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Journal articles on the topic 'Acetylferrocene'

Author: Grafiati

Published: 5 June 2025

Last updated: 24 June 2025

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1

Fang, C. J., G. Han, Y. J. Liu, C. Y. Duan, and Q. J. Meng. "Acetylferrocene thiosemicarbazone." Acta Crystallographica Section C Crystal Structure Communications 55, no. 12 (1999): 2058–60. http://dx.doi.org/10.1107/s010827019901077x.

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2

Khalaf, Mai M., Hany M. Abd El-Lateef, Mohamed Gouda, Fatma N. Sayed, Gehad G. Mohamed, and Ahmed M. Abu-Dief. "Design, Structural Inspection and Bio-Medicinal Applications of Some Novel Imine Metal Complexes Based on Acetylferrocene." Materials 15, no. 14 (2022): 4842. http://dx.doi.org/10.3390/ma15144842.

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Some novel imine metal chelates with Cr3+, Mn2+, Fe3+, Co2+, Ni2+, Cu2+, Zn2+, and Cd2+ cations were produced from 2-acetylferrocene and 3-aminophenol. The new acetylferrocene azomethine ligand ((Z)-cyclopenta-1,3-dien-1-yl(2-(1-((3-hydroxyphenyl)imino)ethyl)cyclopenta-2,4-dien-1-yl)iron) and its metal ion chelates were constructed and elucidated using FT-IR, UV/Vis, 1HNMR, DTA/TGA, CHNClM studies, mass spectrometry and SEM analysis. According to the TGA/DTG investigation, the ferrocene moiety spontaneously disintegrates to liberate FeO. The morphology of the free acetylferrocene azomethine via SEM analysis was net-shaped with a size of 64.73 nm, which differed in Cd(II) complex to be a spongy shape with a size of 42.43 nm. The quantum chemical features of the azomethine ligand (HL) were computed, and its electronic and molecular structure was refined theoretically. The investigated acetylferrocene imine ligand behaves as bidinetate ligand towards the cations under study to form octahedral geometries in case of all complexes except in case of Zn2+ is tetrahedral. Various microorganisms were used to investigate the anti-pathogenic effects of the free acetylferrocene azomethine ligand and its metal chelates. Moreover, the prepared ligand and its metal complexes were tested for anticancer activity utilizing four different concentrations against the human breast cancer cell line (MCF7) and the normal melanocyte cell line (HBF4). Furthermore, the binding of 3-aminophenol, 2-acetylferrocene, HL, Mn2+, Cu2+, and Cd2+ metal chelates to the receptor of breast cancer mutant oxidoreductase was discovered using molecular docking (PDB ID: 3HB5).

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3

Ogini, Francis O., Philip J. W. Elder, James F. Britten, and Ignacio Vargas-Baca. "An investigation of (C5H5)Fe(C5H4–C(OBF3)–CH3),." Canadian Journal of Chemistry 87, no. 7 (2009): 1055–62. http://dx.doi.org/10.1139/v09-075.

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Acetylferrocene readily forms an adduct with BF3. The product is a neutral model for protonated acetylferrocene, a species that is a crucial intermediate in the formation of 1,3,5-trisferrocenyl-benzene and other conjugated heterometallic derivatives by cyclocondensation. The title compound’s structure was determined in the solid state by X-ray diffraction and its spectroscopic properties were examined in detail, particularly the electronic excitation spectrum, which confirms the previous identification of the in situ generated protonated ketone.

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4

Erben, Milan, Aleš Růžička, Jaromír Vinklárek, Vít Šťáva, and Karel Handlíř. "1′-Acetylferrocene-1-carbonitrile." Acta Crystallographica Section E Structure Reports Online 63, no. 8 (2007): m2145—m2146. http://dx.doi.org/10.1107/s1600536807033892.

