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Journal articles on the topic '2-dioxaphospholanes'

Author: Grafiati

Published: 4 June 2021

Last updated: 14 February 2022

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1

Nuretdinova, O. N., and L. B. Troitskaya. "Transformations of 2-(2-thiocyanatoalkoxy)-1,3,2-dioxaphospholanes." Bulletin of the Academy of Sciences of the USSR Division of Chemical Science 40, no. 4 (1991): 845–46. http://dx.doi.org/10.1007/bf00958588.

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2

Heine, Joachim, and Gerd-Volker Röschenthaler. "Trimethylsilylphosphite und Hexafluoraceton: Phosphonate versus Dioxaphospholane — 1:1- und/oder 1:2-Addukte / Trimethylsilylphosphites and Hexafluoroacetone: Phosphonates versus Dioxaphospholanes —1:1 and/or 1:2 Adducts." Zeitschrift für Naturforschung B 43, no. 2 (1988): 196–202. http://dx.doi.org/10.1515/znb-1988-0211.

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The [2,2,2-trifluoro-1-(trifluoromethyl)-1-(trimethylsiloxy)ethyl]phosphonates 2a-g and/or the 4,4,5,5-tetrakis(trifluoromethyl)-1,3,2λ5σ4-dioxaphospholanes 4a-c, e were obtained from the silylphosphites 1a-g and hexafluoroacetone depending on the reaction conditions. Intermediates were the λ5σ5-phosphoranes 3a-e formed by an 1:2 oxidative addition of hexafluoroacetone whereas in the case of the cyclic phosphites 1f and g thermally stable phosphoranes, 3f, 6 and 3g were found to undergo no substituent exchange

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3

NURETDINOVA, O. N., and L. B. TROITSKAYA. "ChemInform Abstract: On the Transformations of 2-(2-Thiocyanatoalkoxy)-1,3,2- dioxaphospholanes." ChemInform 23, no. 44 (2010): no. http://dx.doi.org/10.1002/chin.199244250.

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4

Breuer, E., R. Karaman, D. Gibson, and A. Goldblum. "Structure and Reactivity of 2-Hydroxyiminobenzyl-2-oxo-4,4,5,5-tetramethyl[1,3,2]dioxaphospholanes." Phosphorus, Sulfur, and Silicon and the Related Elements 41, no. 3-4 (1989): 433–37. http://dx.doi.org/10.1080/10426508908039733.

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5

Maffei, Michel, and Gérard Buono. "A two step synthesis of 2-oxo-2-vinyl 1,3,2-dioxaphospholanes and -dioxaphosphorinanes." Tetrahedron 59, no. 44 (2003): 8821–25. http://dx.doi.org/10.1016/j.tet.2003.08.067.

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6

Gusarova, N. K., S. I. Verkhoturova, S. N. Arbuzova, et al. "Synthesis and Isomer Composition of 2-Polyfluoroalkoxy-1,3,2-dioxaphospholanes and -phosphinanes." Russian Journal of General Chemistry 88, no. 4 (2018): 705–12. http://dx.doi.org/10.1134/s107036321804014x.

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7

Christov, Valerij Ch. "Cyclic Phosphonium Salts by Chlorination of Benzo[c]-2-(2-Chloro-1,3-Alkadienyl)-2-Oxo-1,3,2-Dioxaphospholanes." Phosphorus, Sulfur, and Silicon and the Related Elements 134, no. 1 (1998): 373–79. http://dx.doi.org/10.1080/10426509808545477.

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8

Christov, Valerij Ch, and Christo Angelov. "2(2-Chloro-1,3-Alkadiene)-2-Oxo-1,3,2-Dioxaphospholanes and their Heterocyclization in the Reaction with Electrophilic Reagents." Phosphorus, Sulfur, and Silicon and the Related Elements 51, no. 1 (1990): 304. http://dx.doi.org/10.1080/10426509008544356.

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9

CHRISTOV, V. C., and C. M. ANGELOV. "ChemInform Abstract: 2-(2-Chloro-1,3-alkadiene)-2-oxo-1,3,2-dioxaphospholanes and Their Heterocyclization in the Reaction with Electrophilic Reagents." ChemInform 22, no. 1 (2010): no. http://dx.doi.org/10.1002/chin.199101300.

