Academic literature on the topic 'Bromosuccinimide'

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Journal articles on the topic "Bromosuccinimide"

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OIZUMI, Mitsuru. "N-Bromosuccinimide." Journal of Synthetic Organic Chemistry, Japan 51, no. 1 (1993): 68–69. http://dx.doi.org/10.5059/yukigoseikyokaishi.51.68.

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Mavračić, Juraj, Dominik Cinčić, and Branko Kaitner. "Halogen bonding ofN-bromosuccinimide by grinding." CrystEngComm 18, no. 19 (2016): 3343–46. http://dx.doi.org/10.1039/c6ce00638h.

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Two halogen bonded cocrystals ofN-bromosuccinimide and 4,4′-bipyridine, with stoichiometric ratios 1 : 1 and 2 : 1, have been synthesized and characterized. We present the first mechanochemical cocrystallization ofN-bromosuccinimide.
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Andin, A. N., and M. A. Engelgardt. "Synthesis of Functionalized Spiro[1-benzofuran-2,5'-pyrimidine] Derivatives of 5-Arylidenebarbituric Acids." Russian Journal of Organic Chemistry 60, no. 11 (2024): 2125–29. https://doi.org/10.1134/s1070428024110058.

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Abstract Adducts of dimedone and 5-arylidenebarbituric acids react with N-bromosuccinimide in aqueous ethanol to give functionalized spiro[1-benzofuran-2,5'-pyrimidine] derivatives with moderate yields. The reaction of 5-benzylidenebarbituric acid with ethyl acetoacetate in the presence of N-bromosuccinimide provides spiro[pyrimidine-5,6'-furo[2,3-d]pyrimidine].
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Ghassemzadeh, Mitra, Klaus Harms, Kurt Dehnicke та Dieter Fenske. "μ2-Halogenokomplexe von N-Bromsuccinimid und N-Bromphthalimid. Die Kristallstrukturen von PPh4[X(N-Bromsuccinimid)2] und von PPh4[X(N-Bromphthalimid)2] mit X = CI und Br / μ2-Halogeno Complexes of N-Bromosuccinimide and N-Bromophthalimide. The Crystal Structures of PPh4 [X(N-Bromosuccinimide)2] and PPh4 [X(N-Brom ophthalimide)2] with X = Cl and Br". Zeitschrift für Naturforschung B 49, № 5 (1994): 593–601. http://dx.doi.org/10.1515/znb-1994-0504.

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The μ2-halogeno complexes PPh4[X(N-bromosuccinimide)2] and PPh4[X(N-bromophthali- mide)2] with X = Cl and Br have been prepared by reactions of N-bromosuccinimide and N-bromophthalimide, respectively, with the corresponding tetraphenylphosphonium halides PPh4X in acetonitrile solutions. The compounds form pale yellow crystal needles, which were characterized by IR spectroscopy and by crystal structure determinations. PPh4[Cl(N-Bromosuccinimide)2] (1): Space group P21/n, Z = 4, structure solution with 2516 observed unique reflections, R = 0.040. Lattice dimensions at -25 °C: a = 1775.9(1), b =
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Singh, Minu. "Kinetic Treatment of the Reaction of Fructose and N-Bromosuccinimide in Cationic/Anionic/Nonionic Micelles." Journal of Soft Matter 2014 (September 30, 2014): 1–10. http://dx.doi.org/10.1155/2014/791563.

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The kinetics of oxidation of fructose by N-bromosuccinimide in acidic medium in the absence and presence of cationic, anionic, and nonionic surfactants has been measured iodometrically under pseudo-first-order condition. The oxidation kinetics of fructose by N-bromosuccinimide shows a first-order dependence on N-bromosuccinimide, fractional order dependence on fructose, and negative fractional order dependence on sulfuric acid. The kinetics is treated using Berezin’s micellar model that was previously used for the catalysis and inhibition of the reaction. The determined stoichiometric ratio wa
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Bera, Smritilekha, Dhananjoy Mondal, and Bhaskar Chatterjee. "Application of N-Bromosuccinimide in Carbohydrate Chemistry." SynOpen 07, no. 04 (2023): 501–10. http://dx.doi.org/10.1055/s-0042-1751501.

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AbstractThis article describes the use of N-bromosuccinimide in different organic group transformations in carbohydrate chemistry. A comprehensive discussion on the synthesis of deoxysugars through selective O-benzylidene fragmentation, photobromination, halogenation, oxidation, and polymerisation of different carbohydrate moieties with the aid of N-bromosuccinimide (NBS) is presented. The use of NBS in the most significant glycosylation methods and in oligosaccharide synthesis is also discussed.
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Sanad, H. M., and Alhussein A. Ibrahim. "Radioiodination, diagnostic nuclear imaging and bioevaluation of olmesartan as a tracer for cardiac imaging." Radiochimica Acta 106, no. 10 (2018): 843–50. http://dx.doi.org/10.1515/ract-2018-2960.

