Dissertations / Theses on the topic 'Aluminum alloys Bauschinger effect'
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Jordon, James Brian. "DAMAGE AND STRESS STATE INFLUENCE ON BAUSCHINGER EFFECT IN ALUMINUM ALLOYS." MSSTATE, 2006. http://sun.library.msstate.edu/ETD-db/theses/available/etd-04172006-133053/.
Full textBoger, Richard Keith. "Non-monotonic strain hardening and its constitutive representation." Columbus, Ohio : Ohio State University, 2006. http://rave.ohiolink.edu/etdc/view?acc%5Fnum=osu1138979144.
Full textFielding, S. E. "Fatigue and the Bauschinger effect in ferritic alloys." Thesis, University of Cambridge, 1985. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.304216.
Full textGan, Wei. "Precipitation and strengthening in AL-GE-SI alloys." The Ohio State University, 2006. http://rave.ohiolink.edu/etdc/view?acc_num=osu1135275701.
Full textEaton, James Allen. "Effect of temperature and percent cold work on the mechanical properties of aluminum alloy 3104." Master's thesis, This resource online, 1992. http://scholar.lib.vt.edu/theses/available/etd-03302010-020243/.
Full textKhosla, Maya. "The effect of moisture exposure on pretreated aluminum alloys." Thesis, Virginia Polytechnic Institute and State University, 1988. http://hdl.handle.net/10919/80060.
Full textMaster of Science
Laurent, Michel P. "A continuum surface layer effect in polycrystalline aggregates." Thesis, This resource online, 1994. http://scholar.lib.vt.edu/theses/available/etd-06082009-170819/.
Full textSarkar, Jaydeep. "Characterisation of yield stress anisotropy and the Bauschinger effect in alloys and composites : an application of neutron diffraction." Thesis, University of Cambridge, 1999. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.624289.
Full textGolbahar, Behnam. "Effect of grain refiner-modifier interaction on the performance of A356.2 alloy." Thèse, Chicoutimi : Université du Québec à Chicoutimi, 2008. http://theses.uqac.ca.
Full textLa p. de t. porte en outre: Mémoire présenté à l'Université du Québec à Chicoutimi comme exigence partielle de la maîtrise en ingénierie. CaQQUQ Comprend des réf. bibliogr. (f. 149-155). Publié aussi en version électronique. CaQQUQ
Shang, Lihong. "Effect of microalloying on microstructure and hot working behavior for AZ31 based magnesium alloy." Thesis, McGill University, 2008. http://digitool.Library.McGill.CA:80/R/?func=dbin-jump-full&object_id=115880.
Full textTo include the effect of solidification rate these alloys were cast in different moulds (preheated steel mould, Cu-mould, and water cooled Cu-mould). One-hit compression testing at temperatures between 250°C ∼ 400 °C, strain rates of 0.001, 0.01, 0.1 s-1 and strains from 0.2 up to 1.0, was performed to investigate the basic hot compression behavior, while two-hit compression testing was conducted to determine the static softening behavior. Hot rolling of the microalloyed AZ31 alloys was then carried out to study the effects of microalloying on as-hot rolled structure under two sets of rolling schedules. To investigate the formability of these microalloyed sheets, tensile tests were completed over a temperature range between ambient and 450°C, at strain rates between 0.1 and 0.0003 s-1.
Results show that Ca and Sr act to refine the as cast grain size and the second phases, consistently promoting fine and uniform as-hot rolled grain structure. With regard to grain refinement, calcium has the strongest effect, whereas Ce is most effective for second phase refinement. In addition, microalloying retards grain growth during hot tensile testing. Multiple alloying presents a combined and complementary effect.
A refined and uniform grain structure combined with well dispersed and thermally stable second phases significantly improves the hot formability of AZ31 sheets by promoting dynamic recrystallization (DRX) in the matrix, resisting grain coarsening, and retarding the development of cavitation and necking. Under the superplastic condition of 450°C and 0.0003 s -1, the elongation was improved by 17% with Ca only, 26% with Ca and Ce, 51% with Ca and Sr, and 59% with Ca, Sr and Ce.
Hsu, Emilie Chia Ching 1979. "Effect of deformation conditions on texture and microstructure of magnesium sheet AZ31." Thesis, McGill University, 2006. http://digitool.Library.McGill.CA:80/R/?func=dbin-jump-full&object_id=99768.