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10

Brunel, Jean-Michel, Olivier Pardigon, Michel Maffei, and Gérard Buono. "The use of (4r,5r)-dicarboalkoxy 2-chloro 1,3,2-dioxaphospholanes as new chiral derivatizing agents for the determination of enantiomeric purity of alcohols by 31P NMR." Tetrahedron: Asymmetry 3, no. 10 (1992): 1243–46. http://dx.doi.org/10.1016/s0957-4166(00)82082-0.

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11

BRUNEL, J. M., O. PARDIGON, M. MAFFEI, and G. BUONO. "ChemInform Abstract: The Use of (4R,5R)-Dicarboalkoxy-2-chloro-1,3,2-dioxaphospholanes as New Chiral Derivatizing Agents for the Determination of Enantiomeric Purity of Alcohols by 31P NMR." ChemInform 24, no. 7 (2010): no. http://dx.doi.org/10.1002/chin.199307094.

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12

Wolf, Thomas, Johannes Naß, and Frederik R. Wurm. "Cyclohexyl-substituted poly(phosphonate)-copolymers with adjustable glass transition temperatures." Polymer Chemistry 7, no. 17 (2016): 2934–37. http://dx.doi.org/10.1039/c6py00358c.

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13

Müller, Laura K., Tobias Steinbach, and Frederik R. Wurm. "Multifunctional poly(phosphoester)s with two orthogonal protective groups." RSC Advances 5, no. 53 (2015): 42881–88. http://dx.doi.org/10.1039/c5ra07167d.

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2-(2-(Benzyloxy)ethoxy)-1,3,2-dioxaphospholane-2-oxide was developed for the ring-opening polymerization to multifunctional poly(phosphoester)s. An acetal-protected comonomer allows selective release of the hydroxyl groups by hydrolysis and hydrogenation.

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14

Nifant'ev, I. E., V. A. Roznyatovskii, Yu A. Ustynyuk, et al. "UNUSUAL BEHAVIOR OF 2-CYCLOPENTADIENYL-1,3-DIOXAPHOSPHOLANE." Phosphorus, Sulfur, and Silicon and the Related Elements 69, no. 3-4 (1992): 283–91. http://dx.doi.org/10.1080/10426509208040648.

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15

Lewis, Andrew L., and Howard C. K. Stokes. "Formation of a Stabilised Phospholane Salt." Journal of Chemical Research 23, no. 10 (1999): 612–13. http://dx.doi.org/10.1177/174751989902301013.

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N,N′-Substituted amines (as illustrated using TMEDA) will react with a short chain 2-alkoxy-2-oxo-1,3,2-dioxaphospholane, to form a stabilised phospholane salt and not the corresponding phosphobetaine as anticipated.

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16

Kibardina, L. K., A. R. Burilov, and M. A. Pudovik. "Reaction of 2-bromo-1,3,2-dioxaphospholane with salicylalethanediamine." Russian Journal of General Chemistry 82, no. 5 (2012): 942–43. http://dx.doi.org/10.1134/s1070363212050246.

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17

Coffer, Philippa K., Keith B. Dillon, Judith A. K. Howard, Michael R. Probert, and Helena J. Shepherd. "Coordination properties of a 2-aryl-1,3,2-dioxaphospholane." Inorganica Chimica Acta 479 (July 2018): 24–29. http://dx.doi.org/10.1016/j.ica.2018.04.030.

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18

NIFANT'EV, I. E., V. A. ROZNYATOVSKII, YU A. USTYNYUK, et al. "ChemInform Abstract: Unusual Behavior of 2-Cyclopentadienyl-1,3-dioxaphospholane." ChemInform 23, no. 51 (1992): no. http://dx.doi.org/10.1002/chin.199251240.

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19

Preut, H., V. D. Ngo, and F. Huber. "Structure of triphenyl(4,4,5,5-tetramethyl-2-thioxo-1,3,2-dioxaphospholane-2-thiolato)tin." Acta Crystallographica Section C Crystal Structure Communications 43, no. 1 (1987): 164–65. http://dx.doi.org/10.1107/s0108270187096616.

