To see the other types of publications on this topic, follow the link: Amide-assisted synthesis.

Journal articles on the topic 'Amide-assisted synthesis'

Create a spot-on reference in APA, MLA, Chicago, Harvard, and other styles

Select a source type:

Consult the top 50 journal articles for your research on the topic 'Amide-assisted synthesis.'

Next to every source in the list of references, there is an 'Add to bibliography' button. Press on it, and we will generate automatically the bibliographic reference to the chosen work in the citation style you need: APA, MLA, Harvard, Chicago, Vancouver, etc.

You can also download the full text of the academic publication as pdf and read online its abstract whenever available in the metadata.

Browse journal articles on a wide variety of disciplines and organise your bibliography correctly.

1

Song, Xizhong, Xiaoyu Liu, Wei Yu, and Yi Jin. "Amide-Assisted Rearrangement of Hydroxyarylformimidoyl Chloride to Diarylurea." Molecules 26, no. 21 (2021): 6437. http://dx.doi.org/10.3390/molecules26216437.

Full text
Abstract:
A novel amide-assisted rearrangement reaction of hydroxybenzimidoyl chloride has been established for the efficient synthesis of 1,3-diphenylurea derivatives. A variety of electronically and sterically different 1,3-diphenylurea derivatives can be obtained in good to excellent yields, and a proposed reaction mechanism is also presented.
APA, Harvard, Vancouver, ISO, and other styles
2

Kamanna, Kantharaju, S. Y. Khatavi, and P. B. Hiremath. "Microwave-assisted One-pot Synthesis of Amide Bond using WEB." Current Microwave Chemistry 7, no. 1 (2020): 50–59. http://dx.doi.org/10.2174/2213335606666190828114344.

Full text
Abstract:
Background: Amide bond plays a key role in medicinal chemistry, and the analysis of bioactive molecular database revealed that the carboxamide group appears in more than 25% of the existing database drugs. Typically amide bonds are formed from the union of carboxylic acid and amine; however, the product formation does not occur spontaneously. Several synthetic methods have been reported for amide bond formation in literature. Present work demonstrated simple and eco-friendly amide bond formation using carboxylic acid and primary amines through in situ generation of O-acylurea. The reaction was
APA, Harvard, Vancouver, ISO, and other styles
3

Willert, Anne, Sherif Zein El Abedin, and Frank Endres. "Synthesis of Silicon and Germanium Nanowire Assemblies by Template-Assisted Electrodeposition from an Ionic Liquid." Australian Journal of Chemistry 67, no. 6 (2014): 875. http://dx.doi.org/10.1071/ch13549.

Full text
Abstract:
We report on the template-assisted synthesis of silicon and germanium nanowires from the air- and water-stable ionic liquid, 1-butyl-1-methylpyrrolidinium bis(trifluoromethylsulfonyl)amide ([Py1,4] TFSA). The synthesis was done by electrochemical deposition in the pores of a commercial track-etched polycarbonate membrane. After chemical dissolution of the polycarbonate membrane in dichloromethane, nanowire assemblies with a regular arrangement were obtained. Different lengths of nanowires can be obtained by varying the applied potential and the time of deposition. The nanowire assemblies were
APA, Harvard, Vancouver, ISO, and other styles
4

Wang, Xiao‐Jian, Qian Yang, Fei Liu, and Qi‐Dong You. "Microwave‐Assisted Synthesis of Amide under Solvent‐free Conditions." Synthetic Communications 38, no. 7 (2008): 1028–35. http://dx.doi.org/10.1080/00397910701860372.

Full text
APA, Harvard, Vancouver, ISO, and other styles
5

Manikandan, Rajendran, and Masilamani Jeganmohan. "Recent advances in the ruthenium-catalyzed hydroarylation of alkynes with aromatics: synthesis of trisubstituted alkenes." Organic & Biomolecular Chemistry 13, no. 42 (2015): 10420–36. http://dx.doi.org/10.1039/c5ob01472g.

Full text
Abstract:
The hydroarylation of alkynes with amide, azole, carbamate, phosphine oxide, amine, acetyl, sulfoxide and sulphur substituted aromatics in the presence of a ruthenium catalyst via chelation-assisted C–H bond activation is discussed.
APA, Harvard, Vancouver, ISO, and other styles
6

Helliwell, Philip A., Ruth E. Fake, Kevin G. Kerr, Barbara Santry, Austen Speakman, and Anne Routledge. "Microwave-Assisted Synthesis of Aryl Amide Bonds on Solid Phase." Synthetic Communications 40, no. 20 (2010): 3058–66. http://dx.doi.org/10.1080/00397910903370618.

