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1

Diwekar, Urmila M., and K. P. Madhavan. "Multicomponent batch distillation column design." Industrial & Engineering Chemistry Research 30, no. 4 (April 1991): 713–21. http://dx.doi.org/10.1021/ie00052a014.

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2

Noda, Masaru, Akifumi Kato, Shinji Hasebe, and Iori Hashimoto. "Optimal structure of batch distillation column." Computers & Chemical Engineering 23 (June 1999): S105—S108. http://dx.doi.org/10.1016/s0098-1354(99)80027-1.

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3

Hawaidi, Ebrahim Ali Mohamed, Mustafa T. Yagub, and Riyad Ageli Saleh. "ACETONE RECOVERY USING BATCH DISTILLATION." Scientific Journal of Applied Sciences of Sabratha University 2, no. 2 (September 27, 2019): 82–98. http://dx.doi.org/10.47891/sabujas.v2i2.82-98.

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This study focuses on determining the feasibility of obtaining maximum mole percentage of acetone (99 mole%) in the distillate stream from a 3 mole% acetone waste stream using batch distillation. The device which is used in this work has eight trays that will act as the stages of the batch distillation. The effects of varying reflux ratio and heat load (power) on acetone concentration were studied. Moreover, the operating conditions for the bath distillation column such as flooding and weeping with the extreme limits of operation were considered. The temperatures were also be recorded at each tray. The McCabe-Thiele method was used to determine the theoretical number of trays and compared with actual trays (column efficiency). For a chemical analysis of acetone/water compositions a refractometer was used for a chemical analysis, known acetone/water concentrations were analysed and used to construct a calibration curve. The results obtained showed that, the acetone concentration increases with increasing reflux ratio until a highest concentration was reached. Then, the concentration gradually decreases with increasing reflux ratio. However, the distillate stream with 99 mole % acetone was achieved at a reflux ratio of R=3 and at both powers 0.5 kw and 0.7 kw. Finally, the highest overall column efficiency reached by this work was about 75%.
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4

Zhao, Shuo, Peng Bai, Xianghai Guo, Ke Tang, and Guangzhong Li. "Time requirements in closed and open batch distillation arrangements for separation of a binary mixture." Polish Journal of Chemical Technology 16, no. 4 (December 1, 2014): 66–74. http://dx.doi.org/10.2478/pjct-2014-0072.

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Abstract Batch time requirements are provided for the separation of binary zeotropic mixtures in two different multivessel columns (with and without vapor bypass), a non-cyclic two-vessel column and a regular batch column based on dynamic simulations. The first three columns are operated as closed (total reflux) systems and the regular batch column is operated as an open (partial reflux) system. We analyze the effects of feed composition, relative volatility and product specification on the time requirements. The multivessel arrangements perform better than the regular batch column, which requires from 4.00 to 34.67% more time to complete a given separation. The elimination of the vapor bypass in the multivessel column is impractical though it has a positive effect on the batch time requirements. Thus, the multivessel column, with the vapor stream bypassing the intermediate vessel, is proposed as the best candidate for a binary zeotropic mixture with low concentration of light component, low relative volatility and high product purity demand. Furthermore, an experimental multivessel column with vapor bypass is built and the corresponding experiments verify the simulations.
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5

Rohman, Arief Syaichu, Pranoto Hidaya Rusmin, Renny Maulidda, Egi Muhammad Idris Hidayat, Carmadi Machbub, and Dimitri Mahayana. "Modelling of the Mini Batch Distillation Column." International Journal on Electrical Engineering and Informatics 10, no. 2 (June 30, 2018): 350–68. http://dx.doi.org/10.15676/ijeei.2018.10.2.11.

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6

Bahar, Almιla, and Canan Özgen. "State Estimation for a Reactive Batch Distillation Column." IFAC Proceedings Volumes 41, no. 2 (2008): 3304–9. http://dx.doi.org/10.3182/20080706-5-kr-1001.00561.

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7

Denes, F., P. Lang, G. Modla, and X. Joulia. "New double column system for heteroazeotropic batch distillation." Computers & Chemical Engineering 33, no. 10 (October 2009): 1631–43. http://dx.doi.org/10.1016/j.compchemeng.2009.01.011.

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8

Tang, Ke, and Peng Bai. "Cascaded Columns of Total Reflux Batch Distillation with Periodic Liquid Exchange." Advanced Materials Research 690-693 (May 2013): 1495–99. http://dx.doi.org/10.4028/www.scientific.net/amr.690-693.1495.

