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Journal articles on the topic 'Amido (or Imido) Methyl Derivatives'

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Published: 5 June 2025

Last updated: 1 August 2025

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1

Castro, Aurora, Mikhail V. Galakhov, Manuel Gómez, and Fernando Sánchez. "Half-sandwich dichloro, alkyl chloro, dialkyl, alkyl methyl and amido methyl imido cyclopentadienyl niobium and tantalum(V) complexes. Dynamic behaviour of amido imido tantalum derivatives." Journal of Organometallic Chemistry 580, no. 1 (1999): 161–68. http://dx.doi.org/10.1016/s0022-328x(98)01142-5.

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2

Lupea, Xenia, Iuliana Popescu, Corneliu Tarabasanu, Ioana Ienascu, and Valentin Badea. "The synthesis and characterization of some ortho-substituted phenoxyalkanoic acids and their derivatives." Journal of the Serbian Chemical Society 71, no. 12 (2006): 1247–61. http://dx.doi.org/10.2298/jsc0612247l.

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The synthesis of 2-phenoxyalkanoic acids (ethanoic, propanoic, butanoic) was realized by the reaction of ortho-hydroxybenzamide respectively N-phenyl-o-hydroxybenzamide with ?-halogenated acids in aqueous sodium hydroxide solution. 2-[o-(carbamoyl)phenoxy]-2-methyl- and 2-[o-(phenylcarbamoyl)phenoxy]-2-methyl- propanoic acids were obtained by reaction of the appropriate amide with acetone, chloroform and sodium hydroxide. Ethyl esters of 2-phenoxyalkanoic acids were obtained by the reaction of the amide with ethyl esters of ?-halogenated acids in different reaction media. Starting from the eth

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3

Razali, Mohd R., Aron Urbatsch, Stuart K. Langley, et al. "Linear Trinuclear Copper(II) Complexes Derived from the Nucleophilic Addition Products of Dicyanonitrosomethanide [C(CN)2(NO)]–: Syntheses, Structures, and Magnetic Properties." Australian Journal of Chemistry 65, no. 7 (2012): 918. http://dx.doi.org/10.1071/ch12100.

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Two novel trinuclear CuII complexes have been synthesised from the nucleophilic addition derivatives of the small cyano anion, dicyanonitrosomethanide (dcnm). The reaction of CuII with the water adduct ligand, carbamoylcyanonitrosomethanide (ccnm) and teaH3 (triethanolamine) in a basic MeOH/MeCN solution results in the formation of [Cu3(acnm)2(teaH2)2]·2MeOH (1) (acnm = amidocarbonyl(cyano)nitrosomethanide and teaH2– = singly deprotonated triethanolamine). The reaction of CuII with dicyanonitrosomethanide (dcnm) and m-xylenediamine in a basic MeOH/MeCN solution results in the formation of [Cu3

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4

Popovic-Djordjevic, Jelena, Vesna Vitnik, Zeljko Vitnik, and Milovan Ivanovic. "Glutarimides: Biological activity, general synthetic methods and physicochemical properties." Chemical Industry 69, no. 5 (2015): 523–36. http://dx.doi.org/10.2298/hemind140701073p.

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Glutarimides, 2,6-dioxopiperidines are compounds that rarely occur in natural sources, but so far isolated ones exert widespread pharmacological activities, which makes them valuable as potential pharmacotherapeutics. Glutarimides act as androgen receptor antagonists, anti-inflammatory, anxiolytics, antibacterials, and tumor suppressing agents. Some synthetic glutarimide derivatives are already in use as immunosuppressive and sedative (e.g., thalidomide) or anxiolytics (buspirone) drugs. The wide applicability of this class of compounds, justify the interest of scientists to explore new pathwa

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5

Haratipour, Pouya, Maryam Zangi, Mahshid Yaghoubi, et al. "Abstract 4481: Enhancing AOH1996 through structure activity relationship exploration for caPCNA inhibition." Cancer Research 84, no. 6_Supplement (2024): 4481. http://dx.doi.org/10.1158/1538-7445.am2024-4481.

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Abstract Recently, we have developed AOH1996, a small molecule PCNA ligand currently in phase I clinical trial, designed to selectively inhibit the functions of cancer-associated PCNA (caPCNA). Seeking to enhance the potency and selectivity of AOH1996, we conducted an exhaustive Structure-Activity-Relationship (SAR) investigation. Over 100 analogues of AOH1996 were synthesized, systematically modifying its three main components: the naphthyl group, glycine linker, and diphenyl ether. The glycine linker underwent substitution with various natural and unnatural amino acids, while the 1-naphthyl

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6

Khalifa, Nagy M., Ahmed M. Naglah, Mohamed A. Al-Omar, Mohamed H. Abo-Ghalia, and Abd El-Galil E. Amr. "Synthesis and Reactions of New Chiral Linear Carboxamides with an Incorporated Peptide Linkage Using Nalidixic Acid and Amino Acids as Starting Materials." Zeitschrift für Naturforschung B 69, no. 3 (2014): 351–61. http://dx.doi.org/10.5560/znb.2014-3282.

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4bA series of chiral linear carboxamide derivatives (2- 15) with an incorporated peptide linkage have been prepared via the coupling of 1-ethyl-1,4-dihydro-7-methyl-4-oxo-quinoline-3-carboxylic acid (nalidixic acid, 1) with appropriate amino acid methyl esters. Coupling of 1 with amino acid methyl esters gave the corresponding peptide methyl esters 2, which were hydrolyzed with methanolic sodium hydroxide to the corresponding acids 3. Hydrazinolysis of esters 2with hydrazine hydrate afforded the corresponding acid hydrazide derivatives 4. The latter compounds were coupled with appropriate alde

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7

Neamah, Rawaa, та Shaimaa Adnan. "Study the Biological Activity for Shiff Base and Β – Lactam Compounds that Synthesis and Identification from Pyrimidine Derivatives". International Journal of Pharmaceutical Quality Assurance 11, № 01 (2013): 37–39. http://dx.doi.org/10.25258/ijpqa.11.1.12.

