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Journal articles on the topic 'Benzoquinone-1,2(methoxy-5 methoxy-4p phenoxy-4)|ent'

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Published: 9 July 2021

Last updated: 29 July 2025

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1

Asmau, Nasiru Hamza, and Kizito Igomu George. "Microwave Assisted Synthesis and Antimicrobial Screening of 3-(4-Methoxy)-1-Phenylprop-2-en-1-One." Pharmaceutical and Chemical Journal 3, no. 2 (2016): 300–303. https://doi.org/10.5281/zenodo.13754340.

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In an effort to develop novel antimicrobial agents, 3-(4-methoxy)-1-phenylprop-2-en-1-one was synthesized from acetophenone and methoxybenzaldehyde using the conventional Claisen-Schmidt condensation and microwave assisted methods. The conventional Claisen-Schmidt condensation afforded a yield of 35.29% in three hours. Whereas, the microwave assisted method gave 73.94% yield of 3-(4-methoxy)-1-phenylprop-2-en-1-one with two minutes. The synthesized 3-(4-methoxy)-1-phenylprop-2-en-1-one was characterized by means of Fourier transform Infrared (FTIR) spectroscopy, Shinoda’s test and meltin

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2

Koshetova, Zh A., V. K. Yu, T. K. Iskakova, et al. "Novel 7-Aryliden-3,3a,4,5,6,7-(hexahydro-5-(2-ethoxyethyl)-2-phenyl-3-aryl-2H-pyrazolo[4,3-c]pyridine Hydrochloride: Synthesis and Structure." Eurasian Chemico-Technological Journal 24, no. 1 (2022): 43. http://dx.doi.org/10.18321/ectj1147.

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A Claisen-Schmidt type reaction of 1-(2-ethoxyethyl)piperidin-4-one with differ¬ent aromatic aldehydes led to corresponding dienones with a yield of 65‒71%. 7-Arylidene-3,3a,4,5,6,7-(hexahydro-5-(2-ethoxyethyl)-2-phenyl-3-aryl-2H-pyrazolo[4,3-c]pyridines were synthesized by heterocyclization of 3,5-dia¬rylidene-piperidin-4-ones with phenylhydrazine hydrochloride in methanol at 70 °C over 4‒6 h. The X-ray crystal structure determination of 7-(p-methoxy¬benzyliden)-3,3a,4,5,6,7-(hexahydro-5-(2-ethoxyethyl)-2-phenyl-3-(p-methoxy¬phenyl)-2H-pyrazolo[4,3-c]pyridine hydrochloride (the deposition num

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3

Manguro, Lawrence Onyango Arot, Sylvia Awino Opiyo, Eberhardt Herdtweck, and Peter Lemmen. "Triterpenes of Commiphora holtziana oleo-gum resin." Canadian Journal of Chemistry 87, no. 8 (2009): 1173–79. http://dx.doi.org/10.1139/v09-078.

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Chemical analysis of the acetone extract of Commiphora holtziana gum resin has led to the isolation of triterpenes characterized as methyl 3-oxo-1α,19α,28-trihydroxyurs-12-en-24-oate (1), methyl 3β-acetyl-2α,11α,19α,28-tetrahydroxyurs-12-en-24-oate (2), methyl 3β,11α-diacetyl-1α,2α,28-trihydroxyurs-12-ene-24-oate (3), and 3β,28-diacetyl-1α,2α,25-trihydroxydammar-23-ene (4). The known compounds isolated from the same extract included cabraleadiol monoacetate (5), mansumbinol (6), 3β-acetylamyrin (7), 3α-acetylboswellic acid (8), 2-methoxy-8,12-epoxygermacra-1(10),7,11-trien-6-one (9), 2-methoxy

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4

Gedara, Sahar R., Osama B. Abdel-Halim, Saleh H. El-Sharkawy, Osama M. Salama, Thomas W. Shier, and Ahmed F. Halim. "New Erythroxane-Type Diterpenoids from Fagonia boveana (Hadidi) Hadidi & Graf." Zeitschrift für Naturforschung C 58, no. 1-2 (2003): 23–32. http://dx.doi.org/10.1515/znc-2003-1-204.

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The aerial parts of Fagonia boveana afforded two new erythroxane-type diterpenes, 3β, 15, 16-trihydroxy-erythrox-4(18)-ene (2) and 15, 16-dihydroxy-cis-ent-erythrox-3-ene (fagonene) (3) together with two known ones; 16-O-acetylfagonone (1) and 7β-hydroxy fagonene (8). Also a new guaiane sesquiterpene alcohol, 6,10-epoxy-4α-hydroxy guaiane type sesquiterpene (4) has been isolated In addition three 8-methoxy flavonols, 8-methoxy-quercetin-3, 7, 3′-trimethyl ether (ternatin) (5), gossypetin, 3, 8, 3′, 4′ tetramethyl ether (6) and herbacetin- 3, 8-dimethyl ether (7) were also isolated. The structu

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5

Cambie, Richard C., Carrie C. Liu, Clifford E. F. Rickard, and Peter S. Rutledge. "Skeletal Rearrangements of Ring C Aromatic Diterpenoids." Australian Journal of Chemistry 51, no. 7 (1998): 605. http://dx.doi.org/10.1071/c97198.

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The structure of a naphthalene derivative obtained by rearrangement of 13-methoxytotara-5,8,11,13-tetraen-7α-ol (2) has been revised to 5-(5′-isopropyl-6′-methoxy-2′-methyl-1′-naphthyl)-2-methylpent-2-ene (7). A minor oxidation product of 13-methoxytotara-8,11,13-triene (4) has been identified as 4-methoxy-3,3-dimethyl-7-(1′,3′,3′-trimethyl-2′-oxocyclohexanyl)isobenzofuran-1(3H)-one (16) and its structure confirmed by X-ray crystallography. Methyl 12-methoxypodocarpa-8,11,13-trien-19-oate (12) has been converted into an intermediate used in the synthesis of the linear diterpenoid umbrosone [3-

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6

Alves, José C. F. "Study of Catalytic Hydrogenation and Methanol Addition to α-Methylene-γ-Lactone of Eremanthine Derivatives". Organic Chemistry International 2010 (19 грудня 2010): 1–11. http://dx.doi.org/10.1155/2010/603436.

