe in detail the progress of reactions encounters such difficulties as complexity to describe problems with many variab

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21

Laplaze, D., L. Alvarez, T. Guillard, J. M. Badie, and G. Flamant. "Carbon nanotubes: dynamics of synthesis processes." Carbon 40, no. 10 (2002): 1621–34. http://dx.doi.org/10.1016/s0008-6223(02)00005-2.

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22

Halasz, L., G. Povoden, and M. Narodoslawsky. "Sustainable processes synthesis for renewable resources." Resources, Conservation and Recycling 44, no. 3 (2005): 293–307. http://dx.doi.org/10.1016/j.resconrec.2005.01.009.

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23

Pilishkin, V. N., and A. V. TsaregorodtsevC. "Control synthesis for multistage technological processes." IFAC Proceedings Volumes 33, no. 20 (2000): 239–44. http://dx.doi.org/10.1016/s1474-6670(17)38056-4.

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24

Hao, C. "Synthesis of Well Behaved Synchronized Processes." IFAC Proceedings Volumes 19, no. 6 (1986): 233–37. http://dx.doi.org/10.1016/s1474-6670(17)59753-0.

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25

Vasquez-Alvarez, E., M. E. Lienqueo, and J. M. Pinto. "Optimal Synthesis of Protein Purification Processes." Biotechnology Progress 17, no. 4 (2001): 685–96. http://dx.doi.org/10.1021/bp010031d.

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26

Scott, K. "Membrane reactors for electrochemical synthesis processes." Journal of Membrane Science 90, no. 1-2 (1994): 161–72. http://dx.doi.org/10.1016/0376-7388(94)80043-x.

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27

Molander, G. A., and Konrad Mautner. "Novel processes for stereoselective organic synthesis." Pure and Applied Chemistry 62, no. 4 (1990): 707–12. http://dx.doi.org/10.1351/pac199062040707.

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28

Peppas, N. A. "Materials synthesis based on biological processes." Journal of Controlled Release 20, no. 3 (1992): 261. http://dx.doi.org/10.1016/0168-3659(92)90128-e.

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29

Spieker, A., K. Najim, M. Chtourou, and J. Thibault. "Neural network synthesis for thermal processes." Journal of Process Control 3, no. 4 (1993): 233–39. http://dx.doi.org/10.1016/0959-1524(93)80029-b.

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30

Munir, Z. A. "Reaction synthesis processes: mechanisms and characteristics." Metallurgical Transactions A 23, no. 1 (1992): 7–13. http://dx.doi.org/10.1007/bf02660845.

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31

Orrù, Roberto, Roberta Licheri, Clara Musa, and Giacomo Cao. "Coupling SHS and SPS Processes." Advances in Science and Technology 88 (October 2014): 111–20. http://dx.doi.org/10.4028/www.scientific.net/ast.88.111.

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Анотація:

The consolidation of refractory ceramic powders at relatively milder conditions with respect to conventional methods represents an important target to achieve. Based on results recently reported in the literature, it is possible to state that the combination of the Self-propagating High-temperature Synthesis (SHS) with the Spark Plasma Sintering (SPS) technologies provides a useful contribution in this direction. Specifically, the two-steps processing route consisting in the synthesis of the ceramic powders by SHS and their subsequent densification by SPS is successfully utilized to obtain var

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32

Subbotin, S. A., H. V. Pukhalska, S. D. Leoshchenko, A. O. Oliinyk, and Ye O. Gofman. "NEUROMODELING OF OPERATIONAL PROCESSES." Radio Electronics, Computer Science, Control, no. 1 (April 11, 2022): 120. http://dx.doi.org/10.15588/1607-3274-2022-1-13.

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Context. The problem of synthesis a neural network model of operational processes with the determination of the optimal topology, which is characterized by a high level of logical transparency and acceptable accuracy, is considered. The object of the study is the process of neural network modeling of operational processes using an indicator system to simplify the selection of the topology of neuromodels.  Objective of the work is to synthesis a neural network model of operational processes with a high level of logical transparency and acceptable accuracy based on the use of an indicator

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33

DaBell, Peter, and Stephen P. Thomas. "Iron Catalysis in Target Synthesis." Synthesis 52, no. 07 (2020): 949–63. http://dx.doi.org/10.1055/s-0039-1690813.