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20

Eckert, Christine, Lutz Dahlenburg, and Alexander Wolski. "Oligophosphan-Liganden, XXXIX. (1S,2S)-trans-Cyclopentan-1,2-diyl-bis(phosphan), C5H8(PH2)2, durch Reduktion eines diastereomerenreinen Cyclopentandiyl-bis(dioxaphospholans) / Oligophosphine Ligands, XXXIX. (1 S,2S)-trans-Cyclopentane-1,2-diyl-bis(phosphine), C5H8(PH2)2, by Reduction of a Diastereomerically Pure Cyclopentanediyl-bis(dioxaphospholane)." Zeitschrift für Naturforschung B 50, no. 7 (1995): 1004–8. http://dx.doi.org/10.1515/znb-1995-0703.

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The title compound (S,S)-2, has been obtained by reduction with Li[AlH4] of the cyclopentane- 1,2-diyl-bis(1′,3′,2′-dioxaphospholane) (1S ,2S)-trans-C5H8[P(OCH (CO2Pr-i)- (R) - )2]2, (S,S)-1, which itself was isolated in diastereomerically pure form (X-ray structure analysis) from the reaction between rac, trans-C5H8(PCl2)2 and (2R,3R)-(+)-diisopropyl tartrate. Cleavage of (S,.S)-1 withPCl3 yielded an unseparable mixture of (1S,2S)-trans-C5H8(PCl2)2 and (4R.5R) -ClP [OCH(CO2Pr-i)-]2.

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21

Xu, Guangqiang, Xin-Qi Hao, Qinggang Wang, et al. "Organocatalytic Ring-Opening Polymerization Strategies for Synthesis of Poly(phosphothioesters) with a Pendent Phenyl Group." Synlett 31, no. 12 (2020): 1167–71. http://dx.doi.org/10.1055/s-0040-1707947.

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A novel type of phosphothioester substrate, 2-phenyl-1,3,2-dioxaphospholane 2-sulfide (PTP), has been synthesized and subjected to ring-opening polymerization. DBU/thiourea served as an efficient cooperative organocatalyst for the synthesis of poly(PTP), delivering the polymer with a well-defined structure, a relatively narrow molecular-weight distribution (1.14–1.20), and high molecular weight (up to 45.2 kg/mol). The ring-opening polymerization process showed a controlled/living nature. In addition, diblock copolymers of PTP with rac-lactide with well-defined structures were also synthesized

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22

Pudovik, M. A., L. K. Kibardina, and A. N. Pudovik. "Synthesis and some properties of 2-acetylamido-4,5-benzo-1,3,2-dioxaphospholane." Bulletin of the Russian Academy of Sciences Division of Chemical Science 41, no. 1 (1992): 183–85. http://dx.doi.org/10.1007/bf00863944.

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23

Sinyashina, T. N., V. F. Mironov, E. N. Ofitserov, I. V. Konovalova, and A. N. Pudovik. "Reaction of 2-tert-butoxy-4,5-benzo-1,3,2-dioxaphospholane with tribromoacetaldehyde." Bulletin of the Academy of Sciences of the USSR Division of Chemical Science 38, no. 8 (1989): 1755–57. http://dx.doi.org/10.1007/bf00956969.

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24

Tuzova, L. L., V. Yu Nesterov, V. A. Naumov, and R. I. Tarasova. "Molecular structure of 2-isocyanato-1,3,2-dioxaphospholane by gas electron diffraction." Journal of Structural Chemistry 27, no. 3 (1986): 379–83. http://dx.doi.org/10.1007/bf00751813.

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25

Xiao, Chun-Sheng, Yu-Cai Wang, Jin-Zhi Du, Xue-Si Chen, and Jun Wang. "Kinetics and Mechanism of 2-Ethoxy-2-oxo-1,3,2-dioxaphospholane Polymerization Initiated by Stannous Octoate." Macromolecules 39, no. 20 (2006): 6825–31. http://dx.doi.org/10.1021/ma0615396.

