Relevant bibliographies by topics / 5-Dienes

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  2. Dissertations / Theses
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  4. Book chapters

Academic literature on the topic '5-Dienes'

Author: Grafiati
Published: 4 June 2021
Last updated: 1 February 2022

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Journal articles on the topic "5-Dienes"

1

Bończa-Tomaszewski, Zbigniew. "The potassium permanganate oxidation of steroidal homoannular dienes." Canadian Journal of Chemistry 65, no. 3 (1987): 656–60. http://dx.doi.org/10.1139/v87-112.

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The oxidation of 3β-acetoxycholesta-5,7-diene (1) with potassium permanganate–sodium periodate reagent gave epoxy-diol 2 with almost quantitative yield. Similar oxidation of cholesta-2,4-diene (3) afforded, as well as epoxy-diols 5 and 6, products of cleavage of the double bonds. These results show that formation of epoxy-diols predominates in the case of hindered steroidal dienes (e.g., diene 1), whereas oxidation of unhindered steroidal dienes (e.g., diene 2) gives, in addition to epoxy-diols, products of cleavage of the double bonds.
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2

Butler, MS, and RJ Capon. "Norterpene Dienes From an Australian Marine Sponge Latrunculia brevis." Australian Journal of Chemistry 44, no. 1 (1991): 77. http://dx.doi.org/10.1071/ch9910077.

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The norditerpene diene acid (4) and norsesterterpene diene acid (5), along with their corresponding methyl esters (6) and (7), were isolated from an Australian marine sponge, Latrunculia brevis, and their structures determined by detailed spectroscopic analysis, chemical derivatization and degradation. Comment is made on the possible intermediacy of dienes such as (4)-(7) in the biosynthesis of norterpene cyclic peroxides, common to other Latrunculia species from the same locality.
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3

Piers, Edward, Richard W. Friesen, and Steven J. Rettig. "Annulation sequences employing methyl (E)- and (Z)-6-iodo-3-trimethylstannyl-2-hexenoates and related bifunctional reagents. Preparation of cisoidcis and cisoidtrans bicyclic dienes." Canadian Journal of Chemistry 70, no. 5 (1992): 1385–96. http://dx.doi.org/10.1139/v92-177.

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A useful annulation method leading to the stereospecific synthesis of structurally novel, functionalized bicyclic dienes is described. Alkylation of 2-(methoxycarbonyl)cyclopentanone (34) and 2-(methoxycarbonyl)cyclohexanone (35) with methyl (E)- and (Z)-6-iodo-3-trimethylstannyl-2-hexenoates (27, 28) provided the keto diesters 36–39. Conversion of these substances into the corresponding enol triflates 47–50, followed by palladium(0)-catalyzed ring closure of the latter compounds, afforded the bicyclic dienes 55–58. In similar fashion, the keto esters 34 or 35 were transformed into the dienes
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Maas, Gerhard, and Rainer Rahm. "A Proton-Catalyzed Dimerization of a 2-Amino-1,3-diene which Ultimately Yields a 3-Aminobicyclo[4.2.0]octa-2,4-diene." Zeitschrift für Naturforschung B 60, no. 6 (2005): 673–76. http://dx.doi.org/10.1515/znb-2005-0611.

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The 2-pyrrolidino-1,3-dienes (E)-5 and (Z)-5 are obtained by the reaction of lithium di(tertbutyl) cuprate with propyne iminium salt 3. Quantitative Z→E isomerization of 5 takes place within 4 hours at 20 °C. In benzene solution, (E)-5 slowly equilibrates with a [1,5]-H shift to form the 1-amino-1,3-diene derivative 6. In concentrated chloroform solution, however, (E)-5 is transformed into the 3-pyrrolidino-bicyclo[4.2.0]octa-2,4-diene 7 which is identified by X-ray crystal structure analysis. A mechanism for this transformation is proposed.
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5

Wang, Lizhong, Ting Wang, Chenlu Dai, Yang Li, and Cunde Wang. "Nickel-Catalysed Synthesis of 17-Arylandrosta-5,16-Dienes." Journal of Chemical Research 41, no. 11 (2017): 653–56. http://dx.doi.org/10.3184/174751917x15094552081206.