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In This study We are synthesis and characterization of some Schiff base and β- lactam derivatives) by three steps. The First react 2-amino-4-Chloro-6-methyl pyrimidine with 4-amino acetophenone in an acid medium to get shiff base derivative(E)-4-(1-((4-Chloro-6-methyl pyridine-2-yl)imino)ethyl)aniline (1), the second step (1) react with (3,4- dimethoxybenzal dehyde,4-methyl benzaldehyde,4-dimethylamino benzaldehyde,4-bromo benzaldehyde,4–hydroxy benzaldehyde, 4-Nitro benzaldehyde) to get Schiff base derivatives (2-7), the last step (2-7) derivatives react with Chloro acetyl chloride to get –β-

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8

Pedrosa, Sergio, Fernando Vidal, Lucia Myongwon Lee, Ignacio Vargas-Baca, Pilar Gómez-Sal, and Marta E. G. Mosquera. "Imido-pyridine Ti(iv) compounds: synthesis of unusual imido–amido heterobimetallic derivatives." Dalton Transactions 44, no. 24 (2015): 11119–28. http://dx.doi.org/10.1039/c5dt01320h.

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Controlled generation of novel bridging or terminal imido-pyridine complexes is achieved, including the unusual species [Li(THF)][Ti(η<sup>5</sup>-C<sub>5</sub>Me<sub>5</sub>)(NR)(NHR)<sub>2</sub>]. Computational studies corroborate its charge-separated nature.

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9

El-Naggar, Mohamed, Abdel-Nasser El-Shorbagi, Dina H. Elnaggar, Abd El-Galil E. Amr, Mohamed A. Al-Omar, and Elsayed A. Elsayed. "Synthesis, Characterization, and Cytotoxic Evaluation of Some Newly Substituted Diazene Candidates." Journal of Chemistry 2018 (November 1, 2018): 1–9. http://dx.doi.org/10.1155/2018/3626824.

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A series of azocompounds containing methyl salicylate 4a–k and 1-naphthyl moiety 6–8 was synthesized and tested as anticancer agents. Nitrosation of methyl 5-amino-2-hydroxybenzoate or 1-aminonaphthalene by using NaNO2 in the presence of HCl afforded diazonium salt derivatives 2 and 5, which were treated with substituted imino or substituted amino derivatives, to give the corresponding substituted amino-pent-2-en-3-yl-diazenylbenzoate 4a–k or 2-substituted-1-(naphthalen-1-yl)diazene derivatives 6a–h, 7a,b, and 8a,b. All the synthesized compounds were elucidated by elemental analysis and spectr

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10

Gray, Steven D., Joseph L. Thorman, Lisa M. Berreau, and L. Keith Woo. "Alkoxido, Amido, and Imido Derivatives of Titanium(IV) Tetratolylporphyrin." Inorganic Chemistry 36, no. 3 (1997): 278–83. http://dx.doi.org/10.1021/ic960977y.

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11

Mohammed, Tiba Ibrahim. "Synthesis of New Azo–Schiff Base Complexes and Study of their Antibacterial Activity." International Journal Papier Advance and Scientific Review 4, no. 1 (2023): 42–56. http://dx.doi.org/10.47667/ijpasr.v4i1.206.

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In this research, we synthesized new azo-schiff base derivatives (4-9). These derivatives of azo compounds (1-3) that synthesized from 4-ethoxyaniline and drivatives of aldehyde such as, 4-aminobenzaldehyde, 4- hydroxybenzaldehyde and 4-ethoxybenzaldehyse to produce azo compounds (1-3). The compounds (1-3) reacted with differents aldehyde such as, isonicotinic hydrazide to produce N'-[(Z)-{3-[(E)-(4-ethoxyphenyl)diazenyl]-4-subs.phenyl}-methylidene]pyridine-4-carbohydrazide derivatives (4-6) and 3-amino pyridine to produce 2-[(E)-(4-ethoxyphenyl)diazenyl]-4-{(E)-[(pyridin-3-yl)imino]-methyl}su

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12

Abu-Hashem, Ameen Ali, and Sami A. Al-Hussain. "Design, Synthesis of New 1,2,4-Triazole/1,3,4-Thiadiazole with Spiroindoline, Imidazo[4,5-b]quinoxaline and Thieno[2,3-d]pyrimidine from Isatin Derivatives as Anticancer Agents." Molecules 27, no. 3 (2022): 835. http://dx.doi.org/10.3390/molecules27030835.

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The current work aims to design and synthesis a new series of isatin derivatives and greatly enhances their cytotoxic activity. The derivatives 3-((bromophenyl) imino)-1-(morpholino (pyridine) methyl) indolin-2-one, 2-((oxoindoline) amino) benzoic acid, 3-(thiazolo-imino) indolinone, ethyl-2-((oxoindolin-3-ylidene)amino)-benzothiophene-3-carboxylate, 1-(oxoindoline)-benzo[4,5] thieno [2,3-d]pyrimidin-4(1H)-one, ethyl-2-(2-oxoindoline) hydrazine-1-carboxylate, N-(mercapto-oxo-pyrimidine)-2-(oxoindoline) hydrazine-1-carboxamide, N-(oxo-thiazolo[3,2-a] pyrimidine)-2-(oxoindolin-ylidene) hydrazine

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13

El-Hashash, Maher A., Eman A. El-Bordany, Magda I. Marzouk, Abeer M. El-Naggar, Tarek M. S. Nawar, and Wael M. El-Sayed. "Novel Nicotinonitrile Derivatives Bearing Imino Moieties Enhance Apoptosis and Inhibit Tyrosine Kinase." Anti-Cancer Agents in Medicinal Chemistry 18, no. 11 (2019): 1589–98. http://dx.doi.org/10.2174/1871520618666180510112614.