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26

Christov, Valerij Ch, and Christo M. Angelov. "HETEROCYCLIZATION OF 2-(2-CHLORO-1,3-ALKADIENYL)-1,3,2-DIOXAPHOSPHOLANE 2-OXIDES IN THE REACTION WITH SULFENYL CHLORIDES." Phosphorus, Sulfur, and Silicon and the Related Elements 68, no. 1-4 (1992): 223–26. http://dx.doi.org/10.1080/10426509208038388.

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27

Preut, H., V. D. Ngo, and F. Huber. "Dimethylbis(4,4,5,5-tetramethyl-2-thioxo-1,3,2-dioxaphospholane-2-thiolato)tin, (CH3)2Sn[SP(S)O2C2(CH3)4]2." Acta Crystallographica Section C Crystal Structure Communications 42, no. 7 (1986): 809–11. http://dx.doi.org/10.1107/s0108270186094453.

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28

Kobayashi, Shiro, Junichi Kadokawa, Hiroshi Uyama, Shinichiro Shoda, and Stefan Lundmark. "Ring-opening-closing alternating copolymerization of 2-phenyl-1,3,2-dioxaphospholane with muconic acid." Macromolecules 23, no. 14 (1990): 3541–43. http://dx.doi.org/10.1021/ma00216a028.

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29

Meier, T., M. Braun, and W. Frank. "Triphenylethanediol-Derived 2-Chloro-1,3,2- dioxaphospholane: Synthesis, Structure, and Reaction with Chiral Alcohols." Phosphorus, Sulfur, and Silicon and the Related Elements 184, no. 10 (2009): 2536–44. http://dx.doi.org/10.1080/10426500802509624.

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30

PUDOVIK, M. A., L. K. KIBARDINA, and A. N. PUDOVIK. "ChemInform Abstract: Synthesis and Some Properties of 2-Acetylamino-4,5-benzo-1,3,2- dioxaphospholane." ChemInform 25, no. 3 (2010): no. http://dx.doi.org/10.1002/chin.199403196.

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31

Zaripov, N. M., and R. M. Galiakberov. "A repeated electron diffraction study of the structure of 2-chloro-1,3,2-dioxaphospholane." Journal of Structural Chemistry 25, no. 4 (1985): 645–49. http://dx.doi.org/10.1007/bf00747258.

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32

CHRISTOV, V. CH, and C. M. ANGELOV. "ChemInform Abstract: Heterocyclization of 2-(2-Chloro-1,3-alkadienyl)-1,3,2- dioxaphospholane 2-Oxides in the Reaction with Sulfenyl Chlorides." ChemInform 23, no. 37 (2010): no. http://dx.doi.org/10.1002/chin.199237259.

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33

Kibardin, A. M., P. I. Gryaznov, and A. N. Pudovik. "Reaction of 2-N-butyl-N-isobutenylamido-4,5-benzo-1,3,2-dioxaphospholane with benzenesulfonyl chloride." Bulletin of the Academy of Sciences of the USSR Division of Chemical Science 34, no. 11 (1985): 2459. http://dx.doi.org/10.1007/bf00956839.

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34

Mironov, V. F., M. N. Dimukhametov, E. V. Mironova, D. B. Krivolapov, G. A. Ivkova, and L. M. Abdrakhmanova. "Caged phosphorane with P-C bond based on chloral and 4,5-dimethyl-2-(2-oxo-1,2-diphenylethoxy)-1,3,2-dioxaphospholane." Russian Journal of General Chemistry 85, no. 2 (2015): 450–61. http://dx.doi.org/10.1134/s1070363215020164.

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35

Gryaznov, P. I., A. N. Pudovik, and A. M. Kibardin. "Synthesis and reaction of N-butyl-N-isobutenyl-aminotrimethylsilane with 4,5-benzo-2-chloro-1,3,2-dioxaphospholane." Bulletin of the Russian Academy of Sciences Division of Chemical Science 41, no. 8 (1992): 1507–8. http://dx.doi.org/10.1007/bf00864358.

