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Journal articles on the topic 'Amino -6 methyl Pyridine'

Author: Grafiati

Published: 5 June 2025

Last updated: 2 August 2025

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1

Beuchel, Andreas, Richard Goddard, Peter Imming, and Rüdiger W. Seidel. "A solid solution of ethyl and d 3-methyl 2-[(4-methylpyridin-2-yl)amino]-4-(pyridin-2-yl)thiazole-5-carboxylate." Acta Crystallographica Section E Crystallographic Communications 76, no. 8 (2020): 1255–59. http://dx.doi.org/10.1107/s2056989020008956.

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The synthesis of ethyl 2-[(4-methylpyridin-2-yl)amino)-4-(pyridin-2-yl)thiazole- 5-carboxylate via the Hantzsch reaction and partial in situ transesterification during recrystallization from methanol-d 4 to the d 3-methyl ester, resulting in the title solid solution, ethyl 2-[(4-methylpyridin-2-yl)amino)-4-(pyridin-2-yl)thiazole-5-carboxylate–d 3-methyl 2-[(4-methylpyridin-2-yl)amino)-4-(pyridin-2-yl)thiazole-5-carboxylate (0.88/0.12), 0.88C17H16N4O2S·0.12C16D3H11N4O2S, is reported. The refined ratio of ethyl to d 3-methyl ester in the crystal is 0.880 (6):0.120 (6). The pyridine ring is signi

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2

Katta, Srinivasa Rao, and Gajanand Thakre. "Characterization of Degradation Products of Selpercatinib by Mass Spectrometry: Optimization of Stability-Indicating HPLC Method for Separation and Quantification of Process Related Impurities of Selpercatinib." Asian Journal of Chemistry 36, no. 2 (2024): 341–52. http://dx.doi.org/10.14233/ajchem.2024.30884.

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The study aimed to investigate a novel approach by utilizing liquid chromatography in coupled with mass spectrometry (LC-MS) to resolve, analyze and characterize significantly less quantity of stress degradation products (DPs) of selpercatinib along with its process related impurities. The analytes resolved on ZORBAX Eclipse (250 mm) stationary phase that was maintained employing 0.5 M sodium perchlorate at pH 5.4 methanol and acetonitrile in 50:20:30 (v/v) pumped at 0.8 mL/min isocratic flow and 241 nm wavelength. The method produces very high correlate linear curve in 30-240 μg/mL for selper

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3

Halim, Shimaa Abdel, and Magdy A. Ibrahim. "Synthesis, spectral analysis, quantum studies, NLO, and thermodynamic properties of the novel 5-(6-hydroxy-4-methoxy-1-benzofuran-5-ylcarbonyl)-6-amino-3-methyl-1H-pyrazolo[3,4-b] pyridine (HMBPP)." RSC Advances 12, no. 21 (2022): 13135–53. http://dx.doi.org/10.1039/d2ra01469f.

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Ring opening followed by ring closure reactions of 4-methoxy-5-oxo-5H-furo[3,2-g] chromene-6-carbonitrile with 5-amino-3-methyl-1H-pyrazole gave the novel 5-(6-hydroxy-4-methoxy-1-benzofuran-5-ylcarbonyl)-6-amino-3-methyl-1H-pyrazolo[3,4-b] pyridine.

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4

Carter, Emma, Katherine M. Sharples, James A. Platts, and Damien M. Murphy. "Structure determination of bound nitrogen-based adducts with copper(ii) acetylacetonato; an EPR, ENDOR and DFT study." Physical Chemistry Chemical Physics 17, no. 17 (2015): 11445–54. http://dx.doi.org/10.1039/c5cp00559k.

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<sup>1</sup>H ENDOR spectroscopy and DFT have been used to characterize the coordination and geometry of bound pyridine and substituted pyridine substrates in the [Cu(acac)<sub>2</sub>](pyridine) and [Cu(acac)<sub>2</sub>](2-amino-6-methyl-pyridine) adducts.

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5

Ghalia, Mohamed H., Mohamed Abd El-Hamid, Mohamed A. Zweil, Abd El-Galil E. Amr, and Shimaa A. Moafi. "Synthesis and Reactions of New Chiral Linear and Macrocyclic Tetraand Penta-peptide Candidates." Zeitschrift für Naturforschung B 67, no. 8 (2012): 806–18. http://dx.doi.org/10.5560/znb.2012-0116.

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9a A series of linear and macrocyclic pentapeptide derivatives have been prepared via the coupling of pyridine-2,6-dicarboxylic acid (1) or pyridine-2,6-dicarbonyl dichloride (2) with appropriate amino acid methyl esters. The coupling of 1or 2with aminoacid methyl esters gave the corresponding pyridine dipeptide methyl esters 3, which were hydrolyzed with sodium hydroxide to the corresponding acids 4. The latter compounds 4were coupled with other amino acid methyl esters to afford the corresponding tetrapeptide esters 5, which were hydrolyzed with sodium hydroxide to the corresponding acids 6.

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6

Dmitrieva, I. G., V. K. Vasilin, V. V. Dotsenko, and N. A. Aksenov. "6-(Pyrazol-1-yl)pyrazolo[3,4-b]pyridines: Synthesis, Structure, and Wheat Growth Regulating Activity." Russian Journal of General Chemistry 94, no. 10 (2024): 2603–15. http://dx.doi.org/10.1134/s1070363224100050.