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Background: Fused heterocyclic containing pyrazolopyridine systems have several medicinal activities including cytotoxic and carcinostatic activities. Objective: To investigate the antiproliferative activity and associated mechanism(s) of a novel series of nicotinonitrile derivatives. Method: The series has been synthesized by the reaction of hydrazonoyl chlorides with each of 4-(4- methoxyphenyl)-3-methyl-6-oxo-6,7-dihydro-1H-pyrazolo[3,4-b]pyridine-5-carbonitrile and 2-amino-4-(4- methoxyphenyl)-6,7-dihydro-5H-cyclopenta[b]pyridine-3-carbonitrile in dioxane in basic medium. The assigned stru

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14

Y., A. AMMAR, M. ISMAIL I., M. SH. EL-SHARIEF A., A. MOHAMED Y., and M. AMER R. "Synthesis of some Newer Thiazolo and Thiadiazino Derivatives from 6-Methyl- or 6-Nitro-2 3-dichloroquinoxalines." Journal of Indian Chemical Society Vol. 66, Feb 1989 (1989): 124–27. https://doi.org/10.5281/zenodo.5995537.

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Chemistry Department, Faculty of Science, Al-Azhar University, Nasr-City, Cairo, Egypt <em>Manuscript received 23 October 1987, revised 18 August 1988, accepted 18 November 1988</em> <strong>Interaction of 6-methyl- or 6-nitro-2,3-diehloroquinozaline (la, b) with thiourea </strong><strong>in ethanol led to the formation of diquinoxalino[2,3-b 2</strong><strong><sup>′</sup></strong><strong>,3</strong><strong>′</strong><strong>-e)-1,4-dithlien derivatives (2a, b) with 2-imino-2,3-dihydrothiazolo[4,5-b]quinoxalines (3a, b). 7-Methyl- or 7- </strong><strong>nitro-3-amino-2-imino-2,3-di

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15

Y., A. AMMAR, M. ISMAIL I., M. SH. EL-SHARIEF A., A. MOHAMED Y., and M. AMER R. "Synthesis of some Newer Thiazolo and Thiadiazino Derivatives from 6-Methyl- or 6-Nitro-2,3-dichloroquinoxalines." Journal of Indian Chemical Society Vol. 66, Feb 1989 (1989): 124–27. https://doi.org/10.5281/zenodo.6303632.

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Chemistry Department, Faculty of Science, Al-Azhar University, Nasr City, Cairo, Egypt <em>Manuscript received 23 October 1987, revised 18 August 1988, accepted 18 November 1988</em> lnteraction or 6-methyl or 6-nitro-2,3-dichloroquinoxaline (1a, b) with thiourea in ethanol led to the formation or diquinoxalino[2,3-<em>b</em>: 2',3'-<em>e</em>]-1,4-dithiien derivatives (2a, b) with 2-imino-2,3-dihydrothiazolol [4,5-<em>b</em> ]quinoxalines (3a, b). 7-Methyl- or 7- nitro-3-amino-2-imino-2,3-dihydrothiazolo[4,5-<em>b</em>]quinoxaline (6a, b) were prepared and reacted with acid

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16

El-Agrody, Ahmed M., Fathy A. Eid, Hussein A. Emam, Hany M. Mohamed, and Ahmed H. Bedair. "Synthesis of 9-Methoxy and 9-Acetoxy-3-amino-1-(4-methoxyphenyl)- 1H-benzo[f]chromene-2-carbonitriles via 2-(Imino-piperidin-1-yl-methyl)- 3-(4-methoxyphenyl)acrylonitrile as Intermediate." Zeitschrift für Naturforschung B 57, no. 5 (2002): 579–85. http://dx.doi.org/10.1515/znb-2002-0516.

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Several new 1H-benzo[f]chromene derivatives (3aÐd) were prepared by the reaction of 7-substituted-2-naphthols (1a,b) with substituted α-cyano-4-methoxycinnamonitriles (2a,b) together with 2-(imino-piperidin-1-yl-methyl)-3-(4-methoxyphenyl)acrylonitrile (4) as intermediate. Also, the reaction of 1a,b with 4 without catalyst afforded 9-methoxy and 9-acetoxy- 3-amino-1-(p-methoxyphenyl)-1H-benzo[f]chromene-2-carbonitrile (3b,e). The reaction of 3a,b with different electrophilic and nucleophilic reagents afforded the 12H-7-oxa-8,10-diazabenzo[ a]anthracene derivatives 5, 9, 10 and 1H-benzo[f]chrom

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17

Cheon, Cheol-Hong, Sang Lee, and Seong Lee. "Concise Total Syntheses of Paullone and Kenpaullone via Cyanide-Catalyzed Intramolecular Imino-Stetter Reaction." Synthesis 49, no. 18 (2017): 4247–53. http://dx.doi.org/10.1055/s-0036-1588749.

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Highly concise total syntheses of paullone and kenpaullone were developed. Cyanide-catalyzed intramolecular imino-Stetter reaction of aldimines derived from methyl 2-aminocinnamate derivatives and 2-nitrobenzaldehyde provided 2-(2′-nitrophenyl)indole-3-acetic acid derivatives. Subsequent reduction of the nitro group with zinc under acidic conditions to an amino group followed by spontaneous lactam formation allowed for the total syntheses of paullone and kenpaullone to be completed in two steps starting from commercially available materials. The direct use of a nitro group as the precursor of

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18

L. Khaleel, Zina, and Yassir S. Al-Jawaheri. "Synthesis of and characterization some platinum(IV) complexes derived from substituted imides and evaluation of their biological activity." Bulletin of the Chemical Society of Ethiopia 39, no. 3 (2024): 459–72. https://doi.org/10.4314/bcse.v39i3.6.