Full text
APA, Harvard, Vancouver, ISO, and other styles
7

Priyosetyoko, Priyosetyoko, Suzery Meiny, and Widayat Widayat. "Calcium reduction of stingray (Himantura gerrardi) bones with EDTA disodium salt assisted ultrasound." E3S Web of Conferences 605 (2025): 03061. https://doi.org/10.1051/e3sconf/202560503061.

Full text
Abstract:
Calcium reduction of bone is crucial to collagen purification and gelatin synthesis from fish bones. Research on the effect of immersion time on the reduction of calcium products assisted by ultrasound at 950 W 25 kHz on the bones of Himantura gerrardi stingrays has been carried out. This study used 0.1 M EDTA disodium salt as a chelating agent to form complex Ca-EDTA compounds with variations in immersion time for 0, 2, 4, 6, 10, 16, 18, 20, 22, and 24 hours. The results of X-ray fluorescence (XRF) analysis showed that soaking for 24 hours produced calcium at a level of 1.16%, which was the l
APA, Harvard, Vancouver, ISO, and other styles
8

Park, Mi-Sun, Hyun-Sik Oh, Hyeongjin Cho, and Keun-Hyeung Lee. "Microwave-assisted solid-phase synthesis of pseudopeptides containing reduced amide bond." Tetrahedron Letters 48, no. 6 (2007): 1053–57. http://dx.doi.org/10.1016/j.tetlet.2006.11.151.

Full text
APA, Harvard, Vancouver, ISO, and other styles
9

Thalluri, Kishore, Ashim Paul, Srinivasa Rao Manne, Dharm Dev, and Bhubaneswar Mandal. "Microwave assisted chemoselective organocatalytic peptide alcohol synthesis from C-terminal amide." RSC Adv. 4, no. 88 (2014): 47841–47. http://dx.doi.org/10.1039/c4ra09091h.

Full text
APA, Harvard, Vancouver, ISO, and other styles
10

Suresh, Kumar Verma, and Kishor Verma Kamal. "Green Synthesis, Magnetic, Spectroscopic and in-vitro Antimicrobial Studies of Transition Metal Complexes with Biologically Active O,O-Donor Ligand Containing Amide Moiety." Pharmaceutical and Chemical Journal 9, no. 1 (2022): 77–83. https://doi.org/10.5281/zenodo.13970292.

Full text
Abstract:
The present study deals with transition metal complexes of an <em>O,O</em>-chelating ligand possessing amide moity. The Ligand 2-Hydroxypyridine-3-carboxamide(L) and its new mononuclear complexes [M(H<sub>2</sub>O]<sub>2</sub>L<sub>2</sub>]Cl<sub>2</sub> with Co(II), Ni(II) and Cu(II) have been prepared using&nbsp; microwave assisted synthesis, an environmentally benign method of synthesis.&nbsp; The ligand and the metal complexes have been characterized by elemental analyses, magnetic susceptibility measurements and spectroscopic methods like Fourier Transform-Infrared spectroscopy and UV-vis
APA, Harvard, Vancouver, ISO, and other styles
11

Gharib, Maniya, Vahid Safarifard, and Ali Morsali. "Ultrasound assisted synthesis of amide functionalized metal-organic framework for nitroaromatic sensing." Ultrasonics Sonochemistry 42 (April 2018): 112–18. http://dx.doi.org/10.1016/j.ultsonch.2017.11.009.

Full text
APA, Harvard, Vancouver, ISO, and other styles
12

Grbović, Ljubica, Bojana Radovan Vasiljević, Ksenija Pavlović, et al. "Microwave-assisted synthesis of biologically active amide derivatives of naphthenic acids under neat conditions." Macedonian Journal of Chemistry and Chemical Engineering 37, no. 1 (2018): 13. http://dx.doi.org/10.20450/mjcce.2018.1371.

Full text
Abstract:
Within the field of green chemistry, a noticeable results were obtained in the solvent-free synthesis of amide derivatives of naphthenic acids under microwave irradiation. Naphthenic acid amides, anilides, and morpholides were synthesized directly from free carboxylic acids and amines in the absence of solvent and catalyst under high-temperature heating in a closed-vessel system of microwave reactor. With this new and efficient method, different primary, secondary, and tertiary amide derivatives of naphthenic acids were obtained in good to excellent yields. Synthesized derivatives were assayed
APA, Harvard, Vancouver, ISO, and other styles
13

T., Bansal, Sharma S., Gaba J., and Behal R. "Eco-friendly synthesis of amides and their microbial activity." Journal of Indian Chemical Society Vol. 92, Feb 2015 (2015): 255–61. https://doi.org/10.5281/zenodo.5602803.