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Abstract 4-Methyl-6-pyrazolyl-2-chloronicotinonitriles were synthesized by the reaction of 6-hydrazino-4-methyl-2-chloronicotinonitriles with 1,3-diketones. Upon treatment with hydrazine and methylhydrazine, 4-methyl-6-pyrazolyl-2-chloronicotinonitriles were converted into the corresponding 3-amino-4-methyl-6-pyrazolyl-1H-pyrazolo[3,4-b]pyridines. A similar reaction involving 1,1-dimethylhydrazine and ethylhydrazine was accompanied by elimination of the alkyl substituent and also led to the formation of 3-amino-6-pyrazolyl-1H-pyrazolo[3,4-b]pyridines. Acylation and carbamoylation of the prepar

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7

Bhuva, V. V., V. N. Bhadani, H. D. Purohit, and Dipak M. Purohit. "Synthesis, Spectral Studies Antibacterial and Antifungal Activity of 2"-Amino-4"-[2 -(4'-Chlorophenyl)-6-Methyl Imidazo[1, 2-a]Pyridin-3-yl]-6"-Aryl Nicotinonitrile." International Letters of Chemistry, Physics and Astronomy 49 (April 2015): 161–66. http://dx.doi.org/10.18052/www.scipress.com/ilcpa.49.161.

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Pyridine nucleus plays an important role in medicine, agriculture and industrial chemistry. With a view of biological activities and variety of industrial applications, some new 2" – amino - 4" - [2 - (4' -chlorophenyl)-6-methyl imidazo [1, 2-a] pyridin-3-yl]-6"-aryl nicotinonitriles ( 4a-4l ) have been synthesized. The products have been assayed for their biological activity against Gram +ve, Gram –ve bacteria and fungi. Some of the products showed moderate activity in concentration 50μg/ml. The structures of the products have been elucidated by IR, 1H-NMR, Mass spectral data, elemental analy

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8

Bhuva, V. V., V. N. Bhadani, H. D. Purohit, and Dipak M. Purohit. "Synthesis, Spectral Studies Antibacterial and Antifungal Activity of 2"-Amino-4"-[2 -(4'-Chlorophenyl)-6-Methyl Imidazo[1, 2-a]Pyridin-3-yl]-6"-Aryl Nicotinonitrile." International Letters of Chemistry, Physics and Astronomy 49 (April 7, 2015): 161–66. http://dx.doi.org/10.56431/p-1ap4oq.

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Pyridine nucleus plays an important role in medicine, agriculture and industrial chemistry. With a view of biological activities and variety of industrial applications, some new 2" – amino - 4" - [2 - (4' -chlorophenyl)-6-methyl imidazo [1, 2-a] pyridin-3-yl]-6"-aryl nicotinonitriles ( 4a-4l ) have been synthesized. The products have been assayed for their biological activity against Gram +ve, Gram –ve bacteria and fungi. Some of the products showed moderate activity in concentration 50μg/ml. The structures of the products have been elucidated by IR, 1H-NMR, Mass spectral data, elemental analy

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9

Panaetov, A. O., V. D. Strelkov, V. V. Dotsenko, et al. "Mannich reaction involving 6-amino-4-methyl2-(thio)oxo-1,2-dihydropyridine-3,5-dicarbonitriles." Журнал общей химии 93, no. 7 (2023): 1007–22. http://dx.doi.org/10.31857/s0044460x23070041.

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The reaction of (1-ethoxyethylidene)malononitrile with cyanoacetamide or cyanothioacetamide yielded 6-amino4-methyl-2-(thio)oxo-1,2-dihydropyridine-3,5-dicarbonitriles. The resulting pyridine derivatives enter into an aminomethylation reaction with an excess of formaldehyde and primary amines with the formation of previously unknown 8-methyl-6-oxo-3-R-1,3,4,6-tetrahydro-2 H -pyrido[1,2- a ][ 1,3,5]triazine-7,9-dicarbonitriles. Further treatment of 6-amino-4-methyl-2-thioxo-1,2-dihydropyridine-3,5-dicarbonitrile and its oxygen analogue with excess formaldehyde leads to the formation of 3,10-dim

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10

Shin, Jong Won, Dong Won Lee, Dae-Woong Kim та Dohyun Moon. "Crystal structure of dichlorido{2-methyl-2-[(pyridin-2-ylmethyl)amino]propan-1-ol-κ3N,N′,O}copper(II) from synchrotron data". Acta Crystallographica Section E Crystallographic Communications 72, № 10 (2016): 1400–1403. http://dx.doi.org/10.1107/s2056989016013773.

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The title compound, [CuCl2(C10H16N2O)], has been synthesized and characterized by synchrotron single-crystal X-ray diffraction and FT–IR spectroscopy. The 2-methyl-2-[(pyridin-2-ylmethyl)amino]propan-1-ol (mpmapOH) ligand, including pyridine, amine and hydroxy groups, was synthesized by the reaction of 2-amino-2-methylpropan-1-ol with pyridine-2-carbaldehyde and was characterized by NMR spectroscopy. In its CuIIcomplex, the metal ion has a distorted square-pyramidal coordination geometry with two N and one O atom of the mpmapOH ligand and one chloride anion in the equatorial plane, and the sec

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11

Xue, Xiaoyan, Xia Chen та Hongbo Tong. "Dichloridobis{6-methyl-2-[(trimethylsilyl)amino]pyridine-κN1}cobalt(II)". Acta Crystallographica Section E Structure Reports Online 65, № 8 (2009): m957. http://dx.doi.org/10.1107/s1600536809027937.

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12

Ravlee, Inguva, Ramaiah Sivakumar, Nithyanantham Muruganantham, Navaneetharaman Anbalagan, Vedachalam Gunasekaran, and Joseph Thomas Leonard. "Pharmacological Evaluation of Some New 6-Amino/Methyl Pyridine Derivatives." CHEMICAL & PHARMACEUTICAL BULLETIN 51, no. 2 (2003): 162–70. http://dx.doi.org/10.1248/cpb.51.162.

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13

Sachdeva, Harshita, Diksha Dwivedi, and Rekha Saroj. "Alum Catalyzed Simple, Efficient, and Green Synthesis of 2-[3-Amino-5-methyl-5-(pyridin-3-yl)-1,5-dihydro-4H-1,2,4-triazol-4-yl]propanoic Acid Derivatives in Aqueous Media." Scientific World Journal 2013 (2013): 1–7. http://dx.doi.org/10.1155/2013/716389.

