Academic literature on the topic 'Aldol condensation'

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Journal articles on the topic "Aldol condensation"

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Donaire-Arias, Ana, Martin L. Poulsen, Jaime Ramón-Costa, Ana Maria Montagut, Roger Estrada-Tejedor, and José I. Borrell. "Synthesis of Chalcones: An Improved High-Yield and Substituent-Independent Protocol for an Old Structure." Molecules 28, no. 22 (2023): 7576. http://dx.doi.org/10.3390/molecules28227576.

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Chalcones are a type of molecule that can be considered as easily synthesizable through aldol condensation or that can be readily purchased from habitual commercial vendors. However, on reviewing the literature, one realizes that there are no standard procedures for such aldol condensations, that there exists a wide range of alternative methods for the aldol condensation (indicating that such a condensation is not always simple), and that, in many cases, low yields are obtained that involve purifications by recrystallization or column chromatography. To develop a robust standard protocol indep
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Witzig, Reto M., and Christof Sparr. "Synthesis of Enantioenriched Tetra-ortho-3,3′-substituted Biaryls by Small-Molecule-Catalyzed Noncanonical Polyketide Cyclizations." Synlett 31, no. 01 (2019): 13–20. http://dx.doi.org/10.1055/s-0039-1690215.

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The arene-forming aldol condensation is a fundamental reaction in the biosynthesis of aromatic polyketides. Precisely controlled by the polyketide synthases, the highly reactive poly-β-carbonyl substrates are diverged into numerous aromatic natural products by selective cyclization reactions; a fascinating biosynthetic strategy that sparked our interest to investigate atroposelective aldol condensations. In this Account, we contextualize and highlight the ability of small-molecule catalysts to selectively convert noncanonical hexacarbonyl substrates in a double arene-forming aldol condensation
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Fairhurst, Magnus, Muhammad Zeeshan, Bengt Haug, and Annette Bayer. "Aldol Condensations on a 3-Alkylidene-2,5-diketopiperazine: Synthesis of Two Marine Natural Products." Synlett 29, no. 10 (2018): 1303–6. http://dx.doi.org/10.1055/s-0036-1591755.

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The synthesis of two marine natural products containing a 3-alkylidene-6-arylidene-2,5-diketopiperazine scaffold by employing two consecutive aldol condensations starting with 1,4-diacetyl-2,5-diketopiperazine is reported. The target compounds contain a phenol or an imidazole group as aryl substituents, respectively, and suitable conditions for the aldol condensation of 1-acyl-3-alkylidene-2,5-diketopiperazine with the required functionalised aromatic aldehydes were developed. Provided the optimal base was used, introduction of the phenol group did not require use of a protecting group. Boc-pr
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Saito, Susumu, and Hisashi Yamamoto. "Directed Aldol Condensation." Chemistry - A European Journal 5, no. 7 (1999): 1959–62. http://dx.doi.org/10.1002/(sici)1521-3765(19990702)5:7<1959::aid-chem1959>3.0.co;2-7.

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Zhang, Rui, Aleksi Eronen, Xiangze Du, et al. "A catalytic approach via retro-aldol condensation of glucose to furanic compounds." Green Chemistry 23, no. 15 (2021): 5481–86. http://dx.doi.org/10.1039/d1gc01429c.

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The strategy for converting glucose directly to new types of furanic compounds under mild conditions is based on retro-aldol condensation followed by aldol condensation of C2 and C4 fragments with acetylacetone.
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Inegbenebor, Adedayo I., Raphael C. Mordi, and Oluwakayode M. Ogunwole. "Zeolite Catalyzed Aldol Condensation Reactions." International Journal of Applied Sciences and Biotechnology 3, no. 1 (2015): 1–8. http://dx.doi.org/10.3126/ijasbt.v3i1.12291.

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The review is based on the description of zeolite structure, uses, synthesis, and catalytic aldol reaction in aldol condensation. An internal aldolcondensation reaction has been achieved over ZSM-5 zeolite with high silica-alumina ratio at 350oC. It therefore follows that zeolite canfunction as a catalyst in aldol type condensation reactions and that weak acid sites as well as a small number of active sites favor the aldolcondensation reaction of carbonyl compounds. However, the mixed condensation product was found to be favored at temperatures above 300oCand the self-condensation of ethanal t
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Vrbková, Eva, Tereza Kovářová, Eliška Vyskočilová, and Libor Červený. "Heterogeneous catalysts in the aldol condensation of heptanal with cyclopentanone." Progress in Reaction Kinetics and Mechanism 45 (October 10, 2019): 146867831982571. http://dx.doi.org/10.1177/1468678319825713.