Full text
Abstract:
Department of Chemistry, Punjab Agricultural University, Ludhiana-141 004, Punjab, India E-mail : taniabansal2@yahoo.com, jyotgcw@gmail.com Department of Plant Breeding and Genetics, Punjab Agricultural University, Ludhiana-141 004, Punjab, India <em>E-mail</em> : sunita_sharma@pau.edu <em>Manuscript received online 23 July 2014, accepted 18 August 2014</em> A series of <em>N</em>-(1,5-dimethyl-3-oxo-2-phenyl-2,3-dihydro-1<em>H</em>-pyrazol-4-yl)-2-phenoxy-3-phenylacrylamide 5a-e, 1-morpholino-2-phenoxy-3-phenyl prop-2-ene-1-one 7a-e and 2-phenoxy-3-phenyl-N-(4<em>H</em>-1,2,4-triazole-4-yl)ac
APA, Harvard, Vancouver, ISO, and other styles
14

Wojtkielewicz, Agnieszka, Damian Pawelski, Przemysław Bazydło, Aneta Baj, Stanisław Witkowski та Jacek W. Morzycki. "A Convenient Synthesis of (16S,20S)-3β-Hydroxy-5α-pregnane-20,16-carbolactam and Its N-alkyl Derivatives". Molecules 25, № 10 (2020): 2377. http://dx.doi.org/10.3390/molecules25102377.

Full text
Abstract:
A concise synthesis of (16S,20S)-3β-hydroxy-5α-pregnane-20,16-carbolactam from tigogenin via the corresponding lactone is described. The most efficient synthetic route consisted of the lactone ring-opening with aminoalane reagent followed by PDC or Dess-Martin oxidation. The oxo-amide obtained was subjected to cyclization with Et3SiH/TFA or Et3SiH/Bi(TfO)3. Alternately, the lactone was converted first to the oxo-acid, which was then subjected to the microwave-assisted reductive amination. N-Alkyl derivatives were also obtained in a similar way.
APA, Harvard, Vancouver, ISO, and other styles
15

Al-Salman, Rihab, Xiangdong Meng, Jiupeng Zhao, et al. "Semiconductor nanostructures via electrodeposition from ionic liquids." Pure and Applied Chemistry 82, no. 8 (2010): 1673–89. http://dx.doi.org/10.1351/pac-con-09-09-25.

Full text
Abstract:
The fascinating properties of ionic liquids make it possible to synthesize semiconductor nanostructures via a simple and low-cost electrochemical pathway. The present paper summarizes our recent work on the synthesis of Si, Ge, and SixGe1–x nanostructures from ionic liquids: thin films, nanowires and photonic crystals. We also introduce our first results on the template-assisted electrodeposition of SixGe1–x photonic crystals from 1-ethyl-3-methylimidazolium bis(trifluoromethylsulfonyl)amide ([EMIm]Tf2N) ionic liquid, and some optical measurements on the previously prepared Ge photonic crystal
APA, Harvard, Vancouver, ISO, and other styles
16

Bhojak, N., D. D. Gudasaria, N. Khiwani, and R. Jain. "Microwave Assisted Synthesis Spectral and Antibacterial Investigations on Complexes of Mn(II) With Amide Containing Ligands." E-Journal of Chemistry 4, no. 2 (2007): 232–37. http://dx.doi.org/10.1155/2007/785626.

Full text
Abstract:
The present research work describes the synthesis, spectral and antibacterial studies on the complexes of Mn(II) with amide group containing ligands. Synthesis of complexes has been carried out by conventional method as well as by microwave method. The complexes have been characterized on the basis of elemental analysis, infrared, electronic spectra and magnetic susceptibility studies. The diffuse reflectance spectrums of the complexes show bands in the region 20,000 cm-1to 26,000 cm-1assignable to6A1g→4T2gand6A1g→4E1gtransitions. These are also typical of tetrahedral environment around the ma
APA, Harvard, Vancouver, ISO, and other styles
17

Wang, Chao, Li Zhang, Changpeng Chen, Jian Han, Yingming Yao та Yingsheng Zhao. "Oxalyl amide assisted palladium-catalyzed synthesis of pyrrolidones via carbonylation of γ-C(sp3)–H bonds of aliphatic amine substrates". Chemical Science 6, № 8 (2015): 4610–14. http://dx.doi.org/10.1039/c5sc00519a.

Full text
APA, Harvard, Vancouver, ISO, and other styles
18

Ikejiri, Masahiro, Kazuyuki Miyashita, Atsufumi Watanabe, Mari Katsuda, Mayu Funakoshi, and Aki Fujisaka. "Acetate/Acetic Acid-Assisted One-Pot Synthesis of (Diarylmethylene)imidazolone from Amide or Thioamide." HETEROCYCLES 102, no. 3 (2021): 516. http://dx.doi.org/10.3987/com-20-14396.

