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Dissertations / Theses on the topic 'Chromatography of aromatic amines'

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Published: 5 June 2025

Last updated: 1 August 2025

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1

Riddar, Jakob B. "Isocyanates, Amines and Alkanolamines : Sampling, Chromatography and Detection." Doctoral thesis, Stockholms universitet, Institutionen för analytisk kemi, 2013. http://urn.kb.se/resolve?urn=urn:nbn:se:su:diva-94067.

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Isocyanates, aromatic-, aliphatic- and alkanolamines are commonly used in the industry today. Millions of workers in Europe are exposed. The most frequent health symptoms are respiratory and dermal disorder. Due to the health risk most of the compounds in this thesis are regulated by authorities and have occupational exposure limits (OELs). Consequently, reliable and robust air sampling methods are urgently needed. In this thesis dry samplers for isocyanates, aliphatic- and alkanolamines have been developed and evaluated. The isocyanate sampler is now a commercial product (ASSET EZ4-NCP Dry Sa

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2

Lamani-Dixon, Xolelwa [Verfasser], and Torsten Claus [Akademischer Betreuer] Schmidt. "Analysis of aromatic amines in human urine using comprehensive multi-dimensional gas chromatography mass spectrometry / Xolelwa Lamani-Dixon ; Betreuer: Torsten Claus Schmidt." Duisburg, 2018. http://d-nb.info/1173616055/34.

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3

Marczylo, Timothy Hywel. "Bioactivation of aromatic amines." Thesis, University of Surrey, 1996. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.336523.

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4

Walsh, Kelly Ann. "The alkylation of aromatic amines." Thesis, University of Ottawa (Canada), 1992. http://hdl.handle.net/10393/7659.

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N-alkylated anilines can be obtained in moderate yields from aniline and methyl formate in the presence of Rh$\sb6$(CO)$\sb $ and KI after 72 hours at 180-200$\sp\circ$C. Ru$\sb3$(CO)$\sb $ gave similar results to the unpromoted rhodium carbonyl system. Formanilide and N-methylformanilide were also formed in the reaction. The (HCr(CO)$\sb5$) -anion in the form of its PPN$\sp+$ and Et$\sb4$N$\sp+$ salts also catalysed this reaction (under hydrogen) but was selective to the formanilide products. The presence of an electron donating group on the aromatic ring favoured the formation of alkylated p

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5

Gibson, E. M. "Spectroscopy of jet-cooled aromatic amines." Thesis, Imperial College London, 1988. http://hdl.handle.net/10044/1/47075.

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6

Wang, Xuan. "Studies on preparation of aromatic amines and their synthetic and biological applications /." View abstract or full-text, 2005. http://library.ust.hk/cgi/db/thesis.pl?CHEM%202005%20WANG.

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7

Howell, Rachel. "Laser induced fluorescence studies of jet-cooled aromatic amines." Thesis, Imperial College London, 1990. http://hdl.handle.net/10044/1/46347.

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8

Rohaly, Matthew Joseph. "Decomposition of Aromatic Amines in a Jet Fuel Surrogate." University of Dayton / OhioLINK, 2014. http://rave.ohiolink.edu/etdc/view?acc_num=dayton1417777531.

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9

Brunmark, Per. "Methods for assessment of exposure to aromatic amines/isocyanates by air monitoring and biomarkers." Lund : Dept. of Analytical Chemistry and Dept. of Occupational and Environmental Medicine, Lund University, 1994. http://catalog.hathitrust.org/api/volumes/oclc/38948330.html.

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10

Yeatts, Karin Beatrice. "An investigation of structure activity relationships for aryl nitrenium stability and mutagenicity for amino polyaromatic hydrocarbons." Thesis, This resource online, 1990. http://scholar.lib.vt.edu/theses/available/etd-02132009-170829/.

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11

Sakamaki, Daisuke. "Studies on Electronic Properties of Aromatic Amines with Unique Structures." 京都大学 (Kyoto University), 2013. http://hdl.handle.net/2433/174890.

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12

Powell, C. J. "Studies of the nephrotoxicity of some alkyl and aromatic amines." Thesis, University of Surrey, 1985. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.332745.

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13

GHAANI, MASOUD. "Food Packaging Innovations- Electrochemical Nanosensors far Primary Aromatic Amines Quantification." Doctoral thesis, Università degli Studi di Milano, 2018. http://hdl.handle.net/2434/584740.