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5

Xie, Hong Fang, Yan Chun Xiao, Shao Bin Li, and Chen Zhen. "Electro-Generation of 2, 3, 5, 6-TCP in Zn, Ni,P-mSA/mCS Bipolar Membrane Equipped Electrolysis Cell." Advanced Materials Research 295-297 (July 2011): 1074–78. http://dx.doi.org/10.4028/www.scientific.net/amr.295-297.1074.

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P-ferrocene-SA/acetylferrocene-CS Bipolar Membrane (BPM) was prepared with phosphorylated agent as the cation exchange layer, and chitosan (CS) modified with acetylferrocene as the anion exchange layer. Zinc/Nickel alloy layer was placed on the surface of cation exchange layer to realize zero polar distance in the cathode chamber. The 2, 3, 5, 6-tetrachlopyridine (2,3,5,6-TCP) was electro-synthesized by reducing of pentachloropyridine(PCP). At the current density of 30mA·cm-2, the current efficiency was 70.1% and the yield of 2, 3, 5, 6-TCP was up to 96%. Compared with the traditional method, the electro-generation technology greatly eliminated the environmental pollution.

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6

Zhong-Lin, Lu, Wu Xiao-Li, Liang Yong-Min, Song Qing-Bao, and Ma Yong-Xiang. "ACETYLFERROCENE SALICYLHYDRAZONE CHELATES WITH LANTHANIDE." Bulletin des Sociétés Chimiques Belges 103, no. 2 (2010): 47–51. http://dx.doi.org/10.1002/bscb.19941030203.

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7

Moon, Sook Young, Seung-Yeol Jeon, Sung-Hyun Lee, Anna Lee, and Seung Min Kim. "High Purity Single Wall Carbon Nanotube by Oxygen-Containing Functional Group of Ferrocene-Derived Catalyst Precursor by Floating Catalyst Chemical Vapor Deposition." Nanomaterials 12, no. 5 (2022): 863. http://dx.doi.org/10.3390/nano12050863.

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Single wall carbon nanotubes (SWCNTs) were synthesized using oxygen-containing ferrocene derived catalysts. The mechanism of synthesizing carbon nanotubes was clarified by the catalyst’s exothermic or endothermic decomposition processes. By monitoring the decomposition process of ferrocene-derived catalyst precursors with and without sulfur, we found that the types of oxygen function groups closely influence catalyst formation and nanotube growth. The ferrocene-derived catalyst precursors have a different oxygen containing groups, which are hydroxyl (–OH, ferrocenenemethanol) and carbonyl (C=O, acetylferrocene, and 1,1′-diacetylferrocene). The sulfur chemical state (S 2p) on synthesized catalyst particles using acetylferrocene and 1,1′-diacetylferrocene has more sulfate (SO42−) than others, and there also is a carbon state (C-S-C). The catalyst particle using ferrocenemethanol predominant formed metal–sulfur bonds (such as S2− and Sn2−). The hydroxyl group (–OH) of ferrocenemethanol enhanced the etching effect to remove amorphous carbon and prevented oxidation on the catalyst particle surfaces; however, the carbonyl group (C=O) of acetylferrocene reacted with the catalyst particles to cause partial oxidation and carbon dissociation on the surface of the catalyst particles. The partial oxidation and carbon contamination on catalyst particles controlled the activity of the catalyst. The DFT study revealed that the ferrocene-derived catalyst precursor was dissociated according to following process: the functional groups (such as CH3CO and COH) => first Cp ligands => second Cp ligands. The pyrolysis and release of Fe ions were delayed by the functional groups of ferrocene-derived precursors compared to ferrocene. The thermal-decomposition temperature of the catalyst precursor was high, the decomposition time was be delayed, affecting the formation of catalyst particles and thus making smaller catalyst particles. The size and composition of catalyst particles not only affect the nucleation of CNTs, but also affect physical properties. Therefore, the IG/ID ratio of the CNTs changed from 74 to 18 for acetylferrocene and ferrocene, respectively. The purity also increased from 79 to 90% using ferrocene-derived precursors.