Full text
APA, Harvard, Vancouver, ISO, and other styles
19

Behrens, Karsten, Suvendu Sekhar Mondal, Robert Nöske, et al. "Microwave-Assisted Synthesis of Defects Metal-Imidazolate-Amide-Imidate Frameworks and Improved CO2 Capture." Inorganic Chemistry 54, no. 20 (2015): 10073–80. http://dx.doi.org/10.1021/acs.inorgchem.5b01952.

Full text
APA, Harvard, Vancouver, ISO, and other styles
20

Peng, Xingzhou, Marc Behl, Pengfei Zhang, Magdalena Mazurek-Budzyńska, Yakai Feng, and Andreas Lendlein. "Synthesis and Characterization of Multiblock Poly(Ester-Amide-Urethane)s." MRS Advances 2, no. 47 (2017): 2551–59. http://dx.doi.org/10.1557/adv.2017.486.

Full text
Abstract:
ABSTRACTIn this study, a multiblock copolymer containing oligo(3-methyl-morpholine-2,5-dione) (oMMD) and oligo(3-sec-butyl-morpholine-2,5-dione) (oBMD) building blocks obtained by ring-opening polymerization (ROP) of the corresponding monomers, was synthesized in a polyaddition reaction using an aliphatic diisocyanate. The multiblock copolymer (pBMD-MMD) provided a molecular weight of 40,000 g·mol−1, determined by gel permeation chromatography (GPC). Incorporation of both oligodepsipeptide segments in multiblock copolymers was confirmed by 1H NMR and Matrix Assisted Laser Desorption/Ionization
APA, Harvard, Vancouver, ISO, and other styles
21

Swamy, T., B. Maheshwar Rao, J. S. Yadav, V. Ravinder, B. Sridhar, and B. V. Subba Reddy. "Microwave-assisted, ruthenium-catalyzed intramolecular amide-alkyne annulation for the rapid synthesis of fused tricyclic isoquinolinones." RSC Advances 5, no. 84 (2015): 68510–14. http://dx.doi.org/10.1039/c5ra11133a.

Full text
APA, Harvard, Vancouver, ISO, and other styles
22

Yang, Shang-Feng, Pei Li, Zi-Lin Fang, et al. "A one-pot electrochemical synthesis of 2-aminothiazoles from active methylene ketones and thioureas mediated by NH4I." Beilstein Journal of Organic Chemistry 18 (September 15, 2022): 1249–55. http://dx.doi.org/10.3762/bjoc.18.130.

Full text
Abstract:
The electrochemical preparation of 2-aminothiazoles has been achieved by the reaction of active methylene ketones with thioureas assisted by ᴅʟ-alanine using NH4I as a redox mediator. The electrochemical protocol proceeds in an undivided cell equipped with graphite plate electrodes under constant current conditions. Various active methylene ketones, including β-keto ester, β-keto amide, β-keto nitrile, β-keto sulfone and 1,3-diketones, can be converted to the corresponding 2-aminothiazoles. Mechanistically, the in situ generated α-iodoketone was proposed to be the key active species.
APA, Harvard, Vancouver, ISO, and other styles
23

Alborzi, Ali Reza, Saeed Zahmatkesh, Karim Zare, and Javad Sadeghi. "Optically active: microwave-assisted synthesis and characterization of l-lysine-derived poly (amide-imide)s." Amino Acids 41, no. 2 (2010): 485–94. http://dx.doi.org/10.1007/s00726-010-0767-0.

Full text
APA, Harvard, Vancouver, ISO, and other styles
24

Khadilkar, Bhushan M., and Virendra R. Madyar. "TOTALLY SELECTIVE DRY MICROWAVE ASSISTED AMIDE SYNTHESIS BY HYDRATION OF NITRILE USING SILICA SUPPORTED MnO2REAGENT." Synthetic Communications 32, no. 11 (2002): 1731–34. http://dx.doi.org/10.1081/scc-120004268.

Full text
APA, Harvard, Vancouver, ISO, and other styles
25

Awasthi, Neeraj Praphulla, and Rajinder Pal Singh. "Microwave-assisted facile and convenient synthesis of fatty acid amide (erucamide): Chemical-catalyzed rapid method." European Journal of Lipid Science and Technology 111, no. 2 (2009): 202–6. http://dx.doi.org/10.1002/ejlt.200800186.

Full text
APA, Harvard, Vancouver, ISO, and other styles
26

Pal, Ashish Kumar, and Raja Sundararajan. "ASSESSMENT OF ARSENIC, MERCURY, CADMIUM, LEAD, AND PALLADIUM IN ROPIVACAINE HYDROCHLORIDE MONOHYDRATE BY AN INDUCTIVELY COUPLED PLASMA MASS SPECTROMETER (ICPMS)." RASAYAN Journal of Chemistry 15, no. 04 (2022): 2612–19. http://dx.doi.org/10.31788/rjc.2022.1548093.