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Alum (KAl(SO4)2·12H2O) is an inexpensive, efficient, and nontoxic catalyst used for the synthesis of 2-[3-amino-5-methyl-5-(pyridin-3-yl)-1,5-dihydro-4H-1,2,4-triazol-4-yl]propanoic acid derivatives in aqueous media by the reaction of 3-acetyl pyridine(1), amino acids(2)/(6), and thiosemicarbazide(4)at 80°C. This methodology offers significant improvements for the synthesis of products with regards to the yield of products, simplicity in operation, and green aspects by avoiding toxic catalysts which uphold the motto of green chemistry. Synthesized compounds have been characterized by FT-IR,13C

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14

Sundaraganesan, N., C. Meganathan, and Mustafa Kurt. "Molecular structure and vibrational spectra of 2-amino-5-methyl pyridine and 2-amino-6-methyl pyridine by density functional methods." Journal of Molecular Structure 891, no. 1-3 (2008): 284–91. http://dx.doi.org/10.1016/j.molstruc.2008.03.051.

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15

Deuther-Conrad, Winnie, Dirk Schepmann, Isabel Iriepa та ін. "2-{N-[ω-(1-Benzylpiperidin-4-yl)alkyl]amino}-6-[(prop-2-yn-1-yl)amino]pyridine-3,5-dicarbonitriles Showing High Affinity for σ1/2 Receptors". International Journal of Molecular Sciences 26, № 3 (2025): 1266. https://doi.org/10.3390/ijms26031266.

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Sigma receptors (σRs) represent very attractive biological targets for the development of potential agents for the treatment of several neurological disorders. In the search for new small molecule drugs against neuropathic pain, we identified 2-{[2-(1-benzylpiperidin-4-yl)ethyl]amino}-6-[methyl(prop-2-yn-1-yl)amino]pyridine-3,5-dicarbonitrile (5) as a polyfunctionalized small pyridine with potent dual-target activities against acetylcholinesterase (AChE) (IC50 = 13 nM) and butyrylcholinesterase (BuChE) (IC50 = 3.1 µM), exhibiting high σ1R affinity (Ki(hσ1R) = 1.45 nM) and 290-fold selectivity

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16

Wang, Qian, Dianxiang Zhou, Chunmei Li, Qingqing Shao, and Shujiang Tu. "Methyl 6-amino-5-cyano-4-(4-fluorophenyl)-2-methylpyridine-3-carboxylate." Acta Crystallographica Section E Structure Reports Online 63, no. 11 (2007): o4220. http://dx.doi.org/10.1107/s1600536807047502.

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In the molecule of the title compound, C15H12FN3O2, the benzene and pyridine rings are oriented at a dihedral angle of 54.91 (2)°. In the crystal structure, there are intermolecular N—H...N hydrogen bonds.

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17

Karpov, Sergey, Arthur Grigor’ev, Yakov Kayukov, Iuliia Gracheva, and Victor Tafeenko. "Cascade Regioselective Heterocyclization of 2-Acyl-1,1,3,3-tetracyanopropenides: Synthesis of Pyrrolo[3,4-c]pyridine and Pyrrolo[3,4-d]thieno[2,3-b]pyridine Derivatives." Synlett 28, no. 13 (2017): 1592–95. http://dx.doi.org/10.1055/s-0036-1588823.

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2-Acyl-1,1,3,3-tetracyanopropenides (ATCN) undergo cascade heterocyclization under the action of aliphatic thiols, resulting in the formation of 6-(alkylthio)-4-amino-1-aryl(alkyl)-1-hydroxy-3-oxo-2,3-dihydro-1H-pyrrolo[3,4-c]pyridine-7-carbonitriles. The involvement of methyl mercaptoacetate to this reaction leads to the formation of the methyl 4,8-diamino-1-aryl-1-hydroxy-3-oxo-2,3-dihydro-1H-pyrrolo[3,4-d]thieno[2,3-b]pyridine-7-carboxylates, containing a new fused heterocyclic scaffold.

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18

Prek, Benjamin, Uroš Grošelj, Marta Kasunič, Silvo Zupančič, Jurij Svete, and Branko Stanovnik. "Reactions of Methyl Ketones and (Hetero)arylcarboxamides with N,N-Dimethylacetamide Dimethyl Acetal. A Simple Metal-Free Synthesis of 2,4,6-Trisubstituted Pyridines." Australian Journal of Chemistry 68, no. 2 (2015): 184. http://dx.doi.org/10.1071/ch14349.

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Two metal-free syntheses of 2,4,6-trisubstituted pyridines 10a–m and 16a–j are described. N,N,6-Trimethyl-4-(substituted)pyridin-2-amines 10 were prepared from aryl or heteroaryl methyl ketones which were transformed with N,N-dimethylacetamide dimethyl acetal (DMADMA) into enaminones 4a–m, followed by treatment with ammonium acetate to give (Z)-3-amino-1-(substituted)but-2-en-1-ones 5a–m. These were treated with DMADMA under microwave irradiation in a closed vessel at 130°C, to give via intermediates 7–9 the final products 10a–m. N2,N2,N4,N4-Tetramethyl-6-(substituted) pyridine-2,4-diamines 16

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19

Napitupulu, Mery, Geoffrey A. Lawrance, Guy J. Clarkson, and Peter Moore. "Methyl 2-[N-(2′-Pyridylmethyl)carbamyl]pyridine-6-carboxylate: A Precursor for Unsymmetrical Diamide Ligands." Australian Journal of Chemistry 59, no. 11 (2006): 796. http://dx.doi.org/10.1071/ch06310.

