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Relevant bibliographies by topics / 1-azabicyclo(2.2.1)hept-2-ene

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Journal articles

Academic literature on the topic '1-azabicyclo(2.2.1)hept-2-ene'

Author: Grafiati

Published: 4 June 2021

Last updated: 28 July 2025

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Journal articles on the topic "1-azabicyclo(2.2.1)hept-2-ene"

1

Puerto Galvis, Carlos E., and Vladimir V. Kouznetsov. "An unexpected formation of the novel 7-oxa-2-azabicyclo[2.2.1]hept-5-ene skeleton during the reaction of furfurylamine with maleimides and their bioprospection using a zebrafish embryo model." Org. Biomol. Chem. 11, no. 3 (2013): 407–11. http://dx.doi.org/10.1039/c2ob26699g.

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An unexpected intramolecular cyclization during the reaction of furfurylamine with maleimides is reported as a novel strategy for the efficient green synthesis of the 7-oxa-2-azabicyclo[2.2.1]hept-5-ene skeleton.

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2

Sousa, Carlos A. D., M. Luísa C. Vale, José E. Rodríguez-Borges, and Xerardo García-Mera. "Phosphorylation of 2-azabicyclo[2.2.1]hept-5-ene and 2-hydroxy-2-azabicyclo[2.2.1]hept-5-ene systems: synthesis and mechanistic study." New Journal of Chemistry 34, no. 11 (2010): 2546. http://dx.doi.org/10.1039/c0nj00239a.

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3

Durham, Robin, Jérémie Mandel, Nicolas Blanchard, and William Tam. "Ruthenium-catalyzed [2+2] cycloaddition reactions of a 2-oxa-3-azabicyclo[2.2.1]hept-5-ene with unsymmetrical alkynes." Canadian Journal of Chemistry 89, no. 12 (2011): 1494–505. http://dx.doi.org/10.1139/v11-135.

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Ruthenium-catalyzed [2+2] cycloaddition reactions of a 2-oxa-3-azabicyclo[2.2.1]hept-5-ene with unsymmetrical alkynes were investigated. Yields of up to 90% were obtained though regioselectivity was modest. Select cycloadducts could be separated and used to access a highly functionalized [3.2.0] bicyclic structure through reductive cleavage of the N–O bond. These ring-opened products displayed a chemical exchange phenomenon in 1D carbon NMR and required characterization by 2D NMR techniques.

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4

Brown, RFC, KJ Coulston, FW Eastwood, and MP Hill. "Synthesis of Precursors Suitable for Pyrolytic Fragmentation to Pentatetraenone." Australian Journal of Chemistry 41, no. 2 (1988): 215. http://dx.doi.org/10.1071/ch9880215.

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Reaction of 2-phenylselenopropanoyl chloride with methyl ( triphenylphosphoranylidene ) ethanoate yielded methyl 4- phenylselenopenta-2,3-dienoate (3). Distillation of the ester (3) gave dimethyl (E,E)-3′,4′-dimethylcyclobut-3′-ene-1′,2′- diylidenebisethanoate (5) and oxidation of (3) with potassium peroxymonosulfate yielded methyl 2-oxopent-3-ynoate (8). The ester (3) with cyclopentadiene at 160-180° gave a Diels-Alder adduct methyl 3- (1′-phenylselenoethylidene) bicyclo [2.2.1]hept-5-ene-2-carboxylate (4) as a mixture of four isomers. Treatment of the mixture with lithium diisopropylamide an

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5

Mamaghani, Manouchehr, and Alireza Alizadehnia. "Enzyme Catalysed Kinetic Resolution of Racemic Methyl 3-acethylbicyclo [2.2.1] hept-5-ene-2-carboxylate using pig's liver esterase†." Journal of Chemical Research 2002, no. 8 (2002): 386–87. http://dx.doi.org/10.3184/030823402103172400.

