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Dissertations / Theses on the topic '4-Ethyl-2'

Author: Grafiati

Published: 5 June 2025

Last updated: 1 August 2025

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1

Koulibaly, Issa. "Automatisation et optimisation de la synthèse du ((pyridyl-4)-2 ethyl)-3 indole, précurseur d'un antidépresseur." Paris 6, 1986. http://www.theses.fr/1986PA066413.

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Dans le cadre des recherches concernant l'application des techniques d'automatisation et des méthodes d'optimisation, sur les procédés de fabrications industrielles de produits pharmaceutiques, nous avons choisi l'automatisation et l'optimisation de la synthèse d'un précurseur de l'indalpine, qui est un produit pharmaceutique important par ses propriétés d'antidépresseur. Nous montrons, dans la première partie de ce travail, qu'il est possible d'automatiser, à l'échelle du laboratoire, et pour un cout réduit, une synthèse organique complexe à l'aide d'un automate de bas de gamme et de capteurs

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2

Mikhedkina, E. I., I. I. Melnik, A. V. Tsygankov, D. T. Kozhich, and M. V. Vasyleiko. "Synthesis of ethyl 3,5-dimethyl-4-(aryliminomethyl)-1h-pyrrole-2-carboxylates and their reactions with thioglycolic acid." Thesis, Ekskluziv Publ, 2018. http://repository.kpi.kharkov.ua/handle/KhPI-Press/45015.

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3

Yassin-Hussan, Saad. "Photolyse des ethers aromatiques halogenes : bromo phenetole, paradibromo phenetole, parabromo phenetole, parabromodiphenyl ether." Toulon, 1990. http://www.theses.fr/1990TOUL0004.

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Nous avons etudie la photolyse, par rayonnement ultra-violet, de quatre ethers halogenes aromatiques (bromophenetole, parabromophenetole et parabromobiphenylether) dans l'acenotrile, l'eau et dans les melanges eau-acetonitrile, eau-methanol, en presence ou en absence de peroxyde d'hydrogene, compose jouant le role de photooxydant. L'irradiation ultra-violette de ces composes genere de nombreux photoproduits qui ont ete identifies, apres extraction liquide-liquide, par analyse en chromatographie liquide et gazeuse et c. P. V. Couplee a la spectrometrie de masse. Les cinetiques de photodecomposi

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4

Toth, Christopher A. "Synthesis of Coupling Substrates for Use in a Highly Enantioselective Conjugated Triene Cyclization Enabled by a Chiral N-Heterocyclic Carbene." Digital Archive @ GSU, 2012. http://digitalarchive.gsu.edu/chemistry_theses/48.

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The ability to generate chiral building blocks is of paramount importance to organic chemists. This problem presents itself most notably at the interface of chemistry and biology, where molecules of only a single enantiomer can induce function to many biological systems. In this context, recent developments in the field of organocatalysis, most notably the employment of chiral N-heterocyclic carbenes (NHCs) have shown much promise. Our group has recently shown that one possible chiral NHC catalyzed Stetter cyclization product of a conjugated triene, a highly functionalized cyclopentenone, cont

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5

Patil, N. "Synthetic studies towards quinagolide 3-ethyl-4-methyl-1,5-dihydro-2H-pyrrol-2-one and continuous flow synthesis of miltefosine." Thesis(Ph.D.), CSIR-National Chemical Laboratory, Pune, 2021. http://dspace.ncl.res.in:8080/xmlui/handle/20.500.12252/6009.

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6

Marshall, Christopher Scott. "The Use of Plant Growth Regulators to Improve the Traffic Tolerance and Repair of Overseeded Bermudagrass." Thesis, Virginia Tech, 2007. http://hdl.handle.net/10919/34282.