Full text
Abstract:
Ropivacaine hydrochloride monohydrate is prolonged acting amide local anesthesia. In its guidelines, the International Conference on Harmonization notes that elemental inorganic contaminants may enter active pharmaceutical ingredients and drug formulations from various causes. Arsenic, mercury, cadmium, mercury, and lead are examples of class 1 elements, which occur as inorganic contaminants that have hazardous effects on the human body. During the synthesis of ropivacaine hydrochloride monohydrate, palladium assisted as a catalyst. A simple, reliable, and reproducible inductively-coupled plas
APA, Harvard, Vancouver, ISO, and other styles
27

Rappenglück, Sebastian, Karin Niessen, Thomas Seeger, Franz Worek, Horst Thiermann, and Klaus Wanner. "Regioselective and Transition-Metal-Free Addition of tert-Butyl Magnesium Reagents to Pyridine Derivatives: A Convenient Method for the Synthesis of 3-Substituted 4-tert-Butylpyridine Derivatives." Synthesis 49, no. 17 (2017): 4055–64. http://dx.doi.org/10.1055/s-0036-1589025.

Full text
Abstract:
A variety of 3,4-disubstituted pyridine derivatives with a tert-butyl group in the 4-position were synthesized in a transition-metal-free, two-step reaction sequence from 3-substituted pyridine precursors. Highly regioselective addition of t-Bu2Mg to TIPS-activated pyridines and an efficient microwave-assisted aromatization with sulfur as oxidant afforded the desired 3,4-disubstituted pyridine derivatives in moderate to excellent yields. The method is compatible with many functional groups such as ester, amide, halide, nitrile or alkyne groups present in the 3-position.
APA, Harvard, Vancouver, ISO, and other styles
28

Khaldoun, Khadidja, Abdelmounaim Safer, Salima Saidi-Besbes, Bertrand Carboni, Rémy Le Guével, and François Carreaux. "An Efficient Solvent-Free Microwave-Assisted Synthesis of Cinnamamides by Amidation Reaction Using Phenylboronic Acid/Lewis Base Co-catalytic System." Synthesis 51, no. 20 (2019): 3891–900. http://dx.doi.org/10.1055/s-0039-1690132.

Full text
Abstract:
A microwave-assisted dehydrative amide condensation reaction is reported as an efficient access to cinnamamide derivatives under solvent-free conditions. This protocol between conjugated carboxylic acids and amines is based on the use of a co-catalytic system, including the presence of the commercially available phenylboronic acid and 4-(N,N-dimethylamino)pyridine N-oxide (DMAPO), with a complete chemoselectivity in favor of the corresponding α,β-unsaturated amides. The implementation of the reaction needs no special precaution, and less reactive amines, such as substituted anilines, are also
APA, Harvard, Vancouver, ISO, and other styles
29

Aljuhani, Ateyatallah, Mohamed Reda Aouad, Nadjet Rezki, et al. "Novel pyridinium based ionic liquids with amide tethers: Microwave assisted synthesis, molecular docking and anticancer studies." Journal of Molecular Liquids 285 (July 2019): 790–802. http://dx.doi.org/10.1016/j.molliq.2019.04.143.

Full text
APA, Harvard, Vancouver, ISO, and other styles
30

Mallakpour, Shadpour E., Abdol-Reza Hajipour, and Khalil Faghihi. "Microwave-assisted synthesis of optically active poly(amide–imide)s with benzophenone and l-alanine linkages." European Polymer Journal 37, no. 1 (2001): 119–24. http://dx.doi.org/10.1016/s0014-3057(00)00097-5.

Full text
APA, Harvard, Vancouver, ISO, and other styles
31

B., D. Mistry, R. Desai K., and B. Rana P. "Conventional and microwave irradiation technique for the synthesis of some pyrimidine and pyrazoline derivative from 1-{4'-[(4"-methylpiperazinyl)diazenyl] phenyl}-3-(substitutedphenyl)prop-2-en-1-one and studies of their antimicrobial activity." Journal of Indian Chemical Society Vol. 88, Jun 2011 (2011): 869–77. https://doi.org/10.5281/zenodo.5771335.

