Relevant bibliographies by topics / 2-trifluoroethyl

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Academic literature on the topic '2-trifluoroethyl'

Author: Grafiati
Published: 4 June 2021
Last updated: 12 February 2022

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Journal articles on the topic "2-trifluoroethyl"

1

Fu, Xian-Shu, Xiao-Ping Yu, Wei-Min Wang, and Fang Lin. "2-(2,2,2-Trifluoroethyl)isoindoline-1,3-dione." Acta Crystallographica Section E Structure Reports Online 66, no. 7 (2010): o1745. http://dx.doi.org/10.1107/s1600536810020222.

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2

Liška, František, Jiří Fikar, and Petr Kuzmič. "Radical Reduction of C-Cl Bonds in Chlorofluoro Ethers." Collection of Czechoslovak Chemical Communications 58, no. 3 (1993): 565–74. http://dx.doi.org/10.1135/cccc19930565.

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Reduction of C-Cl bonds in 2,2-dichloro-1,1,2-trifluoroethyl trichloromethyl ether (I), 2-chloro-1,1,2-trifluoroethyl trichloromethyl ether (II), and 2,2-dichloro-1,1,2-trifluoroethyl dichloromethyl ether (III) with 2-propanol, 2-butanol, cyclohexanol, tetrahydrofurane, diethyl ether, and 1,3-dioxolane initiated photochemically and by radiation has been investigated. Beside the main reduction products - 2-chloro-1,1,2-difluoroethyl trichloromethyl ether (IV) and 2-chloro-1,1,2-difluoroethyl chloromethyl ether (V) - it was also possible to prove the formation of 1,2-dichloro-1,2-bis(2-chloro-1,
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3

Fu, Weijun, Mei Zhu, Chen Xu, Guanglong Zou, Zhiqiang Wang, and Baoming Ji. "Visible-light-mediated trifluoroethylation of 2-isocyanobiaryl with trifluoroethyl iodide: Synthesis of 6-trifluoroethyl-phenanthridines." Journal of Fluorine Chemistry 168 (December 2014): 50–54. http://dx.doi.org/10.1016/j.jfluchem.2014.08.022.

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4

Li, Man, Fu-Sheng He, Long-Shan Ji, et al. "Synthesis and biological evaluation of fluorinated 3,4-dihydroquinolin-2(1H)-ones and 2-oxindoles for anti-hepatic fibrosis." RSC Advances 11, no. 11 (2021): 5923–27. http://dx.doi.org/10.1039/d0ra09430g.

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5

Langler, Richard Francis, and Nancy Ann Morrison. "Chemoselective reaction of a sulfonate ester with methoxide ions in preference to benzyl mercaptide anions." Canadian Journal of Chemistry 65, no. 10 (1987): 2385–89. http://dx.doi.org/10.1139/v87-398.

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Trifluoroethyl benzyl sulfide was prepared (in 2-propanol) and subsequently chlorinated as a further test of substituent electronegativity based regiochemical predictions. The initial attempt to prepare that sulfide by reaction of 2,2,2-trifluoroethyl methanesulfonate and benzyl mercaptide anions (in methanol) furnished benzyl methyl sulfide. Mechanistic possibilities are discussed in detail and some synthetic consequences of this novel reaction are presented.
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6

Fu, Xian-Shu, Xiao-Ping Yu, Wei-Min Wang, and Fang Lin. "4,5,6,7-Tetrachloro-2-(2,2,2-trifluoroethyl)isoindoline-1,3-dione." Acta Crystallographica Section E Structure Reports Online 66, no. 7 (2010): o1743. http://dx.doi.org/10.1107/s1600536810023019.

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7

Zhu, Wen-Run, Zhen-Wei Zhang, Wei-Hua Huang, et al. "Asymmetric Synthesis of Vicinally Bis(trifluoromethyl)-Substituted 3,3′-Pyrrolidinyl Spirooxindoles via Organocatalytic 1,3-Dipolar Cycloaddition Reactions." Synthesis 51, no. 09 (2019): 1969–79. http://dx.doi.org/10.1055/s-0037-1612089.