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An active football season during the fall acclimation period tests the traffic tolerance of bermudagrass. Exogenous applications of synthetic cytokinins or cytokinin-enhancing plant growth regulators (PGRs), such as trinexapac-ethyl, may improve the traffic tolerance of "Patriot" and "Tifsport" hybrid berudagrasses (Cynodon dactylon var. dactylon x Cynodon transvaalensis). This study was designed to mimic the agronomic practices and traffic stresses experienced at Virginia Tech's Worsham Field. Starting in September 2005, treatments were applied with a differential-slip traffic simulator. Foll

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7

Gansser, Simon. "Läsion noradrenerger Afferenzen zum Hippocampus der Ratte durch N-2-Chlorethyl-N-Ethyl-2-Bromobenzylamin (DSP-4) Beeinflussung der hippocampalen Freisetzung von Noradrenalin, Serotonin und Acetylcholin /." [S.l. : s.n.], 2007. http://nbn-resolving.de/urn:nbn:de:bsz:25-opus-60274.

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Freiburg i. Br., Univ., Diss., 2007.<br>Aus: Naunyn-Schmiedeberg's Archives of Pharmacology, Vol. 377, 217, Supplement 1, March 2008, Experimental Neurology 2008, Oct; 213(2): 345-53. Epub 2008 Jun 28.

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8

Zalavadia, Ankit. "QUANTITATIVE ANALYSIS OF 5-CHLORO-2-METHOXY-N-[2-(4-SULFAMOYLPHENYL)ETHYL]BENZAMIDE (GLYBURIDE ANALOGUE, GA) IN MOUSE PLASMA AND WHOLE BLOOD USING A MICRO-EXTRACTION AND LIQUID CHROMATOGRAPHY-TANDEM MASS SPECTROMETRY." VCU Scholars Compass, 2016. http://scholarscompass.vcu.edu/etd/4279.

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Pharmacokinetic evaluation of 5-chloro-2-methoxy-N-[2-(4- sulfamoylphenyl)ethyl]benzamide in mouse plasma demanded for a suitable bioanalytical method. No reported bioanalytical method exists to-date that can quantify concentration of this compound in any biological matrix. The purpose of this study was 1) to develop and validate a new bioanalytical method using a micro-extraction and LC-MS/MS to quantify the target analyte in mouse plasma and 2) to partially validate the method in whole blood. A bioanalytical method was developed and validated in both matrices for a linear concentration range

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9

Swigelaar, Wendell Peter. "The synthesis of 3-allyl-4-ethyl-2- (1'-hydroxyethyl)-1-methoxynaphthalene and its behaviour towards base- and palladium-promoted cyclisation under aerobic and anaerobic conditions." Thesis, University of the Western Cape, 2005. http://etd.uwc.ac.za/index.php?module=etd&amp.

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Over the years, Giles and co-workers have established that, upon treatment with potassium tert-butoxide, tetra-substituted naphthalenes undergo cyclisations to afford naphthopyrans. It was suggested that these base-induced cyclisations was as a result of the reacting centers being forced into close proximity as a consequence of steric crowding.<br /> <br /> This thesis describes the synthesis of 3-allyl-4-ethyl-2-(1&prime<br>-hydroxyethyl)-1-methoxy-naphthalene 177 and its behaviour towards Pd(0) and potassium tert-butoxide under aerobic and anaerobic conditions, to verify whether the base-pro

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10

Lampinen, Salomonsson Matilda. "Chemical Derivatization in Combination with Liquid Chromatography Tandem Mass Spectrometry for Detection and Structural Investigation of Glucuronides." Doctoral thesis, Uppsala University, Analytical Pharmaceutical Chemistry, 2008. http://urn.kb.se/resolve?urn=urn:nbn:se:uu:diva-8670.

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<p>This thesis presents novel approaches for structural investigation of glucuronides using chemical derivatization in combination with liquid chromatography-electrospray ionization-tandem mass spectrometry (LC-ESI-MS<sup>n</sup>).</p><p>Today, LC-ESI-MS<sup>n</sup> is the dominant technique for quantitative as well as qualitative analyses of metabolites, due to its high sensitivity and selectivity. However, for compounds without an easily ionizable group, e.g., steroids, the sensitivity is limited. In the work presented in this thesis, a derivatization procedure forming a basic oxime signific

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11

Kitagawa, Kristen. "Studies in the asymmetric reduction of (3s)-3-amino-1-chloro-4-phenyl-2-butanone derivatives." Diss., Georgia Institute of Technology, 2010. http://hdl.handle.net/1853/39464.