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This research paper explores preparation of furanoanthracene-12,14-dione (1) via the addition of malic anhydride to anthracene. The resultant compound was treated with urea to form the imide derivative (2). Subsequently (2) was reacted with formaldehyde, leading to the substitution of the nitrogen-bound proton with a hydroxymethyl group, yielding hydroxymethyl pyrroloanthracene (3). In the following step, various substituted anilines were reacted with (3) in the presence of triethylamine through an SN2 reaction to replace the hydroxyl group and producing substituted amino methyl-epipyrroloanth

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19

Gomes, Pedro T., Malcolm L. H. Green та Ana M. Martins. "Ansa-bridged η-cyclopentadienyl imido and amido derivatives of titanium, zirconium and molybdenum". Journal of Organometallic Chemistry 551, № 1-2 (1998): 133–38. http://dx.doi.org/10.1016/s0022-328x(97)00516-0.

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20

Martinelli, Fabio, Alessandro Palmieri та Marino Petrini. "Metal-Free Synthesis of Imido Derivatives by Direct Oxidation of α-Amido Sulfones". European Journal of Organic Chemistry 2010, № 26 (2010): 5085–89. http://dx.doi.org/10.1002/ejoc.201000634.

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21

Shein, Anatoliy B., Mariya D. Plotnikova, and Alexander E. Rubtsov. "PROTECTIVE PROPERTIES OF SOME THIADIAZOLE DERIVATIVES IN SULFURIC ACID SOLUTIONS." IZVESTIYA VYSSHIKH UCHEBNYKH ZAVEDENII KHIMIYA KHIMICHESKAYA TEKHNOLOGIYA 62, no. 7 (2019): 123–29. http://dx.doi.org/10.6060/ivkkt.20196207.5968.

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The work presents the results of the study of some thiadiazole derivatives as corrosion inhibitors for mild steel in 5-20% H2SO4. Gravimetric tests and electrochemical studies were performed on low-carbon steel St3 at ambient temperature. The exposure time of the samples was 24 h. Polarization curves were obtained by potentiodynamic method (v = 1 mV/s) in a three-electrode cell, using the SOLARTRON 1280 C electrochemical measuring complex. The following thiadiazole derivatives were studied: (E)-N,N-dimethyl-4-{[(5-phenyl-1,3,4-thiadiazol-2-yl)imino]methyl}aniline, (E)-5-{[4-(dimethylamino)benz

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22

Bernotas, R. C., and B. Ganem. "Easy assembly of ligands for glycosidase affinity chromatography." Biochemical Journal 270, no. 2 (1990): 539–40. http://dx.doi.org/10.1042/bj2700539.

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An improved, high-yield synthesis of the corresponding N-carboxypentyl derivatives of three iminoalditol glycosidase inhibitors has been developed for affinity chromatography enzyme purification. Reductive amination of 1-deoxynojirimycin (or its D-manno or D-galacto analogues) with methyl 5-formylvalerate and NaBH3CN at neutral pH afforted an aminoester which upon hydrolysis with aqueous 5% HCl gave the desired aminoacid in 97% overall yield. These amino acids could then be covalently attached using water-soluble carbodi-imide to 6-aminohexyl Sepharose 4B.

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23

Panaetov, A. O., V. D. Strelkov, V. V. Dotsenko, et al. "Mannich reaction involving 6-amino-4-methyl2-(thio)oxo-1,2-dihydropyridine-3,5-dicarbonitriles." Журнал общей химии 93, no. 7 (2023): 1007–22. http://dx.doi.org/10.31857/s0044460x23070041.

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The reaction of (1-ethoxyethylidene)malononitrile with cyanoacetamide or cyanothioacetamide yielded 6-amino4-methyl-2-(thio)oxo-1,2-dihydropyridine-3,5-dicarbonitriles. The resulting pyridine derivatives enter into an aminomethylation reaction with an excess of formaldehyde and primary amines with the formation of previously unknown 8-methyl-6-oxo-3-R-1,3,4,6-tetrahydro-2 H -pyrido[1,2- a ][ 1,3,5]triazine-7,9-dicarbonitriles. Further treatment of 6-amino-4-methyl-2-thioxo-1,2-dihydropyridine-3,5-dicarbonitrile and its oxygen analogue with excess formaldehyde leads to the formation of 3,10-dim

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24

Elhady, A. N. El-Sharabasy A. S. Kassab S. R. R. Soliman A. M. F. &. Ali A. A. E. "New anticorrosion and flame retardant coating compositions based on 4-amino triazole derivatives , their Schiffs' bases and epoxy varnish." International Journal of Applied Research 6, no. 1 (2020): 60–72. https://doi.org/10.5281/zenodo.4013369.

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In this study, some recently amino triazole derivatives mainly 4-amino-5-phenyl-2,4-dihydro-3H-1,2,4-triazole-3-thione(I),4-((furan-2-yl-methylene)amino)-5-phenyl-2,4-dihydro-3H-1,2,4-triazole-3-thione(II), 4-((4-nitrobenzyl- idene)amino)-5-phenyl-2,4-dihydro-3H-1,2,4-triazole-3-thione (III),4-((4-(dimethylamino)benzylidene)amino)-5-phenyl-2,4-dihydro-3H-1,2,4-triazole-3-thione (IV), 5-phenyl-4-((3-phenyl-4-((3-phenylallylidene) amino)-2,4-dihydro-3H-1,2,4-triazole-3-thione(V),4-(((3-phenyl-5-thioxo-1,5-dihydro-4H-1,2,4-triazole-4yl)imino)methyl)benzal-  dehyde(VI),and3-(((3-phenyl-5-thio

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25

Filippov, Andrey S., Svetlana V. Amosova, Alexander I. Albanov, and Vladimir A. Potapov. "Regioselective Synthesis of Novel Functionalized Dihydro-1,4-thiaselenin-2-ylsufanyl Derivatives under Phase Transfer Catalysis." Catalysts 12, no. 8 (2022): 889. http://dx.doi.org/10.3390/catal12080889.