Full textIt was observed that only basal slip and twinning contributed to room temperature deformation. As deformation temperature increased, an increase in ductility in Mg contributed to dynamic recrystallization occurring readily at elevated temperatures (≥300°C). Even coarse grain material experienced significant tensile elongation due grain refinement. Depending on temperature and strain rate, different deformation mechanisms were activated and lead to different failure modes (moderate necking, cavity, strong necking). More specifically, deformation at elevated temperature in the low-strain-rate regime with stress exponent n about 2-3 and activation energy close to grain-boundary diffusion of Mg (Q = 92 kJ/mol) is characteristic of GBS. Deformation at elevated temperature in the high strain rate regime showed that the stress exponent increased to a value close to 5 and that the activation energy was consistent with the one for Mg self-diffusion (135 kJ/mol) and for diffusion of Al in Mg (143 kJ/mol). This was indicative of a dislocation creep deformation mechanism. Plus the six-fold symmetric patterns of the {1 100} and {1120} pole figures and the splitting of basal plane distribution are another indication of slip mechanism or of dislocation creep mechanism.
The optimum deformation behavior for AZ31 sheet was found to be for the material with fine grain microstructure. The highest elongation of 265% was obtained with the material having initial grain size of 8 mum. In addition, strain-rate sensitivity, which is a good indication of material's ductility, also was the highest in material with 8 mum grain size. As a common trend, the strain-rate sensitivity increased with decreasing strain rate, increasing temperature and decreasing grain size.
In terms of drawability of AZ31 sheet, the deformation controlled by GBS resulted in a fair drawability/formability property with r-value about 1 whereas a deformation mechanism controlled by dislocation creep showed a good drawability with r-value above 1.5. Due to activation of additional slip systems (non-basal and
Deshpande, Jayesh U. "The effect of mechanical mold vibration on the characteristics of aluminum alloys." Link to electronic thesis, 2006. http://www.wpi.edu/Pubs/ETD/Available/etd-092106-151830/.
Full textKlinter, Andreas. "Wetting behaviour of aluminum alloys on ceramic substrates and its effect on the stability of aluminum foams." Thesis, McGill University, 2010. http://digitool.Library.McGill.CA:8881/R/?func=dbin-jump-full&object_id=92344.
Full textKubiak, Angela Dawne. "Effect of homogenization on high temperature deformation behaviour of AA3xxx aluminum alloys." Thesis, University of British Columbia, 2009. http://hdl.handle.net/2429/7382.
Full textOzdemir, Ozgur. "Effect of strontium on the oxidation behavior of molten aluminum-magnesium alloys." Thesis, McGill University, 2006. http://digitool.Library.McGill.CA:80/R/?func=dbin-jump-full&object_id=102689.
Full textThe effects of various levels of strontium addition on the oxidation behaviour of aluminum-magnesium alloy melts were investigated by monitoring sample weight gains with time using a thermogravimetric balance at 750°C. Sample cross-sections have been examined in detail using Hitachi S-4700 Field Emission Gun Scanning Electron Microscope, and phases formed on the oxide layer and in the alloy morphology were identified by EDS, WDS and low angle X-ray diffraction techniques. It was observed that in the absence of Sr, the Al-Mg samples gained substantial amounts of weight by formation of spinel (MgAl2O4) phase at the oxide-metal interface. Samples containing Sr had significantly lower weight gains. The drop in total weight gain by Sr additions was about 98% in low Mg-containing Al-Mg alloys. This change in oxidation behavior was linked to the presence of a Sr-enriched liquid phase underneath the first formed MgO layer, suppressing the formation of spinel crystals. In addition, spherical equilibrium shapes are found in the different as-cast and oxidized alloys of Al-Mg-Sr.
Crepeau, Paul Noles. "The effect of processing and microstructure on the mechanical properties of aluminum alloy 339-T5." Diss., Georgia Institute of Technology, 1989. http://hdl.handle.net/1853/20193.
Full textRivero, Paz Ive. "The effect of key microstructure features on the machining of an aluminum-silicon casting alloy /." View online, 2010. http://ecommons.txstate.edu/engttad/1.