Full text
Abstract:
Department of Chemistry, B. K. M. Science College, Valsad-396 001, Gujarat, India <em>E-mail</em> : bhavana_mistryll@yahoo.co.in <em>Manuscript received 08 March 2010, revised 21 September 2010, accepted 05 October 2010</em> A series of compounds namely 6-{4&#39;-((4&quot;-methylpiperazinyl)diazenyl]phenyl}-4-(substitutedphenyl)pyrimidine 2-yl-amide (Ja-j), 3-{4&#39; -[(4&quot; -methylpiperazinyl)diazenyl]phenyl}-5-(substitutedphenyl)pyrazole (4a-j) and 3-{ 4&#39;-((4<em>&quot;</em>methylpiperazinyl) diazenyl]phenyl}-5-(substitutedphenyl)pyrazolecarboxamide (Sa-j) have been prepared by the rea
APA, Harvard, Vancouver, ISO, and other styles
32

Vaithiyalingam, Dhanamoorthy, Malini Nelson, Muniyappan Chinnamadhaiyan, and Siva Ayyanar. "Microwave Assisted Synthesis of 3, 5-Disubstituted 1, 2, 4-Triazole Based Piperazine Amide and Urea Derivatives." Trends Journal of Sciences Research 01, no. 01 (2021): 7–17. http://dx.doi.org/10.31586/ojc.2021.010102.

Full text
APA, Harvard, Vancouver, ISO, and other styles
33

Azizoglu, Sevil S., Seref Kaplan, Gulsen Ozturk, Yilmaz Turgut, and Mahmut Togrul. "Microwave-assisted synthesis of novel amide based chiral tripodal receptors for recognition of cation and anion sensors." Arkivoc 2016, no. 4 (2016): 44–58. http://dx.doi.org/10.3998/ark.5550190.p009.434.

Full text
APA, Harvard, Vancouver, ISO, and other styles
34

Ayush, Madhuram, and Shilpa. "Corrosion Inhibition Activity of Transition Metal (II) Complexes of a Bidentate Ligand for Mild Steel in Acidic Medium Pertinent to Green Chemistry." International Research Journal of Pure and Applied Chemistry 26, no. 1 (2025): 49–65. https://doi.org/10.9734/irjpac/2025/v26i1897.

Full text
Abstract:
A new bidentate amide ligand 2-(2-acetylaminophenyl)-N-benzothiazol-2-oxo-acetamide (apba) and its complexes with Co2+, Ni2+ and Cu2+ have been synthesized using microwave-assisted synthesis (MAS) under mild conditions with excellent yields (up to 85%) in shorter reaction times (in 5-10 min). All compounds have been characterized by spectro-analytical techniques. The corrosion inhibitory effects of the investigated ligand and its metal (II) complexes on mild steel were studied in 1.0 M HCl at different concentrations using the 'weight loss method' which revealed the high inhibition efficiency
APA, Harvard, Vancouver, ISO, and other styles
35

Karimova, Oygul Razzakberganovna. "SYNTHESIS OF QUINOLINE ALKALOIDS USING AMIDES." Multidisciplinary Journal of Science and Technology 5, no. 2 (2025): 722–26. https://doi.org/10.5281/zenodo.14921331.

Full text
Abstract:
This article provides an in-depth analysis of the synthesis of quinoline alkaloids using amides. Amides play a crucial role as directing groups in C-H activation, participate in cascade reactions, and enable stereochemical control. The latest advancements in catalytic systems, including green chemistry approaches and computational methodologies, are reviewed to enhance the efficiency and environmental safety of synthetic processes. The practical applications of these findings extend to pharmaceuticals, medicine, agrochemicals, and materials science. This research paper presents the results of
APA, Harvard, Vancouver, ISO, and other styles
36

Suryakala, K., and R. Venckatesh. "Synthesis of Nano-Crystalline LiNdxMn2-xO4Powder by Novel Cam-Microwave Assisted Sol-Gel Method." E-Journal of Chemistry 4, no. 4 (2007): 487–95. http://dx.doi.org/10.1155/2007/123132.

Full text
Abstract:
With the advancement of nanotechnology, there is an interest in the replacement of conventional materials by nanomaterials. There is a reasonable chance that as the active mass of electrode for lithium batteries is comprised of smaller particles, they will perform better in terms of capacity, power, rate capability and stability. LiMn2O4is inexpensive material but it shows rather poor cyclic performance. The electrochemical performance of spinel type LiMn2O4has been effectively improved with doping of Nd the “bottom–up” approach of LiMn2O4and LiNdxMn2-xO4(x = 0.1, 0.2, 0.3 and 0.4) synthesized
APA, Harvard, Vancouver, ISO, and other styles
37

Spandana, Zanjam, Tadigiri M. Rekha, Mandava V. B. Rao, and Manojit Pal. "One-Pot Synthesis of 5-(Het)Aryl 8-Aminoquinoline Amide Derivatives as Potential Antibacterial / Cytotoxic Agents." Current Bioactive Compounds 16, no. 2 (2020): 142–51. http://dx.doi.org/10.2174/1573407214666180910130225.