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The sesquiterpene lactones guaia-1(10),11(13)-dieno-4α-hydroxy,9α-acetyl-15-iodine-12,6α-lactone (2), guaia-1(10),4(15),11(13)-trieno-9α-hydroxy-12,6α-lactone (3), (11S)-guaia-4(15),10(14)-dieno-9α-hydroxy-13-methoxy-12,6α-lactone (4), (11S)-guai-1(10)-eno-4α,9α-dihydroxy-13-methoxy-12,6α-lactone (5), and guaia-1(10),11(13)-dieno-4α,9α-dihydroxy-15-iodine-12,6α-lactone (6) were previously obtained starting from the natural product eremanthine (1). In this paper we report the catalytic hydrogenation reactions of allylic derivatives 2–5 and the methanol addition to α-methylene-γ-lactone of the i

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7

Arnold, Donald R., and Kimberly A. McManus. "Photochemical nucleophile-olefin combination, aromatic substitution (photo-NOCAS) reaction: methanol, beta-myrcene, and 1,4-dicyanobenzene. Intramolecular cyclization of an ene-diene radical cation." Canadian Journal of Chemistry 76, no. 9 (1998): 1238–48. http://dx.doi.org/10.1139/v98-156.

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The photochemical nucleophile-olefin combination, aromatic substitution (photo-NOCAS) reaction of methanol, 7-methyl-3-methylene-1,6-octadiene ( β-myrcene, 1), and 1,4-dicyanobenzene yields five 1:1:1 adducts:cis-2-(4-cyanophenyl)-4-(1-methoxy-1-methylethyl)-1-methylenecyclohexane (15), trans-2-(4-cyanophenyl)-4-(1-methoxy-1-methylethyl)-1-methylenecyclohexane (16), 1-(4-cyanophenylmethyl)-4-(1-methoxy-1-methylethyl)cyclohexene (17), 4-[4-methoxy-3,3-dimethylcyclohex-(E)-1-ylidenyl]methylbenzonitrile (18), and 4-(1-vinyl-4-trans-methoxy-3,3-dimethylcyclohexyl)benzonitrile (19). All of these ad

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8

Collins, DJ, and HA Jacobs. "Synthesis of 3-(4′-Methoxyphenyl)-2,2,4,4-Tetramethylpentane and Some Cyclic Analogs." Australian Journal of Chemistry 39, no. 12 (1986): 2095. http://dx.doi.org/10.1071/ch9862095.

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Reaction of 1-methoxy-2-methyl-1-trimethylsilyloxyprop-1-ene (8) with 1-acetoxy-1-(4′-methoxyphenyl)-2,2-dimethylpropane (7b) in the presence of zinc iodide gave 84% of methyl 3-(4′methoxyphenyl)-2,2,4,4- tetramethylpentanoate (9a), which was reduced with lithium aluminium hydride to 3-(4′-methoxyphenyl)-2,2,4,4-tetramethylpentan-1-ol(12a). Hydride reduction of the derived tosylate (12b) afforded 3-(4′-methoxyphenyl )-2,2,4,4-tetramethylpentane (5b) which upon demethylation yielded the corresponding phenol (10a). In an analogous manner, 1-acetoxy-1-(4′-methoxyphenyl)-2-methylpropane (7d) was c

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9

Yan, FuLin, LaiBin Zhang, JiXia Zhang, and HanDong Sun. "Two New Diterpenoids and other constituents from Isodon serra." Journal of Chemical Research 2007, no. 6 (2007): 362–64. http://dx.doi.org/10.3184/030823407x225536.

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Two new ent-6,7-seco-kaurane-type diterpenoids, 15α,20β-dihydroxy-6β-methoxy-6,7-seco-6,20-epoxy-ent-kaur-16-en-1,7-olide (1), 6α,15α-dihydroxy-20-aldehyde-6,7-seco-6,11α-epoxy-ent-kaur-16-en-1,7-olide (2), together with seven known diterpenoids, enmein (3), nodosin (4), isodocarpin (5), nervosin (6), epinodosin (7), epinodosinol (8) and rabdosin (9) were isolated from the aerial part of Isodon serra. Their structures were elucidated by spectroscopic means.

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10

Li, Hongqi, A. N. Mayekar, B. Narayana, H. S. Yathirajan, and William T. A. Harrison. "(±)-Ethyl 6-(6-methoxy-2-naphthyl)-4-(4-methylphenyl)-2-oxocyclohex-3-ene-1-carboxylate." Acta Crystallographica Section E Structure Reports Online 65, no. 6 (2009): o1186. http://dx.doi.org/10.1107/s1600536809016341.

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In the title compound, C27H26O4, the dihedral angle between the naphthalene ring system and the benzene ring is 73.10 (5)°. In the crystal, a weak C—H...O interaction occurs. Two C—H groups of the cyclohexene ring are disordered over two sets of sites in a 0.796 (5):0.204 (5) ratio, which corresponds to partial overlap of the two enantiomeric molecules.

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11

Daucher, Birgit, Volker Gettwert, Ruth Striegler та Gerhard Maas. "Intramolecular Carbene and Carbenoid Reactions of α-(Vinyloxy)silyl-α-diazoacetates". Zeitschrift für Naturforschung B 59, № 11-12 (2004): 1444–50. http://dx.doi.org/10.1515/znb-2004-11-1212.