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The regioselective one-pot synthesis of novel functionalized 2,3-dihydro-1,4-thiaselenin-2-ylsufanyl derivatives in high yields based on 2-bromomethyl-1,3-thiaselenole and activated alkenes was developed under phase transfer catalysis conditions. The reactions proceed under mild conditions at room temperature in a regioselective manner with the addition of sodium dihydro-1,4-thiaselenin-2-ylthiolate exclusively at the terminal carbon atom of the double bond of vinyl methyl ketone, alkylacrylates, acrylamide, acrylonitrile, divinyl sulfone, and divinyl sulfoxide. The sodium dihydro-1,4-thiasele

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26

VARAPRASADU, B. DURGA, K. SHIVA KUMAR, and B. PULLA RAO. "Design, Synthesis, Characterization and Antibacterial Activity of Some Novel Furan Supported 1,2,4-Triazoles." Asian Journal of Chemistry 35, no. 10 (2023): 2493–97. http://dx.doi.org/10.14233/ajchem.2023.27959.

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A methodical approach to synthesize several novel 2-phenyl-4-methylfuran [2,3-e][1,2,4]triazolo [1,5-c]pyrimidine derivatives (5a-c) as final compounds, N-(4-imino-4-methylfuro [2,3-d]pyrimidin-3(4H)-ylbenzamides (4a-c) by involving 2-amino-3-cyano-4-methyl furan (1) and N-(3-cyano-4-methylfuran)formimidic ethyl ether (2) and N’-((Z-(3-cyano-4-methylfuran-2-ylimino)methyl)benzohydrazides (3a-c) as intermediates and their antibacterial activity was tested. The chemical structures of all the newly synthesized intermediates and title compounds have been characterized by 1H NMR, IR, HRMS and eleme

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27

Sun, Yi, Wenfei Huang, Zhiqiang Li, Tao Wang, and Jin Luo. "Design, synthesis, and herbicidal activity of novel 2-(arylamino)-5-methyl-4-methylene-7-(methylthio)-4H-pyrido[4,3-d][1,3]oxazine-8-carbonitrile derivatives." Journal of Chemical Research 43, no. 3-4 (2019): 119–23. http://dx.doi.org/10.1177/1747519819845771.

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A series of 5-methyl-4-methylene-7-methylthio-2-arylmino-4 H-pyrido[4,3- d][1,3]oxazine-8-carbonitrile derivatives were synthesized via tandem aza-Wittig and annulation reactions with { N-[3-acetyl-5-cyano-2-methyl-6-(methylthio)pyridin-4-yl]imino}triphenylphosphorane and aryl isocyanate in dry dichloromethane. Their structures were clearly confirmed by infrared, 1H NMR, 13C NMR, high-resolution mass spectrometry, and X-ray single-crystal diffraction. All newly synthesized compounds were screened for herbicidal activities against monocotyledonous and dicotyledonous plants. The results indicate

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28

Behpour, M., and N. Mohammadi. "Inhibiting Effects of Two Derivatives of Amino-Thiophenol on the Corrosion of Copper by Electrochemical Methods." Corrosion 68, no. 12 (2012): 1119–25. http://dx.doi.org/10.5006/0607.

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Corrosion inhibition of the two thio compounds, 2-{[(2-sulfanyl-phenyl)imino]methyl}phenol (SIMP) and 2-{[(Z)-1-(4-methyl-phenyl)methylidene]amino}-1-benzenthiol (MMAB), as corrosion inhibitors for copper in 15% hydrochloric acid (HCl) have been investigated by potentiodynamic polarization measurements and electrochemical impedance spectroscopy. Potentiodynamic polarization results show that corrosion potentials shift more toward the anodic region in the presence of thio compounds than that of blank solution. The adsorption of inhibitors on the copper surface follows from Langmuir adsorption i

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29

Gomes, Pedro T., Malcolm L. H. Green, Ana M. Martins та Philip Mountford. "Ansa-bridged η-cyclopentadienyl imido and amido derivatives of titanium, zirconium, niobium and molybdenum". Journal of Organometallic Chemistry 541, № 1-2 (1997): 121–25. http://dx.doi.org/10.1016/s0022-328x(97)00022-3.

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30

Vatsadze, Sergey Z., Marina A. Manaenkova, Evgeny V. Vasilev, Nikolai U. Venskovsky, and Victor N. Khrustalev. "Crystal structures and supramolecular features of 9,9-dimethyl-3,7-diazabicyclo[3.3.1]nonane-2,4,6,8-tetraone, 3,7-diazaspiro[bicyclo[3.3.1]nonane-9,1′-cyclopentane]-2,4,6,8-tetraone and 9-methyl-9-phenyl-3,7-diazabicyclo[3.3.1]nonane-2,4,6,8-tetraone dimethylformamide monosolvate." Acta Crystallographica Section E Crystallographic Communications 73, no. 7 (2017): 1097–101. http://dx.doi.org/10.1107/s2056989017009458.

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Compounds (I), C9H10N2O4, (II), C11H12N2O4, and (III), C14H12N2O4·C3H7NO represent 9,9-disubstituted-3,7-diazabicyclo[3.3.1]nonane-2,4,6,8-tetraone derivatives with very similar molecular geometries for the bicyclic framework: the dihedral angle between the planes of the imide groups is 74.87 (6), 73.86 (3) and 74.83 (6)° in (I)–(III), respectively. The dimethyl derivative (I) is positioned on a crystallographic twofold axis and its overall geometry deviates only slightly from idealizedC2vsymmetry. The spiro-cyclopentane derivative (II) and the phenyl/methyl analog (III) retain only internalCs

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31

A. Ameen, Husam, and Ahlam J. Qasir. "Synthesis and Preliminary Antimicrobial Study of 2-Amino-5-Mercapto-1,3,4-Thiadiazole Derivatives." Iraqi Journal of Pharmaceutical Sciences ( P-ISSN 1683 - 3597 E-ISSN 2521 - 3512) 21, no. 1 (2017): 98–104. http://dx.doi.org/10.31351/vol21iss1pp98-104.

