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Journal articles on the topic 'Adsorption of pure EB and MB'

Author: Grafiati

Published: 5 June 2025

Last updated: 1 August 2025

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1

Debashish, Palit, and Priya Moulik Satya. "Adsorption of cationic dyes ethidium bromide and methylene blue individually as well as from their binary mixture on silica." Journal of Indian Chemical Society Vol. 78, Oct-Dec 2001 (2001): 611–18. https://doi.org/10.5281/zenodo.5910285.

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Centre for Surface Science, Department of Chemistry, Jadavpur University, Kolkata-700 032, India <em>E-mat!</em>: cssju@yahoo.co.uk           <em>  Fax</em> : 91-33-4734266 <em>Manuscript received 26 March 2001</em> The adsorption bebaviours of the cationic dyes, ethidium bromide (EB) and methylene blue (MB) individually as well as from their 1 : 1 (mol/mol) binary mixture on negative surface of Silica in aqueous medium have been investigated. The effects of temperature, the salt KCI and pH on the said adsorption process have been also examined. The resu

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2

Debashish, Palit, and Priya Moulik Satya. "Adsorption of cationic dyes ethidium bromide and methylene blue individually as well as from their binary mixture on silica." Journal of Indian Chemistry Society Vol. 78, October-December 2001 (2001): 611–18. https://doi.org/10.5281/zenodo.5892279.

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Centre for Surface Science, Department of Chemistry, Jadavpur University, Kolkata-700 032, India <em>E-mail</em>: cssju@yahoo.co.uk   <em>Fax</em> : 91-33-4734266 <em>Manuscript received 26 March 2001</em> The adsorption bebaviours of the catronic dyes, ethidium bromide (EB) and methylene blue (MB) indiviually as well as from their I : I (mol/mol) binary mixture on negative surface of Silica in aqueous medium have been investigated. The effects of temperature, the salt KCI and pH on the said adsorption process have been also examined. The results have been analyzed in terms

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3

Aquino, Ruth R., Marvin S. Tolentino, Bianca Mae Z. Crisogono, and Sarah Katrina V. Salvacion. "Adsorption of Methylene Blue (MB) Dye in Wastewater by Electrospun Polysulfone (PSF)/Organo-Montmorillonite (O-MMT) Nanostructured Membrane." Materials Science Forum 916 (March 2018): 120–24. http://dx.doi.org/10.4028/www.scientific.net/msf.916.120.

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In this study, organo-montmorillonite was utilized as an additive for the fabrication of the nanostructured membrane via electrospinning process.The purpose of this study is to investigate the performance of 95% PSF and 5% O-MMT blend in terms of its adsorption capacity towards MB dye in wastewater and comparing it to pure PSF membranes. Pure PSF and 5% O-MMT blend were immersed in the simulated wastewater at different time intervals (1, 5, 12, 24 and 48 hours), and the change in MB dye concentration was observed by UV-Vis absorbance reading. To determine the mechanism of adsorption, the data

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4

Saha, Sati, M. Yousuf Ali Mollah, Md Abu Bin Hasan Susan, and Md Mominul Islam. "Treatment of Wastewater Containing Organic Dyes: Recovery of Dye Adsorbed on Starch-Based Materials Through Conversion of Adsorbent into Alcohol." Dhaka University Journal of Science 63, no. 2 (2015): 119–24. http://dx.doi.org/10.3329/dujs.v63i2.24446.

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The recovery of a cationic dye, methylene blue (MB), from the residue generated during its removal via adsorption on starch-based adsorbents from aqueous solution was studied. Adsorption characteristics of MB on wheat flour (WF) and pure starch were analyzed using UV-visible spectroscopy. WF and starch were loaded with an optimum amount of MB producing MB-WF and MB-starch, respectively, leaving residues. The desorption characteristics and % recovery of MB from both the synthetic wastes were determined. The effects of yeast and temperature on the recovery of MB were also investigated. The mecha

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5

Gao, Jie, Zhenzhen Li, Ziwen Wang, et al. "Facile Synthesis of Sustainable Tannin/Sodium Alginate Composite Hydrogel Beads for Efficient Removal of Methylene Blue." Gels 8, no. 8 (2022): 486. http://dx.doi.org/10.3390/gels8080486.

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To meet the requirement of sustainable development, bio-based adsorbents were developed for the removal of dye contaminant. To improve the adsorption capacity of pure sodium alginate (SA) adsorbent for the removal of methylene blue (MB), aromatic bio-based tannin (Tan) was incorporated through the cross-linking with calcium ion. The obtained Tan/SA composite hydrogel beads were characterized with SEM, FTIR and TG, demonstrating that millimeter-sized beads were obtained through calcium cross-linking with enhanced thermal stability. The maximum capacity (247.2 mg/g) at optimal condition (pH = 12

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Sivapatarnkun, Janjira, K. Hathaisamit, and S. Pudwat. "Enhancement for Photocatalytic Activity of TiO₂ Combined with Activated Carbon under Surface Fluorination (F-TiO₂/AC)." Key Engineering Materials 675-676 (January 2016): 560–63. http://dx.doi.org/10.4028/www.scientific.net/kem.675-676.560.

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The prepared TiO2 and commercial grade of TiO2 with anatase and rutile phase combined with bulk and powder of activated carbon (TiO2/AC) observed the photocatalytic activity under weak UV. The surface fluorination was applied for all photocatalysts (F-TiO2/AC) to enhance photocatalytic activity. The decolorization of methylene blue (MB) was used to indicate the efficiency of adsorption and degradation of the samples. The prepared TiO2 was prepared by Sol-Gel method under condition of the titanium tetraisopropoxide (TTIP) to 2-propanol (2-PP) ratio of 1:30 and adjusts pH of 2 by HCl acid. Under

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7

Zhang, Xuelun, Feng Li, Xiyu Zhao, et al. "Bamboo Nanocellulose/Montmorillonite Nanosheets/Polyethyleneimine Gel Adsorbent for Methylene Blue and Cu(II) Removal from Aqueous Solutions." Gels 9, no. 1 (2023): 40. http://dx.doi.org/10.3390/gels9010040.