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Thermolysis of α-[diisopropyl-1-(methylvinyl)oxysilyl]-α-diazoacetate 5a at 160 °C yields mainly 2,5-dihydro-1,2-oxasilole-3-carboxylate 6a and 3-[diisopropyl(methoxy)silyl]-2(5H)-furan- 2-one 7. From the thermolysis reaction of α-[diisopropyl-1-(phenylvinyl)oxysilyl]-α-diazoacetate 5b, only 1-oxa-2-sila-3-cylopentene-3-carboxylate 6b could be isolated in low yield. UV-irradiation of 5a,b generates 6a,b as the main products. The Rh2(C3F7COO)4-catalyzed decomposition of 5a provides primarily the ketene 2-[diisopropyl(methoxy)silyl]-pent-1-ene-1,4-dione (9) in high yield. After work-up, 3-[diiso

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12

Yahya, Yahya, Asep A. Prihanto, Dwi Setijawati, Hartati Kartikaningsih, and Abida Rahmi Efendi. "Inhibitory Effects of Powdered Liquid Smoke from Mangrove (Avicennia marina) Twigs on Spoilage Bacteria." Research Journal of Chemistry and Environment 28, no. 11 (2024): 1–6. http://dx.doi.org/10.25303/2811rjce0106.

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This study investigated the inhibitory effects of powdered liquid smoke derived from Avicennia marina (mangrove) twigs on spoilage bacteria. The research method used was experimental. Branches of mangrove (A. marina) were burned and distilled to produce liquid smoke. The powdered liquid smoke was subsequently tested for its antibacterial capabilities against foodborne pathogen bacteria. The damage to the bacterial formation was further illustrated using a Scanning electron micrograph. The components of liquid smoke were analysed using GC-MS. GC-MS test results on liquid smoke from mangrove twi

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13

Kostova, Ivanka, Dragomir Dinchev, Gudrun Hopp Rentsch, Vladimir Dimitrov, and Antoaneta Ivanova. "Two New Sulfated Furostanol Saponins from Tribulus terrestris." Zeitschrift für Naturforschung C 57, no. 1-2 (2002): 33–38. http://dx.doi.org/10.1515/znc-2002-1-206.

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The known furostanol saponins methylprotodioscin and protodioscin and two new sulfated saponins, sodium salt of 26-O-β-glucopyranosyl-22α-methoxy-(25R)-furost-5-ene-3β,26-diol- 3-O-α-rhamnopyranosyl-(1→2)-β-4-O-sulfo-glucopyranoside (methylprototribestin) and sodium salt of 26-O-β-glucopyranosyl-22α-hydroxy-(25R)-furost-5-ene-3β,26-diol-3-O-α-rhamnopyranosyl-( 1→2)-β-4-O-sulfo-glucopyranoside (prototribestin) have been isolated from the aerial parts of Tribulus terrestris L. growing in Bulgaria. The structures of the new compounds were elucidated on the basis of 1D and 2D (DQF-COSY, TOCSY, HSQ

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14

Harrison, William T. A., A. N. Mayekar, H. S. Yathirajan, B. Narayana, and B. K. Sarojini. "Ethyl 4-(2,4-dichlorophenyl)-6-(6-methoxy-2-naphthyl)-2-oxocyclohex-3-ene-1-carboxylate." Acta Crystallographica Section E Structure Reports Online 66, no. 10 (2010): o2478. http://dx.doi.org/10.1107/s1600536810035130.

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15

Singh, Onkar, Mohammed Ali, and Nida Akhtar. "New Antifungal Xanthones from the Seeds of Rhus coriaria L." Zeitschrift für Naturforschung C 66, no. 1-2 (2011): 17–23. http://dx.doi.org/10.1515/znc-2011-1-203.

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Phytochemical investigations of the ethanolic extract of the seeds of Rhus coriaria L. (Anacardiaceae) led to the identification of four new xanthones, characterized as 2,3-dihydroxy- 7-methyl xanthone (1), 2,3,6-trihydroxy-7-hydroxymethylene xanthone-1-carboxylic acid (2), 2-methoxy-4-hydroxy-7-methyl-3-O-β-D-glucopyranosyl xanthone-1,8-dicarboxylic acid (4), and 2-hydroxy-7-hydroxymethylene xanthone-1,8-dicarboxylic acid 3-O-β-D-glucopyranosyl- (2’ → 3’’)-3’’-O-stigmast-5-ene (5), along with the known steroidal glucoside β-sitosterol-β-Dglucoside (3). The structures of the isolated compounds

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16

Li, Hongqi, Anil N. Mayekar, B. Narayana, H. S. Yathirajan, and W. T. A. Harrison. "Ethyl 6-(6-methoxy-2-naphthyl)-2-oxo-4-(2-thienyl)cyclohex-3-ene-1-carboxylate." Acta Crystallographica Section E Structure Reports Online 65, no. 7 (2009): o1533. http://dx.doi.org/10.1107/s1600536809021308.

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17

Chandrima Debi and Vipin Parkash. "Influence of microbial bioinoculants on the accumulation of new phytocompounds in Oroxylum indicum (L.) Benth. ex Kurz." GSC Biological and Pharmaceutical Sciences 13, no. 3 (2020): 228–43. http://dx.doi.org/10.30574/gscbps.2020.13.3.0413.

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The seedlings of Oroxylum indicum were inoculated with plant growth promoting microbes (PGPMs) mainly, Glomus mosseae, Trichoderma harzianum and Pseudomonas putida both alone and consortium. The GCMS analysis of the methanolic root extract of inoculated seedlings of O. indicum showed that seedlings treated with mixed consortium of mycorrhizal fungi, bacteria and fungus showed the presence of maximum number of phytocompounds. The GC-MS analysis of control seedlings showed presence of 55 compounds where three new compounds were found i.e. 2-Cyclobutene-1-Carboxamide; Tetradecanoic Acid, 10, 13-d

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18

Kaur, Manpreet, Jerry P. Jasinski, Ray J. Butcher, Hemmige S. Yathirajan, Anil N. Mayekar, and Badiadka Narayana. "Crystal and Molecular Structure Studies of Ethyl 4-(4-Hydroxyphenyl)-6-(6-methoxy-2-naphthyl)-2-oxocyclohex-3-ene-1-carboxylate and Ethyl 4-(3-Bromophenyl)-6-(6-methoxy-2-naphthyl)-2-oxocyclohex-3-ene-1-carboxylate." Crystals 2, no. 3 (2012): 1239–47. http://dx.doi.org/10.3390/cryst2031239.