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Primary aromatic amines (PAAs) are substances that can be transferred from food packaging materials into foodstuffs and are “possibly carcinogenic to humans”. The formation of PAAs from multilayer packaging materials consisting of aromatic polyurethane (PU) adhesives occurs from the reaction between residual isocyanic monomers (the most widely used of which are 2,4-toluene diisocyanate – TDI and 4,4’-methylene diphenyl diisocyanate – MDI) that have migrated to the surface of the inner layer of the package and water molecules making contact with the same plastic surface. However, for foods subj

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14

Davies, Ilona Lynn. "Analysis of polycyclic aromatic compounds by multidimensional chromatography." Thesis, University of Leeds, 1989. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.328575.

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15

Nicolae, Toma Gabriel. "Cobalt-Catalyzed Carbon-Nitrogen Bond-Forming Reaction between Secondary Amines and N-Aromatic or Aromatic Chlorides." Kyoto University, 2011. http://hdl.handle.net/2433/142304.

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Kyoto University (京都大学)<br>0048<br>新制・課程博士<br>博士(人間・環境学)<br>甲第16176号<br>人博第559号<br>新制||人||134(附属図書館)<br>22||人博||559(吉田南総合図書館)<br>28755<br>京都大学大学院人間・環境学研究科相関環境学専攻<br>(主査)教授山口良平, 教授田村類, 准教授藤田健一<br>学位規則第4条第1項該当

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16

Debruin, Lillian S. "The detection of aromatic amines, possible mammary carcinogens, in human milk." Thesis, National Library of Canada = Bibliothèque nationale du Canada, 2001. http://www.collectionscanada.ca/obj/s4/f2/dsk3/ftp04/NQ58303.pdf.

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17

Hubbard, Sara E. "The solid-matrix luminescence of heterocyclic aromatic amines in sugar glasses." Laramie, Wyo. : University of Wyoming, 2008. http://proquest.umi.com/pqdweb?did=1597616951&sid=1&Fmt=2&clientId=18949&RQT=309&VName=PQD.

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18

Robotham, Ian A. "Mechanistic studies of aromatic substitutions with aniline and phenoxide nucleophiles." Thesis, Durham University, 1997. http://etheses.dur.ac.uk/5063/.

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Kinetic studies are reported of the reactions of 1,3,5-trinitrobenzene with aniline in dimethyl sulfoxide (DMSO). In the presence of buffers containing 1,4- diazabicyclo(2.2.2)octane, (Dabco), and its acid salt, DabcoH(^+), the anilide σ-adduct is formed. The reaction of ethyl 2,4,6-trinitrophenyI ether with aniline in DMSO containing Dabco occurs in two stages. The first gives σ-adduct intermediate on the substitution pathway, which has been identified spectroscopically. The second yields 2,4,6-trinitrodiphenyIamine, the substitution product. Kinetic studies show that proton transfer is rate-

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19

Bagheri, Habib. "Vapour-phase fluorescence detection in gas chromatography." Thesis, University of East Anglia, 1991. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.280036.

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20

Wagner, Elizabeth Diane. "Modulation of genotoxic responses by environmental agents." Thesis, University of Surrey, 1999. http://epubs.surrey.ac.uk/843395/.

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A metabolite of a widely used pesticide, paraoxon, exerted a dramatic mutagenic synergistic effect in Salmonella typhimurium with a number of mammalian-activated or plant-activated aromatic amines and heterocyclic amines. The mutagenic synergy required an activated an aromatic amine, and was not attributable to the generation of new mutagenic products or to the modification of the stability of the activated aromatic amine products. Paraoxon modulated the genotoxic potency of dietaiy heterocyclic amines in human cells. The results of this study raise the concern of the environmental effects of

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21

Ayrton, Andrew David. "Food mutagens : factors that modulate their metabolic activation." Thesis, University of Surrey, 1989. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.328576.

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22

Sen, Subhabrata. "Sythesis of diaryl ethers and diaryl amines via Dötz benzannulation /." free to MU campus, to others for purchase, 2001. http://wwwlib.umi.com/cr/mo/fullcit?p3030540.

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23

Tugnait, Meera. "Multinuclear magnetic resonance studies on the metabolism model of fluoroaromatic xenobiotics." Thesis, Birkbeck (University of London), 1994. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.296519.

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24

Collier, Simon Andrew. "The reactions of N-chloroamines and related N-substituted amines with aromatic substrates." Thesis, University of York, 1993. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.333736.