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This thesis focuses on the asymmetric reduction of N-protected derivatives of (3S)-3-amino-1-chloro-4-phenyl-2-butanone to their corresponding diastereomeric alcohol products, which are key intermediates in the synthesis of HIV protease inhibitors. Although the stereoselective synthesis of the (S,S) alcohol product is easily achieved, preparing the (R,S) diastereomer is much more challenging. I investigated three diastereoselective reduction processes: 1) Meerwein-Ponndorf-Verley (MPV) reduction, 2) asymmetric transfer hydrogenation, and 3) boron reducing agents. The diastereoselectivity of

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12

Renaud, Jean-Paul. "Oxydations d'alcanes et d'alcènes par des systèmes métalloporphyriniques modelés du cytochrome P-450." Paris 6, 1986. http://www.theses.fr/1986PA066139.

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La synthèse d'une pophyrine de fer à "anses de panier" chirale comportant des aminoacidés de configuration déterminée est décrite. On a étudié sa pureté optique et sa conformation en solution. Dans une deuxième partie on décrit un nouveau système oxydant catalytique utilisant l'eau oxygénée en présence d'une porphyrine de manganèse et d'imidazole permettant la conversion quantitative d'alcènes en époxydes et d'alcanes en alcools et cétones.

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13

Ferroud, Clotilde. "Étude de la réaction de Diels-Adler intra et intermoléculaire sous haute pression : application à la synthèse stéréosélective d'alcaloïdes de l'indole du groupe des yohimbanes." Paris 6, 1986. http://www.theses.fr/1986PA066023.

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Le schéma de synthèse repose sur une unité bicyclique, précurseur direct des unités (d,e) du squelette pentacyclique. Cet intermédiaire est basé sur une réaction de Diels-Alder sous haute pression, utilisant la cycloaddition de diènes de structure donneur-accepteur 1,4 avec une lactone insaturée comme diénophile. La synthèse du système pentacyclique est exposée à partir de cet intermédiaire clé.

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14

Shiu, Shu-wei, and 許書瑋. "Study on [ 3+2 ] cycloaddition of L-proline and (E)-ethyl 4-oxobut-2-enoate." Thesis, 2009. http://ndltd.ncl.edu.tw/handle/15267388181607106857.

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碩士<br>國立中正大學<br>化學所<br>97<br>The first part of this study involved 1, 3-dipolar cycloaddition of L-proline and (E)-ethyl 4-oxobut-2-enoate. The structure was determined by NMR, and the mechanism was proposed. The second part of this study involved the preparation of some α, β –unsaturated aldehydes, and the study in the proline-catalysted self-condensation.

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15

詹淑秦. "Investigation of synthesis and anti-allergic activityof 2-ethyl-3, 4-dimethylfuro [ 2, 3-c ] pyrazoles." Thesis, 1987. http://ndltd.ncl.edu.tw/handle/61087201187943624709.

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16

He, Qing-Po, and 何清波. "Synthesis and antihypertensive activity evaluation of 2-{2-[4-(4-fluorobenzoyl)-1-piperidyl]-ethyl}-1,2,4-benzothiadiazine-3(4H)-one-1,1-dioxide." Thesis, 1989. http://ndltd.ncl.edu.tw/handle/74215914621474585401.

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17

Wu, Hsien-Ming, and 吳憲銘. "Cardiovascular pharmacology of GPFER:3-[4'-(2-hydroxy- 3-tert- butylaminopropoxy)3'methoxyphenyl]-2-propenoic acid ethyl ester." Thesis, 1995. http://ndltd.ncl.edu.tw/handle/71666430449483545434.

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18

朱瑞元. "Synthesis of Ethyl 2-[N-substituted benzyl-3-(or 4-)methoxy]anilino-4-oxo-4,5-dihydrofuran-3- carboxylate as Anticancer Agents." Thesis, 2004. http://ndltd.ncl.edu.tw/handle/19775827190625320450.