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19

Syah, Yana M., Nyoman S. Suastri, Jalifah Latip, and Bohari M. Yamin. "4,5-Dimethoxy-2-(1-methoxy-3-phenylallylidene)cyclopent-4-ene-1,3-dione (methyl linderone)." Acta Crystallographica Section E Structure Reports Online 61, no. 6 (2005): o1530—o1531. http://dx.doi.org/10.1107/s1600536805012833.

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20

Fun, Hoong-Kun, Ching Kheng Quah, Chengmei Huang, and Haitao Yu. "1-Benzyl-5-methoxy-2′,3-dimethyl-4,6-dioxa-2-azaspiro[bicyclo[3.2.0]hept-2-ene-7,4′-isoquinoline]-1′,3′(2′H,4′H)-dione." Acta Crystallographica Section E Structure Reports Online 67, no. 6 (2011): o1311—o1312. http://dx.doi.org/10.1107/s160053681101600x.

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21

Chandrima, Debi, and Parkash Vipin. "Influence of microbial bioinoculants on the accumulation of new phytocompounds in Oroxylum indicum (L.) Benth. ex Kurz." GSC Biological and Pharmaceutical Sciences 13, no. 3 (2020): 228–43. https://doi.org/10.5281/zenodo.4415241.

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The seedlings of <em>Oroxylum indicum</em> were inoculated with plant growth promoting microbes (PGPMs) mainly, <em>Glomus mosseae</em>, <em>Trichoderma harzianum</em> and<em> Pseudomonas putida </em>both alone and consortium. The GCMS analysis of the methanolic root extract of inoculated seedlings of <em>O. indicum </em>showed that seedlings treated with mixed consortium of mycorrhizal fungi, bacteria and fungus showed the presence of maximum number of phytocompounds. The GC-MS analysis of control seedlings showed presence of 55 compounds where thr

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22

Przezdziecka, Agnieszka, Alicja Kurek-Tyrlik, and Jerzy Wicha. "Pd-Catalyzed Cross-Coupling Reaction of Sterically Hindered Vinyl Iodides and Organozinc Reagents. Synthesis of Vitamin D Analogues with an Aromatic Ring Attached at C-17." Collection of Czechoslovak Chemical Communications 67, no. 11 (2002): 1658–68. http://dx.doi.org/10.1135/cccc20021658.

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Palladium-catalyzed coupling of steroid 17-iodo-6β-methoxy-3α,5-cyclo-5α-androst-16-ene (4) 17-iodoandrosta-5,16-dien-3β-ol (5), and structurally similar (3aS,7R,7aR)-benzenesulfonyl-3-iodo-3a-methyl-3a,4,5,6,7,7a-hexahydro-1H-indene (6) with various arylzinc chlorides, which were generated from aryl bromides 8 [1-bromomethylbenzene (8a), O-(triethylsilyl-2-bromophenyl)propan-2-ol (8b), 2-(4-bromophenyl)propan-2-ol (8c), 4-bromobenzonitrile (8d), 4-bromobenzoic acid methyl ester (8e), 4-bromobenzoic acid tert-butyl ester (8f) and 3-bromopyridine (8g)] via aryllihium derivatives (the Negishi co

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23

Fun, Hoong-Kun, Ching Kheng Quah, Chengmei Huang, and Haitao Yu. "(1S*,4′S*,5R*)-1-Isopropyl-5-methoxy-2′,3-dimethyl-4,6-dioxa-2-azaspiro[bicyclo[3.2.0]hept-2-ene-7,4′-isoquinoline]-1′,3′(2′H,4′H)-dione." Acta Crystallographica Section E Structure Reports Online 67, no. 5 (2011): o1271—o1272. http://dx.doi.org/10.1107/s1600536811015315.

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Fun, Hoong-Kun, Ching Kheng Quah, Chengmei Huang, and Haitao Yu. "(1S*,4′S*,5R*)-1-Isobutyl-5-methoxy-2′,3-dimethyl-4,6-dioxa-2-azaspiro[bicyclo[3.2.0]hept-2-ene-7,4′-isoquinoline]-1′,3′(2′H,4′H)-dione." Acta Crystallographica Section E Structure Reports Online 67, no. 5 (2011): o1273—o1274. http://dx.doi.org/10.1107/s1600536811015327.

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Fun, Hoong-Kun, Ching Kheng Quah, Chengmei Huang, and Haitao Yu. "5-Methoxy-1,2′,3-trimethyl-4,6-dioxa-2-azaspiro[bicyclo[3.2.0]hept-2-ene-7,4′-isoquinoline]-1′,3′(2′H,4′H)-dione." Acta Crystallographica Section E Structure Reports Online 67, no. 6 (2011): o1340—o1341. http://dx.doi.org/10.1107/s1600536811016266.

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26

Küçükgül, Azime. "Balık Hastalıkları ile Mücadelede Bitki Esansiyel Yağlarının Major Komponentlerinin Önemi Üzerine bir Araştırma." Turkish Journal of Agriculture - Food Science and Technology 6, no. 10 (2018): 1501. http://dx.doi.org/10.24925/turjaf.v6i10.1501-1506.2151.