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8

Dvorikova, R. A., P. V. Dorovatovski, A. V. Mitrophanova, V. N. Khrustalev, and A. I. Kovalev. "Homocondensation of acetylferrocene under ultrasonic conditions." Russian Chemical Bulletin 71, no. 4 (2022): 717–21. http://dx.doi.org/10.1007/s11172-022-3471-9.

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9

Dvorikova, R. A., P. V. Dorovatovski, A. V. Mitrophanova, V. N. Khrustalev, and A. I. Kovalev. "Homocondensation of acetylferrocene under ultrasonic conditions." Russian Chemical Bulletin 71, no. 4 (2022): 717–21. http://dx.doi.org/10.1007/s11172-022-3471-9.

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10

Dvorikova, R. A., V. N. Khrustalev, A. S. Peregudov, and A. I. Kovalev. "Cyclocondensation of acetylferrocene under ultrasonic conditions." Russian Chemical Bulletin 65, no. 1 (2016): 223–27. http://dx.doi.org/10.1007/s11172-016-1288-0.

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11

Yongxiang, Ma, and Zhao Gang. "Chelates of acetylferrocene benzoylhydrazone with lanthanides." Polyhedron 7, no. 12 (1988): 1101–5. http://dx.doi.org/10.1016/s0277-5387(00)86402-5.

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12

Erben, Milan, Jaromír Vinklárek, and Aleš Růžička. "Acetylferrocene–2-chloro-1-ferrocenylethanone (1/1)." Acta Crystallographica Section E Structure Reports Online 67, no. 10 (2011): m1447—m1448. http://dx.doi.org/10.1107/s1600536811038244.

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13

Sobociková, Marie, Petr Štěpnička, Daniele Ramella, and Martin Kotora. "Synthesis of 1-Alkanoyl-1'-(trifluoroacetyl)ferrocenes." Collection of Czechoslovak Chemical Communications 71, no. 2 (2006): 190–96. http://dx.doi.org/10.1135/cccc20060190.

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Synthesis of the first representatives of mixed acyl(perfluoroacyl)ferrocenes, 1-acetyl-1'-(trifluoroacetyl)ferrocene (3a) and 1-propionyl-1'-(trifluoroacetyl)ferrocene (3b), by stepwise Friedel-Crafts acylation is described. A comparison of redox potentials of acetylferrocene, (trifluoroacetyl)ferrocene, and 3a as determined by cyclic voltammetry shows that the substitution effect is not purely additive.

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14

Tauchman, Jiří, M. Fernanda N. N. Carvalho, and Petr Štěpnička. "Selective hydration of ferrocenylethyne mediated by a palladium complex with a camphorhydrazone ligand." Collection of Czechoslovak Chemical Communications 76, no. 11 (2011): 1277–83. http://dx.doi.org/10.1135/cccc2011130.

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Complex [PdCl2L2], where L is a camphor hydrazone ligand, (1R,4S)-1,7,7-trimethyl-3-(2,2-dimethylhydrazone)-bicyclo[2.2.1]heptane-2,3-dione, efficiently promotes Markovnikov hydration of ethynylferrocene to acetylferrocene in aqueous methanol at room temperature. 1-Ferrocenylprop-1-yne and simple organic alkynes such as 1-octyne or ethynylbenzenes are not affected or polymerize under the reaction conditions.

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15

Okada, Yutaka, and Ryuichi Maeda. "Effect of Microwave Irradiation on Oximation of Acetylferrocene." Green and Sustainable Chemistry 11, no. 01 (2021): 1–8. http://dx.doi.org/10.4236/gsc.2021.111001.

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16

Gang, Zhao, and Ma Yongxiang. "Coordination complexes of acetylferrocene-m- nitrobenzoylhydrazone with lanthanides." Polyhedron 10, no. 18 (1991): 2185–89. http://dx.doi.org/10.1016/s0277-5387(00)86139-2.