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碩士<br>中國醫藥大學<br>藥物化學研究所<br>92<br>As part of our continuing search for potential antimitotic agents and cytotoxicity agent, ethyl 2-(N-benzyl-2-anilino)-4-oxo-4,5-dihydrofuran- 3-carboxylate (5) was selected as the lead compound. The starting material diethyl malonate was added to sodium hydride which suspended in tetrahydrofuran, and then treated with chloroacetyl chloride to yield ethyl 2-ethoxy-4-oxo-4,5-dihydrofuran- 3-carboxylate (i). The intermediate i was condensed with m- (or p-)anisidine to yield ethyl 2-(3-methoxyanilino)-4-oxo-4,5-dihydrofuran- 3-carboxylate (2) or ethyl 2

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19

Shyu, Yun-Yaw, and 徐昀耀. "SYNTHESIS AND APPLICATION!OF 2-(2-NAPHTHOXY)ETHYL 2-[1-(4- BENZYL)PIPERAZYL]ETHANESULFONATE AS A CHEMICALLY REMOVABLE DERIVATIZATION REAGENT FOR LIQUID CHROMATOGRAPHY." Thesis, 1996. http://ndltd.ncl.edu.tw/handle/25362509846462391910.

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碩士<br>高雄醫學院<br>藥學研究所<br>84<br>I. 本研究以 2-naphthol (0.1 mol) 和 ethylene carbonate (0.2 mol) 為反應物, 於 195℃ (± 5℃) 油浴中進行反應, 得到 2-(2-naphthoxy)ethanol(NOE) (79.7 mmol;79.7% yield), 之後取 NOE (50 mmol) 與 2-chloroethanesulfonyl chloride (150 mmol) 於冰浴中進行 Hofmann elimination, 而得到中間產物 2-(2-naphthoxy) ethyl ethenesulfonate (NOEES) (20.83 mmol; 41.66% yield); 最後以此中間產物 NOEES (20mmol) 於 dichloromethane 溶媒中與二級胺 (N-benzylpiperazine) (25 mmol) 在冰浴下進行 Michael addition, 得到新的衍生試劑 2-(2-naph

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20

Huang, Shih-Ming, and 黃士鳴. "Synthesis and Biological Activity of Ethyl 2-{N-substituted benzyl-[2'-fluoro(or methoxy)]}anilino-4-oxo-4,5-dihydrofuran-3-carboxylate." Thesis, 2004. http://ndltd.ncl.edu.tw/handle/92983984445905645428.

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碩士<br>中國醫藥大學<br>藥物化學研究所<br>92<br>A series of ethyl 2-{N-substituted benzyl- [2'-fluoro(or methoxy)]}anilino-4-oxo-4,5-dihydrofuran-3-carboxylate and related compounds has been synthesized and assigned by their spectra data. All of these synthetic compounds were evaluated for anti-arrhythmias activity and cardiovascular effect. Among the investigations of the inhibitory effect on the heart rate , ethyl 2-[N- benzyl-(2'-fluoro)]anilino-4-oxo-4,5-dihydrofuran-3-carboxylate（2）was found to exhibit the most significant activities at 30μM while pacermaker S.A. node was inhibited at concent

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21

Gieschen, Tobias. "Synthese, strukturelle Studien und chemische Funktionalität eines Lewis-Säure-Lewis-Base-transformierten Organo-Zinn(IV)-Präkursors." Doctoral thesis, 2020. https://repositorium.ub.uni-osnabrueck.de/handle/urn:nbn:de:gbv:700-202009183558.

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Mit der präparativen Synthese der Tetraorganozinn(IV)-verbindung 4-[2-(Triphenylstannyl)ethylpyridin, Ph3Sn-(CH2)2-4Py, ausgehend von der Lewis-Säure Triphenylzinnchlorid, Ph3SnCl, konnte eine Blockade der reaktiven Lewis-Säure in Form des Zinnatoms dargestellt werden, in dem vier organische Liganden das zentrale Zinnatom einerseits topologisch und andererseits durch die weitreichende Stabilität von Zinn-Kohlenstoff-Bindungen abschirmen. Die Funktionalität konnte dadurch auf das funktionelle Stickstoffatom mit seiner Lewis-Base-Funktion, was neben der strukturellen Charakterisierung von 4-[2-(

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22

Su, I. Fang, and 蘇怡芳. "Synthesis and Biological Activity of Ethyl 2-[N-substituted benzyl-4¢(or 3¢)-bromo]anilino-4-oxo-4,5-dihydro- furan-3-carboxylate." Thesis, 2006. http://ndltd.ncl.edu.tw/handle/40810184770007644607.