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A large number of heterogeneous catalysts were tested in the aldol condensation of heptanal with cyclopentanone. There are many possible products from this aldol condensation, among which the most desired is 2-heptylidenecyclopentanone. As heterogeneous catalysts, the following were tested: caesium modified zeolites, functionalized MCM-41, and single (MgO, CaO, ZnO) and double (Mo–Si, Mg–Al, Zn–Al) metal oxides. The activity of modified zeolites and functionalized zeolites in this aldol condensation was low, whereas single and double metal oxides possessed high activity. The highest selectivit
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Hopf, Henning, Swaminathan Vijay Narayanan, and Peter G. Jones. "Five-membered ring annelation in [2.2]paracyclophanes by aldol condensation." Beilstein Journal of Organic Chemistry 10 (August 28, 2014): 2021–26. http://dx.doi.org/10.3762/bjoc.10.210.

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Under basic conditions 4,5,12,13-tetraacetyl[2.2]paracyclophane (9) cyclizes by a double aldol condensation to provide the two aldols 12 and 15 in a 3:7 ratio. The structures of these compounds were obtained from X-ray structural analysis, spectroscopic data, and mechanistic considerations. On acid treatment 12 is dehydrated to a mixture of the condensed five-membered [2.2]paracyclophane derivatives 18–20, whereas 15 yields a mixture of the isomeric cyclopentadienones 21–23. The structures of these elimination products are also deduced from X-ray and spectroscopic data. The sequence presented
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Khdera, Hadi Aqel. "Design, synthesis and characterization of new azoflavone derivatives through diazotisation - coupling reactions of aromatic amines (sulfanilic acid, 2-amino pyridine)." Current Chemistry Letters 13, no. 3 (2024): 477–82. http://dx.doi.org/10.5267/j.ccl.2024.3.002.

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In this research, new azochalcone derivatives (6, 7) were synthesized by using three methods: the first one is diazotization - coupling method of different aromatic amines (sulfanilic acid, 2-aminopyridine) with chalcone (5), the second, aldol condensation method of azoaryl hydroxyacetophenone compounds with 4-dimethylamino benzaldehyde in presence of sodium hydroxide as a catalyst, the last one is method of aldol condensation of azoaryl hydroxyacetophenone compounds with 4-dimethylaminobenzaldehyde in presence of piperidine as an organic catalyst. The yield was the best by using the aldol con
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Zhang, Ya-Fei, Shao-Jie Yin, Min Zhao, Jun-Qi Zhang, Hai-Yan Li, and Xing-Wang Wang. "Dinuclear zinc-catalyzed desymmetric intramolecular aldolization: an enantioselective construction of spiro[cyclohexanone-oxindole] derivatives." RSC Advances 6, no. 36 (2016): 30683–89. http://dx.doi.org/10.1039/c6ra02296k.

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A bis-ProPhenol zinc complex-catalyzed asymmetric desymmetrizing intramolecular aldol or aldol condensation reaction is reported, which furnishes spiro[cyclohexanone-oxindole] derivatives in good yields with moderate to high enantioselectivities.
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Dissertations / Theses on the topic "Aldol condensation"

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Motsoetsoe, Phalali. "The study of aldol condensation of ketones using zoelites as catalysts." Master's thesis, University of Cape Town, 2001. http://hdl.handle.net/11427/5435.

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Bibliography: leaves 78-82.<br>In this investigation, zeolites HZSM-5 (Si/Al: 22), HZSM-5 (Si/A: 45), H-Beta and H-USY were evaluated as catalysts for aldol condensation reactions of acetone and cyclohexanone and the results compared with those using H₂SO₄. Cross-aldol condensation reactions of acetone and benzaldehyde were also performed.
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Hui, Andrew W. H. "Synthesis of polyfunctionalised cyclopentanes." Thesis, University of Oxford, 1995. http://ora.ox.ac.uk/objects/uuid:c78234b5-92e5-4dd4-8a94-94201f1471b5.

