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Journal articles on the topic 'Chlorothiazolo'

Author: Grafiati

Published: 5 June 2025

Last updated: 1 August 2025

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1

JAG, MOHAN, and VERMA PRATIMA. "Condensed Heterocyclic Systems. Synthesis and Antimicrobial Activities of Thiazolo[3',2' : 2,3 ][1 ,2,4 ]triazino[ 5,6-b ]indoles and Isomeric Thiazolo- [2'3' : 3,4](1 ,2,4)triazino[5,6-b]indoles." Journal Of India Chemical Society Vol.66, Apr 1989 (1989): 252–54. https://doi.org/10.5281/zenodo.5948697.

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Department of Chemistry, Maharshi Dayanand University, Rohtak-124 001 <em>Manuscript received 7 November 1988, accepted 19 January 1989</em> 6-Chloro-5<em>H -</em>2,3-dihydro[1,2 4]triazino[5,6 <em>b</em>]indole-3-thione (2) on condensation with \(\propto\) -haloketones gives 5<em>H</em>-3-aroylmethylthio-6-chloror[1,2,4]triazino[5,6-<em>b</em>]indole hydrohalides (3) which on PPA-catatysed cyclisation furnish 3-aryl-9-chlorothiazolo[ 3',2' :2,3][1 2,4] triazino[5,6-<em>b</em>]indoles (4) and not the augular isomeric 1-aryl-9- chlorothiazolo [2&#

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2

Hanoun, J. P., G. Boyer, and J. P. Galy. "Crystal structure of 6-butyl-2-chlorothiazolo[5,4-a]acridin-11(6H)-one, C18H15ClN2OS." Zeitschrift für Kristallographie - New Crystal Structures 215, no. 3 (2000): 455–56. http://dx.doi.org/10.1515/ncrs-2000-0373.

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3

Liu, Jian, Raymond J. Patch, Carsten Schubert, and Mark R. Player. "Single-Step Syntheses of 2-Amino-7-chlorothiazolo[5,4-d]pyrimidines: Intermediates for Bivalent Thiazolopyrimidines." Journal of Organic Chemistry 70, no. 24 (2005): 10194–97. http://dx.doi.org/10.1021/jo0517702.

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4

Kaya, Hüseyin Oğuzhan, Ceylin Bozdemir, Hüseyin İstanbullu, and Seda Nur Topkaya. "Probing Redox Responses and DNA Interactions in Drug Discovery." Drugs and Drug Candidates 4, no. 2 (2025): 20. https://doi.org/10.3390/ddc4020020.

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Background/Objectives: The thiazolo [5,4-d]pyrimidine scaffold is a class of drugs known for its anticancer, antitumor, anti-inflammatory, and antimicrobial properties. In this study, the electrochemical properties of novel thiazolo [5,4-d]pyrimidine derivatives and their interactions with DNA were characterized for the first time using voltammetric methods. Determining the interactions of new drug candidate molecules with DNA is crucial for drug development studies and is the main objective of this research. Methods: Both molecules were immobilized on the surface of the electrodes by passive

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5

Wang, Peng, Hao Xu, and Wen-long Huang. "(2-Chlorothiazol-5-yl)methyl 4-nitrophenyl carbonate." Acta Crystallographica Section E Structure Reports Online 63, no. 12 (2007): o4624. http://dx.doi.org/10.1107/s1600536807055420.

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6

Debski, Norbert, Wolfgang Hanefeld, and Martin Schlitzer. "Improved synthesis of 2-substituted 4-chlorothiazole-5-carbaldehydes." Journal of Heterocyclic Chemistry 34, no. 5 (1997): 1427–29. http://dx.doi.org/10.1002/jhet.5570340509.