Full text
Abstract:
Background: The 8-Aminoquinoline (8-AQ) framework has attracted particular attention in the discovery and development of antimalarial and anti-bacterial agents or drugs. However, the clinical uses of 8-AQ based drugs are often associated with toxic side effects such as methemoglobinemia and hemolytic anemia with deficiency in Glucose-6-Phosphate Dehydrogenase (G6PD) Activity. The 4-aryl- 8-amino(acetamido)quinoline derivatives, on the other hand, have shown antiproliferative activities against cancer cell lines. These reports prompted us to assess the antibacterial and cytotoxic activities of
APA, Harvard, Vancouver, ISO, and other styles
38

Shankaraiah, P., V. Sunitha, A. Kishore Kumar, and R. Madhu. "MICROWAVE ASSISTED SYNTHESIS OF N-(1-ISOPROPYL-2- OXOINDOLIN-5-YL) SUBSTITUTED AMIDE DERIVATIVES AND THEIR ANTIMICROBIAL ACTIVITY." Rasayan Journal of Chemistry 12, no. 04 (2019): 1850–56. http://dx.doi.org/10.31788/rjc.2019.1245445.

Full text
APA, Harvard, Vancouver, ISO, and other styles
39

Mallakpour, Shadpour, and Amin Zadehnazari. "CHIRAL POLY(AMIDE-THIOESTER-IMIDE)S HAVING THIADIAZOL GROUP: MICROWAVE-ASSISTED SYNTHESIS AND STUDY OF THERMO-OPTICAL BEHAVIOR." Chemical Engineering Communications 201, no. 5 (2014): 635–49. http://dx.doi.org/10.1080/00986445.2013.782293.

Full text
APA, Harvard, Vancouver, ISO, and other styles
40

Gallienne, Estelle, Giulio G. Muccioli, Didier M. Lambert, and Michael Shipman. "Microwave-assisted four-component reaction for the synthesis of a monothiohydantoin inhibitor of a fatty acid amide hydrolase." Tetrahedron Letters 49, no. 46 (2008): 6495–97. http://dx.doi.org/10.1016/j.tetlet.2008.08.100.

Full text
APA, Harvard, Vancouver, ISO, and other styles
41

Chi, Yushi, Huibin Zhang, Wenlong Huang, et al. "Microwave-assisted solid phase synthesis, PEGylation, and biological activity studies of glucagon-like peptide-1(7–36) amide." Bioorganic & Medicinal Chemistry 16, no. 16 (2008): 7607–14. http://dx.doi.org/10.1016/j.bmc.2008.07.019.

Full text
APA, Harvard, Vancouver, ISO, and other styles
42

Jaipuri, Firoz A., M. Francisca Jofre, Kimberly A. Schwarz, and Nicola L. Pohl. "Microwave-assisted cleavage of Weinreb amide for carboxylate protection in the synthesis of a ( R )-3-hydroxyalkanoic acid." Tetrahedron Letters 45, no. 21 (2004): 4149–52. http://dx.doi.org/10.1016/j.tetlet.2004.03.148.

Full text
APA, Harvard, Vancouver, ISO, and other styles
43

Hajipour, Abdol R., Saeed Zahmatkesh, and Arnold E. Ruoho. "Microwave-assisted synthesis and characterization of heterocyclic, and optically active poly(amide-imide)s incorporating L-amino acids." Polymers for Advanced Technologies 19, no. 12 (2008): 1710–19. http://dx.doi.org/10.1002/pat.1166.

Full text
APA, Harvard, Vancouver, ISO, and other styles
44

Khadilkar, Bhushan M., and Virendra R. Madyar. "ChemInform Abstract: Totally Selective Dry Microwave Assisted Amide Synthesis by Hydration of Nitrile Using Silica Supported MnO2 Reagent." ChemInform 33, no. 43 (2010): no. http://dx.doi.org/10.1002/chin.200243104.

Full text
APA, Harvard, Vancouver, ISO, and other styles
45

Moreno-Fuquen, Rodolfo, Kevin Arango-Daraviña, Diana Becerra, Juan-Carlos Castillo, Alan R. Kennedy, and Mario A. Macías. "Catalyst- and solvent-free synthesis of 2-fluoro-N-(3-methylsulfanyl-1H-1,2,4-triazol-5-yl)benzamide through a microwave-assisted Fries rearrangement: X-ray structural and theoretical studies." Acta Crystallographica Section C Structural Chemistry 75, no. 3 (2019): 359–71. http://dx.doi.org/10.1107/s2053229619002572.