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An efficient Ni-catalysed coupling reaction between arylboronic acids and 17-trifluoromethanesulfonyl- 3β-acetoxyandrosta-5,16-diene which was obtained by the sulfonylation of 3β-acetoxylandrost-5-ene-17-one was developed to afford 17-aryl- 3β-acetoxy-androsta-5,16-dienes in moderate to good yields (52–85%). The structure of the 3,4-dimethoxyaryl product was confirmed by X-ray crystallography.
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Kreiter, Cornelius G., Kurt Nist та Joachim Kögler. "Gehinderte Ligandbewegungen in Übergangsmetallkomplexen, XXXI [1]. Synthese und Dynamik von Acetyl-carbonyl-η5-cyclopentadienyl-η4-dien-wolfram-Komplexen / Hindered Ligand Movements in Transition Metal Complexes, XXXI [1]. Syntheses and Dynamics of Acetyl-carbonyl-η5-cyclopentadienyl-η4-diene-tungsten Complexes". Zeitschrift für Naturforschung B 41, № 5 (1986): 599–605. http://dx.doi.org/10.1515/znb-1986-0512.

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Tricarbonyl-η5-cyclopentadienyl-methyl-tungsten (1) reacts upon UV irradiation with conjugated dienes, like 1,3-butadiene (2), E-1,3-pentadiene (3), 2-methyl-1,3-butadiene (4), 2,3-dimethyl-1,3- butadiene (5), 1,3-cyclopentadiene (6) and 1,3-cyclohexadiene (7), to give the corresponding, quasisquare- pyramidal [(η5-C5H5)W(CO)(COCH3)(η4-diene)] complexes (8-13). With the unsymmetrically substituted dienes 3 and 4, only one of the possible diastereotopic complexes are obtained. At 200 to 230 K, 8-12 show two isomers, which are distinguished by the orientations (o or u) of the diene with respect
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Liu, Hsing-Jang, Teng Ko Ngooi, and Eric N. C. Browne. "Diels–Alder reactions of 2-carbomethoxy-2-cyclohexen-1-one." Canadian Journal of Chemistry 66, no. 12 (1988): 3143–52. http://dx.doi.org/10.1139/v88-485.

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Under stannic chloride catalysis, 2-carbomethoxy-2-cyclohexen-1-one (5) was found to undergo Diels–Alder reaction with a variety of dienes to give directly the cis-1-octalone system possessing a functionalized substituent at the angular position. With unsymmetrically substituted dienes, the adducts were those predicted on the basis of the normal rules (ortho and para) governing the orientation of Diels–Alder addition. In cases where differing secondary orbital overlap would affect the stereochemistry of the adducts, the major isomer in each case was that produced by secondary overlap of the di
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Paquet, Jacques, and Paul Brassard. "Reactions of polar dienes with o-quinones." Canadian Journal of Chemistry 67, no. 8 (1989): 1354–58. http://dx.doi.org/10.1139/v89-207.

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The behaviour of various types of polar dienes towards halogenated ortho quinones has been investigated in a number of representative cases. As compared to the commonly used para analogues, o-quinones provide a wide range of products that indicate a keener response to the nature, number, and position of substituents on both reactants. 3-Halogenated-o-naphthoquinones 1 and 2 react smoothly with a representative vinologous ketene acetal 3, vinylketene acetals 4 and 5, and a monooxygenated diene 6 to provide variously substituted phenanthrenequinones 7–11. Only monooxygenated dienes on the other
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Mazerolles, Pierre, and Fabienne Gregoire. "5-germaspiro[4.4]nona-2,7-dienes." Journal of Organometallic Chemistry 301, no. 2 (1986): 153–60. http://dx.doi.org/10.1016/0022-328x(86)80006-7.