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7

Zhu, Xiao-Fei, De-Qing Shi, Fang Luo, and Zhi-Fang Wang. "1-{1-[(2-Chlorothiazol-5-yl)methyl]-2-[(2-chlorothiazol-5-yl)methylsulfanyl]-4-methyl-6-phenyl-1,6-dihydropyrimidin-5-yl}ethanone." Acta Crystallographica Section E Structure Reports Online 63, no. 8 (2007): o3516. http://dx.doi.org/10.1107/s1600536807033764.

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8

Borbone, Fabio, Antonio Carella, Laura Ricciotti, Angela Tuzi, Antonio Roviello, and Alberto Barsella. "High nonlinear optical response in 4-chlorothiazole-based azo dyes." Dyes and Pigments 88, no. 3 (2011): 290–95. http://dx.doi.org/10.1016/j.dyepig.2010.07.011.

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9

DEBSKI, N., W. HANEFELD, and M. SCHLITZER. "ChemInform Abstract: Improved Synthesis of 2-Substituted 4-Chlorothiazole-5-carbaldehydes." ChemInform 29, no. 16 (2010): no. http://dx.doi.org/10.1002/chin.199816120.

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10

Zhang, Hong-Kun, Jin-Sheng Gao, Xiao-Hui Jiang, and Guang-Feng Hou. "Hexaaquanickel(II) bis{4-[(2-chlorothiazol-5-yl)methoxy]benzoate} dihydrate." Acta Crystallographica Section E Structure Reports Online 64, no. 4 (2008): m585. http://dx.doi.org/10.1107/s1600536808007836.

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11

Kornienko, A. N., V. S. Zyabrev, and V. S. Brovarets. "New method for synthesis of 4-tosyl-5-chlorothiazole-2-thiol derivatives." Russian Journal of General Chemistry 84, no. 11 (2014): 2273–74. http://dx.doi.org/10.1134/s1070363214110401.

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12

Bello, Kasali A. "Colour and constitution of 4-chlorothiazole azo dyes: application of PPP method." Journal of the Society of Dyers and Colourists 113, no. 12 (2008): 361–64. http://dx.doi.org/10.1111/j.1478-4408.1997.tb01864.x.

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13

Wang, Qingmin, Heng Li, Yonghong Li, and Runqiu Huang. "Synthesis and Herbicidal Activity of 2-Cyano-3-(2-chlorothiazol-5-yl)methylaminoacrylates." Journal of Agricultural and Food Chemistry 52, no. 7 (2004): 1918–22. http://dx.doi.org/10.1021/jf035312a.

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14

Chen, Xiao-Bao, Jia-Hua Tian, Jing Xu, Yong Yu, and Qun Wang. "1-{1-[(2-Chlorothiazol-5-yl)methyl]-5-methyl-1H-1,2,3-triazol-4-yl}ethanone." Acta Crystallographica Section E Structure Reports Online 65, no. 11 (2009): o2840. http://dx.doi.org/10.1107/s1600536809042937.

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15

Hawk, Mai Khanh, Sarah J. Ryan, Xin Zhang, et al. "Tetramethylammonium Fluoride Tetrahydrate for SNAr Fluorination of 4-Chlorothiazoles at a Production Scale." Organic Process Research & Development 25, no. 5 (2021): 1167–75. http://dx.doi.org/10.1021/acs.oprd.1c00042.

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16

Shen, Hong-Feng, Xi Chen, Pin Liao, Xu-Shen Shao, Zhong Li, and Xiao-Yong Xu. "Design, synthesis, and insecticidal bioactivities evaluation of pyrrole- and dihydropyrrole-fused neonicotinoid analogs containing chlorothiazole ring." Chinese Chemical Letters 26, no. 5 (2015): 509–12. http://dx.doi.org/10.1016/j.cclet.2015.03.017.

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17

Shao, Xusheng, Xinglong Huang, Qian Shi, Zhong Li, Liming Tao, and Gonghua Song. "Synthesis and Insecticidal Activities of Chlorothiazolyl Analogs of Nitromethylene Neonicotinoids with Tetrahydropyridine Fixedcis-Configuration." Journal of Heterocyclic Chemistry 49, no. 5 (2012): 1136–42. http://dx.doi.org/10.1002/jhet.969.