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The use of iron-catalysed organic transformations in the total syntheses of natural products has increased significantly. Iron-catalysed cross-coupling reactions are now widely applied in total syntheses and many other transformations, such as alkene functionalisation, oxidation, and cyclisation. The development of these processes, as well as many examples of their use in target synthesis, is presented here.1 Introduction2 Cross-Coupling Reactions3 Functionalisation of Unactivated Alkenes4 Carbocyclisation Reactions5 Oxidations6 Further Examples7 Conclusions

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34

Comito, Marziale, Riccardo Monguzzi, Silvia Tagliapietra, Giovanni Palmisano, and Giancarlo Cravotto. "Towards Antibiotic Synthesis in Continuous-Flow Processes." Molecules 28, no. 3 (2023): 1421. http://dx.doi.org/10.3390/molecules28031421.

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Continuous-flow chemistry has become a mainstream process and a notable trend among emerging technologies for drug synthesis. It is routinely used in academic and industrial laboratories to generate a wide variety of molecules and building blocks. The advantages it provides, in terms of safety, speed, cost efficiency and small-equipment footprint compared to analog batch processes, have been known for some time. What has become even more important in recent years is its compliance with the quality objectives that are required by drug-development protocols that integrate inline analysis and pur

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35

Pinaeva, L. G., and A. S. Noskov. "Chemical Recovery Processes of CO2." Ecology and Industry of Russia 25, no. 12 (2021): 30–37. http://dx.doi.org/10.18412/1816-0395-2021-12-30-37.

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Анотація:

Existing (production of urea, dimethyl carbonate, polypropylene carbonate) and promising (production of methanol, synthesis gas, monomers dedicated to synthesis of polyurethanes and polycarbonate) chemical technologies which any, time soon, may become CO2 based economy for producing motor fuels and basic chemicals have been overviewed. Based on estimates of CO2 removals in these processes, it has been concluded that there is a potential for developing technologies to produce methanol from CO2 to a competitive cost of the target product. It is expected that interest in this process will decreas

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36

Najimova, Nursuliw Bazarbaevna. "GENERAL INFORMATION ABOUT CHEMICAL PROCESSES AND REACTORS." EURASIAN JOURNAL OF ACADEMIC RESEARCH 3, no. 3 (2023): 28–37. https://doi.org/10.5281/zenodo.7773462.

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Анотація:

The synthesis of chemicals has a significant positive impact on the environment. Because of the effect on pollution, energy consumption, air quality and global warming, the scientific community and the chemical industry is increasingly interested in concepts such as the atomic economy, renewable energy feed stocks and stable solvents as an integral part of green synthesis. For example, the solver losses are the main source of organic pollution, and solvent cleaning consumes a lot of energy and energy more environmentally friendly or sustainable solvents have been proposed and developed the las

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37

Mansurov, Zulkhair A. "Obtaining of Nanomaterials in Combustion Processes." Advanced Materials Research 486 (March 2012): 134–39. http://dx.doi.org/10.4028/www.scientific.net/amr.486.134.

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An experimental study has been conducted in premixed and counterflow diffusion flames in order to obtain the nanocarbon materials. In this paper the synthesis of fullerenes, carbon nanotubes and superhydrophobic soot surface in the regime of hydrocarbon flames were studied. The original results in the field of synthesis of fullerenes, carbon nanotubes and syperhydrophobic soot in hydrocarbon flames were carried out for the last years at the Institute of Combustion Problems.

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38

Jarkin, Vladimir N., Oleg A. Kisarin, and Tatyana V. Kritskaya. "Methods of trichlorosilane synthesis for polycrystalline silicon production. Part 2: Hydrochlorination and redistribution." Modern Electronic Materials 7, no. (2) (2021): 33–43. https://doi.org/10.3897/j.moem.7.2.65572.