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碩士<br>中國醫藥大學<br>藥物化學研究所碩士班<br>94<br>A series of ethyl 2-[N-substituted benzyl- 4´(or 3´)-bromo]anilino- 4-oxo-4,5-dihydrofuran-3-carboxylate and related compounds has been synthesized and assigned by their spectra data. All of these synthetic compounds were evaluated for anti-arrhythmics activity and cardiovascular effect. Among the investigations of the inhibitory effect on the heart rate , Ethyl 2-[N-m-fluorobenzyl-(3´-bromo)]anilino-4-oxo-4,5-dihydrofuran-3-carboxylate （27）、Ethyl 2-[N-m-chlorobenzyl-(3´-bromo)]anilino-4-oxo-4,5-dihydro- furan-3-carboxylate（30）、Ethyl 2-[N- benzyl-(3´-bromo)]

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23

Chiang, Ting-Ta, and 姜廷達. "Michael addition to synthesize 4, 6-diphenyl-1H-phenalen-1-one and ethyl 2-oxo-4, 6-diphenyl-2H-pyran-3-carboxylate." Thesis, 2017. http://ndltd.ncl.edu.tw/handle/7ms3h6.

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碩士<br>國立臺灣師範大學<br>化學系<br>105<br>Scientists have isolated many occurring natural substances from many different organisms, and some of them have specific structure such as pyrone and phenalene. This thesis covers the combination of two separate works. The two parts both synthesized by the diphenylpropynone as the original skeleton. Among them, the first work refers to some references about the natures, functions of this molecule, and some researches and synthesis over the past few years. To explore how to synthesize this kind of molecule by series of processes, we were carried out with 1-napht

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24

劉德厚. "Morphology of thin film of poly[1-methoxy-4-(2'-ethyl-hexyloxy)-2,5-phenylenevinylene] by spin coating." Thesis, 2002. http://ndltd.ncl.edu.tw/handle/22102674983743674030.

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25

Lan, Tzu-Shiu, and 藍子修. "Synthesis and Biological Activity of Ethyl 2-(N-substituted benzyl)pyridylamino-4-oxo-4,5- dihydrofuran-3-carboxylate and Related Compounds." Thesis, 2005. http://ndltd.ncl.edu.tw/handle/96424148534863215657.

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碩士<br>中國醫藥大學<br>藥物化學研究所<br>93<br>A series of Ethyl 2-(N-substituted benzyl)pyridylamino-4-oxo-4,5- dihydrofuran-3-carboxylate and related compounds has been synthesized and assigned by their spectra data. All of these synthetic compounds were evaluated for anti-arrhythmias activity and anticancer effect. Among the investigations of the inhibitory effect on the heart rate , Ethyl 2-[N-o-methoxybenzyl-(5¢-methylpyridyl)]amino-4-oxo-4,5- dihydrofuran-3-carboxylate（22）was found to exhibit the most significant activities at 30μM while pacermaker S.A. node was inhibited at concentrations up to 100 μ

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26

Huang, An-Cheng, and 黃安正. "Synthesis and Biological Activity of Certain Ethyl 2-[N-various Substituted benzyl]Substituted anilino-4-oxo-4,5-dihydrofuran-3-carboxylate." Thesis, 2007. http://ndltd.ncl.edu.tw/handle/69772011086807761891.