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Racemic methyl 3- endo-acetylbicyclo[2.2.1]hept-5-ene-2- exo-carboxylate and methyl 3- exo-acetylbicyclo[2.2.1]hept-5-ene-2- endo-carboxylate were prepared (as a 1:1 mixture in 98% yield) from (E)-methyl 4- oxo-2-pentenoate, using Diels–Alder methodology. The mixture was separated chromatographically and resolved into the enantiomers by pig liver esterase (PLE) with low to high ee's (98%).

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6

Pachuta-Stec, Anna, Urszula Kosikowska, Anna Chodkowska, Monika Pitucha, Anna Malm, and Ewa Jagiełło-Wójtowicz. "Biological Activity of Novel N-Substituted Amides of endo-3- (3-Methylthio-1,2,4-triazol-5-yl)bicyclo[2.2.1]hept-5-ene-2- carboxylic Acid and N-Substituted Amides of 1-(5-Methylthio- 1,2,4-triazol-3-yl)cyclohexane-2-carboxylic Acids." Zeitschrift für Naturforschung C 67, no. 3-4 (2012): 123–28. http://dx.doi.org/10.1515/znc-2012-3-403.

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N-Substituted amides of endo-3-(3-methylthio-1,2,4-triazol-5-yl)bicyclo[2.2.1]hept-5-ene- 2-carboxylic acid and 1-(5-methylthio-1,2,4-triazol-3-yl)cyclohexane-2-carboxylic acid were prepared by the condensation reaction of endo-S-methyl-N1-(bicyclo[2.2.1]hept-5-ene-2,3- dicarbonyl)isothiosemicarbazide and S-methyl-N1-(cyclohexane-2,3-dicarbonyl)isothiosemicarbazide with primary amines. The synthesized compounds were screened for their microbiological and pharmacological activities

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7

Sousa, Carlos A. D., M. Luísa C. Vale, José E. Rodríguez-Borges, and Xerardo Garcia-Mera. "Methyl 2-diphenylphosphoryloxy-2-azabicyclo[2.2.1]hept-5-ene-3-exo-carboxylate." Acta Crystallographica Section E Structure Reports Online 65, no. 1 (2008): o188. http://dx.doi.org/10.1107/s160053680804292x.

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8

Quillian, Brandon, Kennedy Musso, Elizabeth M. Vinson, Joseph G. Bazemore, Allison R. Marks, and Clifford W. Padgett. "Diisoamyl (1R, 4S)-7-oxabicyclo[2.2.1]hept-5-ene-2,3-dicarboxylate." Molbank 2024, no. 3 (2024): M1852. http://dx.doi.org/10.3390/m1852.

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Diisoamyl (1R,4S)-7-oxabicyclo[2.2.1]hept-5-ene-2,3-dicarboxylate (2) was prepared by reacting exo-7-oxabicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic anhydride (1) with isoamyl alcohol in the presence of a sulfuric acid catalyst under sonication conditions. Compound 2 was characterized by 1H, 13C NMR, DEPT-135, infrared, and UV-vis spectroscopy. Gas chromatography–mass spectrometry, elemental analysis, and melting point determination were used to assess purity. The structure of compound 2 was also determined by single-crystal X-ray diffraction. It crystallizes in the monoclinic space group P21/c (

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9

Steinmetz, Mark G., Qing Chen, and Yan Zheng. "The exploratory far-UV photochemistry of 1-methyl-1-silabicyclo[2.2.1]hept-2-ene and 2-trimethylsilylbicyclo[2.2.1]hept-2-ene." Journal of Organometallic Chemistry 516, no. 1-2 (1996): 25–40. http://dx.doi.org/10.1016/0022-328x(95)06087-d.

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10

Bulanov, M. N., S. E. Sosonyuk, and N. V. Zyk. "ChemInform Abstract: Addition of Bromine to 2-Methyl-2-azabicyclo[2.2.1]hept-5-ene." ChemInform 33, no. 1 (2010): no. http://dx.doi.org/10.1002/chin.200201150.

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