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17

Chohan, Zahid H., and M. Praveen. "Ferrocene-Derived Pyrazinoyl and Nicotinoyl Schiff-Bases: Their Synthesis, Characterization and Biological Properties." Metal-Based Drugs 6, no. 3 (1999): 149–52. http://dx.doi.org/10.1155/mbd.1999.149.

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A novel class of acetylferrocene-derived Schiff-bases such as 2-pyrazinoyl-1-(2-ferroceneylmethylene)- hydrazide (HL1) and 2-nicotinoyl-1-(2-ferrocenylmethylene)hydrazide (HL2) have been synthesized and characterized by their IR, H1 NMR, C13 NMR and microanalytical date. The biological effect induced due to the coupling of ferrocene molecule with the aroylhydrazines e.g., pyrazinoylhydrazine and nicotinoylhydrazine has been studied against bacterial species such as Escherichia coli, Pseudomonas aeruginosa , Staphylococcus aureus and Klebsiella pneumonae.

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18

Liu, Yu Ting, Hai Long Guo, and Da Wei Yin. "Synthesis, Characterization and Antimicrobial Activity of Bis-Acetylferrocene Schiff Base." Advanced Materials Research 396-398 (November 2011): 1875–78. http://dx.doi.org/10.4028/www.scientific.net/amr.396-398.1875.

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Three bis-acetylferrocene schiff bases have been synthesized and characterized by IR, 1H NMR, and elemental analysis, the results conformed well with expected structures. The synthesized compounds were screened in vitro for their antimicrobial activity against three Gram-negative (Escherichia coli, Pseudomonas aeruginosa, and Salmonella typhi) and two Gram-positive (Bacillus subtilis and Staphylococcus aureus) bacterial strains. The results showed that these compounds are show excellent antimicrobia activities against Escherichia coli, Pseudomonas aeruginosa, Salmonella typhi ,Bacillus subtilis,Staphylococcus aureus.

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19

Mishra, K. N., O. P. Pandey, and S. K. Sengupta. "Hafnium(IV) Derivatives of Schiff Bases Derived from Acetylferrocene." Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry 27, no. 5 (1997): 661–71. http://dx.doi.org/10.1080/00945719708000217.

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20

Zhao, Zhengping, and Fengying Yu. "Synthesis and Thermal Performance of Poly(cyclotriphosphazene-acetylferrocene) Derivative." Asian Journal of Chemistry 26, no. 12 (2014): 3639–42. http://dx.doi.org/10.14233/ajchem.2014.16761.

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21

Kazemi, Somayeh, Veronica Belandria, Nico Janssen, Dominique Richon, Cor J. Peters, and Maaike C. Kroon. "Solubilities of ferrocene and acetylferrocene in supercritical carbon dioxide." Journal of Supercritical Fluids 72 (December 2012): 320–25. http://dx.doi.org/10.1016/j.supflu.2012.10.009.

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22

Levchenkov, S. I., E. A. Raspopova, A. N. Morozov, K. Yu Suponitskii, Yu O. Tkacheva, and L. D. Popov. "1'-Phthalazinylhydrazone of acetylferrocene: Structure, properties, and complexing ability." Russian Journal of General Chemistry 87, no. 8 (2017): 1759–65. http://dx.doi.org/10.1134/s1070363217080205.

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23

Fomin, V. M., and N. N. Shuklina. "Effect of the Nature of the Solvent on the Formation of Ferrocene Cations during the Protonation of Acetil- and 1,1'-Diacetylferrocene with Perchloric Acid and Their Oxidation with Iodine." Журнал физической химии 97, no. 7 (2023): 932–37. http://dx.doi.org/10.31857/s0044453723070105.

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It is established that the rate of the formation of ferrocenium cations in reaction mixture acetylferrocene (1,1'-diacetylferrocene) + I2 + HClO4 as a result of the protonation of metal complexes (MCs) and their oxidation with iodine in dioxane and acetonitrile depends on different mechanisms and is described by kinetic equations obtained by analyzing schemes of the process. The observed difference is due to different roles of the protonation of metal complexes and their oxidation with iodine in these solvents.