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25

Lu, Fei. "Formation and control of heterocyclic amines and polycyclic aromatic hydrocarbons during meat processing." Thesis, University of Reading, 2018. http://centaur.reading.ac.uk/77712/.

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Heterocyclic amines (HCAs) and polycyclic aromatic hydrocarbons (PAHs) formed during meat processing may pose health risk to the public. This project aimed to investigate the occurrence of HCAs and PAHs in highly consumed cooked meat products including ready-to-eat (RTE) meat, patties and meatballs, and their health risk was also assessed according to the dietary pattern. Different strategies including replacing fat with vegetable oils and adding spices were applied in order to reduce the formation of HCAs and PAHs in final meat products. In addition, inhibitory mechanism of antioxidants in oi

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26

Mohammadi, Nargesi Behrouz [Verfasser], and Georg A. [Akademischer Betreuer] Sprenger. "Biotechnological production of aromatic amines and aromatic alcohols by recombinant Escherichia coli strains / Behrouz Mohammadi Nargesi ; Betreuer: Georg A. Sprenger." Stuttgart : Universitätsbibliothek der Universität Stuttgart, 2019. http://d-nb.info/1181099374/34.

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27

Yi, Ling. "Micellar liquid chromatographic separation of polycyclic aromatic hydrocarbons /." free to MU campus, to others for purchase, 2004. http://wwwlib.umi.com/cr/mo/fullcit?p1426117.

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28

Kennedy, Sean W. (Sean William) Carleton University Dissertation Chemistry. "Studies on porphyria as an indicator of polyhalogenated aromatic hydrocarbon exposure." Ottawa, 1988.

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29

Nakovich, Laura. "Analysis of Biogenic Amines by GC/FID and GC/MS." Thesis, Virginia Tech, 2003. http://hdl.handle.net/10919/35027.

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Low levels of biogenic amines occur naturally, but high levels (FDA sets 50 ppm of histamine in fish as the maximum allowable level) can lead to scombroid poisoning. Amines in general are difficult to analyze by Gas Chromatography (GC) due to their lack of volatility and their interaction with the GC column, often leading to significant tailing and poor reproducibility. Biogenic amines need to be derivatized before both GC and HPLC analyses. The objective of this research was to develop a relatively fast, reproducible method to derivatize and quantitate biogenic amines in fish at trace

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30

Lopez, Sanchez Susana. "Identification of high molecular weight polycyclic aromatic hydrocarbons by chromatography and mass spectrometry." Diss., Georgia Institute of Technology, 1985. http://hdl.handle.net/1853/27115.

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31

Winter, Helen Rayma. "Strategies to reduce arylamine drug toxicity in people with AIDS /." Thesis, Connect to this title online; UW restricted, 1998. http://hdl.handle.net/1773/7937.

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32

Marand, Åsa. "Isocyanates and Amines – Sampling and Analytical Procedures." Doctoral thesis, Stockholm University, Department of Analytical Chemistry, 2004. http://urn.kb.se/resolve?urn=urn:nbn:se:su:diva-204.

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<p>This thesis covers sampling and analytical procedures for isocyanates (R-NCO) and amines (R-NH<sub>2</sub>), two kinds of chemicals frequently used in association with the polymeric material polyurethane (PUR). Exposure to isocyanates may result in respiratory disorders and dermal sensitisation, and they are one of the main causes of occupational asthma. Several of the aromatic diamines associated with PUR production are classified as suspected carcinogens. Hence, the presence of these chemicals in different exposure situations must be monitored. </p><p>In the context of determining isocyan

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33

Fasciano, Jennifer Marie. "Use of Surfactant Modifiers for High-Performance Liquid Chromatography of Aliphatic and Aromatic Acids and Capillary Electrophoresis of Glycosaminoglycans." Miami University / OhioLINK, 2015. http://rave.ohiolink.edu/etdc/view?acc_num=miami1448126648.

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34

SILVA, ANASTACIA SA PINTO DA. "DETERMINATION OF NITROGEN AROMATIC COMPOUNDS IN DIESEL OIL AND GAS OIL BY MICELLAR ELECTROKINETIC CAPILLARY CHROMATOGRAPHY AND MICROEMULSION ELECTROKINETIC CHROMATOGRAPHY." PONTIFÍCIA UNIVERSIDADE CATÓLICA DO RIO DE JANEIRO, 2016. http://www.maxwell.vrac.puc-rio.br/Busca_etds.php?strSecao=resultado&nrSeq=34096@1.