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In recent years, the scarcity of pure water resources has received a lot of attention from society because of the increasing amount of pollution from industrial waste. It is very important to use low-cost adsorbents with high-adsorption performance to reduce water pollution. In this work, a gel adsorbent with a high-adsorption performance on methylene blue (MB) and Cu(II) was prepared from bamboo nanocellulose (BCNF) (derived from waste bamboo paper) and montmorillonite nanosheet (MMTNS) cross-linked by polyethyleneimine (PEI). The resulting gel adsorbent was characterized by Fourier transform

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8

Mabungela, Ntandokazi, Ntaote David Shooto, Fanyana Mtunzi, and Eliazer Bobby Naidoo. "The Adsorption of Copper, Lead Metal Ions, and Methylene Blue Dye from Aqueous Solution by Pure and Treated Fennel Seeds." Adsorption Science & Technology 2022 (March 8, 2022): 1–21. http://dx.doi.org/10.1155/2022/5787690.

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This research work reports on pure and acid-treated fennel seed biomaterials for the removal of metal ions of copper Cu(II), lead Pb(II), and methylene blue (MB) dye from aqueous solution by batch adsorption. Pure fennel seeds were labelled as PFS; nitric and sulphuric acid-treated seeds were designated as NAFS and SAFS, respectively. The adsorbents were characterised by SEM, EDX, FTIR, XRD, and BET. The SEM images revealed that the surface of the adsorbents was porous. However, physicochemical characterization further revealed that BET surface area, pore size, and pore width increased for NAF

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Bai, Xiuzhi, Zhongxiang Liu, Pengfei Liu, Yijun Zhang, Linfeng Hu, and Tongchao Su. "An Eco-Friendly Adsorbent Based on Bacterial Cellulose and Vermiculite Composite for Efficient Removal of Methylene Blue and Sulfanilamide." Polymers 15, no. 10 (2023): 2342. http://dx.doi.org/10.3390/polym15102342.

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In this work, a novel composite of bacterial cellulose (BC) and expanded vermiculite (EVMT) composite was used to adsorb dyes and antibiotics. The pure BC and BC/EVMT composite were characterized using SEM, FTIR, XRD, XPS and TGA. The BC/EVMT composite exhibited a microporous structure, providing abundant adsorption sites for target pollutants. The adsorption performance of the BC/EVMT composite was investigated for the removal of methylene blue (MB) and sulfanilamide (SA) from an aqueous solution. The adsorption capacity of BC/ENVMT for MB increased with increasing pH, while the adsorption ca

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Kaswan, Vipin, Maha Saleem, and Harpreet. "Biochar based tin-oxide nanocomposite for remediation of water." BIO Web of Conferences 86 (2024): 01007. http://dx.doi.org/10.1051/bioconf/20248601007.

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In the present scenario, pure drinking water is a great problem. Scientists are finding out ways to combat this problem. Various approaches are being used for water remediation, but there is always a need to get more economical, eco-friendly and viable method for removal of pollutants from water. In the present study, an attempt have been made to prepare composite (RHAC/SnO2) from biochar from rice husk and SnO2. The comparison of adsorption and photo catalysis for removal of methylene blue (MB)has been done. It was concluded that biochar is efficient in removal of MB by adsorption at all the

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Rahmayanti, Maya, Atika Yahdiyani, and Ika Qurrotul Afifah. "Eco-friendly synthesis of magnetite based on tea dregs (Fe3O4-TD) for methylene blue adsorbent from simulation waste." Communications in Science and Technology 7, no. 2 (2022): 119–26. http://dx.doi.org/10.21924/cst.7.2.2022.965.

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Methylene blue is a popular dye used in the batik industry; however, it potentially causes environmental problems in view of the residual MB content in the liquid waste, which is difficult to naturally degrade. This study aimed to synthesize Fe3O4-TD using tea dregs from household waste and its application as an adsorbent for methylene blue dye. The synthesis was carried out using the reverse co-precipitation method with water as a solvent at room temperature. Fe3O4-TD characterization using FTIR, XRD, and PSA. The adsorption of methylene blue (MB) on Fe3O4-TD was studied at various pH MB, rea

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12

Hajjaji, W., S. Andrejkovičová, R. C. Pullar, et al. "Effective removal of anionic and cationic dyes by kaolinite and TiO2/kaolinite composites." Clay Minerals 51, no. 1 (2016): 19–27. http://dx.doi.org/10.1180/claymin.2016.051.1.02.

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AbstractThe present study investigated the removal of methylene blue (MB) and orange II (OII) dyes from synthetic wastewater by means of adsorption and photocatalysis using natural kaolins. ForMB adsorption, the raw kaolinite-rich samples showed the greatest adsorption capacity, with rapid uptake (90% after 20 min). The experimental results were fitted better using the Langmuir isotherm model parameters compared to the Freundlich model, suggesting that the adsorption corresponds to monolayer coverage of MB molecules over the kaolinite surface. For OII, neither the Langmuir nor the Freundlich m

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Ahmed, Inas A., Moaaz K. Seliem, Eder C. Lima, et al. "Outstanding Performance of a New Exfoliated Clay Impregnated with Rutile TiO2 Nanoparticles Composite for Dyes Adsorption: Experimental and Theoretical Studies." Coatings 12, no. 1 (2021): 22. http://dx.doi.org/10.3390/coatings12010022.