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The presence of different phytochemical components of essential oil such as tannins, alkaloids, terpenoids and phenolic compounds has antibacterial, antifungal, and anti-inflammatory effects. The aim of this study is to investigate importance of the major components of three herb essential oils (Thymus vulgaris L., Centauriumerythraea Rafn. And Foeniculumvulgare Mill) on challenging with fish diseases. The components of essential oils provided from a commercial firm were made GC/MS analyzes. The major component of T. vulgarewas carvacrol called as phenol, 2-methyl-5-(1-methylethyl) with 40%.Th

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27

Gomes, Ligia R., John Nicolson Low, Catarina Oliveira, Fernando Cagide, and Fernanda Borges. "Crystal structures of three 3,4,5-trimethoxybenzamide-based derivatives." Acta Crystallographica Section E Crystallographic Communications 72, no. 5 (2016): 675–82. http://dx.doi.org/10.1107/s2056989016005958.

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The crystal structures of three benzamide derivatives,viz. N-(6-hydroxyhexyl)-3,4,5-trimethoxybenzamide, C16H25NO5, (1),N-(6-anilinohexyl)-3,4,5-trimethoxybenzamide, C22H30N2O4, (2), andN-(6,6-diethoxyhexyl)-3,4,5-trimethoxybenzamide, C20H33NO6, (3), are described. These compounds differ only in the substituent at the end of the hexyl chain and the nature of these substituents determines the differences in hydrogen bonding between the molecules. In each molecule, them-methoxy substituents are virtually coplanar with the benzyl ring, while thep-methoxy substituent is almost perpendicular. The c

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28

Ibrahim, Sabrin R. M. "New Chromone and Triglyceride from Cucumis melo Seeds." Natural Product Communications 9, no. 2 (2014): 1934578X1400900. http://dx.doi.org/10.1177/1934578x1400900217.

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Re-investigation of the MeOH extract of the seeds of Cucumis melo L. var. reticulatus (Cucurbitaceae) led to the isolation of a new chromone derivative (5,7-dihydroxy-2-[2-(3-methoxy-4-hydroxyphenyl)ethyl]chromone (5) and a triglyceride (1,3-di-(6 Z,9 Z)-docosa-6,9-dienoyl-2-(6 Z) hexacos-6-enoylglycerol (1), together with three known compounds; α-spinasterol (2), stigmasta-7,22,25-trien-3-ol (3), and D:B-friedoolean-5-ene-3-β-ol (4), are reported from this species for the first time. Their structures were determined by extensive 1D (1H, 13C, and DEPT) and 2D (1H-1H COSY, HMQC, and HMBC) NMR a

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29

Al-Khatib, Kassim, Robert Parker, and E. Patrick Fuerst. "Rose (Rosa dilecta) Response to Simulated Herbicide Drift." HortTechnology 2, no. 3 (1992): 394–98. http://dx.doi.org/10.21273/horttech.2.3.394.

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This study evaluated the response of rose to different herbicides applied as simulated drift. Chlorsulfuron {2-chloro-N-[[(4-methoxy-6-methyl-1,3,5-triazin-2-yl)amino]carbonyl]benzenesulfonamide}, thifensulfuron {3[[[[(4-methoxy-6-methyl-1,3,5-triazin-2-yl)amino]carbonyl]amino]sulfonyl]-2-thiophenecarboxylic acid}, bromoxynil(3,5-dibromo-4-hydroxybenzonitrile), 2,4-D[(2,4-dichlorophenoxy)acetic acid], glyphosate [N-(phosphonomethyl) glycine], and a combination of 2,4-D and glyphosate were applied over the top of established rose plants at 1/3, 1/10,1/33, and 1/100 of the maximum labeled rate f

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30

Chi, Lu-Ping, Xiao-Ming Li, Li Li, Xin Li, and Bin-Gui Wang. "Cytotoxic Thiodiketopiperazine Derivatives from the Deep Sea-Derived Fungus Epicoccum nigrum SD-388." Marine Drugs 18, no. 3 (2020): 160. http://dx.doi.org/10.3390/md18030160.

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Four new thiodiketopiperazine alkaloids, namely, 5’-hydroxy-6’-ene-epicoccin G (1), 7-methoxy-7’-hydroxyepicoccin G (2), 8’-acetoxyepicoccin D (3), and 7’-demethoxyrostratin C (4), as well as a pair of new enantiomeric diketopiperazines, (±)-5-hydroxydiphenylalazine A (5), along with five known analogues (6–10), were isolated and identified from the culture extract of Epicoccum nigrum SD-388, a fungus obtained from deep-sea sediments (−4500 m). Their structures were established on the basis of detailed interpretation of the NMR spectroscopic and mass spectrometric data. X-ray crystallographic

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31

Ahmad, Viqar Uddin, Saima Arshad, Sadia Bader, et al. "A New Triterpenoidal Saponin and a Flavone Glycoside from Stachys parviflora." Natural Product Communications 2, no. 9 (2007): 1934578X0700200. http://dx.doi.org/10.1177/1934578x0700200903.

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A new triterpenoidal saponin, stachyssaponin C (1), identified as 3β, 15α, 21β-trihydroxy-olean-12-ene-28-oic acid 3- O-[α-L-rhamnopyranosyl-(1→3)- O-6″- O-acetyl-β-D-glucopyranosyl-(1→2)- O-β-D-glucopyranoside] and a flavone glycoside stachyfloroside A (2), characterized as 5,8-dihydroxy-2-(3′-hydroxy-4′-methoxy)-7 [(6″”- O-acetyl-β-D-allopyranosyl-(1→2)- O-α-D-glucopyranosyl-(1→2)- O-β-D-glucopyranosyl)oxy]-4H-1-benzopyran-4-one, were isolated from the n-butanol extract of Stachys parviflora (Lamiaceae). The structures were elucidated by extensive spectroscopic (especially 2D NMR) experiment

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32

Collins, David J., and Ian T. Crosby. "Enolic Ortho Esters. VIII Synthesis of (2S,3S)-2,3-Bis(methoxymethyl)-1,4,6-trioxaspiro[4.5]dec-7-ene." Australian Journal of Chemistry 51, no. 11 (1998): 1025. http://dx.doi.org/10.1071/c98085.