Full text
Abstract:
An efficient approach for the regioselective synthesis of (5-amino-3-methylsulfanyl-1H-1,2,4-triazol-1-yl)(2-fluorophenyl)methanone, C10H9FN4OS, (3), from the N-acylation of 3-amino-5-methylsulfanyl-1H-1,2,4-triazole, (1), with 2-fluorobenzoyl chloride has been developed. Heterocyclic amide (3) was used successfully as a strategic intermediate for the preparation of 2-fluoro-N-(3-methylsulfanyl-1H-1,2,4-triazol-5-yl)benzamide, C10H9FN4OS, (4), through a microwave-assisted Fries rearrangement under catalyst- and solvent-free conditions. Theoretical studies of the prototropy process of (1) and t
APA, Harvard, Vancouver, ISO, and other styles
46

Wei, Xiu-Zhi, Jianguo Liu, and Longlong Ma. "One-Pot Tandem Synthesis of Nitriles and Amides from Biomass Platform Compounds." Catalysis Research 2, no. 1 (2021): 1. http://dx.doi.org/10.21926/cr.2201004.

Full text
Abstract:
In recent years, research on converting biomass platform compounds into high-value chemicals and pharmaceutical intermediates has garnered huge interest. Nitrile and amide groups are key structures in natural products and biologically active molecules. The direct conversion of biomass platform compounds into nitriles and amides will undoubtedly be an important guide for biomass utilization. In this paper, a facile and efficient triphosgene-assisted one-pot conversion for aldehydes and ketones into nitrile and amides is presented. Triphosgene is a phosgene alternative that contains both ester l
APA, Harvard, Vancouver, ISO, and other styles
47

Faghihi, Khalil, Khosrow Zamani, Azizollah Mirsamie, and Mohammad Reza Sangi. "Microwave-assisted rapid synthesis of novel optically active poly(amide-imide)s containing hydantoins and thiohydantoins in main chain." European Polymer Journal 39, no. 2 (2003): 247–54. http://dx.doi.org/10.1016/s0014-3057(02)00200-8.

Full text
APA, Harvard, Vancouver, ISO, and other styles
48

Mallakpour, Shadpour, and Amin Zadehnazari. "New Organosoluble, Thermally Stable, and Nanostructured Poly(Amide-Imide)s with Dopamine Pendant Groups: Microwave-Assisted Synthesis and Characterization." International Journal of Polymer Analysis and Characterization 17, no. 6 (2012): 408–16. http://dx.doi.org/10.1080/1023666x.2012.669646.

Full text
APA, Harvard, Vancouver, ISO, and other styles
49

Xu, Juan, Wei Gao, Qi Zhang, and Lifeng Ning. "Cocrystallization of Progesterone with Nitrogen Heterocyclic Compounds: Synthesis, Characterization, Calculation and Property Evaluation." Molecules 28, no. 10 (2023): 4242. http://dx.doi.org/10.3390/molecules28104242.

Full text
Abstract:
Progesterone injection is oily because of its poor solubility. It is necessary to develop new dosage forms or delivery methods for Progesterone. Six cocrystals of Progesterone with nitrogen heterocyclic compounds (2,6-diaminopyridine, isonicotinamide, 4-aminopyridine, aminopyrazine, picolinamide and pyrazinamide) have been designed and prepared by ethyl acetate-assisted grinding, of which four cocrystals (2,6-diaminopyridine, isonicotinamide, 4-aminopyridine and aminopyrazine) had single crystal data in 1:1 stoichiometry. Metadynamics-genetic crossing was used to search and optimize various cl
APA, Harvard, Vancouver, ISO, and other styles
50

Priya, Disholin Dennison, Thangavel Pichaiappa Rajesh, Rachel Syam Sundar, and Chandrasekhar Narendhar. "Iron Oxide Nanoparticles – Characterization and Antimicrobial Studies." INTERNATIONAL JOURNAL OF APPLIED PHARMACEUTICAL SCIENCES AND RESEARCH 6, no. 03 (2021): 27–32. http://dx.doi.org/10.21477/ijapsr.6.3.01.

Full text
Abstract:
Nanotechnology is one of the most promising technologies that give us better outcomes from biological and industrial issues. This work ismainly based on the green synthesis of iron oxide nanoparticles, assisted by the flower extract. The nanoparticles were synthesized and characterized using UV Visible spectroscopy with characteristic absorbance peaks at 300 nm and 310 nm. Prominent Fourier-Transform Infrared Spectroscopy (FTIR) peaks were obtained corresponding to phenols, amide group, aromatic ring, hydroxyl group, and carbonate ions involved in the stabilization of iron oxide nanoparticles
APA, Harvard, Vancouver, ISO, and other styles
We offer discounts on all premium plans for authors whose works are included in thematic literature selections. Contact us to get a unique promo code!