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Pure rutile TiO2 nanoparticles (Rt) were combined with exfoliated black clay (BC) to prepare a new composite for water decontamination, in particular, for the uptake of methylene blue (MB) and methyl orange (MO) dyes. The as-prepared Rt/BC was characterized by X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), and Field emission scanning electron microscopy (FESEM) techniques, and the dyes’ adsorption isotherms at three temperatures (i.e., 25, 40, and 50 °C) were studied. The results indicated that Rt/BC displayed a high removal performance for MO (96.7%) and MB (91.4%) a

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14

Shuai, Chao, Yun Wen Liao, He Jun Gao, and Luan Luan Zhang. "Removal of Methylene Blue from Aqueous Solution by a Novel PAA@Fe-Si Composite Material." Applied Mechanics and Materials 665 (October 2014): 479–82. http://dx.doi.org/10.4028/www.scientific.net/amm.665.479.

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A novel organic-inorganic PAA@Fe-Si composite material was synthesized by acrylic acid and mesoporous iron-incorporated material and used as an efficient and specific adsorbent for the removal of methylene blue (MB), a cationic dye from aqueous solution. The properties of the composite material were characterized by scanning electron microscopy, Fourier transform infrared and thermogravimetric. The effects of initial solution pH, adsorbent dosage, and contact time on MB adsorption and temperature have been investigated. The results showed that the maximum adsorption capacity of PAA@Fe-Si reach

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15

Cheng, Khley, Socheata Heng, Siteng Tieng, et al. "Mixed Metal Oxide W-TiO2 Nanopowder for Environmental Process: Synergy of Adsorption and Photocatalysis." Nanomaterials 14, no. 9 (2024): 765. http://dx.doi.org/10.3390/nano14090765.

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A mixed metal oxide W-TiO2 nanopowder photocatalyst was prepared by using the sol–gel method with a broad range of elemental compositions x = CW/(CW + CTi), including TiO2 and WO3. The material was structurally characterized and evaluated in adsorption and photocatalytic processes by testing its removal capacity of a representative pollutant methylene blue (MB) in aqueous solutions and under UV-A and sunlight illuminations. The nanopowders appeared to be more effective adsorbents than pure TiO2 and WO3 materials, showing a maximum at 15 mol% W, which was set as the tungsten solubility limit in

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16

Xiang, Hengli, Genkuan Ren, Yanjun Zhong, et al. "Fe3O4@C Nanoparticles Synthesized by In Situ Solid-Phase Method for Removal of Methylene Blue." Nanomaterials 11, no. 2 (2021): 330. http://dx.doi.org/10.3390/nano11020330.

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Fe3O4@C nanoparticles were prepared by an in situ, solid-phase reaction, without any precursor, using FeSO4, FeS2, and PVP K30 as raw materials. The nanoparticles were utilized to decolorize high concentrations methylene blue (MB). The results indicated that the maximum adsorption capacity of the Fe3O4@C nanoparticles was 18.52 mg/g, and that the adsorption process was exothermic. Additionally, by employing H2O2 as the initiator of a Fenton-like reaction, the removal efficiency of 100 mg/L MB reached ~99% with Fe3O4@C nanoparticles, while that of MB was only ~34% using pure Fe3O4 nanoparticles

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17

Mohadi, Risfidian, Normah Normah, Neza Rahayu Palapa, and Aldes Lesbani. "M2+(Ni, Cu, Zn)/Al-LDH Composites with Hydrochar from Rambutan Peel and Study the Adsorption Efficiency for Organic Dyes." Environment and Natural Resources Journal 20, no. 2 (2022): 1–13. http://dx.doi.org/10.32526/ennrj/20/202100218.

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Ni/Al LDH, Cu/Al LDH, and Zn/Al LDH were composed with rambutan peel hydrochar (Hc) and the materials were applied as adsorbent for the removal of methylene blue from aqueous solution, measured using UV-Vis Spectrophotometric method. The preparation of the LDH-Hc composites were proven by XRD, FT-IR, and SEM analysis which showed similar characteristics of the LDH-Hc composites with pure LDH and hydrochar. The methylene blue removal efficiency was optimized by various parameters including adsorption selectivity, adsorption regeneration, pH, contact time, adsorption concentration, and temperatu

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18

Wang, Yuquan, Yidong Xu, Xinjie Cai, and Jinting Wu. "Adsorption and Visible Photocatalytic Synergistic Removal of a Cationic Dye with the Composite Material BiVO4/MgAl–LDHs." Materials 16, no. 21 (2023): 6879. http://dx.doi.org/10.3390/ma16216879.

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Adsorption and photocatalysis are effective in removing organic pollutants from wastewater. This study is based on the memory effects of MgAl–layered double hydroxides (MgAl–LDHs) after high-temperature calcination. By introducing bismuth vanadate (BiVO4) during the reformation of the layered structure via contact with water, a composite material BiVO4/MgAl–LDHs with enhanced adsorption and visible light catalytic performance was synthesized. The effects of the calcination temperature, ratio, initial methylene blue (MB) concentration, and catalyst dosage on the adsorption and photocatalytic pe

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19

Faye, Omar, Jerzy A. Szpunar, and Ubong Eduok. "A Comparative Density Functional Theory Study of Hydrogen Storage in Cellulose and Chitosan Functionalized by Transition Metals (Ti, Mg, and Nb)." Materials 15, no. 21 (2022): 7573. http://dx.doi.org/10.3390/ma15217573.

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The focus of this work is hydrogen storage in pristine cellulose, chitosan, and cellulose. Chitosan doped with magnesium, titanium, and niobium is analyzed using spin unrestricted plane-wave density functional theory implemented in the Dmol3 module. The results of this study demonstrate that hydrogen interaction with pure cellulose and chitosan occurred in the gas phase, with an adsorption energy of Eb = 0.095 eV and 0.090 eV for cellulose and chitosan, respectively. Additionally, their chemical stability was determined as Eb= 4.63 eV and Eb = 4.720 eV for pure cellulose and chitosan, respecti

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20

Elmorsi, Taha M., Mohamed Hammad Elsayed, and Mostafa F. Bakr. "Enhancing the removal of methylene blue by modified ZnO nanoparticles: kinetics and equilibrium studies." Canadian Journal of Chemistry 95, no. 5 (2017): 590–600. http://dx.doi.org/10.1139/cjc-2016-0456.