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18

Dong, Zhang-Chao, Yang Shi, Liang-Liang Zheng, et al. "Synthesis and Activity Evaluation of Vinpocetine-Derived Indole Alkaloids." Molecules 29, no. 1 (2023): 14. http://dx.doi.org/10.3390/molecules29010014.

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This study focuses on the synthesis of novel vinpocetine derivatives (2–25) and their biological evaluation. The chemical structures of the synthesized compounds were fully characterized using techniques such as 1H NMR, 13C NMR, and HRMS. The inhibitory activity of the synthesized compounds on PDE1A was evaluated, and the results revealed that compounds 3, 4, 5, 12, 14, 21, and 25 exhibited superior inhibitory activity compared to vinpocetine. Compound 4, with a para-methylphenyl substitution, showed a 5-fold improvement in inhibitory activity with an IC50 value of 3.53 ± 0.25 μM. Additionally

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19

Yang, Yazhe, Dayong Lin, Cuirong Fu, and Xiaomao Zou. "Synthesis and Biological Activity Evaluation of Novel Pyrazole Oxime Ether Derivatives Containing Chlorothiazole Group and Pyrimidine Rings." Chinese Journal of Organic Chemistry 35, no. 1 (2015): 100. http://dx.doi.org/10.6023/cjoc201408004.

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20

Li, Gangyue, Shenggang Yan, Shan Jiang, Xuhong Qian, Qingchun Huang, and Rong Zhang. "Novel Heterocyclic Compounds Containing Sulfur: Synthesis and Insecticidal Activity of (2-Chlorothiazol-5-yl)methyl 2-Phenyliminothiazolidines." Phosphorus, Sulfur, and Silicon and the Related Elements 184, no. 7 (2009): 1825–36. http://dx.doi.org/10.1080/10426500802384135.

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21

Shen, Hong-Feng, Xi Chen, Pin Liao, Xu-Shen Shao, Zhong Li, and Xiao-Yong Xu. "ChemInform Abstract: Design, Synthesis, and Insecticidal Bioactivities Evaluation of Pyrrole- and Dihydropyrrole-Fused Neonicotinoid Analogues Containing Chlorothiazole Ring." ChemInform 46, no. 37 (2015): no. http://dx.doi.org/10.1002/chin.201537152.

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22

Zhao, Benbo, Changchun Yuan, Miao-Miao Xun, and Kai Fu. "Crystal structure of (E)-N-(1-((2-chlorothiazol-5-yl)methyl)pyridin-2(1H)-ylidene)-2,2,2-trifluoroacetamide, C11H7ClF3N3OS." Zeitschrift für Kristallographie - New Crystal Structures 236, no. 4 (2021): 809–10. http://dx.doi.org/10.1515/ncrs-2021-0089.

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Abstract C11H7ClF3N3OS, monoclinic, C2/c (no. 15), a = 21.9623(8) Å, b = 9.7431(4) Å, c = 16.1379(5) Å, β = 132.0530(10)°, V = 2564.09(16) Å3, Z = 8, R gt (F) = 0.0456, wR ref (F 2) = 0.0938, T = 170 K.

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23

Yan, Man, and De-Qing Shi. "1-[(2-Chlorothiazol-5-yl)methyl]-N′-[2-(2,4-dichlorophenoxy)acetyl]-5-methyl-1H-1,2,3-triazole-4-carbohydrazide." Acta Crystallographica Section E Structure Reports Online 63, no. 2 (2007): o953—o954. http://dx.doi.org/10.1107/s1600536807003182.

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24

Xiao, Lin-Xia, and De-Qing Shi. "3-[(2-Chlorothiazol-5-yl)methyl]-5-(isobutylamino)-6-phenyl-3H-1,2,3-triazolo[4,5-d]pyrimidin-7(6H)-one." Acta Crystallographica Section E Structure Reports Online 63, no. 6 (2007): o2843. http://dx.doi.org/10.1107/s1600536807021484.