Full textBalasundaram, Arunkumar. "Effect of stress state and strain on particle cracking damage evolution in 5086 wrought al-alloy." Thesis, Georgia Institute of Technology, 2001. http://hdl.handle.net/1853/14809.
Full textEl, Sebaie Ossama. "L'effet de l'addition du "mischmetal", du taux de refroidissement et du traitement thermique sur la microstructure et la dureté des alliages Al-Si de type 319, 356, et 413 = Effect of mischmetal, cooling rate and heat treatment on the microstructure and hardness of 319, 3456, and 413 Al-Si alloys /." Thèse, Chicoutimi : Université du Québec à Chicoutimi, 2006. http://theses.uqac.ca.
Full textAmmar, Hany. "Effet des imperfections de la coulée sur les propriétés en fatigue des alliages de fonderie aluminium silicium = Effect of casting imperfections on the fatigue properties of aluminum-silicon casting alloys /." Thèse, Chicoutimi : Université du Québec à Chicoutimi, 2006. http://theses.uqac.ca.
Full textGiles, Tanya L. "The effect of friction stir processing on the microstructure and mechanical properties of AF/C458 aluminum lithium alloy." Thesis, Monterey, Calif. : Springfield, Va. : Naval Postgraduate School ; Available from National Technical Information Service, 2005. http://library.nps.navy.mil/uhtbin/hyperion/05Sep%5FGiles.pdf.
Full textCho, Jaeshin. "Effect of microstructure of aluminum alloys on the electromigration-limited reliability of VLSI interconnects." Thesis, Massachusetts Institute of Technology, 1990. http://hdl.handle.net/1721.1/13636.
Full textTash, Mahmoud. "Effect [sic] des paramètres métallurgiques sur le comportement d'usinage des alliages 356 et 319 (étude de forage et de taraudage) /." Thèse, Chicoutimi : Université du Québec à Chicoutimi, 2005. http://theses.uqac.ca.
Full textGomes, Affonseca Netto Nelson. "The Effect of Friction Stir Processing on The Microstructure and Tensile Behavior of Aluminum Alloys." UNF Digital Commons, 2018. https://digitalcommons.unf.edu/etd/790.
Full textAgarwal, Himanshu. "Effect of loading condition, stress state and strain on three-dimensional damage evolution in 6061 wrought Al-alloy." Thesis, Georgia Institute of Technology, 2001. http://hdl.handle.net/1853/14798.
Full textConlon, Kelly Timothy. "The effect of mesoscopic spatial heterogeneity on the plastic deformation of Al-Cu alloys." Thesis, National Library of Canada = Bibliothèque nationale du Canada, 1998. http://www.collectionscanada.ca/obj/s4/f2/dsk1/tape11/PQDD_0004/NQ42838.pdf.
Full textAnderson, Danny. "Effect of the joint addition of aluminum and molybdenum on the precipitation and recrystallization in HSLA steels." Thesis, McGill University, 1986. http://digitool.Library.McGill.CA:80/R/?func=dbin-jump-full&object_id=66207.
Full textSpence, Timothy. "The Effect of Machining Residual Stresses on the Dimensional Stability of Aluminum Alloys used in Optical Systems." Digital WPI, 2010. https://digitalcommons.wpi.edu/etd-dissertations/104.
Full textTodoroff, Peter Kent. "Effect of Turbulence on the Passive Film Growth and Associated Durability of Aluminum Alloys in Simulated Seawater." Thesis, Virginia Tech, 2018. http://hdl.handle.net/10919/83770.
Full textMaster of Science
Enin-Okut, Edu Owominekaje. "The effect of alumina coatings on the oxidation behavior of nickel-base alloys." Thesis, Georgia Institute of Technology, 1998. http://hdl.handle.net/1853/20226.
Full textLi, Jinxia. "THE EFFECT OF MICROSTRUCTURE AND TEXTURE ON HIGH CYCLE FATIGUE PROPERTIES OF AL ALLOYS." UKnowledge, 2007. http://uknowledge.uky.edu/gradschool_diss/522.
Full textSutton, Scott Christopher. "Characterization and Modeling of Lightweight Alloys in the Warm Forming Regime." The Ohio State University, 2018. http://rave.ohiolink.edu/etdc/view?acc_num=osu1524129785253984.