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This research aims to use modified ZnO nanoparticles to enhance the removal rate of the methylene blue (MB) dye. ZnO nanoparticles are modified by coating their surface with Congo red (CR) dye, henceforth referred to as ZnO/CR. This process is used to produce a Lewis acid on the surface of ZnO to attract any Lewis base such as a MB dye (MB+). Therefore, the stability of ZnO/CR improved, and it resists the change in pH value (from 3 to 9). Several analysis techniques such as scanning electron microscopy, X-ray diffraction, FTIR, and BET method were used to characterize ZnO/CR. Nonlinear and lin

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21

Zhou, Yarui, Hailong Zhang, Lu Cai, et al. "Preparation and Characterization of Macroalgae Biochar Nanomaterials with Highly Efficient Adsorption and Photodegradation Ability." Materials 11, no. 9 (2018): 1709. http://dx.doi.org/10.3390/ma11091709.

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In this study, carbonized kelp biochar (AKB) modified by KOH impregnation and photocatalytic Bi2MoO6/AKB composite (BKBC) nanomaterials were the first time successfully synthesized for efficient removal of dyes in aqueous solution. BET, XRD, FT-IR, and SEM were employed to characterize as-prepared samples. UV-vis and other test results indicated that the removal efficiency of methylene blue (MB) was 61.39% and 94.12% for BKBC and AKB, respectively, which was up to 13 times and 20 times higher in comparison with pure Bi2MoO6 (PBM). In addition, the equilibrium adsorption capacity of MB could re

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22

Wasilewska, Małgorzata, Anna Derylo-Marczewska, and Adam W. Marczewski. "Equilibrium and Kinetic Studies on Adsorption of Neutral and Ionic Species of Organic Adsorbates from Aqueous Solutions on Activated Carbon." Molecules 29, no. 13 (2024): 3032. http://dx.doi.org/10.3390/molecules29133032.

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This work presents comprehensive studies of the adsorption of neutral and ionic forms of organic adsorbates from aqueous solutions on activated carbon. The influence of pH on the equilibrium and kinetics of the adsorption of methylene blue (MB) and organic acids, benzoic (BA), 2-nitrobenzoic (2-NBA), 3-nitrobenzoic (3-NBA), and 4-nitrobenzoic (4-NBA) acid, was investigated. Experimental adsorption isotherms were analyzed using the generalized Langmuir isotherm equation (R2 = 0.932–0.995). Adsorption rate data were studied using multiple adsorption kinetics equations, of which the multi-exponen

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23

Hwang, Kyung-Jun, Young Jin Kim, Xing Xing, et al. "Synthesis of Walnut Shaped V2O3 Particles and Its Photocatalytic Activity for Methylene Blue Degradation Under Visible Light Irradiation." Journal of Nanoscience and Nanotechnology 20, no. 7 (2020): 4322–26. http://dx.doi.org/10.1166/jnn.2020.17566.

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In this study, walnut-shaped V2O3 particles with high photocatalytic activity in the visible light were synthesized by hydrothermal process. The V2O3 samples synthesized with the various temperature conditions of the hydrothermal process were characterized using XRD, SEM, TEM, UV-Visible spectrometer and N2gas adsorption/desorption analysis. For investigating the photocatalytic performance of synthesized V2O3 particles in the visible light condition, photodegradation experiments of methylene blue (MB) solution under artificial sunlight irradiation was conducted. As a result, the V2O3 hydrother

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24

Ge, Mingliang, Zhuangzhuang Xi, Caiping Zhu, et al. "Preparation and Characterization of Magadiite–Magnetite Nanocomposite with Its Sorption Performance Analyses on Removal of Methylene Blue from Aqueous Solutions." Polymers 11, no. 4 (2019): 607. http://dx.doi.org/10.3390/polym11040607.

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The magadiite–magnetite (MAG–Fe3O4) nanocomposite has great potential applications in the field of biomaterials research. It has been used as a novel magnetic sorbent, prepared by co-precipitation method. It has the dual advantage of having the magnetism of Fe3O4 and the high adsorption capacity of pure magadiite (MAG). MAG–Fe3O4 was characterized by X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM), and vibrating sample magnetometer (VSM). The results showed that Fe3O4 nanoparticles were deposited on the interlayer and surface of magad

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25

Zhao, Meixia, Jiguo Huang, Xueting Guo, et al. "Preparation of Na2Ti3O7/Titanium Peroxide Composites and Their Adsorption Property on Cationic Dyes." Journal of Chemistry 2015 (2015): 1–12. http://dx.doi.org/10.1155/2015/363405.

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Na2Ti3O7/titanium peroxide composites (TN-TP) were successfully prepared with the reaction of Ti foils, NaOH, and H2O2at 60°C for 24 h in water bath. The Na2Ti3O7appeared as nanorods in composites. Water bath temperature, water bath time, and the concentration of H2O2and NaOH were crucial. The reaction mechanism was proposed. TN-TP was characterized by X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR), scanning electron microscopy (SEM), X-ray photoelectron spectroscopy (XPS), and thermogravimetric and differential scanning calorimetry (TG-DSC). TN-TP was a mesoporous ma

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Chen, Wei-Sheng, Ming-Hong Wu, and Jun-Yi Wu. "Effects of Tb-Doped BiVO4 on Degradation of Methylene Blue." Sustainability 15, no. 8 (2023): 6994. http://dx.doi.org/10.3390/su15086994.