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Enolic ortho ester (2S,3S)-2,3-bis(methoxymethyl)-1,4,6-trioxaspiro[4.5]dec-7-ene (10b) was synthesized in 65% yield by cycloadditon of acrolein with the ketene acetal (4S,5S)-4,5-bis(methoxymethyl)-2-methylidene-1,3-dioxolan (7), derived by potassium t-butoxide treatment of (4S,5S)-4,5-bis(methoxy- methyl)-1,3-dioxolan (4). Lewis acid catalysed reaction (TiCl4, CH2Cl2, –78°) of the enolic ortho ester (10b) with the ketene silyl acetal 3-phenylmethyl-2-trimethylsilyloxy-4,5-dihydrofuran (15) afforded the formyl keto ester 3-[4′,5′-bis(methoxymethyl)-2′-(4′′-oxobutyl)-1′,3′-dioxolan-2′-yl]-3-ph

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Miles, CO, L. Main, and BK Nicholson. "Synthesis of 2', 6'-Dihydroxychalcones by Using Tetrahydropyran-2-yl and Trialkylsilyl Protective Groups; the Crystal Structure Determination of 2',6'-Dihydroxy-2,4,6-trimethoxychalcone." Australian Journal of Chemistry 42, no. 7 (1989): 1103. http://dx.doi.org/10.1071/ch9891103.

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Two improved general routes to 2′,6′-dihydroxychalcones are described in which the final step is protective-group removal from O 2′ under mild acid conditions. The first involves base-catalysed condensation of benzaldehydes with 2′-hydroxy-6′-tetrahydropyran-2-yloxyacetophenone, the second ring-opening of 5-hydroxyflavanones with 1,8-diazabicyclo[5.4.0]undec-7-ene in the presence of a trialkylchlorosilane to trap out the chalcone as a bis silyl ether. Chalcones prepared by the first route are 2',6'-dihydroxychalcone (1), and its 4-methoxy (2), 3,4-dimethoxy (3), 3,4,5-trimethoxy (4), and 2,4,6

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34

Çelikesir, Sevim Türktekin, Mehmet Akkurt, Aliasghar Jarrahpour, Mehdi Mohammadi Chermahini, Pezhman Shiri, and Orhan Büyükgüngör. "Crystal structure of {(E)-4-[(1-allyl-1H-1,2,3-triazol-4-yl)methoxy]benzylidene}[2-(morpholin-4-yl)ethyl]amine." Acta Crystallographica Section E Structure Reports Online 70, no. 9 (2014): o933—o934. http://dx.doi.org/10.1107/s1600536814016754.

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In the title compound, C19H25N5O2, the morpholine ring has a chair conformation. The plane of the central benzene ring makes dihedral angles of 88.75 (12) and 60.02 (7)°, respectively, with the mean plane formed by the four planar C atoms of the morpholine ring and with the plane of the triazole ring. In the crystal, molecules are linkedviaC—H...π interactions, forming slabs lying parallel to (10-1). The C atoms of the bridging ethylene group, between the morpholine and benzene rings, and the terminal ethene group of the prop-1-ene substituent attached to the triazole ring, are disordered over

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Rae, ID, and AK Serelis. "Dimethyl cis- and trans-1,2-Dimethylcyclohexane-1,2-dicarboxylate." Australian Journal of Chemistry 43, no. 11 (1990): 1941. http://dx.doi.org/10.1071/ch9901941.

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1-Methoxy-3-trimethylsilyloxybuta-1,3-diene adds readily to dimethylmaleic anhydride, and the product can be converted into dimethyl cis-1,2-dimethylcyclohex-4-ene-1,2-dicarboxylate (3). The several steps required mean that this route compares unfavourably with direct addition of butadiene to the anhydride. The best route to the cis-diester (3) is cyclialkylation of the dianion from dimethyl 2,3-dimethylbutanedioate with (Z)-1,4-dichlorobut-2-ene. A bismethylation reaction is used to prepare imide (II), which can be converted into the cis-diester (1) only with considerable difficulty, and bism

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Arnold, Donald R., Xinyao Du, and Huub J. P. de Lijser. "The photochemical nucleophile–olefin combination, aromatic substitution (photo-NOCAS) reaction. Part 8: methanol–2-carene, and 1,4-dicyanobenzene." Canadian Journal of Chemistry 73, no. 4 (1995): 522–30. http://dx.doi.org/10.1139/v95-067.

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The structure and reactivity of the radical cation of (+)-2-carene ((1S,6R)-3,7,7-trimethyl-cis-bicyclo[4.1.0]hept-2-ene (3)) have been studied. The radical cation was generated by photoinduced single electron transfer to the first electronically excited singlet state of 1,4-dicyanobenzene in acetonitrile–methanol (3:1). The 1:1:1 (methanol:2-carene:1,4-dicyanobenzene) adducts were formed: trans-3-(4-cyanophenyl)-4-(1-methoxy-1-methylethyl)-1-methylcyclohexene(14), and cis- (15) and trans-3-(4-cyanophenyl)-6-(1-methoxy-1-methylethyl)-3-methylcyclohexene (16) in a combined yield of 80%. The eff

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37

Xie, Cheng Ping, Kai Fu Li, Jin Ling Lin, and Jian Bian Li. "GC-MS Analysis on Heartwood Extractive Chemical Components of Different Provenances Teak（Tectona Grandis L.f.）." Advanced Materials Research 236-238 (May 2011): 1049–53. http://dx.doi.org/10.4028/www.scientific.net/amr.236-238.1049.