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Abstract The present work has been oriented to prepare radioiodinated olmesartan for a potential cardiac imaging. Olmesartan has been labeled using 125I or 131I with N-bromosuccinimide (NBS) as an oxidizing agent. Many factors like amount of N-bromosuccinimide, amount of substrate, pH, reaction temperature and reaction time, have been systematically studied to optimize high yield of [125I]iodoolmesartan. The biological distribution indicates the suitability of [125I]iodoolmesartan as a novel tracer to image heart.
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Khazaei, Ardeshir, Amin Rostami, Ayeh Raiatzadeh, and Marjan Mahboubifar. "N-Bromosuccinimide (NBS) — Selective and effective catalyst for trimethylsilylation of alcohols and phenols using hexamethyldisilazane and their regeneration under mild and neutral reaction conditions." Canadian Journal of Chemistry 85, no. 5 (2007): 336–40. http://dx.doi.org/10.1139/v07-029.

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Structurally diverse alcohols and phenols were trimethylsilylated in a clean and efficient reaction with hexamethyldisilazane (HMDS) based on the use of a catalytic amount of N-bromosuccinimide under both dichloromethane and solvent-free conditions at room temperature. Deprotection of trimethylsilyl ethers was also be achieved efficiently in the presence of a catalytic amount of NBS in methanol at ambient temperature.Key words: N-bromosuccinimide, solvent-free, alcohols, phenols, hexamethyldisilazane, trimethylsilyl ether, catalyst, detrimethylsilylation.
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Giridhar Reddy, P., K. Ramesh, S. Shylaja, K. C. Rajanna, and S. Kandlikar. "Ru (III) Catalyzed Oxidation of Aliphatic Ketones by N-Bromosuccinimide in Aqueous Acetic Acid: A Kinetic Study." Scientific World Journal 2012 (2012): 1–7. http://dx.doi.org/10.1100/2012/456516.

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Kinetics of Ru (III) catalyzed oxidation of aliphatic ketones such as acetone, ethyl methyl ketone, diethyl ketone, iso-butylmethyl ketone by N-bromosuccinimide in the presence of Hg(II) acetate have been studied in aqueous acid medium. The order of [N-bromosuccinimide] was found to be zero both in catalyzed as well as uncatalyzed reactions. However, the order of [ketone] changed from unity to a fractional one in the presence of Ru (III). On the basis of kinetic features, the probable mechanisms are discussed and individual rate parameters evaluated.
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Salman, Noori Y. "Kinetics Study of the Reaction between Serine and N-Bromosuccinimide in the Presence of Palladium (Pd2+)." INTERNATIONAL JOURNAL OF DRUG DELIVERY TECHNOLOGY 12, no. 02 (2022): 771–74. http://dx.doi.org/10.25258/ijddt.12.2.54.

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The oxidation of serine using N-bromosuccinimide (NBS) has been studied at fix pH value. The reaction presents a first-order reaction with respect to both substrate and oxidant. It is noted that the rate of reaction increases with increasing the palladium ion concentration. The addition of the reaction product (succinimide) affects the oxidation reaction rate. The protonated Br+ or NBrS and NBrS are used to be the reactive species of the N-bromosuccinimide. Furthermore, intermediate compounds are noticed through the reaction. Finally, a mechanism for the oxidation reaction is suggested in this
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Dissertations / Theses on the topic "Bromosuccinimide"

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Chiuan, Guo Yi, та 郭益全. "Study of β-CD on the Chemiluminescence from the Oxidation of Luminol with N-Bromosuccinimide". Thesis, 2004. http://ndltd.ncl.edu.tw/handle/43216248641273942456.

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碩士<br>國立臺灣大學<br>化學研究所<br>92<br>Chemiluminescence(CL) has wide analytical applications for the determination of metal ions, antioxidants, and organic compounds. Stopped–Flow spectrometry was employed to determine the CL of luminol system using N-bromosuccinimide(NBS)as the oxidizing agent. We have also investigated the enhancement of CL emission by �牷V cyclodextrin(�牷VCD). The main advantages of NBS over other common inorganic oxidants are that these oxidants are colorless, provides higher sensitivity. In this study, we have found that the CL emission from the Oxidation of luminol with NB
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Lin, Mei-Hui, and 林美慧. "Inhibition of tonoplast ATPase from etiolated mung bean seedlings by N-bromosuccinimide and 2-hydroxy-5-nitrobenzyl bromide." Thesis, 1993. http://ndltd.ncl.edu.tw/handle/46992733862404601020.

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Kuo, Chun-Wei, and 郭俊偉. "(I) Novel synthetic strategy for the synthesis of biologically active N-heterocycles catalyted by N-bromosuccinimide (II) Application of phosphous reagent in organic synthesis (III) SAR study on novel series of oxadiazoles as CB1 cannabinoid receptor anta." Thesis, 2008. http://ndltd.ncl.edu.tw/handle/89076146759847732159.