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24

Yin, Da Wei, Gang Tao Liang, Xiao Ming Sun, and Yu Ting Liu. "Optimization of Synthesis Technology of Acetylferrocene by Response Surface Methodology." Advanced Materials Research 622-623 (December 2012): 162–65. http://dx.doi.org/10.4028/www.scientific.net/amr.622-623.162.

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Acetylferrocene was synthesized by acetyl chloride and ferrocene as raw materials, dichloromethane as the solvent, and ZnO as catalyst. Response surface methodology based on three-level, three-variable central composite rotable design was used to evaluate the interactive effects of the ratio of acetyl chloride and ferrocene(2-4), the amount of ZnO(1.0-1.3mol), reaction time(30-60 min)on the percentage yield of acylferrocene. The optimal raw material ratio, amount catalyst, and reaction time was 3:1, 1.19mol, 40min. Under the optimum conditions, the actual experimental yield can reach 86.72%.

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25

Kubo, Atsushi, Ryuichi Ikeda, and Daiyu Nakamura. "1H NMR Studieson the Molecular Dynamics of Acetylferrocene in Crystals." Zeitschrift für Naturforschung A 43, no. 1 (1988): 78–80. http://dx.doi.org/10.1515/zna-1988-0111.

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Abstract The temperature dependence of 1H spin-lattice relaxation time was determined at 20 MHz for solid acetylferrocene [(C5H5) (C5H4COCH3)Fe] from ca. 80 K up to the m.p. (359 K). Rather large activation energies of 21 and 24 kJ mol-1 for the C5 reorientations of the two crystallographically nonequivalent non-substituted cyclopentadienyl rings were obtained, indicating that the crystal has a closely packed structure. The two kinds of CH3 groups attached to the substituted cyclopentadienyl rings were assumed to be approximately equivalent and gave a low activation energy of 4 kJ mol-1 for the C3 reorientation. No phase transition was observed in the relaxation times or in additional experiments of differential thermal analysis although the presence of two phase transitions has been reported previously at temperatures immediately below the melting temperature by means of differential scanning calorimetry.

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26

YAMAZAKI, Yoshimitsu, and Kuniaki HOSONO. "Microbial asymmetric reduction of organometallic ketones: Acetylferrocene and (Acetophenone)-tricarbonylchromium." Agricultural and Biological Chemistry 52, no. 12 (1988): 3239–40. http://dx.doi.org/10.1271/bbb1961.52.3239.

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27

Yamazaki, Yoshimitsu, and Kuniaki Hosono. "Microbial Asymmetric Reduction of Organometallic Ketones: Acetylferrocene and (Acetophenone)-tricarbonylchromium." Agricultural and Biological Chemistry 52, no. 12 (1988): 3239–40. http://dx.doi.org/10.1080/00021369.1988.10869223.

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28

Yong-xiang, Ma, Lu Zhong-lin, Song Qing-bao, and Wu Xiao-li. "CHELATE COMPLEXES OF FORMYLFERROCENE AND ACETYLFERROCENE SALICYLHYDRAZONE WITH TRANSITION METALS." Journal of Coordination Chemistry 32, no. 4 (1994): 353–59. http://dx.doi.org/10.1080/00958979408024255.

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29

Baciocchi, Enrico, Barbara Floris, and Ester Muraglia. "Reactions of ferrocene and acetylferrocene with carbon-centered free radicals." Journal of Organic Chemistry 58, no. 8 (1993): 2013–16. http://dx.doi.org/10.1021/jo00060a011.

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30

Qing-Shan, Li, Sun Yan-Jun, Li Xiao-Ming, and Ma Yong-Xiang. "ACETYLFERROCENE-5-PHENYL-1,3-OXAZOL-2-YLCARBONYLHYDRAZONE AND ITS COMPLEXES." Journal of Coordination Chemistry 40, no. 4 (1996): 319–26. http://dx.doi.org/10.1080/00958979608024536.