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Nitrogen heterocycles are of a special interest because they constitute an important class of natural and non natural products, many of which exhibit useful biological activities.Among these nitrogen heterocycles are 1, 3, 4-thiadiazole containing compounds. The therapeutic effects of these derivatives have been well studied for a number of pathological conditions including inflammation, pain, or hypertension. Moreover, synthesis of thiadiazoles has attracted wide-spread attention due to their diverse applications as antibacterial, anticancer, antifungal anti-inflammatory and antidepressant ag

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Martinelli, Fabio, Alessandro Palmieri та Marino Petrini. "ChemInform Abstract: Metal-Free Synthesis of Imido Derivatives by Direct Oxidation of α-Amido Sulfones." ChemInform 42, № 5 (2011): no. http://dx.doi.org/10.1002/chin.201105067.

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33

Lozinski, Oleg, Tatyana Shokol, Oleg Shishkin, Vladimir Medvediev, and Vladimir Khilya. "The redeeming features of reaction of the 8-formyl-7-hydroxychromones with malononitrile." French-Ukrainian Journal of Chemistry 2, no. 1 (2014): 10–15. http://dx.doi.org/10.17721/fujcv2i1p10-15.

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A range of 4H,8H-pyrano[2,3-f]chromen-4,8-diones have been prepared using Knoevenagel reaction of the 8-formyl-7-hydroxychromones with malononitrile. The 4H,8H-pyrano[2,3-f]chromen-4,8-dione derivative was also obtained through the acid hydrolysis of the 8-imino-4H,8H-pyrano[2,3-f]chromen-4-one. 8-Formyl-7-hydroxychromone 1 was found to add two molecules of malononitrile through Michael addition resulting in formation of the 2-[8-amino-3-(4-chlorophenyl)-9-cyano-2-methyl-4-oxo-4H,10H-pyrano[2,3-f]chromen-10-yl]malononitrile.

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34

Pankova, Alena S., Pavel R. Golubev, Alexander F. Khlebnikov, Alexander Yu Ivanov, and Mikhail A. Kuznetsov. "Thiazol-4-one derivatives from the reaction of monosubstituted thioureas with maleimides: structures and factors determining the selectivity and tautomeric equilibrium in solution." Beilstein Journal of Organic Chemistry 12 (November 29, 2016): 2563–69. http://dx.doi.org/10.3762/bjoc.12.251.

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2-(Alkyl(aryl)amino)thiazol-4(5H)-ones can regioselectively be prepared from monoalkyl(aryl)thioureas and maleimides. In solution, the former heterocycles exist in a tautomeric equilibrium with 2-(alkyl(aryl)imino)thiazolidin-4-ones and the substituent on the exocyclic nitrogen atom governs the ratio of these tautomers. Isomers with the alkyl group in the endocyclic position can be obtained from N-methyl(ethyl)thioureas. 2D NMR spectroscopy and DFT calculations rationalize experimental results.

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35

Rak, Janusz, Karol Krzyminski, Piotr Skurski, et al. "X-Ray, Quantum Mechanics and Density Functional Methods in the Examination of Structure and Tautomerism of N-Methyl-Substituted Acridin-9-amine Derivatives." Australian Journal of Chemistry 51, no. 8 (1998): 643. http://dx.doi.org/10.1071/c97205.

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X-Ray diffraction has shown that N,N-dimethylacridin-9-amine (4) and N ,10-dimethylacridin-9-imine (5) both crystallize in the monoclinic space group P21/c (No. 14) with four molecules in the unit cell. The dimethylamino group in (4) is twisted through an angle of 58·6° relative to a nearly planar acridine moiety. On the other hand, the central ring in (5) is folded along the C(9) · · · N(10) axis through an angle of 26·3° and the exocyclic nitrogen atom with the methyl group attached to it is directed away from the concave side of the acridine nucleus. Theoretical ab initio Hartree–Fock (HF)

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36

Bakhite, Etify A., Abdu E. Abdel-Rahman, and Elham A. Al-Taifi. "Fluorine-Containing Heterocycles: Part I. Synthesis of New 7-(2-thienyl)-9-Trifluoromethylpyrido[3′,2′:4,5]Thieno[3,2-d]Pyrimidines and Related Fused Tetracyclic Systems." Journal of Chemical Research 2005, no. 3 (2005): 147–54. http://dx.doi.org/10.3184/0308234054213726.

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3-amino-6-(2-thienyl)-4-trifluoromethylthieno[2,3-b]pyridine-2-carboxamide (3) and 2-carbonitrile analogue 5 were prepared by reaction of 3-cyano-6-(2-thienyl)-4-trifluoromethylpyridine-2(1H)-thione (1) with chloroacetamide or chloroacetonitrile respectively. Heating compound 3 with triethyl orthoformate led to the formation of pyridothienopyrimidinone derivative 6. Reaction of 6 with phosphorus oxychloride produced 4-chloropyrimidine derivative 7 which underwent some nucleophilic displacements upon treatment with thiourea, piperidine, morpholine or hydrazine hydrate to give the target 4-subst

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37

Konovalova, S. A., A. P. Avdeenko, V. I. Lubenets, O. Z. Komarovska-Porokhnyavets, I. Yu Yakymenko, and E. N. Lysenko. "BIOLOGICAL ACTIVITY OF N-{3-[(4-METHYLBENZENE-1- SULFONYL)IMINO]-6-OXOCYCLOHEXA-1,4-DIEN-1-YL}ARYLAMIDES AND THEIR DERIVATIVES." Odesa National University Herald. Chemistry 26, no. 1(77) (2021): 37–47. http://dx.doi.org/10.18524/2304-0947.2021.1(77).226136.