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博士<br>國立臺灣師範大學<br>化學系<br>96<br>In the first part of this dissertation, we have focused on the use of relatively low toxic, inexpensive reagents such as N-bromosuccinimide for carrying out the catalytic synthetic methodology. Various biologically important 1,5-benzodiazepine derivatives were efficiently synthesized in excellent yields. Furthermore, 3-indolyl-nitroalkane derivatives can be synthesized utilizing this newly development catalytic system as well. The second part is focused on ethyl dichlorophosphate mediates functional group transormation from primary amides into nitriles under mil
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Book chapters on the topic "Bromosuccinimide"

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Aitken, R. A. "Using -Bromosuccinimide." In Five-Membered Hetarenes with Three or More Heteroatoms. Georg Thieme Verlag KG, 2004. http://dx.doi.org/10.1055/sos-sd-013-01301.

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lvarez, M., and J. A. Joule. "Using -Bromosuccinimide." In Six-Membered Hetarenes with One Nitrogen or Phosphorus Atom. Georg Thieme Verlag KG, 2005. http://dx.doi.org/10.1055/sos-sd-015-01268.

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Yan, L., S. Lin, and P. Liu. "Using -Bromosuccinimide." In Three Carbon-Heteroatom Bonds: Acid Halides; Carboxylic Acids and Acid Salts. Georg Thieme Verlag KG, 2007. http://dx.doi.org/10.1055/sos-sd-020-00682.

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Yan, L., S. Lin, and P. Liu. "Using Bromosuccinimide." In Three Carbon-Heteroatom Bonds: Acid Halides; Carboxylic Acids and Acid Salts. Georg Thieme Verlag KG, 2007. http://dx.doi.org/10.1055/sos-sd-020-00707.

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Hartung, J. "Bromination with -Bromosuccinimide." In Chlorine, Bromine, and Iodine. Georg Thieme Verlag KG, 2007. http://dx.doi.org/10.1055/sos-sd-035-00282.

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Pfeiffer, W. D. "Reaction with -Bromosuccinimide." In Chlorine, Bromine, and Iodine. Georg Thieme Verlag KG, 2007. http://dx.doi.org/10.1055/sos-sd-035-00397.

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Leung, M. k., and T. Y. Luh. "Catalyzed by -Bromosuccinimide." In Acetals: O/N, S/S, S/N, and N/N and Higher Heteroatom Analogues. Georg Thieme Verlag KG, 2007. http://dx.doi.org/10.1055/sos-sd-030-00223.

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Prakash, G. K. S., and J. Hu. "Reaction of -Bromosuccinimide." In Three Carbon-Heteroatom Bonds: Amides and Derivatives; Peptides; Lactams. Georg Thieme Verlag KG, 2005. http://dx.doi.org/10.1055/sos-sd-022-00775.

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Pfeiffer, W. D. "Allylic Bromination Using -Bromosuccinimide." In Chlorine, Bromine, and Iodine. Georg Thieme Verlag KG, 2007. http://dx.doi.org/10.1055/sos-sd-035-00420.

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Yoshimoto, F. K., and Q. Li. "-Bromosuccinimide-Induced Ring Formation." In Six-Membered Hetarenes with Two Identical Heteroatoms. Georg Thieme Verlag KG, 2012. http://dx.doi.org/10.1055/sos-sd-116-00549.

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Conference papers on the topic "Bromosuccinimide"

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Nayif, Shaimaa, and Dawood Alhabbo. "Indirect spectrophotometric determination of cefotaxime using N-bromosuccinimide and crystal violet dye." In INTERNATIONAL CONFERENCE OF COMPUTATIONAL METHODS IN SCIENCES AND ENGINEERING ICCMSE 2021. AIP Publishing, 2023. http://dx.doi.org/10.1063/5.0118286.

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DU, J. X., L. HAO, and J. R. LU. "CHEMILUMINESCENCE DETERMINATION OF RUTIN BASED ON A MICELLE-SENSITIZING N-BROMOSUCCINIMIDE-H2O2 REACTION." In Proceedings of the 15th International Symposium. WORLD SCIENTIFIC, 2008. http://dx.doi.org/10.1142/9789812839589_0041.

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Novák, Zoltán, and Tarek Salama. "Silicon Assisted Halogenation III: Tetrachlorosilane Induced Benzylic Bromination with N-Bromosuccinimide at Room Temperature." In The 14th International Electronic Conference on Synthetic Organic Chemistry. MDPI, 2010. http://dx.doi.org/10.3390/ecsoc-14-00470.

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Atiyah, Ali, Kameran Hussein, and Abdul Majeed Ahmed. "Spectrophotometric Determination of Escitalopram Oxalate in Pure Form and its Pharmaceutical Preparation via Oxidative Coupling Reaction." In 5th International Conference on Biomedical and Health Sciences. Cihan University-Erbil, 2024. http://dx.doi.org/10.24086/biohs2024/paper.1353.

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background: One of the techniques for spectroscopic determination are the oxidative coupling reaction, have been utilized in the estimation of compounds in many fields, such as agriculture, clinical, and pharmacological analysis. Aims: The aim of this studying to locate a sensitive and cheap technique for the estimation of escitalopram-oxalate (ESC) in pharmacological compositions and in pure form. Methods and Material: The process relies on the coupling between the escitalopram oxalate with 4-aminoantipyrine (4-AAP) in a basic medium in the attend of N-Bromosuccinimide (NBS) to produce an int
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