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Methyl 2-[N-(2′-pyridylmethyl)carbamyl]pyridine-6-carboxylate (H1), prepared by reaction of a 1:1 ratio of the methyl diester of pyridine-2,6-dicarboxylic acid and 2-aminomethylpyridine, can form 1:2 M:L complexes by acting as a tridentate ligand, as exemplified by a crystal structure analysis of [CoIII(1)2](ClO4) where each ligand is coordinated by the amido group and its two flanking pyridine groups, with the ester group, a relatively poor donor, remaining unbound. The acid formed upon ester hydrolysis, hydrogen 2-[N-(2′-pyridylmethyl)carbamyl]pyridine-6-carboxylate (H22), has been isolated

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20

Dotsenko, Victor V., Nawras T. Jassim, Azamat Z. Temerdashev, Zainab R. Abdul-Hussein, Nicolai A. Aksenov, and Inna V. Aksenova. "New 6′-Amino-5′-cyano-2-oxo-1,2-dihydro-1′H-spiro[indole-3,4′-pyridine]-3′-carboxamides: Synthesis, Reactions, Molecular Docking Studies and Biological Activity." Molecules 28, no. 7 (2023): 3161. http://dx.doi.org/10.3390/molecules28073161.

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The purpose of this work was to prepare new isatin- and monothiomalondiamide-based indole derivatives, as well as to study the properties of the new compounds. The four-component reaction of 5-R-isatins (R = H, CH3), malononitrile, monothiomalonamide (3-amino-3-thioxo- propanamide) and triethylamine in hot EtOH yields a mixture of isomeric triethylammonium 6′-amino-3′-(aminocarbonyl)-5′-cyano-2-oxo-1,2-dihydro-1′H- and 6′-amino-3′-(aminocarbonyl)- 5′-cyano-2-oxo-1,2-dihydro-3′H-spiro[indole-3,4′-pyridine]-2′-thiolates. The reactivity and structure of the products was studied. We found that oxi

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21

Marchalín, Štefan, Dušan Ilavský, Jaroslav Kováč, and Milan Bruncko. "Synthesis and reactions of 5-acetyl-2-amino-3-cyano-4-(5-X-2-furyl)-6-methyl-4H-pyrans." Collection of Czechoslovak Chemical Communications 55, no. 3 (1990): 718–27. http://dx.doi.org/10.1135/cccc19900718.

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Substituted 2-amino-4-(5-X-2-furyl)-4H-pyrans IIIa-IIIe have been prepared by a cyclization reaction of 5-X-2-furylmethylenepropanedinitriles IIa-IIe with 2,4-pentanedione. In reaction of 3-(5-X-2-furyl)-methylene-2,4-pentanediones Ia-Ie with propanedinitrile the formation of 4H-pyrans IIIa-IIIe is accompanied, depending on the catalyst type, by the formation of 5-X-2-furylmethylenepropanedinitriles IIa-IIe. 2-(4-Methylbenzylideneamino)-4H-pyran (V), 2-formylamino-4H-pyran (VI), and 3H, 5H-pyrano[2,3-d]pyrimidine-4-one (VII) have been synthesized by functional modifications of the amino group

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22

Mohammed, Tiba Ibrahim. "Synthesis of New Azo–Schiff Base Complexes and Study of their Antibacterial Activity." International Journal Papier Advance and Scientific Review 4, no. 1 (2023): 42–56. http://dx.doi.org/10.47667/ijpasr.v4i1.206.

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In this research, we synthesized new azo-schiff base derivatives (4-9). These derivatives of azo compounds (1-3) that synthesized from 4-ethoxyaniline and drivatives of aldehyde such as, 4-aminobenzaldehyde, 4- hydroxybenzaldehyde and 4-ethoxybenzaldehyse to produce azo compounds (1-3). The compounds (1-3) reacted with differents aldehyde such as, isonicotinic hydrazide to produce N'-[(Z)-{3-[(E)-(4-ethoxyphenyl)diazenyl]-4-subs.phenyl}-methylidene]pyridine-4-carbohydrazide derivatives (4-6) and 3-amino pyridine to produce 2-[(E)-(4-ethoxyphenyl)diazenyl]-4-{(E)-[(pyridin-3-yl)imino]-methyl}su

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23

Wanare, Rajendra K. "Design, Synthesis and Evaluation of Novel Thiopyrimidine-Glucuronide Compounds with Promising Biological Activities." Asian Journal of Organic & Medicinal Chemistry 7, no. 3 (2022): 239–44. http://dx.doi.org/10.14233/ajomc.2022.

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3-Methyl-5-acetyl-7-[(2-sulfanylidene-6-aryl-1,2-dihydropyrimidin-4-yl)amino]-1,2-benzisoxazoles (2a-n) were obtained from N-(5-acetyl-3-methyl-1,2-benzoxazol-7-yl)-3-arylprop-2-enamides (1a-n) and thiourea. Products (2a-n) oxidized with KMnO4 to afford 5-acetyl-7-[(2-sulfanylidene-6-aryl-1,2- dihydropyrimidin-4-yl)amino]-1,2-benzisoxazole-3-carboxylic acids (3a-n). Reaction of 3a-n with D-gluconic acid and pyridine yielded β-D-glucuronosyl-5-acetyl-7-[(2-sulfanylidene-6-aryl-1,2- dihydropyrimidin-4-yl)amino]-1,2-benzisoxazol-3-carboxylates (4a-n). The present synthesis featured the formation

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24

K. Wanare, Rajendra. "Design, Synthesis and Evaluation of Novel Thiopyrimidine-Glucuronide Compounds with Promising Biological Activities." Asian Journal of Organic & Medicinal Chemistry 7, no. 3 (2022): 239–44. http://dx.doi.org/10.14233/ajomc.2022.ajomc-p397.