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36

Mironov, V. F., E. N. Ofitserov, I. V. Konovalova, and A. N. Pudovik. "Unstable 2,2-dibromo-2-ethoxy-4,5-benzo-1,3,2-dioxaphospholane in addition reactions to chloral and benzaldehyde." Bulletin of the Academy of Sciences of the USSR Division of Chemical Science 40, no. 7 (1991): 1475–77. http://dx.doi.org/10.1007/bf00961257.

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37

Pudovik, M. A., L. K. Kibardina, and A. N. Pudovik. "Reaction of 2-[N,N-bis(Trimethylsilyl)]amino-4,5-benzo-1,3,2-dioxaphospholane with carboxylic acid halides." Bulletin of the Academy of Sciences of the USSR Division of Chemical Science 36, no. 4 (1987): 866–67. http://dx.doi.org/10.1007/bf00962343.

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38

Korntner, Philipp, Ivan Sumerskii, Markus Bacher, Thomas Rosenau, and Antje Potthast. "Characterization of technical lignins by NMR spectroscopy: optimization of functional group analysis by 31P NMR spectroscopy." Holzforschung 69, no. 6 (2015): 807–14. http://dx.doi.org/10.1515/hf-2014-0281.

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Abstract31P nuclear magnetic resonance (NMR) based on the derivatization reagent 2-chloro-4,4,5,5-tetramethyl-1,3,2-dioxaphospholane is a common approach for the hydroxyl group determination of lignins, but the results are sometimes less reproducible compared to other methods. In the present work, common pitfalls in31P NMR analysis of kraft lignin (KL) and lignosulfonates (LS) are addressed and the results are compared to those obtained by1H NMR spectroscopy. Several experimental parameters are revisited in terms of the reliability of the obtained data, such as the choice of relaxation delay,

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39

Badawi, Hassan M., Wolfgang Förner, and Abdulaziz A. Suwaiyan. "Anomeric effect, ring inversion, structural stability and vibrational assignments of 2-chloro-1,3,2-dioxaphospholane 2-oxide and 2-sulfide, c-C2H4O2PXCl (X is O or S)." Journal of Molecular Structure 917, no. 2-3 (2009): 93–100. http://dx.doi.org/10.1016/j.molstruc.2008.06.030.

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40

Song, Yonghong, Dongdong Li, Yang Lu, et al. "Ferrimagnetic mPEG-b-PHEP copolymer micelles loaded with iron oxide nanocubes and emodin for enhanced magnetic hyperthermia–chemotherapy." National Science Review 7, no. 4 (2020): 723–36. http://dx.doi.org/10.1093/nsr/nwz201.

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Abstract As a non-invasive therapeutic method without penetration-depth limitation, magnetic hyperthermia therapy (MHT) under alternating magnetic field (AMF) is a clinically promising thermal therapy. However, the poor heating conversion efficiency and lack of stimulus–response obstruct the clinical application of magnetofluid-mediated MHT. Here, we develop a ferrimagnetic polyethylene glycol-poly(2-hexoxy-2-oxo-1,3,2-dioxaphospholane) (mPEG-b-PHEP) copolymer micelle loaded with hydrophobic iron oxide nanocubes and emodin (denoted as EMM). Besides an enhanced magnetic resonance (MR) contrast

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41

Becker, Greta, and Frederik R. Wurm. "Breathing air as oxidant: Optimization of 2-chloro-2-oxo-1,3,2-dioxaphospholane synthesis as a precursor for phosphoryl choline derivatives and cyclic phosphate monomers." Tetrahedron 73, no. 25 (2017): 3536–40. http://dx.doi.org/10.1016/j.tet.2017.05.037.

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42

Kelly, Jeffery W., Philip L. Robinson, and Slayton A. Evans. "2,2,2-Triphenyl-4,5-(2',2"-biphenylene)-1,3,2-dioxaphospholane: an effective reagent for converting diols, amino alcohols, and especially mercapto alcohols to the corresponding heterocycles." Journal of Organic Chemistry 51, no. 23 (1986): 4473–75. http://dx.doi.org/10.1021/jo00373a026.