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A new type of operation mode of cascaded columns of total reflux batch distillation with periodic liquid exchange was proposed. The feasibility of the new operation, which is suitable for separations of mixtures of close boiling point, thermo-sensitive material and isotopes, was proved by the experiments in which two columns and three columns in periodic liquid exchange were used with ethanol-isopropanol, ethylbenzene- paraxylene as the experimental mixtures. The results indicate that the new operation mode can generate summation effect of theoretical plates by periodic liquid exchange between columns, while the total pressure drop is the same as that of a single column.
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9

Lukács, T., C. Stéger, E. Rév, M. Meyer, and Z. Lelkes. "Feasibility of Batch Reactive Distillation with Equilibrium-Limited Consecutive Reactions in Rectifier, Stripper, or Middle-Vessel Column." International Journal of Chemical Engineering 2011 (2011): 1–16. http://dx.doi.org/10.1155/2011/231828.

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A general overall feasibility methodology of batch reactive distillation of multireaction systems is developed to study all the possible configurations of batch reactive distillation. The general model equations are derived for multireaction system with any number of chemical equilibrium-limited reactions and for any number of components. The present methodology is demonstrated with the detailed study of the transesterification of dimethyl carbonate in two reversible cascade reactions in batch reactive distillation process. Pure methanol is produced as distillate, and pure diethyl carbonate is produced at the bottom simultaneously in middle-vessel column; in each section, continuous feeding of ethanol is necessary. The results of feasibility study are successfully validated by rigorous simulations.
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10

Hao, Wenfeng. "A Short-Cut Design Technique to Batch Distillation Column." Advances in Chemical Engineering and Science 09, no. 03 (2019): 263–79. http://dx.doi.org/10.4236/aces.2019.93020.

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11

Fernholz, Gregor, Sebastian Engell, Lars-Ulrich Kreul, and Andrzej Gorak. "Optimal operation of a semi-batch reactive distillation column." Computers & Chemical Engineering 24, no. 2-7 (July 2000): 1569–75. http://dx.doi.org/10.1016/s0098-1354(00)00553-6.

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12

Hasebe, Shinji, Badhrulhisham B. Abdul Aziz, Iori Hashimoto, and Tetsuya Watanabe. "Optimal Design and Operation of Complex Batch Distillation Column." IFAC Proceedings Volumes 25, no. 24 (September 1992): 177–82. http://dx.doi.org/10.1016/s1474-6670(17)54028-8.

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13

CLAUS, MICHAEL J., and KRIS A. BERGLUND. "FRUIT BRANDY PRODUCTION BY BATCH COLUMN DISTILLATION WITH REFLUX." Journal of Food Process Engineering 28, no. 1 (February 2005): 53–67. http://dx.doi.org/10.1111/j.1745-4530.2005.00377.x.

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14

Denes, Ferenc, Peter Lang, and Xavier Joulia. "Generalised closed double-column system for batch heteroazeotropic distillation." Separation and Purification Technology 89 (March 2012): 297–308. http://dx.doi.org/10.1016/j.seppur.2012.01.042.

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15

Jana, Amiya K. "Inferential state estimator design for a batch distillation column." International Journal of Modelling, Identification and Control 2, no. 2 (2007): 75. http://dx.doi.org/10.1504/ijmic.2007.014620.

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16

Farschman, Chad A., and Urmila Diwekar. "Dual Composition Control in a Novel Batch Distillation Column." Industrial & Engineering Chemistry Research 37, no. 1 (January 1998): 89–96. http://dx.doi.org/10.1021/ie9703806.

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17

Woodward, John L., Michael D. Moosemiller, and Robert Chopp. "Applying risk assessment principles to a batch distillation column." Process Safety Progress 15, no. 2 (1996): 61–65. http://dx.doi.org/10.1002/prs.680150203.

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18

Vibhute, Madhuri M., and Sujit S. Jogwar. "Model-based Control of Vapor-recompressed Batch Distillation Column." IFAC-PapersOnLine 51, no. 18 (2018): 554–59. http://dx.doi.org/10.1016/j.ifacol.2018.09.366.

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19

Davidyan, Arthur G., Valerii N. Kiva, George A. Meski, and Manfred Morari. "Batch distillation in a column with a middle vessel." Chemical Engineering Science 49, no. 18 (September 1994): 3033–51. http://dx.doi.org/10.1016/0009-2509(94)e0083-3.