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3-Methyl-5-acetyl-7-[(2-sulfanylidene-6-aryl-1,2-dihydropyrimidin-4-yl)amino]-1,2-benzisoxazoles (2a-n) were obtained from N-(5-acetyl-3-methyl-1,2-benzoxazol-7-yl)-3-arylprop-2-enamides (1a-n) and thiourea. Products (2a-n) oxidized with KMnO4 to afford 5-acetyl-7-[(2-sulfanylidene-6-aryl-1,2-dihydropyrimidin-4-yl)amino]-1,2-benzisoxazole-3-carboxylic acids (3a-n). Reaction of 3a-n with D-gluconic acid and pyridine yielded β-D-glucuronosyl-5-acetyl-7-[(2-sulfanylidene-6-aryl-1,2-dihydropyrimidin-4-yl)amino]-1,2-benzisoxazol-3-carboxylates (4a-n). The present synthesis featured the formation of

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25

Bhuva, V. V., V. N. Bhadani, H. D. Purohit, and Dipak M. Purohit. "Synthesis, Spectral Studies and Biological Screening of 2-(4'-Chlorophenyl)-6-Methyl-(3-N, N’-Diaryl/Dialkyl Amino Methyl)-Imidazo[1,2-a]Pyridine." International Letters of Chemistry, Physics and Astronomy 49 (April 2015): 167–71. http://dx.doi.org/10.18052/www.scipress.com/ilcpa.49.167.

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2-(4'-chlorophenyl)-6-methyl- (3-N, N'- diaryl/dialkyl amino methyl)-imidazo [1, 2-a] pyridine (4a-4l) has been synthesized. The products have been assayed for their biological activity against Gram +ve, Gram –ve bacteria and fungi. Some of the products showed moderate activity in concentration 50μg/ml. The structures of the products have been elucidated by IR, 1H-NMR, Mass spectral data, elemental analysis and thin layer chromatography.

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26

Bhuva, V. V., V. N. Bhadani, H. D. Purohit, and Dipak M. Purohit. "Synthesis, Spectral Studies and Biological Screening of 2-(4'-Chlorophenyl)-6-Methyl-(3-N, N’-Diaryl/Dialkyl Amino Methyl)-Imidazo[1,2-a]Pyridine." International Letters of Chemistry, Physics and Astronomy 49 (April 7, 2015): 167–71. http://dx.doi.org/10.56431/p-26vqfo.

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2-(4'-chlorophenyl)-6-methyl- (3-N, N'- diaryl/dialkyl amino methyl)-imidazo [1, 2-a] pyridine (4a-4l) has been synthesized. The products have been assayed for their biological activity against Gram +ve, Gram –ve bacteria and fungi. Some of the products showed moderate activity in concentration 50μg/ml. The structures of the products have been elucidated by IR, 1H-NMR, Mass spectral data, elemental analysis and thin layer chromatography.

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27

Dotsenko, Victor V., Vladimir A. Dushenko, Nikolai A. Aksenov, Inna V. Aksenova, and Evgeniy E. Netreba. "The First Synthesis of [1,2]oxaphosphinino[6,5-c]pyrazoles by Thiophosphorylation of 6-Aminopyrano[2,3-c]pyrazole-5-Carbonitriles." Proceedings 9, no. 1 (2018): 26. http://dx.doi.org/10.3390/ecsoc-22-05680.

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The reaction of 6-amino-3-methyl-2,4-dihydropyrano[2,3-c]pyrazole-5-carbonitriles with phosphorus sulfide in boiling pyridine leads to the formation of the unexpected [1,2]oxaphosphinino[6,5-c]pyrazoles. The structure of the products was confirmed with 2D Nuclear Magnetic Resonance (NMR) spectroscopy and X-ray analysis.

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28

Yao, Jianan, Chunbo Wang, Xiaogang Zhao, Hongwei Zhou, Chunhai Chen, and Daming Wang. "Highly transparent and soluble polyimides with synergistic effects of pyridine and cyclohexane." High Performance Polymers 30, no. 4 (2017): 418–26. http://dx.doi.org/10.1177/0954008317698548.

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In order to prepare novel polyimides (PI) with high transparency and solubility in common solvents, three diamine monomers containing pyridine or methyl-substituted pyridine and cyclohexane, 1,1′-bis[4-(5-amino-2-pyridinoxy)phenyl]cyclohexane (IIIa), 1,1′-bis[4-(5-amino-3-methyl-2-pyridinoxy)phenyl]cyclohexane (IIIb), and 1,1′-bis[4-(5-amino-2-methyl-6-pyridinoxy)phenyl]cyclohexane (IIIc), were synthesized and characterized. The diamine monomer (IIIa) was subsequently polymerized with 3,3′,4,4′-oxydiphthalic anhydride, 4,4′-(hexafluoroisopropylidene)-diphthalic anhydride (6FDA) to obtain PIs,

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29

Reddy, B. Siva, and K. R. S. Prasad. "Design, Synthesis and Antibacterial Activity of N-(3-((4-(6-(2,2,2- Trifluoroethoxy)pyridin-3-yl)-1H-imidazol-2-yl)methyl)oxetan-3-yl)amide Derivatives." Asian Journal of Chemistry 33, no. 3 (2021): 577–82. http://dx.doi.org/10.14233/ajchem.2021.23039.

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A new series of N-(3-((4-(6-(2,2,2-trifluoroethoxy)pyridin-3-yl)-1H-imidazol-2-yl)methyl)oxetan-3- yl)amide derivatives (10a-h)were synthesized by the reaction of 3-((4-(6-(2,2,2-trifluoroethoxy)pyridin- 3-yl)-1H-imidazol-2-yl)methyl)oxetan-3-amine (8) with various carboxylic acids in the presence of T3P catalyst. The reaction is usually furnished within 60 min with good isolated yields. Coupling of 6-(2,2,2-trifluoroethoxy) nicotinic acid (1) with Weinreb amine hydrochloride gave N-methoxy-Nmethyl- 6-(2,2,2-trifluoroethoxy) nicotinamide (2). Compound 3 was synthesized by the Grignard reaction

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30

Kondratov, Ivan S., Oleksandr O. Grygorenko, Oleksandr O. Stepaniuk та ін. "Synthesis of Fused Pyridine Carboxylates by Reaction of β-Alkoxyvinyl Glyoxylates with Amino Heterocycles". Synthesis 52, № 13 (2020): 1915–26. http://dx.doi.org/10.1055/s-0039-1707987.