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Teak (Tectona grandisL.f) is decay resistance and natural durability. These advantages are relationship with inclusion of teak. For breeding, planting, and the wood used to its best advantage by the end-user, further information concerning the heartwood extractive chemical of different provenances teak is necessary, However, because of limitation of analytical instruments, the extractive chemical components of teak centre on decay resistance relationship with napthoquinone, tectoquinone, and so on, nobody systematacially analyzed heartwood extractive chemical components of different teak. We a

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Wrackmeyera, Bernd, Sergej V. Gruener, and Alla S. Zolotareva. "Reactivity of Alkoxyethynyl(trimethyl)silane, -germane and -stannane towards Trialkylboranes. Organometallic-Substituted Enol Ethers." Zeitschrift für Naturforschung B 58, no. 11 (2003): 1035–40. http://dx.doi.org/10.1515/znb-2003-1101.

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Abstract Methoxyethynyl(trimethyl)silane (1a) reacts at 100°C very slowly with triethylborane (4) to give a mixture of alkenes, one of which is the 1,1-organoboration product (Z)-1-methoxy-1-trimethylsilyl- 2-diethylboryl-but-1-ene (7a). Methoxyethynyl(trimethyl)germane (2a) reacts within minutes at 60 - 70°C with 4, tripropylborane (5) and 9-ethyl-9-borabicyclo[3.3.1]nonane (6) by 1,1-organoboration in the usual regio- and stereospecific way to give the corresponding alkenes (9a - 11a). The analogous reactions of the ethoxyethynyl(trimethyl)germane (2b) require longer heating and are accompan

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39

Nam, Nguyen-Hai, Yong Kim, Young-Jae You, Dong-Ho Hong, Hwan-Mook Kim, and Byung-Zun Ahn. "Water soluble prodrugs of the antitumor agent 3-[(3-amino-4-methoxy)phenyl]-2-(3,4,5-trimethoxyphenyl)cyclopent-2-ene-1-one." Bioorganic & Medicinal Chemistry 11, no. 6 (2003): 1021–29. http://dx.doi.org/10.1016/s0968-0896(02)00514-x.

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40

Stennett, Amanda, Norma Ofsthun, John Larkin, et al. "Treatment of a Large National Population of Anemic Hemodialysis Patients with a Long-Lasting Erythropoietin Stimulating Agent." Blood 128, no. 22 (2016): 1268. http://dx.doi.org/10.1182/blood.v128.22.1268.1268.

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Abstract Introduction: Patients with chronic kidney disease who progress to end stage renal disease (ESRD) require renal replacement therapy to assume some functions of the diseased kidney and sustain life. Hemodialysis (HD) is the most common option for renal replacement therapy in ESRD patients and includes routine treatments 3 times per week to filter uremic toxins and remove excess fluid from the blood. The prevalence of anemia is high in the ESRD population with about 80% of HD patients being treated with an erythropoietin stimulating agent (ESA) for management of anemia (United States Re

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Yadav, Veejendra K., Govindaraji Senthil, K. Ganesh Babu, Masood Parvez та Jennifer Lee Reid. "Heteroatom Influence on the π-Facial Selectivity of Diels−Alder Cycloadditions to 1-Oxa-4-thia-6-vinylspiro[4.5]dec-6-ene, 3-Methoxy-3-methyl-2-vinylcyclohexene, and 3-Methoxy-2-vinylcyclohexene†,‡". Journal of Organic Chemistry 67, № 4 (2002): 1109–17. http://dx.doi.org/10.1021/jo0106400.

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Thamotharan, S., V. Parthasarathi, Ranju Gupta, Sheetal Guleria, D. P. Jindal та Anthony Linden. "Two androst-5-ene derivatives: 16-[4-(3-chloropropoxy)-3-methoxybenzylidene]-17-oxoandrost-5-en-3β-ol and 16-[3-methoxy-4-(2-pyrrolidin-1-ylethoxy)benzylidene]-3β-pyrrolidinoandrost-5-en-17β-ol monohydrate". Acta Crystallographica Section C Crystal Structure Communications 60, № 1 (2003): o75—o78. http://dx.doi.org/10.1107/s0108270103025605.

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43

Moreno, Eufemio, Titto Varughese, Carmenza Spadafora, et al. "Chemical Constituents of the New Endophytic Fungus Mycosphaerella sp. nov. and Their Anti-parasitic Activity." Natural Product Communications 6, no. 6 (2011): 1934578X1100600. http://dx.doi.org/10.1177/1934578x1100600620.

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Chemical investigation of a new endophytic fungus, Mycosphaerella sp. nov. strain F2140, associated with the foliage of the plant Psychotria horizontalis (Rubiaceae) in Panama, resulted in the isolation of cercosporin (1) and a new cercosporin analog (3) as the major components. The structures of minor compounds in the extract were elucidated by detailed spectroscopic analysis as 2-(2-butyl)-6-ethyl-3-hydroxy-6-methylcyclohex-2-ene-1, 5-dione (4), 3-(2-butyl)-6-ethyl-5-hydroxy-2-methoxy-6-methyl-cyclohex-2-enone (5), and an isomer of 5 (6). To study the influence of the hydroxy groups on the a

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Cun, Wendy Y., Paul A. Keller та Stephen G. Pyne. "Synthesis of 7α-Methoxy-7-(4-phenyl-1H-1,2,3-triazol-1-yl)acetamino-3′-arylthio-cephalosporic Acid Derivatives from 7-Aminocephalosporic Acid". Molecules 28, № 21 (2023): 7338. http://dx.doi.org/10.3390/molecules28217338.