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PONTIFÍCIA UNIVERSIDADE CATÓLICA DO RIO DE JANEIRO<br>CONSELHO NACIONAL DE DESENVOLVIMENTO CIENTÍFICO E TECNOLÓGICO<br>No presente trabalho foram desenvolvidos dois métodos analíticos baseados na eletroforese capilar (EC), visando a identificação e quantificação de treze compostos policíclicos aromáticos nitrogenados (CAN) em amostras de óleo diesel e gasóleo. As variantes de EC usadas foram a cromatografia capilar eletrocinética micelar (MECC) e a cromatografia eletrocinética em microemulsão (MEEKC). Os compostos estudados foram indol (I), 2-metilindol (2MI), 3-metilindol (3MI), 7-metilindol

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35

李偉安 and Wai-on Lee. "Oxidation chemistry and electrochemistry of ruthenium and chromium complexes of macrocyclic tertiary amines and aromatic diimines." Thesis, The University of Hong Kong (Pokfulam, Hong Kong), 1989. http://hub.hku.hk/bib/B31231846.

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36

Lord, Simon D. "Some studies of the reactions of amines with aldehydes and with aromatic nitro-compounds in acetonitrile." Thesis, Durham University, 1996. http://etheses.dur.ac.uk/5241/.

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Kinetic and equilibrium studies of the reactions between three trinitroaromatic species, 1,3,5-trinitrobenzene, ethyl 2,4,6-trmitrophenyl ether and phenyl 2,4,6- trinitrophenyl ether and the ahphatic amines n-butylamine, pyrrolidine and piperidine, in acetonitrile were undertaken. It was found that the reactions between 1,3,5-trinitrobenzene and each amine were too fast to measure. However kinetic information was gamed from the decomposition of the c-adducts formed from1.3.5- trinitrobenzene and both pyrrolidine and piperidme. Both the 3-adduct and the 1-adduct are observed as intermediates m

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37

Duncanson, Philip. "Synthesis of novel dyes and a study of the photochemistry N-formylated aromatic amines and indoles." Thesis, City University London, 1991. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.302729.

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38

Lee, Wai-on. "Oxidation chemistry and electrochemistry of ruthenium and chromium complexes of macrocyclic tertiary amines and aromatic diimines /." [Hong Kong : University of Hong Kong], 1989. http://sunzi.lib.hku.hk/hkuto/record.jsp?B12505286.

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39

Thigpen, Ashley Lauren Clark C. Randall. "Chromatographic and mass spectral studies on mass equivalent substituted phenethlamines related to MDEA, MDMMA and MBDB." Auburn, Ala., 2006. http://repo.lib.auburn.edu/2006%20Fall/Theses/THIGPEN_ASHLEY_11.pdf.

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40

White, John. "The determination of trace organic micro-pollutants by particle beam liquid chromatography mass spectrometry." Thesis, Sheffield Hallam University, 2000. http://shura.shu.ac.uk/20526/.

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Liquid Chromatography/ Mass Spectrometry (LC/MS) is used to interface the separating power of LC with the sensitivity and specificity of MS for the determination of trace levels of organic compounds in a variety of matrices. The technique is finding increasing application in the field of environmental and pharmaceutical analysis. Particle Beam LC/MS (PB/LC/MS) uses a particle beam interface to connect the LC to the MS. This interface design has the advantage of being able to produce "classical" electron impact (El) spectra which can then be searched against commercial MS libraries. The aim of

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41

Kurata, Ryohei. "Studies on Electronic Properties of Nitrogen-and Boron-Containing π-Electron Systems". Doctoral thesis, 京都大学 (Kyoto University), 2017. http://hdl.handle.net/2433/225623.

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京都大学<br>0048<br>新制・課程博士<br>博士(工学)<br>甲第20398号<br>工博第4335号<br>新制||工||1672(附属図書館)<br>京都大学大学院工学研究科分子工学専攻<br>(主査)教授関修平, 教授今堀博, 准教授伊藤彰浩, 教授白川昌宏<br>学位規則第4条第1項該当<br>Doctor of Philosophy (Engineering)<br>Kyoto University<br>DGAM

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42

Mao, Chunfeng. "Spectroscopic and chromatographic study of selective fluorescence quenchers of polycylcic aromatic hydrocarbons (PAHS) /." free to MU campus, to others for purchase, 2003. http://wwwlib.umi.com/cr/mo/fullcit?p3091946.