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20

Narvaez-Garcia, Asteria, Jose del Carmen Zavala-Loria, Luis Enrique Vilchis-Bravo, and Jose Antonio Rocha-Uribe. "Design of Batch Distillation Columns Using Short-Cut Method at Constant Reflux." Journal of Engineering 2013 (2013): 1–14. http://dx.doi.org/10.1155/2013/685969.

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A short-cut method for batch distillation columns working at constant reflux was applied to solve a problem of four components that needed to be separated and purified to a mole fraction of 0.97 or better. Distillation columns with 10, 20, 30, 40, and 50 theoretical stages were used; reflux ratio was varied between 2 and 20. Three quality indexes were used and compared: Luyben’s capacity factor, total annual cost, and annual profit. The best combinations of theoretical stages and reflux ratio were obtained for each method. It was found that the best combinations always required reflux ratios close to the minimum. Overall, annual profit was the best quality index, while the best combination was a distillation column with 30 stages, and reflux ratio’s of 2.0 for separation of benzene (i), 5.0 for the separation of toluene (ii), and 20 for the separation of ethylbenzene (iii) and purification of o-xylene (iv).
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21

Ramadani, Tarikh Azis, Fadilatul Taufany, and Siti Nurkhamidah. "Study of packed sieve tray column in ethanol purification using distillation process." Malaysian Journal of Fundamental and Applied Sciences 15, no. 1 (February 4, 2019): 69–74. http://dx.doi.org/10.11113/mjfas.v15n2019.936.

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Sieve tray becomes a popular contacting device in distillation process because of its relative simplicity and low cost. There is one way to improve the contact performance, especially mass transfer by modifying the sieve tray into packed sieve tray. This study was aimed to investigate the effect of adding packing in each tray to ethanol content on ethanol purification. This research was conducted via experiment and simulation approaches. The experiment used packed sieve tray that contained 3 cm and 5 cm bed of steel wool with 16 trays in the column, with operating pressure about 760 mmHg and performed in batch condition. The simulation used a reduced rated base model with some modifications for operation in the packed sieve tray column. It was found that the use of packed sieve tray gave better distillate in the batch distillation process than the use of sieve tray. The packed sieve tray raised distillate content about 8.89% when using 3 cm of packing and 23.31% when using 5 cm of packing when it was compared with sieve tray. The use of packed sieve tray could increase the mass transfer and reduce bubble diameter in the batch distillation process.
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22

Bahar, Almıla, and Canan özgen. "Experimental and Modeling Studies for a Reactive Batch Distillation Column." IFAC Proceedings Volumes 42, no. 11 (2009): 845–50. http://dx.doi.org/10.3182/20090712-4-tr-2008.00138.

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23

Rao, C. S., and K. Barik. "Modeling, Simulation and Control of Middle Vessel Batch Distillation Column." Procedia Engineering 38 (2012): 2383–97. http://dx.doi.org/10.1016/j.proeng.2012.06.285.

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24

Betlem, B. H. L. "Batch distillation column low-order models for quality program control." Chemical Engineering Science 55, no. 16 (August 2000): 3187–94. http://dx.doi.org/10.1016/s0009-2509(99)00584-9.

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25

Monroy-Loperena, Rosendo, and Jose Alvarez-Ramirez. "Dual Composition Control in a Middle-Vessel Batch Distillation Column." Industrial & Engineering Chemistry Research 40, no. 20 (October 2001): 4377–90. http://dx.doi.org/10.1021/ie0005405.

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26

Balasubramhanya, Lalitha S., and Francis J. Doyle III. "Nonlinear model-based control of a batch reactive distillation column." Journal of Process Control 10, no. 2-3 (April 2000): 209–18. http://dx.doi.org/10.1016/s0959-1524(99)00024-4.

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27

Barolo, Massimiliano, G. Berto Guarise, Sergio A. Rienzi, Antonio Trotta, and Sandro Macchietto. "Running Batch Distillation in a Column with a Middle Vessel." Industrial & Engineering Chemistry Research 35, no. 12 (January 1996): 4612–18. http://dx.doi.org/10.1021/ie960268s.

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28

Oisiovici, R. M., S. L. Cruz, and J. A. F. R. Pereira. "Digital filtering in the control of a batch distillation column." ISA Transactions 38, no. 3 (July 1999): 217–24. http://dx.doi.org/10.1016/s0019-0578(99)00024-5.