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An efficient approach to the preparation of pyridine carboxylates fused with 5- or 6-membered heteroaromatic rings is described. The method relied on the Combes-type condensation of the low-molecular-weight β-alkoxyvinyl glyoxylates as CCC bis-electrophiles and with heteroaromatic amines as NCC binucleophiles. In most experiments, β-alkoxyvinyl glyoxylates without additional substituent at the β position led to the corresponding α-pyridine carboxylates (67–87% yield). In the case of β-methyl-substituted derivative, γ-pyridine carboxylates were obtained in 84–99% yield. It was found that regi

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31

Zee, Yoke Leng Michelle, Lawrence R. Gahan, and Gerhard Schenk. "A Potentially Polymerizable Heterodinuclear FeIIIZnII Purple Acid Phosphatase Mimic. Synthesis, Characterization, and Phosphate Ester Hydrolysis Studies." Australian Journal of Chemistry 64, no. 3 (2011): 258. http://dx.doi.org/10.1071/ch10424.

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An analogue of the purple acid phosphatase biomimetic 2-((bis(pyridin-2-ylmethyl)amino)methyl)-6-(((2-hydroxybenzyl)(pyridin-2-ylmethyl)amino)methyl)-4-methylphenol has been synthesized. The analogue, 2-((bis(pyridin-2-ylmethyl)amino)methyl)-6-(((2-hydroxy-4-(4-vinylbenzyloxy)benzyl)(pyridin-2-ylmethyl)amino)methyl)-4-methylphenol (H2BPBPMPV) possesses a pendant olefin suitable for copolymerization. Complexation with FeIII/ZnII resulted in the complex [FeIIIZnII(BPBPMPV)(CH3COO)2](ClO4), characterized with mass spectrometry, microanalysis, UV/vis, and IR spectrometry. The catalytic activity of

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32

Neamah, Rawaa, та Shaimaa Adnan. "Study the Biological Activity for Shiff Base and Β – Lactam Compounds that Synthesis and Identification from Pyrimidine Derivatives". International Journal of Pharmaceutical Quality Assurance 11, № 01 (2013): 37–39. http://dx.doi.org/10.25258/ijpqa.11.1.12.

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In This study We are synthesis and characterization of some Schiff base and β- lactam derivatives) by three steps. The First react 2-amino-4-Chloro-6-methyl pyrimidine with 4-amino acetophenone in an acid medium to get shiff base derivative(E)-4-(1-((4-Chloro-6-methyl pyridine-2-yl)imino)ethyl)aniline (1), the second step (1) react with (3,4- dimethoxybenzal dehyde,4-methyl benzaldehyde,4-dimethylamino benzaldehyde,4-bromo benzaldehyde,4–hydroxy benzaldehyde, 4-Nitro benzaldehyde) to get Schiff base derivatives (2-7), the last step (2-7) derivatives react with Chloro acetyl chloride to get –β-

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33

Ho, Yuh-Wen, and Maw Cherng Suen. "Thioxopyrimidine in Heterocyclic Synthesis I: Synthesis of Some Novel 6-(Heteroatom-substituted)-(thio)pyrimidine Derivatives." Journal of Chemistry 2013 (2013): 1–15. http://dx.doi.org/10.1155/2013/765243.

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A series of novel N-cycloalkanes, morpholine, piperazines, pyrazole, pyrimidine, benzimidazolo[1,2-a]pyrimidine, 1,2,3,4-tetrazolo[1,5-a]pyrimidine, azopyrazolo[1,5- a]pyrimidine, pyrimido[4', 5':3,4]pyrazolo[1,5-a]pyrimidines and pyridine derivatives incorporating a 5-cyano-4-methyl-2-phenyl-(thio)pyrimidine moiety were obtained by the intramolecular cyclization of 6-methylthio-pyrimidine, 6-(benzoylmethyl)thio- pyrimidine and 2-[(5-cyano-4-methyl-2-phenylpyrimidin-6-yl)thio]-3-dimethyl- amino-1-phenyl-prop-2-en-1-one with appropriate amines and enaminone compounds, respectively. The structur

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34

Francis, John E., and Michael A. Moskal. "A general synthesis of 5,7-diaminoimidazo[4,5-b]pyridine ribosides ("2-amino-1-deazaadenosines") from 5-amino-4-imidazolecarboxamide riboside (AICA riboside)." Canadian Journal of Chemistry 70, no. 5 (1992): 1288–95. http://dx.doi.org/10.1139/v92-166.

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A short general synthesis of 5-substituted 5,7-diaminoimidazo[4,5-b]pyridines from 5-amino-4-imidazolecarboxamide riboside (AICA riboside) was designed to prepare isosteres of substituted 2-aminoadenosines that are selective adenosine A2 receptor agonists. AICA riboside was converted to a hydroxyl-protected 5-amino-4-imidazolecarbonitrile riboside and reacted with an N,N-disubstituted acetamide in the presence of phosphoryl chloride. Sodium hydride treatment completed the ring closure and introduced the 7-amino group. The hydroxyl protecting groups were removed under standard conditions. N-Sub

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35

Dotsenko, Victor V., Anna E. Sinotsko, Vladimir D. Strelkov, et al. "Alkyl 4-aryl-6-amino-7-phenyl-3-(phenylimino)-4,7-dihydro-3H-[1,2]dithiolo[3,4-b]pyridine-5-carboxylates: Synthesis and Agrochemical Studies." Molecules 28, no. 2 (2023): 609. http://dx.doi.org/10.3390/molecules28020609.