Full textHung, Lie-chung. "Electropolishing of Ti-6A1-4V surgical implant alloy and its effect on corrosion behavior." Thesis, Georgia Institute of Technology, 1994. http://hdl.handle.net/1853/20731.
Full textIyer, A. Vishwanath. "Effect of tool shoulder profile on the axial force and joint strength of friction stir spot welded aluminum alloys." Thesis, Wichita State University, 2012. http://hdl.handle.net/10057/5599.
Full textThesis (M.S.)--Wichita State University, College of Engineering, Dept. of Aerospace Engineering
Meng, Qingjiang. "Effect of cu content on corrosion behavior and chromate conversion coating protection of 7xxx series al alloys." The Ohio State University, 2003. http://rave.ohiolink.edu/etdc/view?acc_num=osu1059574004.
Full textElhadad, Shimaa. "Effect of trace elements on the microstructure and porosity formation in 319 type Al-Si-Cu alloys." Thèse, Chicoutimi : Université du Québec à Chicoutimi, 2003. http://theses.uqac.ca.
Full textKim, Youngseok. "Characterizations of alloying Cu effect on electrochemical reactions of Al-Cu solid solution alloys." Columbus, Ohio : Ohio State University, 2006. http://rave.ohiolink.edu/etdc/view?acc%5Fnum=osu1143130451.
Full textTan, Evren. "The Effect Of Hot-deformation On Mechanical Properties And Age Hardening Characteristics Of Al-mg-si Based Wrought Aluminum Alloys." Master's thesis, METU, 2006. http://etd.lib.metu.edu.tr/upload/12607937/index.pdf.
Full text#945
-Al matrix. Nearly 140HB hardness could be obtained with solutionizing at 530°
C and aging at 175°
C for 8 hours which was determined as the optimum treatment for obtaining peak hardness. When shaping (deformation) was concerned
strength loss was the overall outcome of any hot or cold deformation before solutionizing
which was most probably due to the destruction of the initial microstructure. Improvement in the percent elongation was the promising aspect of this application. Strength loss was increased for samples deformed at higher temperatures and higher reductions.
Taylor, Ryan Chandler. "Effect of a Simulated Butterfly Valve on the Erosion-Corrosion Rate of Nickel Aluminum Bronze Alloys in Highly Turbulent Seawater." Thesis, Virginia Tech, 2018. http://hdl.handle.net/10919/83818.
Full textMaster of Science
Bandi, Raghava. "Effect of Surface Treatment on the Performance of CARALL, Carbon Fiber Reinforced Aluminum Dissimilar Material Joints." Thesis, University of North Texas, 2017. https://digital.library.unt.edu/ark:/67531/metadc1011869/.
Full textMorano, Robert Natale. "Effect of R-ratio on crack closure in Al-Li 2090 T8E41, investigated non-destructively with x-ray microtomography." Thesis, Georgia Institute of Technology, 1998. http://hdl.handle.net/1853/19903.
Full textCevik, Gul. "Investigation Of The Effect Of Orientation And Heat Treatment On The Stress Corrosion Cracking Susceptibility Of 7050 Aluminum Alloy." Master's thesis, METU, 2004. http://etd.lib.metu.edu.tr/upload/3/12605220/index.pdf.
Full text恵子, 名取, and Keiko Natori. "微細複合組織金属の変形機構および塑性加工性に関する研究." Thesis, https://doors.doshisha.ac.jp/opac/opac_link/bibid/BB12867122/?lang=0, 2014. https://doors.doshisha.ac.jp/opac/opac_link/bibid/BB12867122/?lang=0.
Full text博士(工学)
Doctor of Philosophy in Engineering
同志社大学
Doshisha University
Sutton, Kirk C. "An investigation of the effect of steam cleaning and aluminum oxide treatment on the wettability and surface free energy of alloys commonly used in dentistry." Thesis, The University of Texas Health Science Center at San Antonio, 2016. http://pqdtopen.proquest.com/#viewpdf?dispub=10137632.