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29

Balasubramhanya, Lalitha S., and Francis J. Doyle. "Nonlinear Model-Based Control of a Batch Reactive Distillation Column." IFAC Proceedings Volumes 31, no. 11 (June 1998): 125–30. http://dx.doi.org/10.1016/s1474-6670(17)44917-2.

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30

Cesur, Serap, and PoLock Yue. "A Control Configuration Design for a Packed Batch Distillation Column." IFAC Proceedings Volumes 31, no. 11 (June 1998): 449–54. http://dx.doi.org/10.1016/s1474-6670(17)44967-6.

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31

Murlidhar, Gundale Mangesh, and Amiya Kumar Jana. "Nonlinear adaptive control algorithm for a multicomponent batch distillation column." Chemical Engineering Science 62, no. 4 (February 2007): 1111–24. http://dx.doi.org/10.1016/j.ces.2006.11.006.

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32

Stéger, C., V. Varga, L. Horváth, E. Rév, Z. Fonyó, M. Meyer, and Z. Lelkes. "Feasibility of extractive distillation process variants in batch rectifier column." Chemical Engineering and Processing: Process Intensification 44, no. 11 (November 2005): 1237–56. http://dx.doi.org/10.1016/j.cep.2005.02.008.

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33

Marquez-Ruiz, Alejandro, Marco Loonen, M. Bahadır Saltık, and Leyla Özkan. "Model Learning Predictive Control for Batch Processes: A Reactive Batch Distillation Column Case Study." Industrial & Engineering Chemistry Research 58, no. 30 (April 24, 2019): 13737–49. http://dx.doi.org/10.1021/acs.iecr.8b06474.

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34

Ali Bashah, Nur Alwani, Mohd Roslee Othman, and Norashid Aziz. "Neural Network MIMO Model for Production of Isopropyl Myristate in a Semibatch Reactive Distillation Column." Applied Mechanics and Materials 284-287 (January 2013): 403–8. http://dx.doi.org/10.4028/www.scientific.net/amm.284-287.403.

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Batch reactive distillation is an integrated unit of batch reactor and distillation. It provides benefits of having higher conversion and yield by continuous removal of side product. The aim of this paper is to develop an artificial neural network (ANN) based model for production of isopropyl myristate in an industrial scaled semibatch reactive distillation. Two cases of the MIMO model were developed. Case 1 does not consider historical data as inputs while case 2 does. The trained ANN for both cases was validated with independent validation data and the best architecture was optimized. Case 1 resulted to 8 inputs, 14 hidden nodes and 2 outputs [8-14-2] ANN while Case 2 resulted to [12-13-2] ANN. The results show that both ANN models have ability to predict the unknown validation and testing data very well. However, the [8-14-2] ANN model produce higher accuracy than [12-13-2] ANN model with MSE of 0.00094 and 0.0013, respectively.
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35

Bahar, Almıla, and Canan Özgen. "State estimation and inferential control for a reactive batch distillation column." Engineering Applications of Artificial Intelligence 23, no. 2 (March 2010): 262–70. http://dx.doi.org/10.1016/j.engappai.2009.11.003.

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36

Noda, Masaru, Akifumi Kato, Takashi Chida, Shinji Hasebe, and Iori Hashimoto. "Optimal structure and on-line optimal operation of batch distillation column." Computers & Chemical Engineering 25, no. 1 (January 2001): 109–17. http://dx.doi.org/10.1016/s0098-1354(00)00636-0.

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37

Gruetzmann, Sven, and Georg Fieg. "Startup Operation of Middle-Vessel Batch Distillation Column: Modeling and Simulation." Industrial & Engineering Chemistry Research 47, no. 3 (February 2008): 813–24. http://dx.doi.org/10.1021/ie070667v.

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38

Frattini Fileti, Ana M., Sandra L. Cruz, and João A. F. R. Pereira. "Control strategies analysis for a batch distillation column with experimental testing." Chemical Engineering and Processing: Process Intensification 39, no. 2 (March 2000): 121–28. http://dx.doi.org/10.1016/s0255-2701(99)00059-8.

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39

Cheong, Weiyang, and Paul I. Barton. "Azeotropic Distillation in a Middle Vessel Batch Column. 3. Model Validation." Industrial & Engineering Chemistry Research 38, no. 4 (April 1999): 1549–64. http://dx.doi.org/10.1021/ie980471i.