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25

Chen, Xiao-Bao, and De-Qing Shi. "O,O-Diethyl [({1-[(2-chlorothiazol-5-yl)methyl]-5-methyl-1H-1,2,3-triazol-4-yl}carbonyloxy)phenylmethyl]phosphonate." Acta Crystallographica Section E Structure Reports Online 63, no. 1 (2006): o158—o160. http://dx.doi.org/10.1107/s1600536806051841.

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26

Shao, Xusheng, Xinglong Huang, Qian Shi, Zhong Li, Liming Tao, and Gonghua Song. "ChemInform Abstract: Synthesis and Insecticidal Activities of Chlorothiazolyl Analogues of Nitromethylene Neonicotinoids with Tetrahydropyridine Fixed cis-Configuration." ChemInform 44, no. 17 (2013): no. http://dx.doi.org/10.1002/chin.201317150.

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27

El Azab, Islam H., Adil A. Gobouri, and Tariq A. Altalhi. "4‐Chlorothiazole‐5‐carbaldehydes as Potent Precursors for Synthesis of Some New Pendant N ‐heterocyces Endowed with Anti‐Tumor Activity." Journal of Heterocyclic Chemistry 56, no. 1 (2018): 281–95. http://dx.doi.org/10.1002/jhet.3406.

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28

He, Jian-Ling, and Wei-Hua Cheng. "Synthesis, Characterization and Crystal Structure of N-(3-((2-Chlorothiazol-5-yl)methyl)-5-methyl-1,3,5-oxadiazinan-4-ylidene)nitramide." Asian Journal of Chemistry 27, no. 7 (2015): 2383–85. http://dx.doi.org/10.14233/ajchem.2015.17842.

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29

Wang, An-Jia, Yun-Hui Zhang, Zhi Zhang, et al. "Crystal structure of 5-((4-(1H-benzo[d]imidazol-2-yl)-2-methoxyphenoxy)methyl)-2-chlorothiazole - trichloromethane - methanol (1/1/1), C20H19Cl4N3O3S." Zeitschrift für Kristallographie - New Crystal Structures 233, no. 2 (2018): 281–82. http://dx.doi.org/10.1515/ncrs-2017-0279.

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30

CHEN, Xiao-Bao, De-Qing SHI та Xiao-Fei ZHU. "Synthesis, Crystal Structure and Biological Activities ofO,O-Dialkyl α-[1-(2-Chlorothiazol-5-ylmethyl)-5-methyl- 1H-1,2,3-triazol-4-ylcarbonyloxy]alkylphosphonates". Chinese Journal of Chemistry 25, № 12 (2007): 1854–58. http://dx.doi.org/10.1002/cjoc.200790342.

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31

Wrobel, Sonja A., Daniel Bury, Heiko Hayen, Holger M. Koch, Thomas Brüning, and Heiko U. Käfferlein. "Human metabolism and urinary excretion of seven neonicotinoids and neonicotinoid-like compounds after controlled oral dosages." Archives of Toxicology 96, no. 1 (2021): 121–34. http://dx.doi.org/10.1007/s00204-021-03159-0.

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AbstractFew human data on exposure and toxicity are available on neonicotinoids and neonicotinoid-like compounds (NNIs), an important group of insecticides worldwide. Specifically, exposure assessment of humans by biomonitoring remains a challenge due to the lack of appropriate biomarkers. We investigated the human metabolism and metabolite excretion in urine of acetamiprid (ACE), clothianidin (CLO), flupyradifurone (FLUP), imidacloprid (IMI), sulfoxaflor (SULF), thiacloprid (THIAC) and thiamethoxam (THIAM) after single oral dosages at the currently acceptable daily intake levels of the Europe

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32

Liu, M. Y., B. Latli, and J. E. Casida. "Imidacloprid Binding Site in Musca Nicotinic Acetylcholine Receptor: Interactions with Physostigmine and a Variety of Nicotinic Agonists with Chloropyridyl and Chlorothiazolyl Substituents." Pesticide Biochemistry and Physiology 52, no. 3 (1995): 170–81. http://dx.doi.org/10.1006/pest.1995.1042.