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The aim of this project was to develop a synthetic protocol for the preparation of a cephamycin scaffold that would readily allow the synthesis of its analogues with variations at the C-7 amino group and the C-3′ position. We also aimed to develop a method that avoided the use of toxic and potentially explosive diphenyldiazomethane. These aims were achieved via the synthesis of the novel α-bromo acetamide 18 which allowed functionalization at the α-bromo acetamide position by azide and then the introduction of a 4-phenyl-1H-1,2,3-triazol-1-yl moiety via a Cu(I)-catalysed azide–alkyne cycloaddi

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Ogbuchiekwe, Edmund J., Milton E. McGiffen, Joe Nunez, and Steven A. Fennimore. "Tolerance of Carrot to Low-rate Preemergent and Postemergent Herbicides." HortScience 39, no. 2 (2004): 291–96. http://dx.doi.org/10.21273/hortsci.39.2.291.

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Preemergent and postemergent herbicides were evaluated in the Mediterranean climate of the southern San Joaquin Valley and the desert climate of the Imperial Valley from 1998 through 2000. Sixteen herbicide treatments were applied both as preemergence (PRE) and postemergence (POST) applications to carrot (Daucus carota L.). Carrot was generally more tolerant to PRE herbicide applications than to POST applications. Carrot was tolerant to PRE and POST imazamox and triflusulfuron at both locations. Carrot root losses due to herbicide were consistent with visual ratings. Treatments that injured ca

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Batubara, R., B. Wirjosentono, A. H. Siregar, U. Harahap, and Tamrin. "Chemical Compounds and Antioxidant Potential in Hot Water Extract of Cultivated Agarwood (Aquilaria malaccensis) Lamk Leaves." IOP Conference Series: Earth and Environmental Science 830, no. 1 (2021): 012070. http://dx.doi.org/10.1088/1755-1315/830/1/012070.

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Abstract Agarwood (Aquilaria malaccensis Lamk) leaves has potential as a source of antioxidants because in the hot water extract contains secondary metabolite compounds. This research aims to observe the chemical compounds and antioxidant potential in hot water extract of cultivated agarwood leaves. Agarwood leaves are processed into simplicia, and extracted with hot water. Several tests conducted in this research, including phytochemical screening in order to observe the chemical compounds in hot water extract of agarwood leaves; GC-MS test to observe the chemical constituents, and DPPH metho

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Batubara, R., B. Wirjosentono, A. H. Siregar, U. Harahap, and Tamrin. "Chemical Compounds and Antioxidant Potential in Hot Water Extract of Cultivated Agarwood (Aquilaria malaccensis) Lamk Leaves." IOP Conference Series: Earth and Environmental Science 830, no. 1 (2021): 012070. http://dx.doi.org/10.1088/1755-1315/830/1/012070.

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Abstract Agarwood (Aquilaria malaccensis Lamk) leaves has potential as a source of antioxidants because in the hot water extract contains secondary metabolite compounds. This research aims to observe the chemical compounds and antioxidant potential in hot water extract of cultivated agarwood leaves. Agarwood leaves are processed into simplicia, and extracted with hot water. Several tests conducted in this research, including phytochemical screening in order to observe the chemical compounds in hot water extract of agarwood leaves; GC-MS test to observe the chemical constituents, and DPPH metho

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Arey, Brian J., Darlene C. Deecher, Emily S. Shen, et al. "Identification and Characterization of a Selective, Nonpeptide Follicle-Stimulating Hormone Receptor Antagonist." Endocrinology 143, no. 10 (2002): 3822–29. http://dx.doi.org/10.1210/en.2002-220372.

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Abstract The glycoprotein hormones (LH, FSH, and TSH) are critical to the maintenance of physiological homeostasis and control of reproduction. However, despite an obvious utility for synthetic pharmacological agents, there are few reports of selective, nonpeptide agonists or antagonists to receptors for these hormones. We have identified and characterized a novel synthetic molecule capable of inhibiting the action of FSH. This compound, 7-{4-[Bis-(2-carbamoyl-ethyl)-amino]-6-chloro-(1,3,5)-triazin-2-ylamino)-4-hydroxy-3-(4-methoxy-phenylazo)-naphthalene}-2-sulfonic acid, sodium salt (compound

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49

Bensaad, Mohamed Sabri, Saliha Dassamiour, Leila Hambaba, et al. "Chemical Profile by Gas Chromatography/Mass Spectrometry of Ethyl Acetate and N-butanol Extracts of Centaurea tougourensis Boiss. & Reut." Journal of Biobased Materials and Bioenergy 16, no. 1 (2022): 140–49. http://dx.doi.org/10.1166/jbmb.2022.2158.

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Nowadays, plants bioactive compounds are considered as a new source of therapy, especially for the elaboration process of more effective drugs. 80% of the actual drug substances are purely natural and originate from plants, representing a new hope, especially for the treatment of chronic illnesses. The aim of this study is to characterize the phytochemical composition of C. tougourensis via gas chromatography-mass spectrometry (GC-MS) approach. This method allowed the identification of 45 compounds in the n-butanol extract (n-BuOH), in which 12 compounds were in majority, namely; 2H-Furo [2,3-

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Ferdosi, Malik Fiaz Hussain, Iqra Haider Khan, Arshad Javaid, and Ayesha Munir. "BIOCHEMICAL PROFILE OF Calotropis procera FLOWERS." JOURNAL OF WEED SCIENCE RESEARCH 27, no. 3 (2021): 341–49. http://dx.doi.org/10.28941/pjwsr.v27i3.982.

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Calotropis procera is a medicinal weed of family Asclepiadaceae. This study was carried out to explore the biochemical profile of C. procera flowers collected from Southern Punjab region of Pakistan. Methanolic flower extract of C. procera was subjected to GC-MS analysis. There were 30 compounds identified in this extract. The predominant compound was γ-sitosterol with 15.39% peak area. Other abundantly occurring compounds included stigmasterol (9.22%), 9,12-octadecadienoic acid (Z,Z)-, methyl ester (9.01%), campesterol (8.63%), α-amyrin acetate (8.25%), β-amyrin (8.09%), hexadecanoic acid, me

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