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40

Stenz, R., and U. Kuhn. "Automation of a batch distillation column using fuzzy and conventional control." IEEE Transactions on Control Systems Technology 3, no. 2 (June 1995): 171–76. http://dx.doi.org/10.1109/87.388125.

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41

Modla, G., and P. Lang. "NEW COLUMN CONFIGURATIONS FOR PRESSURE SWING BATCH DISTILLATION I. FEASIBILITY STUDIES." IFAC Proceedings Volumes 40, no. 5 (2007): 105–10. http://dx.doi.org/10.3182/20070606-3-mx-2915.00065.

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42

Modla, G. "Reactive pressure swing batch distillation by a new double column system." Computers & Chemical Engineering 35, no. 11 (November 2011): 2401–10. http://dx.doi.org/10.1016/j.compchemeng.2011.01.002.

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43

Modla, G. "Pressure swing batch distillation by double column systems in closed mode." Computers & Chemical Engineering 34, no. 10 (October 2010): 1640–54. http://dx.doi.org/10.1016/j.compchemeng.2010.02.037.

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44

Li, Guangzhong, Yang Yu, and Peng Bai. "Batch extractive distillation of mixture methanol-acetonitrile using aniline as a asolvent." Polish Journal of Chemical Technology 14, no. 3 (October 1, 2012): 48–53. http://dx.doi.org/10.2478/v10026-012-0083-4.

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Methanol and acetonitrile form a minimum azeotrope at 336.74 K, which contains methanol 76.89 mas%. The simulation and the experiment to separate the mixture by batch extractive distillation using aniline as entrainer is performed. Based on the experimental and simulative VLE data, aniline is chosen to be the suitable solvent. The sensitivity analysis about the number of stages, the refl ux ratio, the solvent feed stage and the solvent fl ow rate is conducted to obtain the optimal parameters and confi guration of the extractive distillation column with minimal energy requirements. The most appropriate confi guration is 30 theoretical stages. The optimal entrainer feeding stage is 8 with a solvent fl ow rate of 20kg/h and the refl ux ratio of 2.0, respectively. The simulation results show the effect of the main variables on the extractive distillation process. The experiment is carried out to corroborate the feasibility of the separation of methanol-acetonitrile by batch extractive distillation.
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45

Ceylan, Hatice, and Canan Özgen. "DYNAMIC MODELLING AND OPTIMAL CONTROL OF A MULTICOMPONENT BATCH PACKED DISTILLATION COLUMN." IFAC Proceedings Volumes 41, no. 2 (2008): 4548–53. http://dx.doi.org/10.3182/20080706-5-kr-1001.00765.

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46

Mufrodi, Zahrul, Rochmadi Rochmadi, Sutijan Sutijan, and Arief Budiman. "Synthesis Acetylation of Glycerol Using Batch Reactor and Continuous Reactive Distillation Column." Engineering Journal 18, no. 2 (April 18, 2014): 29–40. http://dx.doi.org/10.4186/ej.2014.18.2.29.

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47

Barolo, Massimiliano, Gian Berto Guarise, Sergio A. Rienzi, and Antonio Trotta. "Understanding the dynamics of a batch distillation column with a middle vessel." Computers & Chemical Engineering 22 (March 1998): S37—S44. http://dx.doi.org/10.1016/s0098-1354(98)00036-2.

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48

Tapp, Michaela, Shehzaad Kauchali, Brendon Hausberger, Craig McGregor, Diane Hildebrandt, and David Glasser. "An experimental simulation of distillation column concentration profiles using a batch apparatus." Chemical Engineering Science 58, no. 2 (January 2003): 479–86. http://dx.doi.org/10.1016/s0009-2509(02)00469-4.

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49

Cheong, Weiyang, and Paul I. Barton. "Azeotropic Distillation in a Middle Vessel Batch Column. 2. Nonlinear Separation Boundaries." Industrial & Engineering Chemistry Research 38, no. 4 (April 1999): 1531–48. http://dx.doi.org/10.1021/ie980470q.

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50

Modla, G., and P. Lang. "NEW COLUMN CONFIGURATIONS FOR PRESSURE SWING BATCH DISTILLATION II. RIGOROUS SIMULATION CALCULATIONS." IFAC Proceedings Volumes 40, no. 5 (2007): 361–66. http://dx.doi.org/10.3182/20070606-3-mx-2915.00108.

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