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The reaction between dithiomalondianilide (N,N’-diphenyldithiomalondiamide) and alkyl 3-aryl-2-cyanoacrylates in the presence of morpholine in the air atmosphere leads to the formation of alkyl 6-amino-4-aryl-7-phenyl-3-(phenylimino)-4,7-dihydro-3H-[1,2]dithiolo[3,4-b]- pyridine-5-carboxylates in 37–72% yields. The same compounds were prepared in 23–65% yields by ternary condensation of aromatic aldehydes, ethyl(methyl) cyanoacetate and dithiomalondianilide. The reaction mechanism is discussed. The structure of ethyl 6-amino-4-(4-methoxyphenyl)-7-phenyl-3-(phenylimino)-4,7-dihydro-3H-[1,2]dith

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36

Chandrakumar, K., M. K. Kokila, Puttaraja, S. Mohan, J. Saravanan, and M. V. Kulkarni. "Ethyl 2-amino-6-methyl-4,5,6,7-tetrahydrothieno[2,3-c]pyridine-3-carboxylate monohydrate." Acta Crystallographica Section E Structure Reports Online 62, no. 6 (2006): o2457—o2459. http://dx.doi.org/10.1107/s1600536806017831.

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37

Frandsen, H., H. Frederiksen, and J. Alexander. "2-Amino-1-methyl-6-(5-hydroxy-)phenylimidazo[4,5-b]pyridine (5-OH-PhIP), a biomarker for the genotoxic dose of the heterocyclic amine, 2-amino-1-methyl-6-phenylimidazo[4,5-b]pyridine (PhIP)." Food and Chemical Toxicology 40, no. 8 (2002): 1125–30. http://dx.doi.org/10.1016/s0278-6915(02)00033-9.

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38

Harnden, MR, and DT Hurst. "The Chemistry of Pyrimidinethiols. III. The Synthesis of Some Substituted Pyrimidinthiols and Some Thiazolo[5,4-D]pyrimidines." Australian Journal of Chemistry 43, no. 1 (1990): 55. http://dx.doi.org/10.1071/ch9900055.

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The preparation of a number of pyrimidinethiols and (substituted) thiopyrimidines has been carried out. The reaction of 5-acetylamino-2-aminopyrimidine-4,6-diol with phosphorus penta -sulfide in pyridine gave 5-amino-2-methylthiazolo[5,4-d]pyrimidine-7-thiol which was used to prepare several additional novel pyrimidine derivatives. Hydrolysis of the 4-carboxymethylthio derivative by using 5M hydrochloric acid gave 2,5-diamino-6-mercaptopyrimidin-4-ol hy -drochloride whilst hydrolysis of 2-methyl-7-methylthiothiazolo[5,4-d]pyrimidin-5-amine gave the corresponding 4-hydroxy derivative. Several 4

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39

Hu, Hua-nan, You Peng, Hua-nan Huang, Tao Yang, Fu-shan Chen, and Ping Yan. "Deacylation during the Synthesis of New 4-Amino-1H-Pyrazolo [3,4-B] Pyridines Catalysed by Sncl4." Journal of Chemical Research 42, no. 8 (2018): 412–15. http://dx.doi.org/10.3184/174751918x15337230783041.

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A series of novel 1-(4-amino-6-methyl-1-aryl-1H-pyrazolo[3,4-b]pyridin-5-yl)-ethanones and 6-methyl-1-aryl-1H-pyrazolo[3,4-b]pyridin-4-amines were prepared by the annulation of 5-amino-1-aryl-1H-pyrazole-4-carbonitriles with acetylacetone in the presence of tin(IV) chloride. The results demonstrated that the ethanones are the precursors of second compounds.

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40

Al-Jaber, Hala I., Mustafa M. El-Abadelah, Salim S. Sabri, Taleb H. Al-Tel, and Wolfgang Voelter. "Thienopyridone Antibacterials V [1]. Synthesis of Some N(7)-Azacyclohexyl-4-oxothieno[2,3-b]pyridine-5-carboxylic Acids and Related Congeners." Zeitschrift für Naturforschung B 64, no. 11-12 (2009): 1625–32. http://dx.doi.org/10.1515/znb-2009-11-1249.

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A series of N(7)-azacyclohexyl-4-oxo-4,7-dihydrothieno[2,3-b]-pyridine-5-carboxylic acids 9a - c, related congeners 9d - g and their methyl esters 8a - g were prepared by cyclization of the respective 2-[(2,5-dichlorothien-3-yl)carbonyl]-3-[(N(7)-azacyclyl/acyclic)amino]acrylates 7a - g. The latter intermediates are accessible from methyl 2-[(2,5-dichlorothien-3-yl)carbonyl]-3-ethoxyacrylate (6). Of the present series, the 7-(N,N-dimethylamino) derivative 9d exhibited good activity, especially against Klebsiella pneumoniae and Salmonella paratyphi A (MIC = 0.5 and 1.0 μgmL−1, respectively).

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41

Abdel-Rahman, Abdu E., Etify A. Bakhite, and Elham A. Al-Taifi. "Fluorine-containing Heterocycles: Part II Synthesis and Reactions of New Thieno[2,3-b]Pyridine Derivatives Bearing Trifluoromethyl Group." Journal of Chemical Research 2005, no. 7 (2005): 461–68. http://dx.doi.org/10.3184/030823405774309014.