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31

Gao, Zuo-Ning, Jin-Fu Ma, and Wan-Yi Liu. "Electrocatalytic oxidation of sulfite by acetylferrocene at glassy carbon electrode." Applied Organometallic Chemistry 19, no. 11 (2005): 1149–54. http://dx.doi.org/10.1002/aoc.975.

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32

Yuan, Pin-Shi, and Qing-Sheng Wu. "Solvent-etching preparation and enhanced emission of acetylferrocene organometallic nanoparticles." Applied Organometallic Chemistry 22, no. 7 (2008): 378–82. http://dx.doi.org/10.1002/aoc.1409.

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33

Gupta, Hari K., Nada Reginato, Francis O. Ogini, Stacey Brydges, and Michael J. McGlinchey. "SiCl4ethanol as a trimerization agent for organometallics: convenient syntheses of the symmetrically substituted arenes 1,3,5-C6H3R3 where R = (C5H4)Mn(CO)3 and (C5H4)Fe(C5H5)." Canadian Journal of Chemistry 80, no. 11 (2002): 1546–54. http://dx.doi.org/10.1139/v02-152.

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Trimerization of acetylferrocene and of (acetylcyclopentadienyl)tricarbonyl-manganese proceeds efficiently in the presence of ethanol and tetrachlorosilane. The resulting 1,3,5-trisubstituted benzenes have been characterized by X-ray crystallography and compared with the structure of (1,3,5-triphenylbenzene)tris(tricarbonylchromium). The efficacy of EtOHSiCl4 as a combined reagent for the trimerization of polycyclic ketones is also discussed. Finally, the synthesis and structure of [CpMn(CO)2]2(µ-C=CHPr), derived from the reaction of cymantrene with butyllithium and phenylacetyl chloride at room temperature, is described.Key words: ketone, condensation, cyclization, organometallics, arenes.

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34

MOHAMED, ABBAS METWALLY, E. M. KANDEL EZZ, and A. AMER FATHY. "Ferrocene Derivatives. Part-I. Synthesis of some Ferrocenyl-pyrimicdobenzimidazole, -triazolopyrimidine, -pyrazolopyridine and -pyrimidine as Antimicrobial Agents." Journal of Indian Chemical Society Vol. 64, Dec 1987 (1987): 753–55. https://doi.org/10.5281/zenodo.6239162.

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Chemistry Department, Faculty of Science, Mansoura University, Mansoura, Egypt <em>Manuscript received 21 October 1986, revised 27 July 1987, accepted 4 November 1987</em> Condensation of 1-acetylferrocene with different aromatic aldehydes resulted in the formation of the α., β-unsaturated ketones (2a— c). The reactivity of 2 towards 3- amino-1,2,4-triazole, 2-aminobenzimidazole, 1-phenyl-3-aminopyrazolone and guanidine hydrochloride to give the linear structures 3, 5, 7 and 8 have been investigated. The structures of the hitherto unknown ring systems have been confirmed by pmr, ir and mass spectral data.

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35

López, Concepción, Ramón Bosque, Xavier Solans та Mercè Font-Bardia. "Activation of σ(C-H) bonds in ferrocenylhydrazones derived from acetylferrocene". Journal of Organometallic Chemistry 547, № 2 (1997): 309–17. http://dx.doi.org/10.1016/s0022-328x(97)00388-4.

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36

Bejblová, Martina, Stacey I. Zones, and Jiří Čejka. "Highly selective synthesis of acetylferrocene by acylation of ferrocene over zeolites." Applied Catalysis A: General 327, no. 2 (2007): 255–60. http://dx.doi.org/10.1016/j.apcata.2007.05.023.

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37

BAI, Yin-Juan, Zhi-Xiang NAN, and Jun LI. "Synthesis and Characterization of Acetylferrocene: Detailed Analysis of a Comprehensive Chemistry Experiment." University Chemistry 31, no. 8 (2016): 81–85. http://dx.doi.org/10.3866/pku.dxhx201510011.