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Griesbaum, Karl, and Ashis R. Bandyopadhyay. "Anomalous ozone degradations of 1-chloro substituted conjugated dienes in methanol." Canadian Journal of Chemistry 65, no. 3 (1987): 487–90. http://dx.doi.org/10.1139/v87-084.

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Diozonolyses in methanol of (E)-4-chloro-2,3-dimethyl-1,3-hexadiene (4a) and of (4E)-5-chloro-3,4-dimethyl-2,4-heptadiene (4b) resulted in complete cleavage of the double bonds and of the single bonds of the respective diene systems. The course of these anomalous cleavage reactions has been established by step-wise ozonolyses of these dienes, and by the identification of labile methoxy hydroperoxides as intermediates.
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Dissertations / Theses on the topic "5-Dienes"

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Chreim, Yamama. "Synthese de polymeres organosilicies par polycondensation de dienes polycycliques." Université Louis Pasteur (Strasbourg) (1971-2008), 1986. http://www.theses.fr/1986STR13134.

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Polycondensation de molecules diinsaturees, mono- ou polycycliques avec des molecules disilylees (hydrosilylation des doubles liaisons par des fonctions si-h. Les polymeres ont des masses moleculaires comprises entre 3000 et 25000. Stabilite thermique jusqu'a 450**(o)c
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Ševčík, Jan. "Studium mechanizmu a kinetiky koordinační polymerace hexa-1,5-dienu katalyzované fenoxyiminovým komplexem titanu a MAO." Master's thesis, Vysoké učení technické v Brně. Fakulta chemická, 2008. http://www.nusl.cz/ntk/nusl-216372.

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This diploma thesis is focused on study of polymerization of hexa-1,5-diene catalyzed by phenoxy-imine titanium dichloride (FI Ti) and methylaluminoxane (MAO) as cocatalyst. Effect of monomer concentration, polymerization temperature and cocatalyst/catalyst ratio on catalytic activity, molecular weights, polydispersities and particularly microstructure of prepared poly(hexa-1,5-diene) was studied. 1H NMR spectroscopy revealed that the poly(hexa-1,5-diene) microstructure contained methylene-1,3-cyclopentane (MCP) as well as vinyl tetramethylene (VTM) units. Kinetics of this polymerization was s
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GUO, YUPING. "Synthese du 11,11-dimethyl bicyclo 5. 3. 1 undec-3,8-diene, sous-structure a/b du taxol." Paris 11, 1992. http://www.theses.fr/1992PA112206.

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Ce travail se divise en deux parties et a pour but l'elaboration des cycles a et b du taxol 5, une substance naturelle aux proprietes antitumorales. Nos efforts ont ete concentres sur l'etude des fragmentations regioselectives de la liaison c4-c12 de 4,8,11-trimethyl-5-methoxy-12-oxo-2,5-epoxytricyclo 5. 31#4#,#1#1 dodecene-8 39, ouvrant une nouvelle voie d'acces aux derives du taxol. La premiere partie decrit les differentes tentatives d'agrandissement de cycle par fragmentations heterolytiques, via la reaction de haller-bauer, le systeme base-solvant: ko-t-bu/h#2o-dmso et la reaction de grob
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Boulet, Serge L. "Total syntheses of (±)-neoverrucosan-5(ß)-ol, (±)-homoverrucosan-5(ß)-ol, (±)-verrucosan-2(ß)-ol, and (±)-(3R,4R, 5R, 6S, 9R)-cyatha-12, 18-diene, a new cyclohexenone annulation sequence." Thesis, National Library of Canada = Bibliothèque nationale du Canada, 1998. http://www.collectionscanada.ca/obj/s4/f2/dsk2/ftp02/NQ34515.pdf.