Full textPurpose: The purpose of this investigation was to evaluate the effect of aluminum oxide airborne particle abrasion, with and without subsequent steam cleaning on the surface free energy of alloys commonly used in dentistry, in an attempt to produce optimal surfaces for adhesion. Materials and Methods: Twelve samples, with dimensions 13 x 18 x 1 mm, of each: Type IV high noble gold alloy, metal ceramic gold-palladium high noble alloy, chrome-cobalt base metal alloy were cast and divested with glass bead airborne particle abrasion. Twelve samples, with dimensions 13 x 18 x 10 mm, of titanium alloy were milled using an Origin Proteus 5x Milling Machine. Samples were treated with 1) Steam cleaning only, 2) Aluminum oxide airborne particle abrasion and 3) Aluminum oxide airborne particle abrasion with subsequent steam cleaning. Contact angle measurements were recorded immediately after each treatment and at 1 and 12 hours, using a goniometer and the sessile drop method. Surface free energy was calculated using VCA Optima XE software.
Results: Steam cleaning treatment showed no significant changes in surface free energy (dynes/cm), compared to pretreatment values for the alloys investigated except Titanium alloy, which showed a modest increase in surface energy (p < 0.05). Aluminum oxide airborne particle abrasion and aluminum oxide airborne particle abrasion with steam cleaning, resulted in an increase in surface free energy for all alloys investigated when compared to pretreatment and steam clean only values. Steam cleaning following airborne particle abrasion produced significantly lower (p<0.001) surface free energy values compared to airborne particle abrasion alone for high noble gold alloy and metal ceramic gold-palladium high noble alloy. Exposure to ambient air following steam cleaning had minimal or non-enduring effects on surface free energy for all alloys investigated except Titanium alloy, which showed a significant decrease (p<0.001) in surface free energy with time of ambient exposure. Exposure to ambient air following airborne particle abrasion with aluminum oxide resulted in a significant decrease (p<0.001) in surface free energy for high noble gold alloy, metal ceramic gold-palladium high noble alloy and chrome-cobalt base metal alloy, however, Titanium alloy showed no ambient exposure effects. Ambient exposure following aluminum oxide airborne particle abrasion with steam cleaning resulted in a significant decrease (p<0.001) in surface free energy for all alloys investigated.
Conclusions: Within the limitations of this study, it was found that aluminum oxide airborne particle abrasion, with and without subsequent steam cleaning, significantly increased the surface free energy of the dental alloys investigated. Steam cleaning following aluminum oxide airborne particle abrasion significantly reduced the surface free energy gain that the high noble alloys experienced with aluminum oxide airborne particle abrasion alone. And finally, exposure to ambient air following aluminum oxide airborne particle abrasion with and without subsequent steam cleaning resulted in a significant decrease in surface free energy for most alloys investigated.
White, Brad Derek. "Cathodoluminescence spectroscopy studies of aluminum gallium nitride and silicon device structures as a function of irradiation and processing." Columbus, Ohio : Ohio State University, 2006. http://rave.ohiolink.edu/etdc/view?acc%5Fnum=osu1141325302.
Full textGhods, Masoud. "Effect of Convection Associated with Cross-section Change during Directional Solidification of Binary Alloys on Dendritic Array Morphology and Macrosegregation." Cleveland State University / OhioLINK, 2017. http://rave.ohiolink.edu/etdc/view?acc_num=csu1500217305972883.
Full textKovarik, Libor. "Microstructural study and modeling of metastable phases and their effect on strenghthening [sic] in Al-Mg-Cu-Si alloying system." The Ohio State University, 2006. http://rave.ohiolink.edu/etdc/view?acc_num=osu1149006665.
Full textDavoodi, Ali. "Mechanistic studies of localized corrosion of Al alloys by high resolution in-situ and ex-situ probing techniques." Doctoral thesis, Stockholm : Kemivetenskap, Kungliga Tekniska högskolan, 2007. http://urn.kb.se/resolve?urn=urn:nbn:se:kth:diva-4588.
Full textZhemchuzhnikova, Daria. "Influence of the extreme grain size reduction on plastic deformation instability in an AlMg and AlMgScZr alloys." Thesis, Université de Lorraine, 2018. http://www.theses.fr/2018LORR0324/document.