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33

Bulatova, K. A., M. I. Mallyabaeva, T. V. Tyumkina, E. M. Zainutdinova, and S. V. Bаlакirеvа. "ENVIRONMENTAL IMPACT AND SAFETY OF AGROPROTECTIVE CHEMICAL BASED ON THIAMETHOXAM." Problems of Gathering Treatment and Transportation of Oil and Oil Products, no. 4 (September 27, 2023): 137–52. http://dx.doi.org/10.17122/ntj-oil-2023-4-137-152.

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The article is devoted to the aspects of environmental safety of the use of Aktara insecticide, widely used in the agro-protective sector, with the active substance thiamethoxam from the class of neonicotinoids. Studies have been carried out on the impact of insecticide on test organisms of soil and aquatic ecosystems, and its transformation in the process of laboratory biodegradation has been studied on the basis of chromato-mass-spectral analysis. In order to identify the anthropogenic load of soil and water ecosystems during the application of the Aktara preparation containing thiamet

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34

Liu, Jian, Raymond J. Patch, Carsten Schubert, and Mark R. Player. "Single-Step Syntheses of 2-Amino-7-chlorothiazolo[5,4-d]pyrimidines: Intermediates for Bivalent Thiazolopyrimidines." ChemInform 37, no. 14 (2006). http://dx.doi.org/10.1002/chin.200614161.

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35

Zhang, Honglei, Haibo Zhu, Yingying Zhang, et al. "A Redox‐neutral Nickel‐catalysed Sulfonylation of (Hetero)aryl Boronic Acids with 2‐Chlorothiazoles." Chemistry – An Asian Journal, October 10, 2023. http://dx.doi.org/10.1002/asia.202300757.

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A redox‐neutral nickel‐catalysed sulfonylation for arylsulfone synthesis were developed. (Hetero)aryl boronic acids reacted with potassium metabisulfite (K2S2O5) and readily available 2‐chlorothiazoles in the presence of air‐stable Ni(OTf)2 and 4,4‐di‐tert‐butyl bipyridine (dtbbpy) as a commercially available ligand to produce the corresponding 2‐sulfonylthiazoles in moderate to excellent yields. This practical protocol tolerates a wide range of substrates including boronic acids and 2‐chloro(benzo)thiazoles without additional bases, allowing the direct synthesis of functional arylsulfones.

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36

Shao, Yiming, Yuan Gao, Rui Sun, Meimei Zhang, and Jie Min. "A Versatile and Low‐Cost polymer donor based on 4‐Chlorothiazole for Highly Efficient Polymer solar cells." Advanced Materials, November 22, 2022, 2208750. http://dx.doi.org/10.1002/adma.202208750.

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37

Cheng, Wei‐long, Zhi‐hui Zhang, Zhi‐Bin Zhang, Guo‐ping Zhao, and Yan‐bo Wang. "Clothianidin Exposure Induces Cell Apoptosis via Mitochondrial Oxidative Damage." Environmental Toxicology, November 22, 2024. http://dx.doi.org/10.1002/tox.24442.

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ABSTRACTClothianidin (CLO) is a high‐frequently detected neonicotinoid pesticide in fruits and vegetables, whose exposure security deserves attention. This study evaluated the apoptotic toxicity of CLO on Caco‐2 cells at doses of 100 nM, 10 μM, and 1 mM. After exposure, CLO induced to a remarkable change of signaling proteins that participated in the process of cell apoptosis, including caspase 3, cleaved‐caspase 3, and caspase 9. CLO treatment further induced a decrease of mitochondrial membrane potential and increased the protein level of cytochrome C. Reactive oxygen species (ROS) and intra

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