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博士<br>中國醫藥大學<br>藥物化學研究所博士班<br>95<br>One series of ethyl 2-(substituted anilino)-4-oxo-4,5-dihydrofuran-3-carboxylate (1~10), multi-series of ethyl 2-[N-various benzyl] substituted anilino-4-oxo-4,5-dihydro-furan -3-carboxylate (11~151), One series of N-various benzyl-7-methoxy-2,3,4,9-tetrahydrofuro- [2,3-b]-quinolin-3,4-diones (155~167) and another series of N-various benzyl-7-methoxy- 4,9-dihydrofuro[2,3-b]quinolin-4-diones (169~180) have been synthesized and assessed their chemical structures by their spectra data. All of these synthetic compound were evaluated for biological activities. In

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27

Li, Shih-Liang, and 李世良. "Synthesis and Biological Activity of Ethyl 2- [N-substituted benzyl]benzylamino-4-oxo-4,5-dihydrofuran-3-carboxylate and related compounds." Thesis, 2007. http://ndltd.ncl.edu.tw/handle/77331452477449678165.

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碩士<br>中國醫藥大學<br>藥物化學研究所碩士班<br>95<br>A series of ethyl 2- [N-substituted benzyl]benzylamino-4-oxo-4,5-dihydrofuran-3-carboxylate and related compounds has been synthesized and assigned by their spectra data. All of these synthetic compound were evaluated for biological activities(anti-arrhythmics activity、cardiovascular effect、Reactive oxygen species antagonist、induces apotosis、anticancer activite). Among the investigations of the inhibitory effect on the heart rate , Ethyl 2-(N-o-fluorobenzyl)benzylamino-4-oxo-4,5-dihydrofuran-3- carboxylate（6）、Ethyl 2-(N′-m-methylbenzyl)phenylhydrazino-4-

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28

Tung, Hsiang-Chun, and 童翔駿. "Physical Properties of Poly(N-isopropylacrylamide)/methanol Semi-dilute Solution and Poly[1-Methoxy-4-(2’-Ethyl-Hexyloxy)-2,5-Phenylene Vinylene]/ Tetrahydrofuran Solution." Thesis, 2004. http://ndltd.ncl.edu.tw/handle/16342314011241310241.

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碩士<br>元智大學<br>化學工程學系<br>92<br>In this thesis, using dynamic light scattering and dynamic viscoelastic analyzer, we studied the physical properties of 5 wt% poly(NIPAM) (poly(N- isopropyl acrylamide) -methanol solution. The overlap concentration C*, obtained from intrinsic viscosity measurement, was around 3.01 wt%. Thus the present solution is a semidilute solution. The viscosity of poly(NIPAM) -methanol solution decreases with increasing temperature, which behaves similar to the ordinary polymer good solutions with a USCT (upper critical solution temperature). The dynamic light scattering exp

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29

Bibak, Niloufar. "Synthesis of (3-Carbazol-9-yl-propyl)-[2-(4-methoxy-phenyl)-ethyl]methylamine and analogues effects as aSmase-inhibitors and their anti-apoptotic effects /." 2000. http://www.gbv.de/dms/bs/toc/326856668.pdf.

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30

Gansser, Simon [Verfasser]. "Läsion noradrenerger Afferenzen zum Hippocampus der Ratte durch N-2-Chlorethyl-N-Ethyl-2-Bromobenzylamin (DSP-4) : Beeinflussung der hippocampalen Freisetzung von Noradrenalin, Serotonin und Acetylcholin / vorgelegt von Simon Gansser." 2008. http://d-nb.info/991343298/34.

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31

Lin, Chia-Hui, and 林佳慧. "Synthesis and Optimization of 2-(1-Ethyl-3,5-dimethyl-1H-pyrazol-4-yl)ethan-1-amine Derivatives with in Vitro Activity against Triple-Negative Breast Cancer Cells." Thesis, 2016. http://ndltd.ncl.edu.tw/handle/77382163953235178318.

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碩士<br>國立中央大學<br>化學學系<br>104<br>Triple negative breast cancer (TNBC) has high mortality rate, high recurrence and high brain metastasis. Chemotherapy is the only treatment, and the worst of all it develops drug resistance. Therefore, we devote to drug discovery and synthesis for alleviating the suffering of patients. According to the previous research, the derivatives of pyrazole scaffold have activity against cancer. Hence, we study pyrazole compound N-(2-(1-ethyl-3,5-dimethyl-1H-pyrazol-4-yl)ethyl)-4-isobutyl- N-methylbenzenesulfonamide (YL-18), which is chosen as the hit compound through hig

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