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Under bifunctional squaramide and thiourea organocatalysis, a series of vicinally bis(trifluoromethyl)-substituted 3,3′-pyrrolidinyl spirooxindoles were successfully synthesized via 1,3-dipolar cycloaddition reactions of 3-(trifluoroethylidene)oxindoles with diethyl 2-((2,2,2-trifluoroethyl)imino)malonate and N-(2,2,2-trifluoroethyl)isatin ketimines. The highlight of this protocol is the efficient construction of the vicinally bis(trifluoromethyl)-substituted pyrrolidine unit of spirooxindoles, including multiple contiguous stereogenic centres, in excellent yields and stereoselectivities.
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8

Wu, Wei, Beibei Luo, Yi You, and Zhiqiang Weng. "Copper-catalyzed one-pot synthesis of 2-(2,2,2-trifluoroethyl)-substituted benzofused heterocycles." Organic Chemistry Frontiers 8, no. 9 (2021): 1997–2001. http://dx.doi.org/10.1039/d1qo00157d.

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A method for copper-catalyzed synthesis of 2-trifluoroethyl-substituted benzofurans and indoles from the reaction of salicylaldehyde/2-aminobenzaldehyde p-tosylhydrazones with 2-bromo-3,3,3-trifluoropropene has been developed.
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9

Li, Zhengyu, Jingnan Dong, Junwen Wang, Ding-Yah Yang, and Zhiqiang Weng. "Elemental sulfur-promoted one-pot synthesis of 2-(2,2,2-trifluoroethyl)benzoxazoles and their derivatives." Chemical Communications 55, no. 87 (2019): 13132–35. http://dx.doi.org/10.1039/c9cc06822h.

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An elemental sulfur promoted one-pot synthesis of 2-(2,2,2-trifluoroethyl)benzoxazole derivatives from the reaction of o-aminophenols, thiols, and anilines with 2-bromo-3,3,3-trifluoropropene is reported.
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10

Fu, Weijun, Mei Zhu, Chen Xu, Guanglong Zou, Zhiqiang Wang, and Baoming Ji. "ChemInform Abstract: Visible-Light-Mediated Trifluoroethylation of 2-Isocyanobiaryl with Trifluoroethyl Iodide: Synthesis of 6-Trifluoroethyl-phenanthridines." ChemInform 46, no. 17 (2015): no. http://dx.doi.org/10.1002/chin.201517215.

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Book chapters on the topic "2-trifluoroethyl"

1

Wohlfarth, Ch. "Viscosity of the mixture (1) 1,3-dioxolan-2-one; (2) 2,2,2-trifluoroethyl methyl carbonate." In Supplement to IV/18. Springer Berlin Heidelberg, 2008. http://dx.doi.org/10.1007/978-3-540-75486-2_869.

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Wohlfarth, Ch. "Viscosity of the mixture (1) 2,2,2-trifluoroethyl methyl carbonate; (2) propylene carbonate." In Supplement to IV/18. Springer Berlin Heidelberg, 2008. http://dx.doi.org/10.1007/978-3-540-75486-2_1087.

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3

Lash, Lawrence H., Wolfgang Dekant, and M. W. Anders. "Bioactivation Mechanism and Cytotoxicity of S(2-Chloro-1,1,2-Trifluoroethyl)-L-Cysteine." In Nephrotoxicity. Springer US, 1989. http://dx.doi.org/10.1007/978-1-4757-2040-2_91.

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4

Wohlfarth, Ch. "Refractive index of the mixture (1) 1,3-dioxolan-2-one; (2) 2,2,2-trifluoroethyl methyl carbonate." In Refractive Indices of Pure Liquids and Binary Liquid Mixtures (Supplement to III/38). Springer Berlin Heidelberg, 2008. http://dx.doi.org/10.1007/978-3-540-75291-2_702.