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Merkel, Dirk. "Untersuchungen zur flexiblen Synthese von potentiell flüssigkristallinen Verbindungen auf der Basis von 2, 5-di-C-substituierten Pyransystemen Synthese und Anwendung von neuen 2-substituierten Danishefsky-Dienen /." [S.l. : s.n.], 2001. http://deposit.ddb.de/cgi-bin/dokserv?idn=963414623.

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Merkel, Dirk [Verfasser]. "Untersuchungen zur flexiblen Synthese von potentiell flüssigkristallinen Verbindungen auf der Basis von 2, 5-di-C-substituierten Pyransystemen : Synthese und Anwendung von neuen 2-substituierten Danishefsky-Dienen / von Dirk Merkel." 2001. http://d-nb.info/963414623/34.

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Books on the topic "5-Dienes"

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Meredith, John Anthony. The interactions of Cis-3, 5-cyclohexadiene-1, 2-diol (cis-1, 2-dihydroxycyclohexa-3, 5-diene) (benzene-cis-glycol/BCG) with boric and phenylboronic acids. University of Birmingham, 1990.

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2

Catalysts for the Controlled Polymerization of Conjugated Dienes. MDPI, 2020. http://dx.doi.org/10.3390/books978-3-03936-191-5.

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Gemeinschaft der Heiligen: Berufung unserer Kirchen und ihre Erfüllung in der säkularisierten Welt : siebtes Gespräch im bilateralen Theologischen Dialog zwischen der Rumänischen Orthodoxen Kirche und der Evangelischen Kirche in Deutschland vom 27. November bis 5. Dezember 1995 im Haus der Communität Christusbruderschaft Selbitz, Bayern. Dienen und Versöhnen : europäische Integration als Herausforderung an unsere Kirche : achtes Gespräch im bilateralen Theologischen Dialog zwischen der Rumänischen Orthodoxen Kirche und der Evangelischen Kirche in Deutschland vom 3. bis 8. Oktober 1998 im Patriarchat in Bukarest. Missionshandlung, 1999.

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Book chapters on the topic "5-Dienes"

1

Pardasani, R. T., and P. Pardasani. "Magnetic properties of cobalt(II) ethylene-di(5′-methylbenzo)-9, 10-(4′, 5′-dimethoxybenzo)-[14]-1, 4, 8, 11-[N4]-7, 12-diene)." In Magnetic Properties of Paramagnetic Compounds. Springer Berlin Heidelberg, 2017. http://dx.doi.org/10.1007/978-3-662-53971-2_293.

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Pardasani, R. T., and P. Pardasani. "Magnetic properties of cobalt(II) ethylene-di(5′-methylbenzo)-9, 10-(4′, 5′-dihydroxybenzo)-[14]-1, 4, 8, 11-[N4]-7, 12-diene)." In Magnetic Properties of Paramagnetic Compounds. Springer Berlin Heidelberg, 2017. http://dx.doi.org/10.1007/978-3-662-53971-2_294.

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Pardasani, R. T., and P. Pardasani. "Magnetic properties of tetrabutylammonium[bis{nickel(II)-(ethylene-5, 6: 13, 14-di(5′-methylbenzo)-9, 10-(4, 5′-catecholate)-[14]-1, 4, 8, 11-[N4]-7, 12-diene)}copper(II)]." In Magnetic Properties of Paramagnetic Compounds. Springer Berlin Heidelberg, 2017. http://dx.doi.org/10.1007/978-3-662-53971-2_549.

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Schmeer, Hans, and Stefan Jennewein. "Biocatalytic Synthesis of Tritium (3H)-Labelled Taxa-4(5),11(12)-diene, the Pathway Committing Precursor of the Taxoid Diterpenoids." In Plant Secondary Metabolism Engineering. Humana Press, 2010. http://dx.doi.org/10.1007/978-1-60761-723-5_12.

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5

von Angerer, S. "Cyclization of 1-(Dimethylamino)-5-(dimethylimino)-2-azapenta-1,3-dienes." In Science of Synthesis Knowledge Updates KU 2011/1. Georg Thieme Verlag KG, 2011. http://dx.doi.org/10.1055/sos-sd-116-00233.