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43

Ayala, Gerardo. "Synthesis, Structure and Optical Memory Properties of Copper (I) Thiocyanate Networks with Aromatic Amines, Diimines and Alkyl Sulfides." W&M ScholarWorks, 2016. https://scholarworks.wm.edu/etd/1477068031.

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A series of CuSCN compounds were synthesized. Ligands included the alkyl sulfides methyl sulfide (Me2S), ethyl sulfide (Et2S), isopropyl sulfide (Pri2S) and tetrahydrothiophene (THT); diimine ligands pyrazine (Pyz), 2,3-dimethylpyrazine (2,3- Me2Pyz), 2,5-dimethylpyrazine (2,5-Me2Pyz), 2-aminopyrazine (2-NH2Pyz) and 2- methoxypyrazine (2-MeOPyz); two-ring diimines quinoxaline (Qox), quinazoline (Qnz), phthalazine (Ptz); and 3-halopyridines 3-chloropyridine (3-ClPy), 3-bromopyridine (3- BrPy), 3-iodopyridine (3-IPy). Crystal structures were solved for twelve products. With the exception of one

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44

Anand, R. "Synthesis of nitrogen containing heterocycles and acid catalyzed reactions of aromatic amines over medium and large pore zeolites." Thesis(Ph.D.), CSIR-National Chemical Laboratory, Pune, 2002. http://dspace.ncl.res.in:8080/xmlui/handle/20.500.12252/2343.

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45

Richardson, Ashley E. "Hydrophilic interaction and micellar liquid chromatography approaches for the separation of aromatic carboxylic acid positional isomers plus ion exchange chromatography for the separation of sulfonated compounds." Miami University / OhioLINK, 2017. http://rave.ohiolink.edu/etdc/view?acc_num=miami1511295591427557.

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46

Ioannou, Anastasia. "Source apportionment of polycyclic aromatic hydrocarbon emissions from transport using gas chromatography-isotope ratio mass spectrometry." Thesis, University of Strathclyde, 2004. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.401523.

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47

Kidd, La Creis R. "Estimation of exposure to two potent heterocyclic aromatic amines in various human populations and their role in colorectal cancer." Thesis, Massachusetts Institute of Technology, 1997. http://hdl.handle.net/1721.1/42653.

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48

Huyghues-Despointes, Alexis. "Development of analytical techniques and mechanistic studies related to the thermal decomposition of Amadori rearrangement products from secondary amines." Thesis, McGill University, 1995. http://digitool.Library.McGill.CA:80/R/?func=dbin-jump-full&object_id=29046.

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Standards of Amadori rearrangement products (ARP) were synthesized for the purpose of developing analytical techniques and performing mechanistic studies related to their thermal decomposition. Several synthetic strategies were explored. An HPLC analytical system with a diode array detector was coupled to a fluorometer and an electrochemical detector, in order to detect simultaneously and on-line, a wide variety of degradation products of ARPs and to follow their kinetics. The potential of such a system to analyze complex Maillard mixtures was demonstrated. The kinetics of the reaction of gluc

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49

Scholtka, Bettina, Dana Kühnel, Felicitas Taugner, and Pablo Steinberg. "Inflammation does not precede or accompany the induction of perneoplastic lesions in the colon of 2-amino-1-methyl-6-phenylimidazo[4,5-b]pyridine-fed rats." Universität Potsdam, 2009. http://opus.kobv.de/ubp/volltexte/2010/4457/.

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Heterocyclic aromatic amines (HCAs) are formed in meat cooked at high temperatures for a long time or over an open flame. In this context 2-amino-1-methyl-6-phenylimidazo[4,5-b]pyridine (PhIP), the most abundant HCA in cooked meat, has been suggested to be involved in colon and prostate carcinogenesis. In the latter case it has been reported that: (1) roughly 50% of Fischer F344 male rats treated with PhIP develop carcinomas in the ventral prostate lobe at 1 year of age; (2) inflammation precedes prostatic intraepithelial neoplasia in PhIP-fed rats; (3) inflammation specifically occurs in the

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50

Richter, Catherine Ann. "Regulation of subcellular localization of the aryl hydrocarbon receptor (AHR)." free to MU campus, to others for purchase, 2000. http://wwwlib.umi.com/cr/mo/fullcitt?p9988694.

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