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This thesis describes the syntheses of some polyfunctionalised cyclopentanes via intramolecular aldol condensations of sugar δ-lactone precursors. The known azido carbpcycle (1S,2R,3S,4R,5R)-methyl [5-azido-1,2,3,4- tetrahydrpxy-2,3-O-isopropylidene-cyclopentane] carboxylate was prepared from 2- deoxy-2-iodo-3,4:6,7-di-O-isopropylidene-D-glycero-D-talo-heptono-1,5-lactone in five steps. The key reaction was a base-induced intramolecular aldol cyclisation of a 5- iodo-formyl-2,6-lactone. Borohydride reduction of the methyl ester gave an azido triol. Deprotection followed by reduction of the azi
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Szeto, Peter. "Recent development in indolizidine alkaloids : a synthesis of (-)-slaframine." Thesis, University of Bristol, 1995. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.294850.

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Waters, Gerrit. "Single Stage Aldol Condensation and Hydrogenation of Acetone to MIBK in the Gas Phase." [S.l. : s.n.], 2007. http://digbib.ubka.uni-karlsruhe.de/volltexte/1000007395.

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Liu, Jing. "Synthesis of resveratrol and its analogs, phase-transfer catalyzed asymmetric glycolate aldol reactions, and total synthesis of 8,9-methylamido-geldanamycin /." Diss., CLICK HERE for online access, 2007. http://contentdm.lib.byu.edu/ETD/image/etd1998.pdf.

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Wang, Zheng. "Preparation and Characterization of Rare Earth Elements Modified Hydrotalcites and Their Catalytic Performances for Aldol Condensation Reactions." Thesis, Lyon 1, 2015. http://www.theses.fr/2015LYO10091.

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Résumé anglais uniquement<br>Nowadays there is an urgent need to develop green chemical processes, where the use and generation of toxic substances can be avoided. Indeed, the lignocellulose feedstock destructuration will produce aqueous solutions of ketones or aldehydes and it would be an important breakthrough to develop solid base catalysts capable to promote the aldol condensation. In this thesis, the main results are shown as follows: Magnesium and rare earth mixed oxides (MgReOx), rare earth modified MgAl-HT catalyst were prepared and were evaluated in liquid phase acetone self-aldolizat
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Pokharel, Uttam Raj. "ORGANOMETALLIC HETEROCYCLES AND ACENE-QUINONE COMPLEXES OF RUTHENIUM, IRON AND MANGANESE." UKnowledge, 2012. http://uknowledge.uky.edu/chemistry_etds/6.

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A variety of organometallic-fused heterocycles and acene quinones were prepared and characterized. This work was divided into three parts: first, the synthesis of 5,5-fused heterocyclic complexes of tricarbonylmanganese and (1’,2’,3’,4’,5’-pentamethylcyclopentadienyl)ruthenium; second, the synthesis of 1,2-diacylcyclopentadienyl p-cymene complexes of ruthenium(II); and third, synthesis of cyclopentadienyl-fused polyacenequinone complexes of ruthenium, iron and manganese. The first examples of the convenient, versatile and symmetric cyclopentadienyl-fused heterocycle complexes of (1’,2’,3’,4’,5
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Scognamillo, Sergio [Verfasser]. "Synthesis of bicyclic compounds using sequential hydroformylation and aldol condensation of cyclic ketones with unsaturated side chains / Sergio Scognamillo." Dortmund : Universitätsbibliothek Technische Universität Dortmund, 2004. http://d-nb.info/1011532905/34.

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Pupovac, Kristina [Verfasser]. "Solid acid-catalyzed dehydration of sugars to 5-hydroxymethylfurfural, subsequent aldol condensation and hydrogenation over bifunctional spinel oxides / Kristina Pupovac." Aachen : Hochschulbibliothek der Rheinisch-Westfälischen Technischen Hochschule Aachen, 2014. http://d-nb.info/1051425611/34.

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Villanueva, Sandra Bizarria Lopes. "Preparação e caracterização de hidrotalcitas Mg/AL calcinadas e suas propriedades cataliticas para reações de conversão de etanol." [s.n.], 2005. http://repositorio.unicamp.br/jspui/handle/REPOSIP/267642.

