Academic literature on the topic 'Amide-assisted synthesis'

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Journal articles on the topic "Amide-assisted synthesis"

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Song, Xizhong, Xiaoyu Liu, Wei Yu, and Yi Jin. "Amide-Assisted Rearrangement of Hydroxyarylformimidoyl Chloride to Diarylurea." Molecules 26, no. 21 (2021): 6437. http://dx.doi.org/10.3390/molecules26216437.

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A novel amide-assisted rearrangement reaction of hydroxybenzimidoyl chloride has been established for the efficient synthesis of 1,3-diphenylurea derivatives. A variety of electronically and sterically different 1,3-diphenylurea derivatives can be obtained in good to excellent yields, and a proposed reaction mechanism is also presented.
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Kamanna, Kantharaju, S. Y. Khatavi, and P. B. Hiremath. "Microwave-assisted One-pot Synthesis of Amide Bond using WEB." Current Microwave Chemistry 7, no. 1 (2020): 50–59. http://dx.doi.org/10.2174/2213335606666190828114344.

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Background: Amide bond plays a key role in medicinal chemistry, and the analysis of bioactive molecular database revealed that the carboxamide group appears in more than 25% of the existing database drugs. Typically amide bonds are formed from the union of carboxylic acid and amine; however, the product formation does not occur spontaneously. Several synthetic methods have been reported for amide bond formation in literature. Present work demonstrated simple and eco-friendly amide bond formation using carboxylic acid and primary amines through in situ generation of O-acylurea. The reaction was
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Willert, Anne, Sherif Zein El Abedin, and Frank Endres. "Synthesis of Silicon and Germanium Nanowire Assemblies by Template-Assisted Electrodeposition from an Ionic Liquid." Australian Journal of Chemistry 67, no. 6 (2014): 875. http://dx.doi.org/10.1071/ch13549.

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We report on the template-assisted synthesis of silicon and germanium nanowires from the air- and water-stable ionic liquid, 1-butyl-1-methylpyrrolidinium bis(trifluoromethylsulfonyl)amide ([Py1,4] TFSA). The synthesis was done by electrochemical deposition in the pores of a commercial track-etched polycarbonate membrane. After chemical dissolution of the polycarbonate membrane in dichloromethane, nanowire assemblies with a regular arrangement were obtained. Different lengths of nanowires can be obtained by varying the applied potential and the time of deposition. The nanowire assemblies were
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Wang, Xiao‐Jian, Qian Yang, Fei Liu, and Qi‐Dong You. "Microwave‐Assisted Synthesis of Amide under Solvent‐free Conditions." Synthetic Communications 38, no. 7 (2008): 1028–35. http://dx.doi.org/10.1080/00397910701860372.

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Manikandan, Rajendran, and Masilamani Jeganmohan. "Recent advances in the ruthenium-catalyzed hydroarylation of alkynes with aromatics: synthesis of trisubstituted alkenes." Organic & Biomolecular Chemistry 13, no. 42 (2015): 10420–36. http://dx.doi.org/10.1039/c5ob01472g.

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The hydroarylation of alkynes with amide, azole, carbamate, phosphine oxide, amine, acetyl, sulfoxide and sulphur substituted aromatics in the presence of a ruthenium catalyst via chelation-assisted C–H bond activation is discussed.
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Helliwell, Philip A., Ruth E. Fake, Kevin G. Kerr, Barbara Santry, Austen Speakman, and Anne Routledge. "Microwave-Assisted Synthesis of Aryl Amide Bonds on Solid Phase." Synthetic Communications 40, no. 20 (2010): 3058–66. http://dx.doi.org/10.1080/00397910903370618.

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Priyosetyoko, Priyosetyoko, Suzery Meiny, and Widayat Widayat. "Calcium reduction of stingray (Himantura gerrardi) bones with EDTA disodium salt assisted ultrasound." E3S Web of Conferences 605 (2025): 03061. https://doi.org/10.1051/e3sconf/202560503061.