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Bismuth vanadate (BiVO4) is a narrow-bandgap semiconductor (~2.41 Ev) that responds to visible light. The efficiency of degradation of organic dyes is indexed by methylene blue (MB). After 150 min, the efficiency of MB degradation by pure BiVO4 was about 20%. Its adsorption performance and electron–hole pair migration ability are weak, and the photocatalytic activity of pure BiVO4 needs to be improved. BiVO4 doped with rare earth ions can facilitate the separation of photogenerated electron–hole pairs, thereby enhancing photocatalytic activity in the visible light range. This study investigate

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Nang An, Vu, Tran T. T. Van, Ha T. C. Nhan, and Le Van Hieu. "Investigating Methylene Blue Adsorption and Photocatalytic Activity of ZnO/CNC Nanohybrids." Journal of Nanomaterials 2020 (March 17, 2020): 1–10. http://dx.doi.org/10.1155/2020/6185976.

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Nanohybrids of zinc oxide/cellulose nanocrystals (ZnO/CNCs) were successfully prepared by using a low cost and green method for adsorption and photocatalytic degradation of methylene blue (MB). CNCs have been derived through the hydrolysis reaction by citric/hydrochloric acid from the pure cellulose isolated from Vietnamese Nypa fruticans trunk. The influence of the Zn2+ ion concentration on the morphology, microstructure, and thermal properties as well as the photocatalytic activity of the ZnO/CNC nanohybrids was investigated in detail. Analyses of FTIR spectra, XRD, and SEM indicated that th

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Mai, Nguyen Thi Tuyet, Nguyen Kim Nga, Dang Thi Minh Hue, Ta Ngoc Dung, Huynh Dang Chinh, and Tran Quang Huy. "Characterization of Co2+- and Fe3+-Codoped TiO2 Nanomaterials for Photocatalytic Degradation of Organic Pollutants under Visible Light Irradiation." Adsorption Science & Technology 2021 (November 18, 2021): 1–12. http://dx.doi.org/10.1155/2021/9193052.

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In this study, TiO2 nanomaterials were prepared using a solvothermal method and codoped with Co2+ and Fe3+ ions for the photocatalytic degradation of organic pollutants under visible light. The physicochemical properties of the obtained materials were studied by powder X-ray diffraction, field emission electron scanning microscopy, energy-dispersive X-ray spectroscopy, and nitrogen adsorption isotherms. Optical absorption was characterized by UV-vis absorption spectroscopy. The photocatalytic activities of the prepared materials were evaluated through methylene blue (MB) degradation under visi

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Liu, Jian, Yan Li, Na Zhang, and Dong Ping Duan. "Preparation and Photocatalytic Properties of Graphene/SrTiO₃ Thin Film Catalyst." Materials Science Forum 972 (October 2019): 191–99. http://dx.doi.org/10.4028/www.scientific.net/msf.972.191.

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A novel graphene-bridged SrTiO3 (STO) thin film loaded on the glass was fabricated using a facile sol-gel method followed by the dip-coating and spin-coating method. As-prepared STO film and GO/STO film were tested by XRD, SEM to identify the composition and surface morphology. The as-prepared thin film catalyst was employed to degrade methylene blue (MB) in water under near ultraviolet ray irradiation. Compared to pure STO, GO/STO prepared by dip-coating method displayed good photocatalytic degradation efficiency with 58% removal of MB (60 mL, 5mg/L) in 6.0 h, the GO/STO prepared by spin-coat

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El yacoubi, Ahmed, Brahim Chafik El idrissi, Amine Rkhaila, and Brahim Sallek. "Antibacterial and photocatalytic performance of Silver orthophosphate/Hydroxyapatite composite." Mediterranean Journal of Chemistry 8, no. 4 (2019): 320–27. http://dx.doi.org/10.13171/mjc841906173ae.

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The present work reports the synthesis of pure hydroxyapatite and HAp supported Ag3PO4 (Ag3PO4/HAp composites) with varying amounts of silver ions Ag+ with a facile in-situ ion exchange method. XRD results of Ag3PO4/HAp composite reveal the peaks characteristic of pure HAp with additional peaks of silver ions which suggest the deposit of silver particles on the support surface (HAp). The nano-composites Ag3PO4/HAp samples show good adsorption and improved photocatalytic activities in methylene blue MB degradation (more than 70%). Antibacterial study of Ag3PO4/HAp nano-composites showed that th

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Duc Vu Quyen, Nguyen, Tran Ngoc Tuyen, Dinh Quang Khieu, et al. "Separation of Spherical Nanosilica from Agricultural Wastes in Vietnam via Ultrasonic-Assisted Precipitation and Application for Effective Removal of Methylene Blue from Aqueous Solution." Journal of Nanotechnology 2023 (September 26, 2023): 1–16. http://dx.doi.org/10.1155/2023/8884113.

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Agricultural wastes including bagasse and rice husk ashes are employed for synthesizing spherical nanosilica materials via the ultrasonic-assisted precipitation process in the present study. The comparison between them and nanosilica prepared from pure sodium silicate is also carried out. The role of the NH4OH : ethanol volume ratio is demonstrated. The obtained nanosilica is characterized by modern methods including X-ray diffraction (XRD), energy-dispersive X-ray spectroscopy (EDS), infrared spectroscopy (IR), scanning electron microscopy (SEM), and nitrogen adsorption/desorption isotherms (

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Jiang, Haiyan, Rui Wang, Daohan Wang, Xiaodong Hong, and Shaobin Yang. "SnO2/Diatomite Composite Prepared by Solvothermal Reaction for Low-Cost Photocatalysts." Catalysts 9, no. 12 (2019): 1060. http://dx.doi.org/10.3390/catal9121060.