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Taber, Douglass. "Intermolecular and Intramolecular Diels-Alder Reactions: (-)-Oseltamivir (Fukuyama), Platensimycin (Yamamoto) and 11,12-Diacetoxydrimane (Jacobsen)." In Organic Synthesis. Oxford University Press, 2011. http://dx.doi.org/10.1093/oso/9780199764549.003.0078.

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Powerful methods for catalytic, enantioselective intermolecular Diels-Alder reactions have been developed. Ben L. Feringa and Gerard Roelfes of the University of Groningen have shown (Organic Lett. 2007, 9, 3647) that a catalyst prepared by combining salmon testes DNA with a Cu complex directed the absolute sense of the addition of 1 to cyclopentadiene 2 . Mukund P. Sibi of North Dakota State University has reported (J. Am. Chem. Soc . 2007, 129 , 395) related work with achiral pyrazolidinone dienophiles and chiral Cu catalysts. Tohru Fukuyama of the University of Tokyo found (Angew. Chem. Int. Ed . 2007, 46, 5734) that the MacMillan catalyst 5 was effective at mediating the addition of acrolein 4 to the pyridine-derived diene 3, enabling an enantioselective synthesis of the prominent antiviral (-)-oseltamivir (tamiflu) 7. Hisashi Yamamoto of the University of Chicago has demonstrated (J. Am. Chem. Soc . 2007, 129, 9534 and 9536) that the novel catalyst 10 effected addition of methyl acrylate 9 to the diene 8, leading to an elegant enantioselective synthesis of the tetracycle 12, the key intermediate in the Nicolaou synthesis of platensimycin. New illustrations of the power of the intramolecular Diels-Alder reaction have been put forward. Demonstrating the influence of a single subsituent on the tether, William R. Roush of Scripps/Florida found (Organic Lett . 2007, 9, 2243) that cyclization of 13 led to the diastereomer 14, complementary to the result observed with an acyclic triene. Ryo Shintani and Tamio Hayashi of Kyoto University have extended (Angew. Chem. Int. Ed . 2007, 46, 7277) their studies of chiral diene-based Rh catalysts to the enantioselective cyclization of alkynyl dienes such as 16. Jonathan W. Burton of the University of Oxford and Andrew B. Holmes of the University of Melbourne employed (Chem. Commun . 2007, 3954) the MacMillan catalyst 5 for the cyclization of 18 to 19. It is impressive that ent- 5 catalyzed the cyclization of 18 cleanly into the diastereomer of 19 in which both of the newly-created stereogenic centers were inverted.
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Ivin, K. J., and J. C. Mol. "Acyclic Dienes." In Olefin Metathesis and Metathesis Polymerization. Elsevier, 1997. http://dx.doi.org/10.1016/b978-012377045-5/50009-4.

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Taber, Douglass F. "Diels-Alder Cycloaddition: Fawcettimine (Williams), Apiosporic Acid (Helmchen), Marginatone (Abad- Somovilla), Okilactomycin (Hoye), Vinigrol (Barriault), Plakotenin (Bihlmeier/Klopper)." In Organic Synthesis. Oxford University Press, 2015. http://dx.doi.org/10.1093/oso/9780190200794.003.0079.