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Calcium reduction of bone is crucial to collagen purification and gelatin synthesis from fish bones. Research on the effect of immersion time on the reduction of calcium products assisted by ultrasound at 950 W 25 kHz on the bones of Himantura gerrardi stingrays has been carried out. This study used 0.1 M EDTA disodium salt as a chelating agent to form complex Ca-EDTA compounds with variations in immersion time for 0, 2, 4, 6, 10, 16, 18, 20, 22, and 24 hours. The results of X-ray fluorescence (XRF) analysis showed that soaking for 24 hours produced calcium at a level of 1.16%, which was the l
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Park, Mi-Sun, Hyun-Sik Oh, Hyeongjin Cho, and Keun-Hyeung Lee. "Microwave-assisted solid-phase synthesis of pseudopeptides containing reduced amide bond." Tetrahedron Letters 48, no. 6 (2007): 1053–57. http://dx.doi.org/10.1016/j.tetlet.2006.11.151.

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Thalluri, Kishore, Ashim Paul, Srinivasa Rao Manne, Dharm Dev, and Bhubaneswar Mandal. "Microwave assisted chemoselective organocatalytic peptide alcohol synthesis from C-terminal amide." RSC Adv. 4, no. 88 (2014): 47841–47. http://dx.doi.org/10.1039/c4ra09091h.

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Suresh, Kumar Verma, and Kishor Verma Kamal. "Green Synthesis, Magnetic, Spectroscopic and in-vitro Antimicrobial Studies of Transition Metal Complexes with Biologically Active O,O-Donor Ligand Containing Amide Moiety." Pharmaceutical and Chemical Journal 9, no. 1 (2022): 77–83. https://doi.org/10.5281/zenodo.13970292.

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The present study deals with transition metal complexes of an <em>O,O</em>-chelating ligand possessing amide moity. The Ligand 2-Hydroxypyridine-3-carboxamide(L) and its new mononuclear complexes [M(H<sub>2</sub>O]<sub>2</sub>L<sub>2</sub>]Cl<sub>2</sub> with Co(II), Ni(II) and Cu(II) have been prepared using&nbsp; microwave assisted synthesis, an environmentally benign method of synthesis.&nbsp; The ligand and the metal complexes have been characterized by elemental analyses, magnetic susceptibility measurements and spectroscopic methods like Fourier Transform-Infrared spectroscopy and UV-vis
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Dissertations / Theses on the topic "Amide-assisted synthesis"

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Orrling, Kristina M. "On the Versatility of Microwave-Assisted Chemistry : Exemplified by Applications in Medicinal Chemistry, Heterocyclic Chemistry and Biochemistry." Doctoral thesis, Uppsala : Acta Universitatis Upsaliensis, 2009. http://urn.kb.se/resolve?urn=urn:nbn:se:uu:diva-101356.

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Book chapters on the topic "Amide-assisted synthesis"

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Taber, Douglass F. "The Reisman Synthesis of (–)-Maoecrystal Z." In Organic Synthesis. Oxford University Press, 2015. http://dx.doi.org/10.1093/oso/9780190200794.003.0087.

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(–)-Maoecrystal Z 3 was isolated as a minor constituent from the Chinese medicinal herb Isodon eriocalyx. The synthesis of 3 reported (J. Am. Chem. Soc. 2011, 133, 14964) by Sarah E. Reisman of the California Institute of Technology, featuring as a key step the cyclization of 1 to 2, is a tribute to the power of one-electron reduction for carbon–carbon bond construction. The synthesis began with a Myers alkylation to prepare 6. The amide was reduced to the alcohol with the convenient ammonia–borane complex, and the alcohol was carried on to the iodide 7. The first carbocyclic ring of 3 was pre
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Conference papers on the topic "Amide-assisted synthesis"

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Joshi, Gaurav, K. K. Verma, D. D. Gudesaria, and N. Bhojak. "Microwave assisted synthesis, spectral, magnetic and bioevolution of few Mn (II)-amide complexes." In INTERNATIONAL CONFERENCE ON CONDENSED MATTER AND APPLIED PHYSICS (ICC 2015): Proceeding of International Conference on Condensed Matter and Applied Physics. Author(s), 2016. http://dx.doi.org/10.1063/1.4946719.

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