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Abundant contaminants in wastewater have a negative effect on the natural environment and ecology. Developing highly efficient photocatalysts is a practical strategy to solve the pollution issue. In order to prevent the agglomeration of SnO2 nanoparticles and improve the photocatalytic efficiency, porous diatomite is adopted as a low-cost template to load monodispersed SnO2 nanoparticles by solvothermal reaction and sintering method. Through adjusting the mass of reactants, monodispersed SnO2 nanoparticles (~15 nm) generated on diatomite template achieved the maximum specific surface area of 2

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Vu, An Nang, Anh Mai Tran, Nghi Tuyet Nguyen, et al. "Green one-step synthesis of cellulose nanocrystal/ ZnO nanohybrid with high photocatalytic activity." Science and Technology Development Journal - Natural Sciences 5, no. 3 (2021): first. http://dx.doi.org/10.32508/stdjns.v5i3.924.

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In this work, nanohybrid of zinc oxide/ cellulose nanocrystals (ZnO/CNC) was successfully prepared by using a low cost and green method for photocatalytic degradation of methylene blue (MB). CNC had been derived through the hydrolysis reaction by citric/hydrochloric acid from the pure cellulose isolated from Vietnamese Nypa fruticans trunk. The obtained CNC with carboxyl groups could act as a stabilizing and supporting agent to anchor ZnO nanoparticles. The chemical and crystal structures, morphology, thermal and photocatalytic properties of the ZnO/CNC nanohybrid were characterized by FESEM,

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Abla, Fatima, Yehya Elsayed, Nedal Abu Farha, et al. "Fabrication of High Surface Area TiO2-MoO3 Nanocomposite as a Photocatalyst for Organic Pollutants Removal from Water Bodies." Catalysts 13, no. 2 (2023): 362. http://dx.doi.org/10.3390/catal13020362.

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A nanocomposite (NC) of titanium (IV) oxide (TiO2) and molybdenum (VI) oxide (MoO3) was synthesized using a hydrothermal route. Detailed analyses using transmission electron microscopy, X-ray diffraction, X-ray fluorescence (XRF), Brunauer–Emmett–Teller (BET) isotherms, X-ray photoelectron spectroscopy, Raman, and diffuse reflectance infrared Fourier transform spectroscopy were carried out and confirmed the successful formation of pure TiO2-MoO3 (Ti-Mo) NC. The Ti-Mo NC possesses sizes in the range of 150–500 nm. XPS, Raman, and DRIFT shift measurements confirmed the formation of mixed oxide l

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Fuziki, Maria E. K., Laura S. Ribas, Eduardo Abreu, et al. "N-Doped TiO2-Nb2O5 Sol–Gel Catalysts: Synthesis, Characterization, Adsorption Capacity, Photocatalytic and Antioxidant Activity." Catalysts 13, no. 9 (2023): 1233. http://dx.doi.org/10.3390/catal13091233.

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TiO2-based semiconductors are formidable photocatalysts for redox reaction applications. Although N-doped TiO2-Nb2O5 catalysts have already been explored in the literature, studies on their antioxidant activity are scarce, and systematic investigations on the effects of synthesis parameters over a wide range of %Nb and NH4OH concentrations are limited. In addition, the relationship between optimal pH and %Nb has not yet been adequately explored. In the present work, the sol–gel synthesis of N-doped TiO2-Nb2O5 catalysts was optimized using a design of experiments approach focused on photocataly

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Hirano, Masanori, and Kazumasa Matsushima. "Effect of Niobium on the Structure and Photoactivity of Anatase (TiO2) Nanoparticles." Journal of Nanoscience and Nanotechnology 6, no. 3 (2006): 762–70. http://dx.doi.org/10.1166/jnn.2006.17948.

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Anatase-type TiO2 nanoparticles doped with 0–30 mol% niobium were directly formed from precursor solutions of TiOSO4 and NbCl5 under mild hydrothermal conditions at 120–180 °C for 5 h using the hydrolysis of urea. When the niobium content increased from 0 to 30 mol%, the crystallite size of anatase increased from 8.5 to 19 nm. The band gap of anatase was slightly decreased by making solid solutions with niobium. Their photocatalytic activity and adsorptivity were evaluated separately by the measurement of the concentration of methylene blue (MB) remained in the solution after maintained in the

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Mousavi, S. A., Z. Arab Aboosadi, A. Mansourizadeh, and B. Honarvar. "Modification of porous polyetherimide hollow fiber membrane by dip-coating of Zonyl® BA for membrane distillation of dyeing wastewater." Water Science and Technology 83, no. 12 (2021): 3092–109. http://dx.doi.org/10.2166/wst.2021.201.

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Abstract Wetting and fouling have significantly affected the application of membrane distillation (MD). In this work, a dip-coating method was used for improving surface hydrophobicity of the polyetherimide (PEI) hollow fiber membrane. An air gap membrane distillation (AGMD) process was applied for treatment of the methylene blue (MB) solution. The porous PEI membrane was fabricated by a dry-wet spinning process and the hydrophobic 2-(Perfluoroalkyl) ethanol (Zonyl® BA) was used as the coating material. From FESEM, the modified PEI-Zonyl membrane showed an open structure with large finger-like

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Bhima, Arun Naidu, Jung-Hee Park, Min Cho, et al. "Simultaneous utilization of soju industrial waste for silica production and its residue ash as effective cationic dye adsorbent." e-Polymers 15, no. 6 (2015): 427–37. http://dx.doi.org/10.1515/epoly-2015-0108.