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Highly substituted dienes and dienophiles are often reluctant participants in intermolecular Diels-Alder cycloaddition. Nevertheless, Robert M. Williams of Colorado State University, in the course of a synthesis of fawcettimine 4, was able (J. Org. Chem. 2012, 77, 4801) to prepare 3 by combining the enone 1 with the diene 2. Günter Helmchen of the Universität Heidelberg set (J. Org. Chem. 2012, 77, 4491) the single stereogenic center of 5 by Ir-catalyzed allylic alkylation. The Lewis acid that promoted the cycloaddition also conveniently removed the trityl protecting group, leading to 6, that was saponified to apiosporic acid 7. Antonio Abad-Somovilla of the Universidad de Valencia prepared (J. Org. Chem. 2012, 77, 5664) the triene 8 in enantiomerically pure form from carvone. Despite the additional substitution on the diene, cycloaddition proceeded smoothly to give 9, which was carried on to marginatone 10. One could envision that okilactomycin 13 could be formed by an intramolecular Diels-Alder cycloaddition. Thomas R. Hoye of the University of Minnesota observed (Org. Lett. 2012, 14, 828) that the tetraene tetronic acid corresponding to 11 was inert, but that the methyl ether 11 cyclized smoothly to 12. Demethylation then gave the natural product The complex polycyclic structure of vinigrol 16 challenged organic synthesis chemists for many years, until a route was established by Phil Baran of Scripps/La Jolla (Highlights September 6, 2010). Louis Barriault cyclized (Angew. Chem. Int. Ed. 2012, 51, 2111) 14 to 15 en route to a late intermediate in the Baran synthesis It had been hypothesized that the natural product plakotenin 19 was formed naturally from a tetraene corresponding to 17. The tetraene 17 was prepared and the cyclization was successful, “confirming” both the structure of the natural product and the biosynthetic hypothesis. Angela Bihlmeier and Wim Klopper of the Karlsruhe Institute of Technology calculated (J. Am. Chem. Soc. 2012, 134, 2154) the relative energies of the four competing transition states for the cyclization, leading to a correction of the structure of 18, and so of the natural product 19.
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Taber, Douglass F. "The Paterson Synthesis of (−)-Leiodermatolide." In Organic Synthesis. Oxford University Press, 2017. http://dx.doi.org/10.1093/oso/9780190646165.003.0096.

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(−)-Leiodermatolide 4, isolated from the lithistid sponge Leiodermatium sp., showed 5.0-nM activity against PANC-1 pancreatic carcinoma cells, and reduced toxicity toward normal cells. Ian Paterson of the University of Cambridge established (Angew. Chem. Int. Ed. 2014, 53, 2692) a synthetic route to 4 based on sp2–sp2 coupling, as exemplified by the combination of 1 with 2 to give 3. Addition of the boron enolate of the enantiomerically-pure benzoate 5 to the iodoaldehyde 6 gave 7, that was silylated, reduced, and deprotected to give 1. Addition of the boron enolate of ent-5 to propanal gave 8. The α-acyloxy ketone of 8 served as a masked acylating agent. The addition of allyl magnesium bromide followed by oxidative cleavage led to the ketone 9. The preparation of 2 was com­pleted by diastereoselective Mukaiyama aldol condensation of 9 with the ketene silyl acetal 10. The intramolecular Heck coupling of 1 with 2 presumably proceeded by way of the organo-Pd intermediate 11. β-Hydride elimination could have given one or more of four possible dienes, but in fact the E,E product 3 dominated, as expected. The allylic H’s are activated for elimination, while the H’s β to the silyl ether are deacti­vated both electronically and sterically. The third component of 4 was the stannane 17. Applying the same strategy, the addition of ent-5 to the aldehyde 12 gave 13, that was protected and condensed with 14 to deliver, after oxidative cleavage, the alkynyl ketone 15. Conjugate addition of iodide proceeded with good geometric control to give 16, that was protected and stan­nylated to complete the preparation of 17. The diol 3 was oxidatively cleaved, and the resulting aldehyde was carried on to the iodide 18. This was coupled with the stannane 17 to give the diene 19. A sequence of deprotection, oxidation, and further deprotection yielded a tetraol, that was lac­tonized with high selectivity to give the 16-membered ring of (−)-leiodermatolide 4.
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Smith, Michael B. "Dienes and Conjugated Carbonyl Compounds in Biochemistry." In Biochemistry. CRC Press, 2020. http://dx.doi.org/10.1201/9781351258081-5.

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