Full textThe elaboration of new alloys sustains a strong interest to the phenomenon of unstable plastic flow, or the Portevin–Le Chatelier (PLC) effect, caused by interaction of dislocations with solute atoms. Moreover, this effect attracts interest as a rich example of self-organization in dynamical systems. It is associated with complex patterns of stress serrations related to nucleation and motion of deformation bands in the deforming material, and requires understanding of self-organization of dislocations. Plastic deformation of Al-Mg alloys is prone to instability in a wide range of experimental conditions. For this reason, binary Al-Mg alloys served for a long time as model objects for investigation of the PLC effect. At the same time, the practical use of binary Al-Mg alloys is limited because of their low strength. A significant improvement of their properties can be achieved by additional alloying, in particular, leading to precipitation. Further, extensive grain refinement could be a key technique used to produce tough and high- strength materials. However, there exists very limited and often contradictory information on the PLC instability in fine-grained Al-Mg alloys containing precipitates. The objective of the present thesis was to investigate specific features of the PLC effect in AlMg-based alloys with and without nanoscale particles, both in coarse-grained and fine-grained states, the latter obtained by severe plastic deformation. Using local extensometry methods, particularly the image correlation technique, these studies revealed an unusual persistence of the propagation of deformation bands in alloys with precipitates and/or fine grains. This dynamic mode is observed in a wide range of strain rates, whereas it only appears at high strain rate in model Al-Mg alloys. Moreover, the analysis of statistical distributions of stress drop amplitudes revealed a tendency to power law statistics characteristic of the propagation mode. This phenomenon was attributed to a modification of the spatial coupling between dislocations due to the concentration of internal stresses. The combination of these studies with the acoustic emission analysis uncovered an influence of the microstructure on the competition between a random factor and the dislocation synchronization. Finally, the study by the image correlation made it possible to observe an interrelation between the PLC instability and the neck formation
Mori, Thiago José de Almeida. "Materiais e técnicas para nanoestruturas magnetoelétricas compósitas." Universidade Federal de Santa Maria, 2014. http://repositorio.ufsm.br/handle/1/3928.
Full textHybrid nanostructures which integrate two or more technologically interesting physical properties are fundamental for developing new generations of electronic devices. Exhibiting at least two coupled ferroic orders, multiferroics are an outstanding class of multifunctional materials. Compounds which present coupling between ferromagnetism and ferroelectricity are specially interesting. Although natural multiferroics are rarely found, the possibility of obtaining strain-mediated magnetoelectric coupling in composite structures, by integrating magnetostrictive and piezoelectric layers, paves the way to control electric properties by applying magnetic field or to the electric control of magnetism. Nevertheless, most scientific efforts have been on monophasic compounds or bulk composites. Considering the incorporation of magnetoelectric nanostructures in devices, expanding the scope of the magnetoelectric effect and targetting it to different kinds of applications is needed. Besides new characterization techniques, seeking new alternative materials to the lead-based piezoelectrics or oxide-based magnetostrictives is necessary. Recently, a few works using semiconductors such as ZnO and AlN, or amorphous magnetic alloys such as those based on Co, Fe and Ni, have been reported. In spite of not presenting remarkable piezoelectric and magnetostrictive effects, the features of such materials are promising for high frequency applications, for instance. Considering these issues, four independent surveys are presented. Firstly, the origin of the coupling, latest advances and current scenario of the field are reviewed. Then magnetostriction measurements in thin films are addressed by employing a direct technique based on the cantilever-capacitance method. The goals are to study magnetoelastic properties of some materials whose magnetostriction are not found very often in literature, and to check the reliability of this technique for investigating thin films. In this sense, measurements of some amorphous magnetic alloys mainly based on Co, Fe and Ni are performed. Most samples presents larger magnetoelastic response for magnetic field applied along the magnetization easy axis, as opposed to the theoretically expected. Two investigations on aluminum nitride thin films are reported. Firstly, the growth of AlN films onto several different substrates and buffer layers is studied. Films grown onto glass and polyimide show excellent structural properties for eletromechanical systems and flexible electronics applications. Samples with low residual stress on silicon substrates, suitable for incorporating in existing technologies, are obtained. Secondly, bilayers composed by AlN and ferromagnetic films are investigated. In addition to the structural and morphological properties of the AlN films which are checked, the magnetic characterization of the structures also contributes to design multilayers for exploring the magnetoelectric effect. Finally, problems involving electric fields in scanning probe microscopies are adressed. Surface images of AlN piezoelectric films are systematically acquired. Among other major observations, the possibility of getting reliable piezoresponse images of strongly polarized areas as well as of visualizing ferroelastic domains, is demonstrated. Furthermore, a new microscopy for investigating a sample s ferro and piezoelectric properties is proposed, exploring the direct piezoelectric effect. By utilizing acoustic excitation and electrical detection, the potency of this technique is illustrated with measurements on quartz and AlN surfaces.