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N-{3-[(4-Methylbenzene-1-sulfonyl)imino]-6-oxocyclohexa-1,4-dien-1-yl}arylamides and their derivatives were synthesized by the reaction of the corresponding N-(4-oxocyclohexa-2,5-dien-1-ylidene)arylsulfonamides with N-chloramides. The biological activity of the synthesized compounds was studied on test cultures of Escherichia coli 67, Staphylococcus aureus 209-p, Mycobacterium luteum VKM B-868 and fungi Candida tenuis VKM Y-70, Aspergillus niger VKM F-1119 by the method of diffusion of substances into agar on a solid nutrient medium. The degree of activity of the test compounds was determined

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Sabry, Nermien M., Eman M. Flefel, Mohamed A. Al-Omar, and Abd El-Galil E. Amr. "Synthesis and Antimicrobial Activities of Some New Synthesized Imide and Schiff's Base Derivatives." Journal of Chemistry 2013 (2013): 1–6. http://dx.doi.org/10.1155/2013/106734.

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A series of 2,6-bis(substituted thiazolopyrimi-dinyl) pyridine(2a,b)and corresponding Schiff's bases(3a–j)were synthesized from 2,6-bis-(3-amino-2-methyl-4-oxo-9-substituted-3,4-dihydropyrido-[30,20 : 4,5]-thieno[3,2-d]pyrimidin-7-yl)pyridines(1a,b)as starting materials. The compounds1a,bwere reacted with 2,3,4,5-tetrachlorophthalic anhydride in glacial acetic acid to give the corresponding bis-imides(2a,b). But they are treated with aromatic aldehydes in refluxing ethanol to afford the Schiff’s base derivatives(3a–j). The antimicrobial screening showed that many of these newly synthesized com

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Neelam, Dhakar, Ojha Swati, Lal Jat Jawahar, and L. Talesara G. "Synthesis and characterization of some 3-N-alkoxyphthalimido-5-arylidene-2- { [ 4-( 4-substituted phenyl)-1 ,3-thiazol-2-yl]imino }-1 ,3-thiazolidin-4-ones." Journal of Indian Chemical Society Vol. 85, June 2008 (2008): 660–64. https://doi.org/10.5281/zenodo.5816939.

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Synthetic Organic Chemistry Research Laboratory, Department of Chemistry, M. L. Sukhadia University. Udaipur-313 001, Rajasthan, India <em>E-mail :</em> gtalesara@yahoo.com <em>Manuscript received 17 July 2006. revised 6 September 2007, accepted 15 April 2008</em> 4-Chloro/methyl phenacyl bromide 1a-b reacted with thiourea to furnish 2-amino thiazole 2a-b through Hantzsch's process, which were converted to their thlazolidinone derivatives 4a-b, by the reaction of corresponding thiazolyl thiourea 3a-b with chloroacetic acid in the presence of sodium acetate. Subsequent treatment of 4a-b wit

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40

Winchester, B., C. Barker, S. Baines, G. S. Jacob, S. K. Namgoong та G. Fleet. "Inhibition of α-l-fucosidase by derivatives of deoxyfuconojirimycin and deoxymannojirimycin". Biochemical Journal 265, № 1 (1990): 277–82. http://dx.doi.org/10.1042/bj2650277.

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Deoxyfuconojirimycin (1,5-dideoxy-1,5-imino-L-fucitol) is a potent, specific and competitive inhibitor (Ki 1 x 10(-8) M) of human liver alpha-L-fucosidase (EC 3.2.1.51). Six structural analogues of this compound were synthesized and tested for their ability to inhibit alpha-L-fucosidase and other human liver glycosidases. It is concluded that the minimum structural requirement for inhibition of alpha-L-fucosidase is the correct configuration of the hydroxy groups at the piperidine ring carbon atoms 2, 3 and 4. Different substituents in either configuration at carbon atom 1 (i.e. 1 alpha- and b

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41

Kitamura, Teruyoshi, Atushi Hikita, Hironori Ishikawa, and Akira Fujimoto. "Photoinduced amino–imino tautomerization reaction in 2-aminopyrimidine and its methyl derivatives with acetic acid." Spectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy 62, no. 4-5 (2005): 1157–64. http://dx.doi.org/10.1016/j.saa.2005.04.008.

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42

Widiyana, Anita Puspa. "COMPUTATION DESIGN OF QUINAZOLINE-4(3H)-ON DERIVATIVES AS CYCLOOXYGENASE-2 (COX-2) INHIBITOR." Jurnal Farmasi Sains dan Praktis 7, no. 2 (2021): 163–70. http://dx.doi.org/10.31603/pharmacy.v7i2.4827.

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    The 3-(benzylideneamino)-2-(2,4-dichlorophenyl)-quinazoline-4(3H)-ones (BDCQ) are compounds developed as anticancer drugs and quinazolines. The activity and bioavailability of BDCQ derivatives as anticancer compounds that inhibit COX-2 can be predicted by computer programs and online servers. Substituents are added at positions 2 and 3 to the quinazoline-4(3H)-on ring, such as -H, -NO2, -OCH3, -N(CH3)2, -SO2NH2, -OH, and –OCH3. QSAR as COX-2 inhibitor analysis was performed by SPSS Ver. 21 software. Lipinski’s rule of five for determining bioavailability is performe

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43

Joy, Muthipeedika Nibin, Yadav D. Bodke, and Sandeep Telkar. "4-Methyl-7-Amino/Amido Coumarin Derivatives as Potential Antimicrobials and Antioxidants." Chemistry of Natural Compounds 56, no. 4 (2020): 614–20. http://dx.doi.org/10.1007/s10600-020-03106-y.