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5

Wohlfarth, Ch. "Refractive index of the mixture (1) 2,2,2-trifluoroethyl methyl carbonate; (2) propylene carbonate." In Refractive Indices of Pure Liquids and Binary Liquid Mixtures (Supplement to III/38). Springer Berlin Heidelberg, 2008. http://dx.doi.org/10.1007/978-3-540-75291-2_840.

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6

Wohlfarth, Ch. "Surface tension of the mixture (1) ethylene carbonate; (2) 2,2,2-trifluoroethyl methyl carbonate." In Supplement to IV/16. Springer Berlin Heidelberg, 2008. http://dx.doi.org/10.1007/978-3-540-75508-1_322.

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7

Wohlfarth, Ch. "Surface tension of the mixture (1) 2,2,2-trifluoroethyl methyl carbonate; (2) propylene carbonate." In Supplement to IV/16. Springer Berlin Heidelberg, 2008. http://dx.doi.org/10.1007/978-3-540-75508-1_350.

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8

Wohlfarth, Ch. "Dielectric constant of the mixture (1) ethylene carbonate; (2) 2,2,2-trifluoroethyl methyl carbonate." In Supplement to IV/6. Springer Berlin Heidelberg, 2008. http://dx.doi.org/10.1007/978-3-540-75506-7_594.

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9

Wohlfarth, Ch. "Dielectric constant of the mixture (1) 2,2,2-trifluoroethyl methyl carbonate; (2) propylene carbonate." In Supplement to IV/6. Springer Berlin Heidelberg, 2008. http://dx.doi.org/10.1007/978-3-540-75506-7_714.

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10

Taber, Douglass F. "The Reisman Synthesis of (–)-Maoecrystal Z." In Organic Synthesis. Oxford University Press, 2015. http://dx.doi.org/10.1093/oso/9780190200794.003.0087.

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(–)-Maoecrystal Z 3 was isolated as a minor constituent from the Chinese medicinal herb Isodon eriocalyx. The synthesis of 3 reported (J. Am. Chem. Soc. 2011, 133, 14964) by Sarah E. Reisman of the California Institute of Technology, featuring as a key step the cyclization of 1 to 2, is a tribute to the power of one-electron reduction for carbon–carbon bond construction. The synthesis began with a Myers alkylation to prepare 6. The amide was reduced to the alcohol with the convenient ammonia–borane complex, and the alcohol was carried on to the iodide 7. The first carbocyclic ring of 3 was prepared by classic chemistry, the condensation of dimethyl malonate 9 with mesityl oxide 8, followed by selective removal of one of the ketone carbonyls. A salt-free Wittig reaction followed by hydrolysis, resolution, and reduction then completed the synthesis of 12. Exposure of 12 to peracid led to the epoxide 13 as an inconsequential mixture of diastereomers. The one-electron Nugent/RajanBabu/Gansäuer protocol was low yielding with methyl acrylate, but dramatically improved when the trifluoroethyl acrylate 14 was used as the acceptor. The lactone 15 was formed as a single diastereomer. Alkylation of 15 with 7 followed by oxidation gave 16, which was deprotected and oxidized to give 1. The cascade cyclization of 1 presumably proceeded by initial one-electron reduction of the more accessible aldehyde. The cyclization of the resulting radical onto the alkene may have been assisted by complexation of the lactone carbonyl with the required second equivalent of SmI2. The Sm enolate so prepared was then added to the second aldehyde to give 2. This cyclization sets one quaternary and three ternary stereogenic centers. Attempted monoprotection of 2 was not successful, so the bis acetate was prepared and ozonized, and the aldehyde was condensed with Eschenmoser’s salt to give 17. Careful monohydrolysis then completed the synthesis of (–)-maoecrystal Z 3
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