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AbstractSoju industrial waste is an important biomass resource. The present study aimed to utilize soju industrial waste for silica extraction, and residual ash (RA) as a low cost adsorbent for the removal of methylene blue (MB) from aqueous solution. A high percentage of pure amorphous nanosilica was obtained from soju industrial waste ash by the acid dissolution-precipitation process. The synthesized nanosilica and the RA were characterized well using various techniques such as X-ray diffraction (XRD), Fourier transform infrared (FTIR), and field-emission electron microscopy with energy disp

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Chems, Myriam, Lázaro Adrián González-Fernández, Manuel Sanchez Polo, Abdellah Anouar, and Ventura Castillo Ramos. "Efficient Photocatalytic Degradation of Triclosan and Methylene Blue by Synthesized Ag-Loaded ZnO under UV Light." Separations 11, no. 8 (2024): 221. http://dx.doi.org/10.3390/separations11080221.

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Industrial discharge of hazardous organic and synthetic chemicals, such as antibacterials and dyes, poses severe risks to human health and the environment. This study was conducted to address the urgent need for efficient and stable zinc-oxide-based photocatalysts to degrade such pollutants. A novel approach to synthesizing silver-loaded zinc oxide (Ag@Z) catalysts was introduced by using a simple and efficient combination of hydrothermal and precipitation methods. Comprehensive characterization of Ag@Z photocatalysts was performed using XRD, XPS, Raman, UV–vis adsorption, FTIR, and SEM, revea

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Yin, Song, Jingya Zhai, Zepeng Zhang, et al. "Study on the effects of cationic dyes species on the structure and performance of sepiolite hybrid pigments." Materials Research Express 9, no. 3 (2022): 035001. http://dx.doi.org/10.1088/2053-1591/ac58ea.

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Abstract In this work, sepiolite hybrid pigments were prepared with four kinds of cationic dyes with different structures and functional groups, Basic orange 2 (BO2), Mytheme blue (MB), Basic red 18 (BR18) and Basic red 2 (BR2), by the vacuum method. The obtained samples were respectively named as BO2/Sep, MB/Sep, BR18/Sep and BR2/Sep. The sepiolite hybrid pigments were characterized and tested by XRD, FT-IR, Microporous physical/chemical adsorption analyzer, thermal analyzer, et al. The effects of cationic dyes structure and functional groups types on the positions and loading capacity of cat

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Nguyen Thi Tu, Anh, Lan Nguyen Huong, and Tuan Vu Anh. "Synthesis of ZnO, g-C3N4 and ZnO/g-C3N4 composite and their photocatalytic activity under vilsible light irradiation." Vietnam Journal of Catalysis and Adsorption 9, no. 2 (2020): 87–93. http://dx.doi.org/10.51316/jca.2020.034.

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ZnO, C3N4 and ZnO/g-C3N4 composite were prepared for degradation of methylene blue (MB) under visible light irradiation. The obtained samples were characterized by N2 adsorption/desorption isotherm and Ultraviolet–Visible Diffuse Reflectance Spectroscopy (UV-vis DRS). The results showed that the ZnO/g-C3N4 composite had a lower surface area and pore volume than ZnO and g-C3N4. The bandgap energy of ZnO/g-C3N4 composite was 3.20 eV showing a slight decrease with that of pure ZnO (3.21 eV). The degradation of MB on g-C3N4 was higher than those of ZnO and ZnO/g-C3N4composite in initial 40 min, bu

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Zhang, Jinyuan, Hui Zhang, Wenjun Li, Limeng Yang, Hailiang Wu, and Ningtao Mao. "Photocatalytic Properties of a Novel Keratin char-TiO2 Composite Films Made through the Calcination of Wool Keratin Coatings Containing TiO2 Precursors." Catalysts 11, no. 11 (2021): 1366. http://dx.doi.org/10.3390/catal11111366.

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In this study, the photocatalytic properties of novel keratin char-TiO2 composite films, made through the calcination of wool keratin coatings containing TiO2 precursors at 400 °C, were investigated for the photodegradation of organic contaminants under visible light irradiation. Its structural characteristics and photocatalytic performance were systematically examined. It was shown that a self-cleaning hydrophobic keratin char-TiO2 composite film containing meso- and micro-pores was formed after the keratin—TiO2 precursors coating was calcined. In comparison with calcinated TiO2 films, the ke

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Esencan Türkaslan, Banu, Aziz Kerim Çelik, Ayça Dalbeyler, and Nicholas Fantuzzi. "The Effect of Different Morphologies of WO3/GO Nanocomposite on Photocatalytic Performance." Materials 15, no. 22 (2022): 8019. http://dx.doi.org/10.3390/ma15228019.

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Tungsten trioxide/graphene oxide (WO3/GO) nanocomposites have been successfully synthesized using in situ and ex situ chemical approaches. Graphite and tungsten carbide (WC) were employed to perform in situ synthesis, and WO3 and GO were employed to perform the ex situ synthesis of WO3/GO nanocomposites. GO, which was required for ex situ synthesis, is synthesized via the modified and improved Hummers method. XRD, SEM/EDS, and FTIR are used for the characterization of the nanocomposite. From the XRD of the WO3/GO nanocomposites, it was observed that WO3 distributed uniformly on graphene oxide

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Andrade-Guel, M., C. A. Ávila-Orta, C. Cabello-Alvarado, et al. "Non-Woven Fabrics Based on Nanocomposite Nylon 6/ZnO Obtained by Ultrasound-Assisted Extrusion for Improved Antimicrobial and Adsorption Methylene Blue Dye Properties." Polymers 13, no. 11 (2021): 1888. http://dx.doi.org/10.3390/polym13111888.

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Approximately 200,000 tons of water contaminated with dyes are discharged into effluents annually, which in addition to infectious diseases constitute problems that afflict the population worldwide. This study evaluated the mechanical properties, surface structure, antimicrobial performance, and methylene blue dye-contaminant adsorption using the non-woven fabrics manufactured by melt-blowing. The non-woven fabrics are composed of nylon 6 (Ny 6) and zinc oxide nanoparticles (ZnO NPs). The polymer nanocomposites were previously fabricated using variable frequency ultrasound assisted-melt-extrus

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Luo, Tong, Yanping Hao, Chao Wang, et al. "Lignin Nanoparticles and Alginate Gel Beads: Preparation, Characterization and Removal of Methylene Blue." Nanomaterials 12, no. 1 (2022): 176. http://dx.doi.org/10.3390/nano12010176.