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Анотація:

Novel technical solutions and ideas for increasing the yield of solar and semiconductor grade polycrystalline silicon processes have been analyzed. The predominant polycrystalline silicon technology is currently still the Siemens process including the conversion of technical grade silicon (synthesized by carbon-thermal reduction of quartzites) to trichlorosilane followed by rectification and hydrogen reduction. The cost of product silicon can be cut down by reducing the trichlorosilane synthesis costs through process and equipment improvement. Advantages, drawbacks and production cost reductio

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39

Kolmogorov, Aleksey, and Anastasia Zudilkina. "SYNTHESIS OF SIMULATOR MODELS OF TECHNOLOGICAL PROCESSES." Bulletin of the Angarsk State Technical University 1, no. 17 (2023): 183–87. http://dx.doi.org/10.36629/2686-777x-2023-1-17-183-187.

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Анотація:

The algorithm of synthesis of mathematical models for computer simulators intended for train-ing of operational personnel of technological installations is proposed. The algorithm is built taking into account the specifics of real production facilities and covers the entire technologi-cal cycle of simulator development

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40

Cravotto, Giancarlo, Marina Caporaso, Laszlo Jicsinszky, and Katia Martina. "Enabling technologies and green processes in cyclodextrin chemistry." Beilstein Journal of Organic Chemistry 12 (February 15, 2016): 278–94. http://dx.doi.org/10.3762/bjoc.12.30.

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Анотація:

The design of efficient synthetic green strategies for the selective modification of cyclodextrins (CDs) is still a challenging task. Outstanding results have been achieved in recent years by means of so-called enabling technologies, such as microwaves, ultrasound and ball mills, that have become irreplaceable tools in the synthesis of CD derivatives. Several examples of sonochemical selective modification of native α-, β- and γ-CDs have been reported including heterogeneous phase Pd- and Cu-catalysed hydrogenations and couplings. Microwave irradiation has emerged as the technique of choice fo

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41

Dohe, Janis, and Thomas J. J. Müller. "Consecutive three- and four-component coupling-Bagley-Bohlmann-Rahtz syntheses of tri- and tetrasubstituted pyridines." Zeitschrift für Naturforschung B 71, no. 6 (2016): 705–18. http://dx.doi.org/10.1515/znb-2016-0046.

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Анотація:

AbstractThe concatenation of the modified Sonogashira alkynone synthesis and the Bagley-Bohlmann-Rahtz pyridine synthesis gives novel consecutive three- and four-component coupling-Bagley-Bohlmann-Rahtz (cBBR) syntheses of tri- and tetrasubstituted pyridines in a one-pot fashion. With these processes 15 differently substituted 3-ethoxycarbonyl 2-methylpyridines can be readily obtained in modest to moderate yields.

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42

Schwarz, Oliver. "Transfer of synthesis, logistic and recycling processes in nature to industrial processes." Procedia CIRP 126 (2024): 887–92. http://dx.doi.org/10.1016/j.procir.2024.08.279.

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43

Yuan, Zhihong, Bingzhen Chen, and Rafiqul Gani. "Applications of process synthesis: Moving from conventional chemical processes towards biorefinery processes." Computers & Chemical Engineering 49 (February 2013): 217–29. http://dx.doi.org/10.1016/j.compchemeng.2012.09.020.

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44

Bozga, Grigore, Ioan T. Apan, and Raluca E. Bozga. "Dimethyl Ether Synthesis Catalysts, Processes and Reactors." Recent Patents on Catalysis 2, no. 1 (2013): 68–81. http://dx.doi.org/10.2174/2211548x11302010004.

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45

Li, Karen J., and Clay S. Bennett. "New chemical processes to streamline carbohydrate synthesis." Current Opinion in Chemical Biology 70 (October 2022): 102184. http://dx.doi.org/10.1016/j.cbpa.2022.102184.

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46

Godineau, Edouard, and Yannick Landais. "Multicomponent Radical Processes: Synthesis of Substituted Piperidinones." Journal of the American Chemical Society 129, no. 42 (2007): 12662–63. http://dx.doi.org/10.1021/ja075755l.

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47

Miller, Noam. "Social learning and associative processes: A synthesis." Journal of Experimental Psychology: Animal Learning and Cognition 44, no. 2 (2018): 105–13. http://dx.doi.org/10.1037/xan0000167.

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48

Balarin, Felice, and Roberto Passerone. "Specification, Synthesis, and Simulation of Transactor Processes." IEEE Transactions on Computer-Aided Design of Integrated Circuits and Systems 26, no. 10 (2007): 1749–62. http://dx.doi.org/10.1109/tcad.2007.895792.

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