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Orientador: Renato Sprung<br>Tese doutorado) - Universidade Estadual de Campinas, Faculdade de Engenharia Quimica<br>Made available in DSpace on 2018-08-06T18:06:45Z (GMT). No. of bitstreams: 1 Villanueva_SandraBizarriaLopes_D.pdf: 2768871 bytes, checksum: ec40bbcbf8152a8c34f6d7fdd395af83 (MD5) Previous issue date: 2005<br>Resumo: Materiais do tipo hidrotalcita foram sintetizados, calcinados e caracterizados, assim como utilizados na conversão catalítica de etanol. As sínteses foram realizadas com razões molares AI/(AI + Mg) iguais a 0,20; 0,25 e 0,33; em todos os casos os difratogramas de r
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Books on the topic "Aldol condensation"

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Mahrwald, Rainer. Aldol Reactions. Springer Netherlands, 2009.

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Fish, Joshua. Pyrite as a catalyst for aldol condensation reactions. Laurentian University, 2001.

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Mahrwald, Rainer. Aldol Reactions. Springer Netherlands, 2010.

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A, Evans David, and Rainer Mahrwald. Modern Aldol Reactions. Wiley & Sons, Limited, John, 2008.

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Mahrwald, Rainer. Modern Methods in Stereoselective Aldol Reactions. Wiley & Sons, Incorporated, John, 2013.

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Mahrwald, Rainer. Modern Methods in Stereoselective Aldol Reactions. Wiley & Sons, Incorporated, John, 2013.

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Modern Methods In Stereoselective Aldol Reactions. Wiley-VCH Verlag GmbH, 2013.

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Mahrwald, Rainer. Modern Methods in Stereoselective Aldol Reactions. Wiley & Sons, Limited, John, 2013.

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Mahrwald, Rainer. Modern Methods in Stereoselective Aldol Reactions. Wiley & Sons, Incorporated, John, 2013.

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Lee, Hong Myung. I. Catalytic enantioselective decarboxylative thioester aldol reactions ; II. Enantioselective synthesis of (+)-cortistatin A. 2009.

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Book chapters on the topic "Aldol condensation"

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Li, Jie Jack. "Aldol condensation." In Name Reactions. Springer Berlin Heidelberg, 2003. http://dx.doi.org/10.1007/978-3-662-05336-2_3.

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Li, Jie Jack. "Aldol condensation." In Name Reactions. Springer International Publishing, 2014. http://dx.doi.org/10.1007/978-3-319-03979-4_2.

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Li, Jie Jack. "Aldol condensation." In Name Reactions. Springer Berlin Heidelberg, 2009. http://dx.doi.org/10.1007/978-3-642-01053-8_2.

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Li, Jie Jack. "Aldol Condensation." In Name Reactions. Springer International Publishing, 2021. http://dx.doi.org/10.1007/978-3-030-50865-4_2.

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Vollhardt, Peter, and Neil Schore. "Enols, Enolates, and the Aldol Condensation." In Organic Chemistry. Macmillan Learning, 2014. http://dx.doi.org/10.1007/978-1-319-19197-9_18.

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Chien Truong, Cong, Dinesh Kumar Mishra, and Young-Woong Suh. "Aldol Condensation of Furfural with Carbonyl Compounds." In Catalytic Transformations of Sustainable and Versatile Furanic Chemicals. CRC Press, 2024. http://dx.doi.org/10.1201/9781003464839-10.

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Wachter, Nanette M. "Using NMR To Investigate Products of Aldol Reactions: Identifying Aldol Addition versus Condensation Products or Conjugate Addition Products from Crossed Aldol Reactions of Aromatic Aldehydes and Ketones." In ACS Symposium Series. American Chemical Society, 2013. http://dx.doi.org/10.1021/bk-2013-1128.ch007.

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Evans, D. A., J. V. Nelson, and T. R. Taber. "Stereoselective Aldol Condensations." In Topics in Stereochemistry. John Wiley & Sons, Inc., 2007. http://dx.doi.org/10.1002/9780470147221.ch1.

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Kassem, Tarek, X. X. Zhu, and William D. Lubell. "Poly (vinyl alcohol)-graft-Poly (ethylene glycol) Supported Hydroxyproline: Synthesis and Application in the Enantioselective Aldol Condensation." In Advances in Experimental Medicine and Biology. Springer New York, 2009. http://dx.doi.org/10.1007/978-0-387-73657-0_103.