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Ethyl [3-cyano-6-(2-thienyl)-4-trifluoromethylpyridin-2-ylthio]acetate (2) and ethyl 3-amino-6-(2-thienyl)-4-trifluoromethylthieno[2,3-b]pyridine-2-carboxylate (3) were prepared by reaction of 3-cyano-6-(2-thienyl)-4-trifluoromethylpyridine-2(1H)-thione (1) with ethyl chloroacetate. The reaction of both 2 and 3 with hydrazine hydrate under different conditions was studied. The main products were [3-cyano-6-(2-thienyl)-4-trifluoromethyl-2-pyridinylthio]acetohydrazide (4) and 3-amino-6-(2-thienyl)-4-trifluoromethylthieno[2,3-b]pyridine-2-carbohydrazide (5). The condensation of acethydrazide 4 wi

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42

Frandsen, Henrik, and Jan Alexander. "N-acetyltransferase-dependent activation of 2-hydroxyamino-1-methyl-6-phenylimidazo[4,5-b]pyridine: formation of 2-amino-1-methyl-6-(5-hydroxy)phenylimidazo [4,5-b]pyridine, a possible biomarker for the reactive dose of 2-amino-1-methyl-6-phenylimidazo[4,5-b]pyridine." Carcinogenesis 21, no. 6 (2000): 1197–203. http://dx.doi.org/10.1093/carcin/21.5.197.

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43

Frandsen, Henrik, and Jan Alexander. "N -acetyltransferase-dependent activation of 2-hydroxyamino-1-methyl-6-phenylimidazo[4,5- b ]pyridine: formation of 2-amino-1-methyl-6-(5-hydroxy)phenylimidazo [4,5- b ]pyridine, a possible biomarker for the reactive dose of 2-amino-1-methyl-6-phenylimidazo[4,5- b ]pyridine." Carcinogenesis 21, no. 6 (2000): 1197–203. http://dx.doi.org/10.1093/carcin/21.6.1197.

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44

Bakhite, Etify A., Abdu E. Abdel-Rahman, and Elham A. Al-Taifi. "Fluorine-Containing Heterocycles: Part I. Synthesis of New 7-(2-thienyl)-9-Trifluoromethylpyrido[3′,2′:4,5]Thieno[3,2-d]Pyrimidines and Related Fused Tetracyclic Systems." Journal of Chemical Research 2005, no. 3 (2005): 147–54. http://dx.doi.org/10.3184/0308234054213726.

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3-amino-6-(2-thienyl)-4-trifluoromethylthieno[2,3-b]pyridine-2-carboxamide (3) and 2-carbonitrile analogue 5 were prepared by reaction of 3-cyano-6-(2-thienyl)-4-trifluoromethylpyridine-2(1H)-thione (1) with chloroacetamide or chloroacetonitrile respectively. Heating compound 3 with triethyl orthoformate led to the formation of pyridothienopyrimidinone derivative 6. Reaction of 6 with phosphorus oxychloride produced 4-chloropyrimidine derivative 7 which underwent some nucleophilic displacements upon treatment with thiourea, piperidine, morpholine or hydrazine hydrate to give the target 4-subst

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45

Otero, Iran, Holger Feist, Dirk Michalik, Manfred Michalik, José Quincoces та Klaus Peseke. "Synthesis of Iso-C-nucleoside Analogues from 1-(Methyl 2-O-benzyl-4,6- O-benzylidene-3-deoxy-α-D-altropyranosid-3-yl)but-3-yn-2-ones". Zeitschrift für Naturforschung B 60, № 11 (2005): 1175–85. http://dx.doi.org/10.1515/znb-2005-1110.

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1-(Methyl 2-O-benzyl-4,6-O-benzylidene-3-deoxy-α-D-altropyranosid-3-yl)but-3-yn-2-one (3a) reacted with 3-amino-1H-1,2,4-triazole and 5-aminopyrazole-4-carboxylic acid derivatives in the presence of base to furnish the triazolo[1,5-a]pyrimidine (5) and the pyrazolo[1,5- a]pyrimidines (8a - d), respectively. Treatment of 1-(methyl 2-O-benzyl-4,6-O-benzylidene-3- deoxy-α-D-altropyranosid-3-yl)-4-phenyl-but-3-yn-2-one (3b) with cyanacetamide, 2-cyano-N- (4-methoxyphenyl)acetamide und N-aryl-3-oxo-butyramides afforded the substituted nicotinonitriles (11a - d). Furthermore, reaction of 3b with 2-b

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46

Çolak, Naki, Dursun Ali Köse, Nazmiye Marım, Ömer Çelik, and Tuncer Hökelek. "Ethyl 2-[(2-hydroxybenzylidene)amino]-6-methyl-4,5,6,7-tetrahydrothieno[2,3-c]pyridine-3-carboxylate." Acta Crystallographica Section E Structure Reports Online 69, no. 7 (2013): o1116—o1117. http://dx.doi.org/10.1107/s1600536813016474.

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47

Takayama, Kyoko, Katsumi Yamashita, Keiji Wakabayashi, Takashi Sugimura, and Minako Nagao. "DNA Modification by 2-Amino-1-methyl-6-phenylimidazo[4,5-b]pyridine in Rats." Japanese Journal of Cancer Research 80, no. 12 (1989): 1145–48. http://dx.doi.org/10.1111/j.1349-7006.1989.tb01644.x.

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48

Zhang, Xin-Ying, Xiao-Yan Li, Xia Wang, Xue-Sen Fan, and Gui-Rong Qu. "6-Amino-3-methyl-4-(4-nitrophenyl)-1-phenylpyrazolo[3,4-b]pyridine-5-carbonitrile." Acta Crystallographica Section E Structure Reports Online 64, no. 4 (2008): o689. http://dx.doi.org/10.1107/s1600536808006156.

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49

Krauze, A. A., �. �. Liepin'sh, Yu �. Pelcher, and G. Ya Dubur. "Synthesis of 3-amino-6-methyl-5-ethoxycarbonyl-4,7-dihydrothieno[2,3-b]pyridine derivatives." Chemistry of Heterocyclic Compounds 23, no. 1 (1987): 102–6. http://dx.doi.org/10.1007/bf00475486.

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50

Kim, Dojung, Young-Joo Lee, Heui-Young Ryu, et al. "Genetic polymorphisms in metabolism of 2-amino-1-methyl-6-phenylimidazo[4,5-b] pyridine." Journal of Applied Toxicology 33, no. 1 (2011): 63–70. http://dx.doi.org/10.1002/jat.1712.

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