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38

BACIOCCHI, E., B. FLORIS, and E. MURAGLIA. "ChemInform Abstract: Reactions of Ferrocene and Acetylferrocene with Carbon-Centered Free Radicals." ChemInform 24, no. 33 (2010): no. http://dx.doi.org/10.1002/chin.199333237.

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39

Ojani, Reza, Jahan-Bakhsh Raoof, and Banafsheh Norouzi. "Acetylferrocene Modified Carbon Paste Electrode; A Sensor for Electrocatalytic Determination of Hydrazine." Electroanalysis 20, no. 12 (2008): 1378–82. http://dx.doi.org/10.1002/elan.200704187.

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40

MOHAMED, ABBAS METWALLY, and A. AMER FATHY. "Ferrocene Derivatives. Part-II. Synthesis of some Ferrocenyl[semicarbazone, 1 ,2-benzodiazepines, cyclohexenone, tetrazolopyrimidine and pyrazolopyrimidine] as Antimicrobial Agents." Journal of Indian Chemical Society Vol. 65, Jan 1988 (1988): 51–53. https://doi.org/10.5281/zenodo.6024218.

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Department of Chemistry, Faculty of Science, University of Mansoura, Mansoura, Egypt <em>Manuscript received 23 February 1987, revised 28 October 1987, accepted 4 November 1981</em> Acetylferrocene (1) undergoes condensation with semicarbazido hydrochloride and aromatic aldehydes to give the semicarbazone (2) and the α,β-unsaturated ketones (3). Michael condensation of 3a with cyclohexanone, α.-tetralone, acetophenone and 1,3- diphenylacetone gives the1,5-dicarbonyl compounds (4, 5, 10) and the ferrocenylcyclo- hexenone (11). 1,5-Dicarbonyl compound (4) undergoes condensation with hydrazines to give the 1,2-diazepines (6, 8). Condensation of 3a with 5-aminotetrazole and/or 5-amino-3-phenylpyrazole gives the pyrimidotetrazole (12) and pyrimidopyrazole (13). The structures of the hitherto unknown ring systems have been confirmed by analytical and spectral methods.

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41

Alvarado, Y., J. Peña-Suárez, N. Cubillán, P. Labarca, J. Caldera-Luzardo, and F. López-Linares. "Influence of the Dielectric Medium on the Carbonyl Infrared Absorption Peak of Acetylferrocene." Molecules 10, no. 2 (2005): 457–74. http://dx.doi.org/10.3390/10020457.

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42

Donahue, Craig J., and Emily R. Donahue. "Beyond Acetylferrocene: The Synthesis and NMR Spectra of a Series of Alkanoylferrocene Derivatives." Journal of Chemical Education 90, no. 12 (2013): 1688–91. http://dx.doi.org/10.1021/ed300544n.

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43

Gao, Zuo-Ning, Juan Zhang, and Wan-Yi Liu. "Electrocatalytic oxidation of N-acetyl-l-cysteine by acetylferrocene at glassy carbon electrode." Journal of Electroanalytical Chemistry 580, no. 1 (2005): 9–16. http://dx.doi.org/10.1016/j.jelechem.2005.03.008.

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44

Buryukin, F. A., V. P. Tverdokhlebov, V. A. Fedorov, E. V. Tetenkova, A. V. Fedorova, and O. O. Azanova. "The solubility of acetylferrocene and diacetylferrocene in dimethylsulfoxide and its mixtures with water." Russian Journal of Physical Chemistry A 82, no. 9 (2008): 1545–48. http://dx.doi.org/10.1134/s0036024408090252.

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Sayed, Abdelwahed R., Mohamed S. M. Ahmed, and Sobhi M. Gomha. "Efficient Methods for the Synthesis of Novel Arylazothiazoles Based on Acetylferrocene or Adamantane." Current Organic Synthesis 17, no. 4 (2020): 282–87. http://dx.doi.org/10.2174/1570179417666200226091711.