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43

Leroux, Y., D. El Manouni, L. Labaudiniere, et al. "ETUDE STRUCTURALE DU(N,N-DIMETHYLAMINOCARBONYL-l-METHOXYCARBONYL-2-ETHENYL(Z))-2-OXO-2-TETRAMETHYL- 4,4,5,5-DIOXAPHOSPHOLANE-1,3,2. PHENOMENE DE PREFIGURATION A L'ETAT SOLIDE D'UN INTERMEDIAIRE REACTIONNEL PENTACOORDINE." Phosphorus, Sulfur, and Silicon and the Related Elements 47, no. 3-4 (1990): 443–55. http://dx.doi.org/10.1080/10426509008038000.

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44

Pudovik, M. A., L. K. Kibardina, and A. N. Pudovik. "Reactions of 2-[N,N-bis(trimethylsilyl)]amino-4,5-benzo-1,3,2-dioxaphospholane with carboxylic and phosphorous acids and acetic anhydride." Bulletin of the Academy of Sciences of the USSR Division of Chemical Science 40, no. 1 (1991): 214–16. http://dx.doi.org/10.1007/bf00959669.

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45

Mironov, Vladimir F., Mudaris N. Dimukhametov, Sergey V. Efimov, et al. "Stereoselective PCO/POC-Rearrangement of P–C-Cage Phosphorane in the Reaction of 4,5-Dimethyl-2-(2-oxo-1,2-diphenyl)ethoxy-1,3,2-dioxaphospholane with Hexafluoroacetone." Journal of Organic Chemistry 81, no. 14 (2016): 5837–50. http://dx.doi.org/10.1021/acs.joc.6b00356.

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46

Mironov, V. F., M. N. Dimukhametov, S. V. Efimov, F. Kh Karataeva, and V. V. Klochkov. "Reaction of 4,5-dimethyl-2-(2-oxo-1,2-diphenylethoxy)-1,3,2-dioxaphospholane with hexafluoroacetone: formation of isomeric caged phosphoranes with phosphorus–carbon and phosphorus–oxygen bonds." Russian Chemical Bulletin 64, no. 10 (2015): 2517–21. http://dx.doi.org/10.1007/s11172-015-1187-9.

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47

Granata, Alessandro, and Dimitris S. Argyropoulos. "2-Chloro-4,4,5,5-tetramethyl-1,3,2-dioxaphospholane, a Reagent for the Accurate Determination of the Uncondensed and Condensed Phenolic Moieties in Lignins." Journal of Agricultural and Food Chemistry 43, no. 6 (1995): 1538–44. http://dx.doi.org/10.1021/jf00054a023.

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48

Khasiyatullina, N. R., V. F. Mironov, E. V. Mironova, D. B. Krivolapov, and I. A. Litvinov. "Preparation and crystal structure of 1,1-tetramethylethylenedioxy-3,4-diphenyl-6-trichloromethyl-2,5,7,1-trioxaphosphabicyclo[2.2.11,4]heptane and 2-(1-hydroxy-2,2,2-trichloroethoxy)-4,4,5,5-tetramethyl- 2-oxo-1,3,2-dioxaphospholane." Russian Journal of General Chemistry 86, no. 3 (2016): 551–63. http://dx.doi.org/10.1134/s1070363216030105.

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49

Fliss, Outaf, Alia Mejri, Khaled Essalah, Marie-Thérèse Boisdon, and Bahoueddine Tangour. "Étude expérimentale et théorique de la cinétique de l’alcoolyse de la liaison P–N extracyclique du 2-diméthylamino-4,4,5,5-tétraméthyl-1,3-dioxaphospholane monocyclique." Comptes Rendus Chimie 19, no. 5 (2016): 585–93. http://dx.doi.org/10.1016/j.crci.2015.11.007.

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50

Khasiyatullina, Nadezhda R., Vladimir F. Mironov, Dmitry B. Krivolapov, Ekaterina V. Mironova, and Oleg I. Gnezdilov. "Synthesis, crystal structure and hydrolysis of novel isomeric cage (P–C/P–O)-phosphoranes on the basis of 4,4,5,5-tetramethyl-2-(2-oxo-1,2-diphenylethoxy)-1,3,2-dioxaphospholane and hexafluoroacetone." RSC Advances 6, no. 89 (2016): 85745–55. http://dx.doi.org/10.1039/c6ra17983e.

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