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Labler, Ludvik, August Rüttimann, and Alfred Giger. "Enol Ether and Aldol Condensations." In Carotenoids. Birkhäuser Basel, 1996. http://dx.doi.org/10.1007/978-3-0348-9323-7_4.

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Conference papers on the topic "Aldol condensation"

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Nazarov, Mikhail A., Irina A. Tolmacheva, and Victoria V. Grishko. "The aldol condensation of lupane 30-aldehydes with acetone." In PROCEEDINGS OF INTERNATIONAL CONFERENCE ON RECENT TRENDS IN MECHANICAL AND MATERIALS ENGINEERING: ICRTMME 2019. AIP Publishing, 2020. http://dx.doi.org/10.1063/5.0018052.

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Cahyana, A. H., B. Ardiansah, and M. B. Maloka. "Magnetite - activated chicken eggshell (Fe3O4-ACE) composite for aldol condensation reaction." In PROCEEDINGS OF THE 3RD INTERNATIONAL SYMPOSIUM ON CURRENT PROGRESS IN MATHEMATICS AND SCIENCES 2017 (ISCPMS2017). Author(s), 2018. http://dx.doi.org/10.1063/1.5064075.

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Редькин, Н. А., and Д. А. Корсиков. "DI(4-METHOXYPHENYL)TELLUROXIDE AS A CATALYST IN THE ALDOLS CONDENSATION REACTION." In Инновации и «зелёные» технологии : IV Всероссийская научно-практическая конференция. Crossref, 2024. http://dx.doi.org/10.34830/sounb-conf.2023.14.11.027.

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Работа посвящена изучению реакции альдольной конденсации в присутствии теллурорганического катализатора. Было исследовано протекание реакции между 3,4-диметоксибензальдегидом с п-бромацетофеноном в присутствии гидроксида натрия и ди(4-метоксифенил)теллуроксида. Показано, что на протекание химических реакций конденсации влияют концентрация катализатора, природа растворителя, температура. The work is devoted to the study of the aldol condensation reaction in the presence of an organotellurium catalyst. The reaction between 3,4-dimethoxybenzaldehyde and p-bromoacetophenone in the presence of sodi
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SASAKI, M., T. HAYAKAWA, K. ARAI, and T. ADSCHIRI. "MEASUREMENT OF THE RATE OF RETRO-ALDOL CONDENSATION OF D-XYLOSE IN SUBCRITICAL AND SUPERCRITICAL WATER." In Proceedings of the Seventh International Symposium on Hydrothermal Reactions. WORLD SCIENTIFIC, 2003. http://dx.doi.org/10.1142/9789812705228_0022.

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Stepanova, L. N., and O. B. Belskaya. "Catalysts based on Mg(Li)Al-Layered double hydroxides for the reaction of aldol condensation of furfural with acetone." In OIL AND GAS ENGINEERING (OGE-2021). AIP Publishing, 2021. http://dx.doi.org/10.1063/5.0075026.

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Nebesnyi, Roman, Volodymyr Ivasiv, Iryna Shpyrka, Yuliia Nebesna, Volodymyr Sydorchuk, and Svitlana Khalameida. "Synthesis of acrylic acid via aldol condensation reaction on titanium and mixed vanadium-titanium phosphate catalysts with different porous structure." In 2017 IEEE 7th International Conference "Nanomaterials: Application & Properties" (NAP). IEEE, 2017. http://dx.doi.org/10.1109/nap.2017.8190167.

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Nebesnyi, Roman, Iryna Kubitska, Oksana Orobchuk, Volodymyr Ivasiv, Volodymyr Sydorchuk, and Svitlana Khalameida. "Effect of Support Nature on the Efficiency of B–P–V–W–Ox Catalysts of Acrylic Acid Synthesis with Aldol Condensation of Acetic Acid with Formaldehyde." In Chemical technology and engineering. Lviv Polytechnic National University, 2019. http://dx.doi.org/10.23939/cte2019.01.102.

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El-Molla, Sahar, and Hala Mahmoud. "The Effect of Transition Metal Oxide Dopants on the Structure, Morphology, Surface Texture and Catalytic Properties of FeMgO Nanomaterials Towards Dehydrogenation and Aldol Condensation Reactions." In The 19th International Electronic Conference on Synthetic Organic Chemistry. MDPI, 2015. http://dx.doi.org/10.3390/ecsoc-19-a055.

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