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44

Budesinsky, Milos, Ivana Cisarova, Jaroslav Podlaha, et al. "Structures of cyclic dipeptides: an X-ray and computational study of cis- and trans-cyclo(Pip-Phe), cyclo(Pro-Phe) and their N-methyl derivatives." Acta Crystallographica Section B Structural Science 66, no. 6 (2010): 662–77. http://dx.doi.org/10.1107/s0108768110040243.

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The crystal structures of eight cyclodipeptides are determined, incorporating pipecolic acid or proline and phenylalanine or N-methyl phenylalanine. This set of structures allows the evaluation of the effects on molecular conformation and crystal packing of imino acid ring-size, relative configuration of the two amino acids, and N-methylation. In the non-methylated compounds, hydrogen-bonding interactions form one-dimensional motifs that dominate the packing arrangement. Three compounds have more than one symmetry-independent molecule in the asymmetric unit (Z′ > 1), indicative of a broad a

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45

Zaid Mahmood Mohammed and Ayad Abed Ali Al-Hamashi. "Molecular Docking, Molecular Dynamic Simulation, ADMET, Synthesis, and Preliminary Cytotoxic Activity of New Triazole-Based Derivatives with Expected Histone Deacetylase Inhibition Activity." Iraqi Journal of Pharmaceutical Sciences 33, (4SI) (2025): 101–10. https://doi.org/10.31351/vol33iss(4si)pp101-110.

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Targeting histone deacetylase enzymes (HDACs) is an effective way to treat a variety of diseases, including cancer. A number of HDAC inhibitors (HDACi) have been clinically used. Most of the clinically used HDACi are pan-inhibitors and have poor pharmacokinetic properties. Therefore, several attempts are ongoing to develop new HDACis with optimum structural features to overcome the structural limitations. In this work, six new triazole-based compounds (k1-k6) were proposed via special modification of common pharmacophores of HDACi using 1,2,4-triazole as a zinc-binding group (ZBG), diverse gro

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46

K., R. JYOTHIKUMARI, and N. RAJASEKHARAN K. "Synthesis of Furopyrimidines : Condensation of Alkyl/Aryl lsothiocyanates with 2-Amino-3-cyanofuran Derivatives." Journal of Indian Chemical Society Vol. 68, Dec 1991 (1991): 660–62. https://doi.org/10.5281/zenodo.5968806.

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Department of Chemistry, University of Kerala, Trivandrum-695 034 <em>Manuscript received 3 July 1990. revised 4 January 1991, accepted 4 December 1991</em> Condensation of a few 2-amino-3-cyano-4,5-disubstituted-furan with isotbiocyanates in the presence of a base has been found to result in the formation or 3-alkyl/aryl-4-imino-5. 6-disubstituted-furo[2, 3-<em>d</em>]pyrimidine-2-thiones (3a- n). These compounds on refluxing with aqueous dimetbylformamide was found to rearrange and form 4-arylaminofuro[1,3-<em>d</em>)pyridine-2-thiones.

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47

Gorina, E. I., T. N. Popova, K. K. Shulgin, S. S. Popov, L. F. Panchenko, and O. A. Safonova. "The effect of biguanide derivatives on oxidative stress in rats with hyperglycemia." Biomeditsinskaya Khimiya 64, no. 3 (2018): 261–67. http://dx.doi.org/10.18097/pbmc20186403261.

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The effect of the synthetic biguanide derivatives N-[imino(1-piperidinyl)methyl]guanidine (NIPMG) and 1,3-dimethyl-5-[(carbamimidamidomethanimidoil) amino]benzoyl-1,3dicarboxylate (DCB) on the degree of proteins oxidative modification (POM) and the DNA fragmentation, the content of the lipid peroxidation primary products – conjugated dienes (CD), and the activity of glutathione antioxidant system in the liver and heart of rats with experimental hyperglycemia was investigated. Administration of the biguanides (15.0 mg/kg) to hypoglycemic rats promoted reduction of the free radical processes int

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Dawson, Denisha Y., and John Arnold. "Organotantalum Bis(amidinate) Complexes: Synthesis and Characterization of Methyl, Methylidene, Benzyl, and Imido Derivatives." Organometallics 16, no. 6 (1997): 1111–13. http://dx.doi.org/10.1021/om961052t.

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49

Ge, Yuan Wen, and Paul R. Sharp. "Late transition metal .mu.-oxo and .mu.-imido complexes. 5. Addition of methylene chloride and methyl iodide to the phenyl ring of aryl imido/amido complexes of rhodium." Journal of the American Chemical Society 112, no. 9 (1990): 3667–68. http://dx.doi.org/10.1021/ja00165a066.

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Satheesh, Sandhya, Akhila Radha, Krishnapriya Girija, Kallikat Rajasekharan та Priya Maheswari. "Hindered phenolic aminothiazoles - synthesis, α-glucosidase, α-amylase inhibitory and antioxidant activities". Journal of the Serbian Chemical Society 82, № 10 (2017): 1087–95. http://dx.doi.org/10.2298/jsc161005084s.

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Base-catalysed heterocyclization of either N-aryl-N'-[imino(nitroamino) methyl]thioureas or N-aryl-N'-cyanothioureas by reaction with 2-bromo- 1-(2,6-di-t-butyl-4-hydroxyphenyl)ethanone afforded 4-amino-2-(arylamino)- -5-(3,5-di-t-butyl-4-hydroxybenzoyl)thiazoles, designed as molecular hybrids of hindered phenolic and 2-aminothiazole moieties. These compounds were screened for their inhibition activity on carbohydrate hydrolyzing enzymes. Thus, [4-amino-2-(phenylamino)-5-thiazolyl](3,5-di-t-butyl-4-hydroxyphenyl)- methanone exhibited ?-glucosidase inhibition activity with an IC50 value of 117

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