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A novel and effective green system consisting of deep eutectic solvent (DES) was proposed to prepare lignin nanoparticles (LNPs) without any lignin modification. The LNPs are obtained through the dialysis of the kraft lignin-DES solution. The particle size distribution, Zeta potential and morphology of the LNPs are characterized by using dynamic light scattering (DLS), scanning electron microscopy (SEM) and transmission electron microscopy (TEM). The average diameter of LNPs is in the range 123.6 to 140.7 nm, and the LNPs show good stability and dispersibility in water. The composite beads com

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Nguyen Thi To Loan, Ha Thi Phuong Thanh, Nguyen Thi Thuy Hang, Nguyen Quang Hai, Vu Van Nhuong, and Bui Duc Nguyen. "Preparation, characterization and photocatalytic activity for degradation of methylene blue by ZnFe<sub>2</sub>O<sub>4</sub>/Bentonite nanocomposite." Vietnam Journal of Catalysis and Adsorption 12, no. 4 (2024): 143–52. http://dx.doi.org/10.62239/jca.2023.078.

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In this work, we report synthesis of bentonite (BT) supported softmagnetic ZnFe2O4 nanoparticles to obtain ZnFe2O4/BT. The composition, surface morphology and optical properties of the sample were characterized by XRD, EDX, FTIR, SEM and DRS analysis. The results of SEM show that the ZnFe2O4 nanoparticles spread on the thin layer of bentonite due to intercalation with bentonite. The band gaps of Bentonite, ZnFe2O4 and ZnFe2O4/BT are 2.18; 1.95 and 1.82 eV respectively. The photocatalytic activity of the samples is evaluated by the degradation of methylene blue (MB) in the presence of H2O2 unde

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Nguyen Thi, Hoa, Tien Nguyen Trung, Phong Le Hong, Tai Vu Van, Hung Nguyen Van, and Nui Pham Xuan. "Photocatalytic activity of Ag-Ag3PO4/Cellulose aerogel composite for degradation of dye pollutants under visible light irradiation." Vietnam Journal of Catalysis and Adsorption 10, no. 4 (2021): xx. http://dx.doi.org/10.51316/jca.2021.062.

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In this research, Ag-Ag3PO4/Cellulose aerogel composite was synthesized using hydrothermal reduction and freeze-drying methods. By combining the photocatalytic activity of the semiconductor Ag-Ag3PO4 and cellulose aerogel synthesized from agricultural waste sources, the synthesized Ag-Ag3PO4/Cellulose aerogel composite has overcome the disadvantages of pure Ag3PO4 and significantly improved the photocatalytic activity. Structural characteristics, morphology, surface area of the materials were analyzed by X-ray diffraction (XRD), scanning electron microscopy (SEM), N2 adsorption-desorption and

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Duhan, Monika, and Raminder Kaur. "Nano-Structured Polyaniline as a Potential Adsorbent for Methylene Blue Dye Removal from Effluent." Journal of Composites Science 5, no. 1 (2020): 7. http://dx.doi.org/10.3390/jcs5010007.

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The textile sector is one of the major culprits of water pollution, and demands immediate attention. The coloured textile effluent, loaded with toxic dyes, when mixed with waterbodies, may harm aquatic life, plants, animals, and humans. Although polyaniline in its different forms was utilised for the adsorption of different dyes, the pure nano-fibrous form of polyaniline, i.e., PANI nanofibers, have reportedly not been used for the removal of dyes from wastewater. The present study aimed to employ nano-structured polyaniline, in the form of polyaniline nanofibers (base; PNB—polyaniline nanofib

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Asif, Maira, Muhammad Zafar, Parveen Akhter, et al. "Effect of Urea Addition on Anatase Phase Enrichment and Nitrogen Doping of TiO2 for Photocatalytic Abatement of Methylene Blue." Applied Sciences 11, no. 17 (2021): 8264. http://dx.doi.org/10.3390/app11178264.

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TiO2-based materials are commonly employed as photocatalysts for industrial wastewater treatment. The primary reasons of employing TiO2 include cost effectiveness, ready availability, eco-friendliness, non-toxic behavior, and exceptional resistance towards photo-corrosion. However, the wider band gap of pure TiO2 restricts its performance because of its optical absorption of solar light to the ultraviolet (UV) region only, and to some extent of photo-excited charge recombination. In the present work an attempt is made to develop a facile synthesis approach by using urea, a cheap chemical precu

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Resmerita, Ana-Maria, Alexandra Bargan, Corneliu Cojocaru, and Aurica Farcas. "Synthesis, Properties and Adsorption Kinetic Study of New Cross-Linked Composite Materials Based on Polyethylene Glycol Polyrotaxane and Polyisoprene/Semi-Rotaxane." Materials 16, no. 16 (2023): 5594. http://dx.doi.org/10.3390/ma16165594.

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New composite materials were prepared via cross-linking of polyethylene glycol/2-hydroxypropyl-β-cyclodextrins polyrotaxane (PEG/HPβCD) and polyisoprene/HPβCD semi-polyrotaxane (PI/HPβCD SR) with 1,6-hexamethylene diizocyanate (HMDI). Advanced instrumental methods (such WAXS (wide angle X-ray scattering), AFM (atomic force microscopy), SEM (scanning electron microscopy), and thermal and dynamic vapor sorption) were employed for the structural, morphological and thermal characterization of the resulting composite materials. The roughness parameters calculated using AFM indicate a smoother surfa

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