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Abstract:

Background: Hydrazonoyl halides are convenient for the synthesis of arylazothiazoles. Materials and Methods: A series of novel arylazothiazoles were efficiently synthesized from the reaction of hydrazonoyl chlorides with 2-(adamantan-2-ylidene)hydrazinecarbothioamide or 2-(ferrocenyl-1-ylidene)hydrazinecarbo-- thioamide in dioxane used as an aprotic solvent because of its lower toxicity and higher boiling point (101 °C) and triethylamine at reflux. The reaction mechanistic pathway proceeded by the nucleophilic substitution reaction by the elimination of hydrogen chloride to give thiohydrazonates as intermediate, which in situ undergo intramolecular cyclization and loss of water molecule to afford the final product of novel arylazothiazoles. This method is simple with good yield and excellent purities. Results and Discussion: The synthetic schemes for the final products are proposed and discussed. The chemical structures of the final products were identified by different techniques, such as elemental analysis, Fourier-transform infrared spectroscopy (FT-IR), nuclear magnetic resonance (NMR), and mass spectrometry (MS). Conclusion: In this article, we prepared arylazothiazoles from the reaction of 2-(adamantan-2-ylidene)hydrazinecarbothioamide or 2-(ferrocenyl-1-ylidene)hydrazinecarbothioamide with hydrazonoyl halides.

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Sultana, Tahmina, Chowdhury A. Waheed, SM Saiful Islam, et al. "Synthesis, characterization and Electrochemical studies of Ferrocenyl-2, 4-Dinitrophenylhydrazone." Journal of Bangladesh Academy of Sciences 38, no. 2 (2014): 177–87. http://dx.doi.org/10.3329/jbas.v38i2.21342.

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A ferrocenyl imine complex, Fc-C(CH3)=N-NH-C6H3-2,4-(NO2)2 (Fc = ferrocenyl) has been synthesized by the condensation reaction between acetylferrocene and 2,4-dinitrophenyl hydrazine. The compound was synthesised previously, and characterized by IR, 1H and elemental analysis. It was further characterized by 13C {1H} NMR spectroscopy and mass spectrometry. The redox property of the complex was studied by cyclic voltammetry, differential pulse voltammetry and chronocoulometry. The redox process of the complex was found to be reversible at a platinum-disc electrode, and the redox potential of the imine complex was shifted to more anodic position with respect to ferrocene. The redox reactivity of the complex was enhanced in the presence of oxygen. DOI: http://dx.doi.org/10.3329/jbas.v38i2.21342 Journal of Bangladesh Academy of Sciences, Vol. 38, No. 2, 177-187, 2014

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D. Yadav, Ganapati, and Santosh R. More. "Cesium Modified Heteropoly Acid Supported on Clay as Catalyst in Selective Synthesis of Acetylferrocene." Current Catalysise 1, no. 1 (2012): 32–40. http://dx.doi.org/10.2174/2211544711201010032.

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D. Yadav, Ganapati, and Santosh R. More. "Cesium Modified Heteropoly Acid Supported on Clay as Catalyst in Selective Synthesis of Acetylferrocene." Current Catalysis 1, no. 1 (2012): 32–40. http://dx.doi.org/10.2174/2211545511201010032.

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Moskalenko, A. I., A. V. Boeva, and V. I. Boev. "Reaction of acetylferrocene with dimethylformamide dimethyl acetal and some transformations of the reaction product." Russian Journal of General Chemistry 81, no. 3 (2011): 521–28. http://dx.doi.org/10.1134/s1070363211030133.

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Fomin, V. M., and A. E. Shirokov. "Kinetics and mechanism of formyl- and acetylferrocene oxidation with molecular oxygen in organic solvents." Russian Journal of General Chemistry 82, no. 6 (2012): 1080–89. http://dx.doi.org/10.1134/s1070363212060072.

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