Nanoestruturas híbridas, integrando duas ou mais propriedades físicas de grande interesse tecnológico, são fundamentais para o desenvolvimento de novas gerações de dispositivos eletrônicos. Uma classe interessante de materiais multifuncionais são os multiferróicos, que exibem pelo menos duas ordens ferróicas acopladas. Dentre eles, os que apresentam acoplamento entre ferromagnetismo e ferroeletricidade despertam interesse especial. Apesar de serem raros de ocorrer naturalmente, a possibilidade de gerar efeito magnetoelétrico em estruturas compósitas, intermediado pela deformação elástica entre camadas magnetostrictivas e piezoelétricas, abre caminho para que seja possível controlar propriedades elétricas aplicando-se campo magnético, ou propriedades magnéticas aplicando-se campo elétrico. Todavia, a maior parte das pesquisas atuais ainda envolve compostos monofásicos ou compósitos em forma massiva. Tendo em vista a incorporação de nanoestruturas magnetoelétricas em dispositivos, é fundamental ampliar a abrangência do efeito magnetoelétrico e direcioná-lo para diferentes tipos de aplicações. Para isto, além de novas técnicas de caracterização, é necessário buscar-se materiais alternativos aos tradicionais piezoelétricos baseados em chumbo e magnetostrictivos baseados em óxidos. Recentemente tem-se encontrado trabalhos pontuais onde são utilizados piezoelétricos semicondutores como ZnO e AlN, e ligas magnéticas amorfas como as baseadas em Co, Fe e Ni. Mesmo sem apresentar efeitos piezoelétrico e magnetostrictivo com magnitudes notáveis, as características destes materiais são promissoras para aplicações envolvendo altas frequências, por exemplo. Neste necessário, são apresentados quatro estudos independentes entre si. Primeiramente, é realizada uma revisão sobre a origem do acoplamento, os últimos avanços e o panorama atual das pesquisas na área. Em seguida, através de uma técnica direta baseada no método do cantiléver-capacitância, aborda-se o problema das medidas de magnetostricção em amostras na forma de filmes finos. Os objetivos são estudar as propriedades magnetoelásticas em alguns materiais que não são frequentemente abordados pela literatura, e avaliar a potencialidade da técnica para a análise de filmes finos. Para isto, são realizadas medidas principalmente em ligas ferromagnéticas amorfas baseadas em Co, Fe e Ni. Para a maioria das amostras analisadas, a resposta magnetoelástica é maior quando o campo magnético é aplicado na direção do eixo de fácil magnetização, de forma contrária à esperada teoricamente. São apresentadas duas investigações envolvendo filmes finos de nitreto de alumínio. Primeiro é estudado o crescimento de filmes de AlN sobre vários substratos e camadas semente. Filmes crescidos sobre vidro e poliimida apresentam excelentes propriedades estruturais para aplicações em sistemas eletromecânicos e eletrônica flexível. Amostras obtidas com baixos valores de tensão residual, sobre substratos de silício, são interessantes para incorporação em tecnologias existentes. Segundo, são investigadas bicamadas de AlN com filmes ferromagnéticos. Além das propriedades estruturais e morfológicas dos filmes de AlN, a análise das características magnéticas das estruturas contribui para o design de multicamadas que exploram o efeito magnetoelétrico. Finalmente, são abordados problemas em medidas de microscopias de varredura por sonda envolvendo campos elétricos. Imagens da superfície de filmes piezoelétricos de AlN foram coletadas sistematicamente. Entre outras observações importantes, demonstra-se que é possível adquirir imagens confiáveis de piezo-resposta em regiões fortemente polarizadas, e visualizar a formação de domínios ferroelásticos. Também é proposta uma nova técnica de microscopia, para investigar as propriedades ferro e piezoelétricas de uma amostra, explorando o efeito piezoelétrico direto. Utilizando excitação acústica e detecção elétrica, o potencial da nova técnica é demonstrado com imagens de superfícies cristalinas de quartzo e AlN.